Automatic control method for high cycle batch tetrabromobisphenol a centrifugal separation process

Abstract

The present application relates to the technical field of automatic control of chemical separation equipment, and particularly relates to an automatic control method for a high-cycle batch four-bromine bisphenol A centrifugal separation process. Data in a feed pipe is collected, corresponding control signals are output until filter cake load feedback data reaches a set threshold value; feed parameters are collected, a dynamic dewatering control algorithm is used to control mother liquor turbidity to be lower than a set threshold value; material liquid temperature and mother liquor turbidity data are collected, two control signals are formed by an intelligent spraying control algorithm, and are output to two gradient spraying pumps; a constant maximum speed control signal is output to a centrifuge main motor driver, filter cake humidity feedback is collected, and when humidity feedback data reaches a set drying target value, a discharge instruction is output and the control process is completed. The present application collects multi-dimensional data of material state and separation effect in real time through an online sensor network, and achieves the technical effect that even if feed conditions fluctuate, the excellent stability of batch product quality can be ensured.

Description

Technical Field

[0001] This invention relates to the field of automatic control technology for chemical separation equipment, and in particular to an automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process. Background Technology

[0002] In order to reduce costs, solvent consumption and environmental pollution, the production process of tetrabromobisphenol A (TBBPA) generally adopts a high recycling mode of organic solvents such as chlorobenzene.

[0003] As the number of solvent cycles increases, impurities accumulate in the reaction system, leading to three interconnected process challenges: (1) Deterioration of crystal morphology: The enrichment of impurities causes the growth of tetrabromobisphenol A crystals to change from "single crystal expansion" to "dendritic aggregation", forming loose aggregates with fractal structure. The median particle size d50 of the crystal is often less than 250 μm, and the particle size distribution width σ increases significantly. (2) Slurry viscosity fluctuation: The oligomers in the impurities cause the slurry to exhibit non-Newtonian fluid characteristics. The apparent viscosity depends not only on the temperature, but also on the shear history. The viscosity fluctuation range can reach ±40%. (3) Difficulty in solid-liquid separation: The dynamic changes in material properties lead to unstable permeability of the filter bed, mismatch between separation driving force and resistance, and traditional fixed parameter control is difficult to adapt.

[0004] Therefore, there is an urgent need in this field for an intelligent centrifugation control method that can sense and adaptively compensate for multiple dynamic variables such as particle size distribution width, viscosity-shear coupling, and temperature difference mass transfer in real time, so as to achieve efficient, low-consumption, and high-purity separation of high-cycle batch tetrabromobisphenol A. Summary of the Invention

[0005] The present invention aims to at least solve one of the technical problems existing in the related art. To this end, the present invention provides an automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process, achieving the technical effect of ensuring excellent stability of product quality between batches even with fluctuations in feed conditions.

[0006] This invention provides an automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process, comprising the following steps: S1: Collect density, temperature and particle size distribution parameters in the feed pipeline, and output corresponding control signals to the feed pump and centrifuge main motor driver until the filter cake load feedback data reaches the first set threshold. S2: Collect feed temperature, mother liquor turbidity, centrifugal torque and particle size parameters, generate centrifuge speed control signal according to dynamic dehydration control algorithm, and output to main motor driver until the mother liquor turbidity is lower than the second set threshold. S3: Output a low-speed control signal to the centrifuge main motor driver, collect data on feed liquid temperature and mother liquor turbidity, and generate two control signals according to the intelligent spray control algorithm, which are then output to the first gradient spray pump and the second gradient spray pump respectively. S4: Outputs a constant maximum speed control signal to the centrifuge main motor driver, collects filter cake humidity feedback, and outputs a discharge command and completes the control process when the humidity feedback data reaches the set drying target value.

[0007] An automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process provided by the present invention includes a dynamic dehydration control algorithm as follows: in, This is the centrifuge speed control signal. For the global security factor, This is the reference speed of the centrifuge. This is the median particle size value. The particle size distribution width, This refers to the temperature of the liquid feed. The turbidity value of the mother liquor. For size control functions, This is a temperature control function. This is the turbidity control function. denoted as shear rate.

[0008] According to the automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process provided by the present invention, the formula of the control function in the dynamic dehydration control algorithm is as follows: in, For effective viscosity function, For reference viscosity, The critical distribution width, The distribution width nonlinearity compensation index, The reference particle size is n, and the separation factor exponent is n. For the amplitude limiting function, The target value for mother liquor turbidity. This refers to the turbidity adjustment range.

[0009] According to the present invention, an automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process is provided, wherein the effective viscosity function formula is: in, Forward factor, For activation energy, The gas constant is For reference temperature, is the Carreau time constant, and m is the shear thinning exponent.

[0010] According to the present invention, an automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process is provided, wherein the formula of the intelligent spray control algorithm is as follows: in, This is the control signal for the first gradient spray pump. This is the upper limit of the sprinkler control signal. The turbidity setpoint for the first gradient spray solvent. The first temperature difference feedforward weighting coefficient, This is the temperature setpoint for the first gradient spray pump. For reference temperature difference, It is a saturation function. For PID control functions, This is the control signal for the second gradient spray pump. The turbidity setpoint for the second gradient spray solvent. This is the temperature setpoint for the second gradient spray pump. This is the second temperature difference feedforward weighting coefficient.

[0011] The formula for the PID control function described in this invention is as follows: in, For normalization bias, This is the proportionality coefficient. The integral coefficient is... The differential coefficients are... This is the turbidity setpoint for the sprayed solvent.

[0012] The present invention also provides an automatic control system for a high-cycle batch tetrabromobisphenol A centrifugal separation process, comprising: Feeding module: Used to collect density, temperature and particle size distribution parameters in the feed pipeline, and output corresponding control signals to the feed pump and centrifuge main motor driver until the filter cake load feedback data reaches the first set threshold. Centrifugal separation module: used to collect feed temperature, mother liquor turbidity, centrifugal force torque and particle size parameters, generate centrifuge speed control signal according to dynamic dehydration control algorithm, and output to main motor driver until the mother liquor turbidity is lower than the second set threshold; The spray washing module is used to output low-speed control signals to the centrifuge main motor driver, collect the temperature of the feed liquid and the turbidity of the mother liquor, and generate two control signals according to the intelligent spray control algorithm, which are output to the first gradient spray pump and the second gradient spray pump respectively. Detection module: Used to output a constant maximum speed control signal to the centrifuge main motor driver, collect filter cake humidity feedback, and output unloading command and complete the control process when the humidity feedback data reaches the set drying target value.

[0013] The present invention also provides an electronic device including a processor, a communication interface, a memory, and a communication bus, wherein the processor is used to execute a computer program to implement the steps of an automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process as described above.

[0014] The present invention also provides a non-transitory computer-readable storage medium having a computer program stored thereon, which, when executed by a processor, implements the steps of an automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process as described above.

[0015] The above-described one or more technical solutions in the embodiments of the present invention have at least one of the following technical effects: The technical solution provided by this invention, by real-time sensing of crystal particle size fluctuations within the range of 150-220 micrometers and other key parameters, and utilizing an adaptive algorithm based on separation science mechanisms for dynamic compensation and optimization, successfully solves the industry problem of low centrifugal separation efficiency and unstable product quality in high-cycle batches of tetrabromobisphenol A due to fine crystal fragmentation and high impurity content. This invention improves product quality and consistency while simultaneously increasing production efficiency and reducing resource consumption.

[0016] Additional aspects and advantages of the invention will be set forth in part in the description which follows, and in part will be obvious from the description, or may be learned by practice of the invention. Attached Figure Description

[0017] To more clearly illustrate the technical solutions in this invention or the prior art, the drawings used in the description of the embodiments or the prior art will be briefly introduced below. Obviously, the drawings described below are some embodiments of this invention. For those skilled in the art, other drawings can be obtained from these drawings without creative effort.

[0018] Figure 1 This is a flowchart illustrating an automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process provided by the present invention.

[0019] Figure 2This is a schematic diagram of the structure of an automatic control system for a high-cycle batch tetrabromobisphenol A centrifugal separation process provided by the present invention.

[0020] Figure 3 This is a schematic diagram of the structure of the electronic device provided by the present invention.

[0021] Figure label: 101. Feeding module; 102. Centrifugal separation module; 103. Spray washing module; 104. Detection module; 810. Processor; 820. Communication interface; 830. Memory; 840. Communication bus. Detailed Implementation

[0022] To make the objectives, technical solutions, and advantages of this invention clearer, the technical solutions of this invention will be clearly and completely described below. Obviously, the described embodiments are only some, not all, of the embodiments of this invention. All other embodiments obtained by those skilled in the art based on the embodiments of this invention without creative effort are within the scope of protection of this invention. The following embodiments are used to illustrate this invention but cannot be used to limit the scope of this invention.

[0023] In the description of this specification, the references to terms such as "one embodiment," "some embodiments," "example," "specific example," or "some examples," etc., refer to specific features, structures, materials, or characteristics described in connection with that embodiment or example, which are included in at least one embodiment or example of the present invention. In this specification, the illustrative expressions of the above terms do not necessarily refer to the same embodiment or example. Furthermore, the specific features, structures, materials, or characteristics described may be combined in any suitable manner in one or more embodiments or examples. Moreover, without contradiction, those skilled in the art can combine and integrate the different embodiments or examples described in this specification, as well as the features of different embodiments or examples.

[0024] The following is combined with Figures 1 to 3 This invention is described.

[0025] Example like Figure 1 As shown, Figure 1 This is a flowchart illustrating an automated control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process provided by the present invention, comprising the following steps: S1: Collect density, temperature and particle size distribution parameters in the feed pipeline, and output corresponding control signals to the feed pump and centrifuge main motor driver until the filter cake load feedback data reaches the first set threshold. S2: Collect feed temperature, mother liquor turbidity, centrifugal torque and particle size parameters, generate centrifuge speed control signal according to dynamic dehydration control algorithm, and output to main motor driver until the mother liquor turbidity is lower than the second set threshold. S3: Output a low-speed control signal to the centrifuge main motor driver, collect data on feed liquid temperature and mother liquor turbidity, and generate two control signals according to the intelligent spray control algorithm, which are then output to the first gradient spray pump and the second gradient spray pump respectively. S4: Outputs a constant maximum speed control signal to the centrifuge main motor driver, collects filter cake humidity feedback, and outputs a discharge command and completes the control process when the humidity feedback data reaches the set drying target value.

[0026] Specifically, the dynamic dehydration control algorithm is as follows: in, This is the centrifuge speed control signal. This is the global safety factor, with a value ranging from 1.0 to 1.3. This is the reference speed of the centrifuge. This is the median particle size value. The particle size distribution width, This refers to the temperature of the liquid feed. The turbidity value of the mother liquor. For size control functions, This is a temperature control function. This is the turbidity control function. This is the shear rate, which is directly related to the centrifuge speed.

[0027] The formula for the control function in the dynamic dehydration control algorithm is: in, The effective viscosity function is based on the Arrhenius-Carreau model. For reference viscosity, The critical distribution width, with a value ranging from 1.8 to 2.5; The distribution width nonlinearity compensation index has a value range of 0.2-0.5. The reference particle size ranges from 150 to 220 μm; n is the separation factor exponent, ranging from 0.5 to 1.0, corresponding to different flow regimes. For the amplitude limiting function, The target value for mother liquor turbidity is 80-150 NTU. The turbidity adjustment range is 150-300 NTU.

[0028] The formula for the effective viscosity function is: in, This is a forward exponentiation factor, with a value range of 0.5-1.5 Pa·s; The activation energy ranges from 15 to 25 kJ / mol. The gas constant is... For reference temperature, the value range is 20-30℃; is the Carreau time constant, ranging from 1.5 to 3.5 s; m is the shear thinning index, ranging from 0.4 to 0.8.

[0029] The formula for the intelligent sprinkler control algorithm is: in, This is the control signal for the first gradient sprinkler pump. This is the upper limit of the sprinkler control signal. The turbidity setpoint for the first gradient spray solvent is 80-120 NTU. This is the first temperature difference feedforward weighting coefficient, with a value ranging from 0.8 to 1.5; The temperature setpoint for the first gradient spray pump is 20-25℃. For reference temperature difference, the value range is 10-20℃; It is a saturation function. For PID control functions, This is the control signal for the second gradient spray pump. The turbidity setpoint for the second gradient spray solvent is 20-50 NTU. This is the temperature setpoint for the second gradient spray pump. This is the second temperature difference feedforward weighting coefficient, with a value range of 0.1-0.3.

[0030] The formula for the PID control function is: in, For normalization bias, This is a proportionality coefficient, with a value ranging from 0.5 to 2.0. This is the integral coefficient, with a value ranging from 0.1 to 0.5; is the differential coefficient, with a value range of 0.01-0.1. This is the turbidity setpoint for the sprayed solvent.

[0031] To quantitatively evaluate the effectiveness of this invention, a system comparative test was conducted on a production line. The experimental group used the control method described in this invention, while the control group used the existing centrifugation program with fixed three speed settings and timed operation. The test continuously processed five high-cycle batches, and the median particle size of the material was... The particle size distribution width fluctuates between 158 and 205 micrometers. It fluctuates within the range of 1.5-2.0.

[0032] The specific results are shown in Table 1: Table 1 Comparative Experiment Results

[0033] To quantitatively evaluate the long-term effectiveness of this invention, a system comparative test was conducted on a production line. The experimental group used the control method described in this invention, running continuously for 30 batches. The d50 of the material fluctuated within the range of 150-230 μm, and σ fluctuated within the range of 1.4-2.2. The statistical results are shown in Table 2. Table 2 Long-term operation results

[0034] The method proposed in this invention utilizes the interfacial tension gradient driven by the temperature difference between the solvent and the feed solution to enhance the mass transfer process of impurities from the crystal surface to the solvent.

[0035] Under typical high-cycle conditions (i.e., more than 20 cycles, with d50 in the range of 150-220μm), the following can be achieved: filter cake moisture content is consistently below 5%, reaching as low as 4.5% in the examples; product purity is better than 99.4%, reaching 99.62% in the examples; single-batch processing time is reduced by more than 12%; solvent consumption is reduced by more than 16%; and unit product power consumption is reduced by more than 19%.

[0036] The method proposed in this invention provides a highly reproducible solution. The algorithm-driven control eliminates the differences in human experience and ensures excellent stability of product quality between batches, even with fluctuations in feeding conditions.

[0037] The mechanical structure applied in this invention involves feeding high-cycle raw materials into the system via a feed pump. Simultaneously, real-time material characteristic data is acquired through an online density meter, temperature sensor, and online viscometer. This data, along with equipment operating status signals collected by vibration and torque sensors, is input into the horizontal screw centrifuge. The solid phase output from the centrifuge is sent to a near-infrared moisture analyzer for final quality determination, while the liquid phase output is sent to an online concentration meter for core quality feedback. Both equipment operating status and quality feedback data are transmitted to the control cabinet. The control cabinet, through an adaptive algorithm, outputs speed commands to the main motor driver, feed control signals to the horizontal screw centrifuge, frequency commands to the washing solvent tank B, and liquid inlet commands to the solvent B storage tank. Simultaneously, it interacts with the human-machine interface to control the entry of washing solvent A from the solvent A storage tank into the annular sprayer. The operating status signal of the annular sprayer is also fed back to the control cabinet. Finally, the system also treats the mother liquor discharged from the centrifuge through a mother liquor collection tank, achieving closed-loop control throughout the entire process.

[0038] The above data shows that even with significant fluctuations in feeding conditions, the present invention can still maintain a high degree of stability in product quality between batches.

[0039] like Figure 2 As shown, the present invention also provides an automatic control system for a high-cycle batch tetrabromobisphenol A centrifugal separation process, comprising: Feeding module 101: Used to collect density, temperature and particle size distribution parameters in the feeding pipeline, and output corresponding control signals to the feed pump and centrifuge main motor driver until the filter cake load feedback data reaches the first set threshold. Centrifugal separation module 102: used to collect feed temperature, mother liquor turbidity, centrifugal force torque and particle size parameters, generate centrifuge speed control signal according to dynamic dehydration control algorithm, and output to main motor driver until the mother liquor turbidity is lower than the second set threshold; Spray washing module 103: It is used to output low-speed control signals to the centrifuge main motor driver, collect the temperature of the feed liquid and the turbidity of the mother liquor, and form two control signals according to the intelligent spray control algorithm, which are output to the first gradient spray pump and the second gradient spray pump respectively. Detection module 104: Used to output a constant maximum speed control signal to the centrifuge main motor driver, collect filter cake humidity feedback, and output unloading command and complete the control process when the humidity feedback data reaches the set drying target value.

[0040] Figure 3 An example is a schematic diagram of the physical structure of an electronic device, such as... Figure 3As shown, the electronic device may include: a processor 810, a communication interface 820, a memory 830, and a communication bus 840, wherein the processor 810, the communication interface 820, and the memory 830 communicate with each other via the communication bus 840. The processor 810 can call logic instructions from the memory 830 to execute an automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process, the method including: S1: Collect density, temperature and particle size distribution parameters in the feed pipeline, and output corresponding control signals to the feed pump and centrifuge main motor driver until the filter cake load feedback data reaches the first set threshold. S2: Collect feed temperature, mother liquor turbidity, centrifugal torque and particle size parameters, generate centrifuge speed control signal according to dynamic dehydration control algorithm, and output to main motor driver until the mother liquor turbidity is lower than the second set threshold. S3: Output a low-speed control signal to the centrifuge main motor driver, collect data on feed liquid temperature and mother liquor turbidity, and generate two control signals according to the intelligent spray control algorithm, which are then output to the first gradient spray pump and the second gradient spray pump respectively. S4: Outputs a constant maximum speed control signal to the centrifuge main motor driver, collects filter cake humidity feedback, and outputs a discharge command and completes the control process when the humidity feedback data reaches the set drying target value.

[0041] Furthermore, the logical instructions in the aforementioned memory 830 can be implemented as software functional units and, when sold or used as independent products, can be stored in a computer-readable storage medium. Based on this understanding, the technical solution of the present invention, essentially, or the part that contributes to the prior art, or a part of the technical solution, can be embodied in the form of a software product. This computer software product is stored in a storage medium and includes several instructions to cause a computer device (which may be a personal computer, server, or network device, etc.) to execute all or part of the steps of the methods described in the various embodiments of the present invention. The aforementioned storage medium includes various media capable of storing program code, such as USB flash drives, portable hard drives, read-only memory (ROM), random access memory (RAM), magnetic disks, or optical disks.

[0042] In another aspect, the present invention also provides a non-transitory computer-readable storage medium having a computer program stored thereon, which, when executed by a processor, implements an automatic control method for a high-cycle batch tetrabromobisphenol A centrifugation separation process provided above, the method comprising: S1: Collect density, temperature and particle size distribution parameters in the feed pipeline, and output corresponding control signals to the feed pump and centrifuge main motor driver until the filter cake load feedback data reaches the first set threshold. S2: Collect feed temperature, mother liquor turbidity, centrifugal torque and particle size parameters, generate centrifuge speed control signal according to dynamic dehydration control algorithm, and output to main motor driver until the mother liquor turbidity is lower than the second set threshold. S3: Output a low-speed control signal to the centrifuge main motor driver, collect data on feed liquid temperature and mother liquor turbidity, and generate two control signals according to the intelligent spray control algorithm, which are then output to the first gradient spray pump and the second gradient spray pump respectively. S4: Outputs a constant maximum speed control signal to the centrifuge main motor driver, collects filter cake humidity feedback, and outputs a discharge command and completes the control process when the humidity feedback data reaches the set drying target value.

[0043] The device embodiments described above are merely illustrative. The units described as separate components may or may not be physically separate. The components shown as units may or may not be physical units; that is, they may be located in one place or distributed across multiple network units. Some or all of the modules can be selected to achieve the purpose of this embodiment according to actual needs. Those skilled in the art can understand and implement this without any creative effort.

[0044] Through the above description of the embodiments, those skilled in the art can clearly understand that each embodiment can be implemented by means of software plus necessary general-purpose hardware platforms, and of course, it can also be implemented by hardware. Based on this understanding, the above technical solutions, in essence or the part that contributes to the prior art, can be embodied in the form of a software product. This computer software product can be stored in a computer-readable storage medium, such as ROM / RAM, magnetic disk, optical disk, etc., and includes several instructions to cause a computer device (which may be a personal computer, server, or network device, etc.) to execute the methods described in the various embodiments or some parts of the embodiments.

[0045] Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention, and not to limit them; although the present invention has been described in detail with reference to the foregoing embodiments, those skilled in the art should understand that modifications can still be made to the technical solutions described in the foregoing embodiments, or equivalent substitutions can be made to some of the technical features; and these modifications or substitutions do not cause the essence of the corresponding technical solutions to deviate from the spirit and scope of the technical solutions of the embodiments of the present invention.

[0046] It should be noted that the embodiments of this disclosure can be implemented using hardware, software, or a combination of both. The hardware portion can be implemented using dedicated logic; the software portion can be stored in memory and executed by a suitable instruction execution system, such as a microprocessor or dedicated-design hardware. Those skilled in the art will understand that the above-described devices and methods can be implemented using computer-executable instructions and / or included in processor control code, for example, such code provided on a programmable memory or a data carrier such as an optical or electronic signal carrier.

[0047] Furthermore, although the operation of the methods of this disclosure is described in a specific order in the accompanying drawings, this does not require or imply that these operations must be performed in that specific order, or that all the operations shown must be performed to achieve the desired result. Rather, the steps depicted in the flowcharts may be performed in a different order. Additionally or alternatively, certain steps may be omitted, multiple steps may be combined into one step, and / or one step may be broken down into multiple steps. It should also be noted that the features and functions of two or more devices according to this disclosure may be embodied in one device. Conversely, the features and functions of one device described above may be further divided and embodied by multiple devices.

[0048] While this disclosure has been described with reference to several specific embodiments, it should be understood that this disclosure is not limited to the specific embodiments disclosed. This disclosure is intended to cover various modifications and equivalent arrangements included within the spirit and scope of the appended claims.

Claims

1. An automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process, characterized in that, Includes the following steps: S1: Collect density, temperature and particle size distribution parameters in the feed pipeline, and output corresponding control signals to the feed pump and centrifuge main motor driver until the filter cake load feedback data reaches the first set threshold. S2: Collect feed temperature, mother liquor turbidity, centrifugal torque and particle size parameters, generate centrifuge speed control signal according to dynamic dehydration control algorithm, and output to main motor driver until the mother liquor turbidity is lower than the second set threshold. S3: Output a low-speed control signal to the centrifuge main motor driver, collect data on feed liquid temperature and mother liquor turbidity, and generate two control signals according to the intelligent spray control algorithm, which are then output to the first gradient spray pump and the second gradient spray pump respectively. S4: Outputs a constant maximum speed control signal to the centrifuge main motor driver, collects filter cake humidity feedback, and outputs a discharge command and completes the control process when the humidity feedback data reaches the set drying target value.

2. The automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process according to claim 1, characterized in that, The dynamic dehydration control algorithm is as follows: in, This is the centrifuge speed control signal. For the global security factor, This is the reference speed of the centrifuge. This is the median particle size value. The particle size distribution width, This refers to the temperature of the liquid feed. The turbidity value of the mother liquor. For size control functions, This is a temperature control function. This is the turbidity control function. denoted as shear rate.

3. The automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process according to claim 2, characterized in that, The formula for the control function in the dynamic dehydration control algorithm is: in, For effective viscosity function, For reference viscosity, The critical distribution width, The distribution width nonlinearity compensation index, The reference particle size is n, and the separation factor exponent is n. For the amplitude limiting function, The target value for mother liquor turbidity. This refers to the turbidity adjustment range.

4. The automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process according to claim 3, characterized in that, The formula for the effective viscosity function is: in, Forward factor, For activation energy, The gas constant is... For reference temperature, is the Carreau time constant, and m is the shear thinning exponent.

5. The automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process according to claim 2, characterized in that, The formula for the intelligent sprinkler control algorithm is: in, This is the control signal for the first gradient spray pump. This is the upper limit of the sprinkler control signal. The turbidity setpoint for the first gradient spray solvent. The first temperature difference feedforward weighting coefficient, This is the temperature setpoint for the first gradient spray pump. For reference temperature difference, It is a saturation function. For PID control functions, This is the control signal for the second gradient spray pump. The turbidity setpoint for the second gradient spray solvent. This is the temperature setpoint for the second gradient spray pump. This is the second temperature difference feedforward weighting coefficient.

6. The automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process according to claim 5, characterized in that, The formula for the PID control function is: in, For normalization bias, This is the proportionality coefficient. The integral coefficient is... The differential coefficients are... Set the turbidity setpoint for the sprayed solvent.

7. An automatic control system for a high-cycle batch tetrabromobisphenol A centrifugal separation process, used to execute the automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process as described in any one of claims 1 to 6, characterized in that, include: Feeding module: Used to collect density, temperature and particle size distribution parameters in the feed pipeline, and output corresponding control signals to the feed pump and centrifuge main motor driver until the filter cake load feedback data reaches the first set threshold. Centrifugal separation module: used to collect feed temperature, mother liquor turbidity, centrifugal force torque and particle size parameters, generate centrifuge speed control signal according to dynamic dehydration control algorithm, and output to main motor driver until the mother liquor turbidity is lower than the second set threshold; The spray washing module is used to output low-speed control signals to the centrifuge main motor driver, collect the temperature of the feed liquid and the turbidity of the mother liquor, and generate two control signals according to the intelligent spray control algorithm, which are output to the first gradient spray pump and the second gradient spray pump respectively. Detection module: Used to output a constant maximum speed control signal to the centrifuge main motor driver, collect filter cake humidity feedback, and output unloading command and complete the control process when the humidity feedback data reaches the set drying target value.

8. An electronic device comprising a processor, a communication interface, a memory, and a communication bus, characterized in that, When the processor executes a computer program, it implements the steps of an automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process as described in any one of claims 1 to 6.

9. A non-transitory computer-readable storage medium having a computer program stored thereon, characterized in that, When the computer program is executed by the processor, it implements the steps of the automatic control method for a high-cycle batch tetrabromobisphenol A centrifugal separation process as described in any one of claims 1 to 6.

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