An organic phase purification device

Abstract

The utility model relates to an organic phase purification device, including organism and set up in the cooling device of organism, collect component and liquid storage component of the collection organic phase of setting, cooling device one end is connected with liquid storage component and is connected with the other end and collection component, be equipped with distillation device between liquid storage component and cooling device, distillation device includes the distillation cup sealed connection with cooling device, distillation cup bottom is equipped with ultrasonic device, distillation cup is open with liquid storage component, be equipped with negative pressure device between cooling device and liquid storage component, distillation cup bottom sets up ultrasonic device, and ultrasonic wave has cavitation effect etc. characteristics, cause liquid's violent vibration and stirring effect under the condition of not with liquid mechanical contact, effectively reduced the interference to liquid element, greatly guaranteed the purity of the extracted organic phase.

Description

Technical Field

[0001] This utility model relates to the field of lifting device technology, specifically to an organic phase purification device. Background Technology

[0002] Organic phase purification equipment is a device that uses liquid-liquid extraction, distillation, or chromatographic separation techniques to achieve precise separation and purification of the organic phase in a mixture by utilizing the difference in solubility or boiling point characteristics between organic solvents and target components. It is widely used in the chemical, pharmaceutical, and food industries, and features efficient removal of impurities and recovery of high-purity organic components. At the same time, combined with automated control, it can improve operational safety and reduce solvent consumption.

[0003] Publication number CN219614909U discloses an organic phase distillation apparatus, including a heating box with an opening at the top, a distillation tank installed inside the heating box, a rotating component installed on the distillation tank, a stirring component installed inside the distillation tank, and a condensing component installed on one side of the heating box, with the condensing component corresponding to and communicating with the distillation tank. Heating is achieved by an electric heating rod inside the heating box, allowing for rapid heating and evaporation of the liquid in the distillation tank. During evaporation, the stirring component drives the liquid to flow within the distillation tank, accelerating the evaporation efficiency and shortening the distillation cycle. The condensing component condenses and liquefies the evaporated vapor, achieving the distillation action. Simultaneously, the rotating component, in conjunction with the rotating component, drives the distillation tank to rotate within the heating box, ensuring uniform heat distribution. However, the mechanical contact stirring of the waste material can affect the elemental composition of the liquid and the purity of the extracted organic phase. Furthermore, this technology still has room for modification. Summary of the Invention

[0004] The technical problem to be solved by this utility model is to provide an organic phase purification device in view of the shortcomings of the prior art.

[0005] To achieve the above objectives, this utility model provides the following technical solution: an organic phase purification device, comprising a body and a cooling device, a collection component for collecting organic phase, and a storage component for storing waste liquid disposed within the body. One end of the cooling device is connected to the storage component and the other end is connected to the collection component. A distillation device is provided between the storage component and the cooling device. The distillation device includes a distillation cup sealed to the cooling device, an ultrasonic device is provided at the bottom of the distillation cup, the distillation cup communicates with the storage component, and a negative pressure device is provided between the cooling device and the storage component.

[0006] The above-mentioned technical solution involves installing an ultrasonic device at the bottom of the distillation cup. Ultrasonic waves have cavitation effects and other characteristics. Without mechanical contact with the liquid, they can generate tiny bubbles inside the liquid and cause them to collapse rapidly, thereby causing violent vibration and stirring of the liquid. The non-contact stirring method avoids direct contact between the mechanical structure and the liquid, effectively reducing interference with the liquid elements, greatly ensuring the purity of the extracted organic phase, and improving the purification quality.

[0007] The aforementioned organic phase purification device can be further configured such that: the negative pressure device includes a negative pressure pump disposed within the machine body, a negative pressure bottle is fixedly installed on one side of the negative pressure pump, and the negative pressure pump is connected to the collection component.

[0008] Using the above technical solution, the negative pressure bottle fixedly installed on one side of the negative pressure pump can effectively store and stabilize the negative pressure environment. The negative pressure pump is connected to the collection component, which can form a stable negative pressure in the collection component, which can accelerate the flow of steam generated by distillation to the collection component, greatly improve the distillation efficiency, and shorten the entire purification cycle.

[0009] The aforementioned organic phase purification device can be further configured as follows: the collecting component includes a sealed bottle for collecting the organic phase, the sealed bottle is connected to a cooling device and a negative pressure pump, the sealed bottle is equipped with a weighing component for measuring the weight of the sealed bottle, an outer cylinder is provided on one side of the machine body, the outer cylinder is connected to the sealed bottle, and when the weighing component reaches a set weight, the organic phase in the sealed bottle is discharged into the outer cylinder.

[0010] By adopting the above technical solution, the sealed bottle ensures the volatilization of the organic phase and the mixing of external impurities, thereby guaranteeing the purity and quality of the collected organic phase. The sealed bottle is connected to a cooling device and a negative pressure pump. The cooling device condenses the vapor generated by distillation into a liquid organic phase and delivers it to the sealed bottle, while the negative pressure pump maintains a negative pressure environment in the entire system, accelerating the flow of the organic phase into the sealed bottle and improving the collection efficiency.

[0011] The aforementioned organic phase purification device can be further configured such that: the weighing component includes a balance disposed at the bottom of the sealed bottle; a control system is provided on one side of the machine body; the balance is electrically connected to the control system; an opening and closing valve is provided on one side of the sealed bottle; and the control system is capable of controlling the opening and closing of the opening and closing valve.

[0012] Using the above technical solution, the balance is electrically connected to the control system, which can transmit the measured weight information to the control system in real time, so that the control system can keep track of the weight change of the organic phase in the sealed bottle. The opening and closing valve on one side of the sealed bottle works with the control system. When the weight measured by the balance reaches the preset value, the control system can react and control the opening or closing of the opening and closing valve. When it is opened, the organic phase in the sealed bottle is discharged into the outer cylinder.

[0013] The aforementioned organic phase purification device can be further configured such that: the liquid storage component includes a waste tank connected to a distillation cup, and a liquid addition pump is provided between the waste tank and the distillation cup.

[0014] With the above technical solution, the waste tank in the liquid storage component is connected to the distillation cup, and the liquid addition pump can also overcome factors such as pipeline resistance to a certain extent, ensuring smooth liquid delivery and stability of liquid delivery. At the same time, the liquid addition pump can send the undistilled waste liquid in the distillation cup back to the waste tank when the machine stops.

[0015] The aforementioned organic phase purification device can be further configured such that: the cooling device includes a condenser bottle sealed to a distillation cup; the machine body is provided with a storage tank for storing cold water; a cold water circulator is provided on one side of the condenser bottle to control the circulation of the cold water; one end of the cold water circulator is connected to the condenser bottle and the other end is connected to the storage tank.

[0016] By adopting the above technical solution, the condenser flask and the distillation cup are sealed together, which can effectively prevent the leakage of steam generated during the distillation process. The cold water circulator plays a circulation control role. It delivers cold water from the storage tank to the condenser flask, absorbs the heat of the distillation steam, and causes the steam to condense rapidly into a liquid organic phase. The water that has absorbed the heat is then sent back to the storage tank by the cold water circulator for cooling, forming a closed circulation system.

[0017] The aforementioned organic phase purification device can be further configured such that: the distillation device includes a heater disposed on the outer periphery of the distillation cup, and a temperature controller is provided on one side of the body, the temperature controller being electrically connected to the control system.

[0018] By adopting the above technical solution, the temperature control heating device is set on the outer periphery of the distillation cup, and the temperature controller is connected to the control system. When the temperature inside the distillation cup is higher or lower than the threshold set in the control system, the temperature controller will automatically adjust the heater temperature, reducing manual operation and controlling the processing power and energy consumption.

[0019] The beneficial effects of this invention are as follows: An ultrasonic device is installed at the bottom of the distillation cup. Ultrasonic waves have the characteristics of cavitation effect, which cause the liquid to vibrate and stir violently without mechanical contact with the liquid. This effectively reduces the interference with the liquid elements and greatly ensures the purity of the extracted organic phase. Attached Figure Description

[0020] Figure 1 This is a schematic diagram of the structure of this utility model; Figure 2 This is a schematic diagram of the anti-loosening mechanism connection of this utility model; Labeling notes: 1-Machine body, 2-Distillation cup, 3-Negative pressure pump, 4-Negative pressure bottle, 5-Sealed bottle, 6-Weighing assembly, 7-Outer cylinder, 8-Balance, 9-Control system, 10-Opening and closing valve, 11-Waste bin, 12-Liquid pump, 13-Condensation bottle, 14-Storage tank, 15-Cold water circulator, 16-Heater, 17-Thermostat. Detailed Implementation

[0021] This specific embodiment is merely an explanation of the present utility model and is not intended to limit the present utility model. After reading this specification, those skilled in the art can make modifications to this embodiment without contributing any inventive step, but as long as they are within the scope of the claims of the present utility model, they are protected by patent law.

[0022] like Figure 1-2 The present invention provides the following technical solution: an organic phase purification device, comprising a body 1, a cooling device, a collection component for collecting the organic phase, and a storage component for storing waste liquid, all disposed within the body 1. One end of the cooling device is connected to the storage component, and the other end is connected to the collection component. A distillation device is provided between the storage component and the cooling device. The distillation device includes a distillation cup 2 sealed to the cooling device. An ultrasonic device is provided at the bottom of the distillation cup 2. The distillation cup 2 is in communication with the storage component. A negative pressure device is provided between the cooling device and the storage component. The ultrasonic device at the bottom of the distillation cup 2 has characteristics such as cavitation effect, which can generate tiny gases inside the liquid without mechanical contact with the liquid. The bubbles quickly collapse, causing violent vibration and stirring of the liquid. This non-contact stirring method avoids direct contact between the mechanical structure and the liquid, effectively reducing interference with the liquid elements and greatly ensuring the purity of the extracted organic phase, thus improving the purification quality. The negative pressure device includes a negative pressure pump 3 installed inside the machine body. A negative pressure bottle 4 is fixedly installed on one side of the negative pressure pump 3. The negative pressure pump 3 is connected to the collection component. The negative pressure bottle 4 fixedly installed on one side of the negative pressure pump 3 can effectively store and stabilize the negative pressure environment. The negative pressure pump 3 is connected to the collection component, which can form a stable negative pressure in the collection component, accelerating the flow of the vapor generated by distillation to the collection component, greatly improving the distillation efficiency and shortening the entire purification cycle.

[0023] like Figure 1-2The present invention provides the following technical solution: an organic phase purification device, comprising a collection component including a sealed bottle 5 for collecting the organic phase, the sealed bottle 5 being connected to a cooling device and a negative pressure pump 3, the sealed bottle 5 being equipped with a weighing component 6 for measuring the weight of the sealed bottle 5, and an outer cylinder 7 being provided on one side of the device body, the outer cylinder 7 being connected to the sealed bottle 5, the organic phase in the sealed bottle 5 being discharged into the outer cylinder 7 when the weighing component 6 reaches the set weight, the sealed bottle 5 ensuring the volatilization of the organic phase and the mixing of external impurities, thereby ensuring the purity and quality of the collected organic phase, the sealed bottle 5 being connected to the cooling device and the negative pressure pump 3, the cooling device condensing the vapor generated by distillation into liquid organic phase and transporting it to the sealed bottle 5, while the negative pressure pump 3 maintaining the negative pressure environment of the entire system, accelerating the flow of the organic phase into the sealed bottle 5. The sealed bottle 5 improves collection efficiency. The weighing component 6 includes a balance 8 located at the bottom of the sealed bottle 5. A control system 9 is located on one side of the machine body, and the balance 8 is electrically connected to the control system 9. An opening and closing valve 10 is located on one side of the sealed bottle 5, and the control system 9 can control the opening and closing of the opening and closing valve 10. The balance 8 is electrically connected to the control system 9 and can transmit the measured weight information to the control system 9 in real time, so that the control system 9 can keep track of the weight change of the organic phase in the sealed bottle 5. The opening and closing valve 10 on one side of the sealed bottle 5 works with the control system 9. When the weight measured by the balance 8 reaches the preset value, the control system 9 can react and control the opening or closing of the opening and closing valve 10. When it is open, the organic phase in the sealed bottle 5 is discharged into the outer cylinder 7. The liquid storage component includes waste material connected to the distillation cup 2. A liquid addition pump 12 is installed between the waste container and the distillation cup 2. The waste container in the liquid storage assembly is connected to the distillation cup 2. The liquid addition pump 12 can also overcome factors such as pipeline resistance to a certain extent, ensuring smooth liquid delivery and maintaining the stability of liquid delivery. Simultaneously, the liquid addition pump 12 can return the undistilled waste liquid in the distillation cup 2 to the waste container when the machine stops. The cooling device includes a condenser 13 sealed to the distillation cup 2. A liquid storage tank 14 for storing cold water is installed inside the machine. A cold water circulator 15 for controlling the cold water circulation is installed on one side of the condenser 13. One end of the cold water circulator 15 is connected to the condenser 13, and the other end is connected to the liquid storage tank 14. The condenser 13 is sealed to the distillation cup 2, effectively preventing steam leakage during distillation. The water circulator 15 plays a circulation control role, transporting cold water from the storage tank 14 to the condenser 13 to absorb heat from the distillation vapor, causing the vapor to rapidly condense into a liquid organic phase. The water, after absorbing heat, is then returned to the storage tank 14 by the cold water circulator 15 for further cooling, forming a closed-loop system. The distillation apparatus includes a heater 16 located around the distillation cup 2, and a temperature controller 17 is located on one side of the machine body. The temperature controller 17 is electrically connected to the control system 9. By placing the temperature-controlled heating device around the distillation cup 2 and connecting the temperature controller 17 to the control system 9, the temperature controller 17 automatically adjusts the temperature of the heater 16 when the temperature inside the distillation cup 2 is higher or lower than the threshold set in the control system 9. This reduces manual operation and controls processing power and energy consumption.All components of the organic purification device are connected by pipes, and the temperature controller 17 and balance 8 are electrically connected to the control system 9.

[0024] The beneficial effects of this invention are as follows: An ultrasonic device is installed at the bottom of the distillation cup 2. Ultrasonic waves have the characteristics of cavitation effect, which cause the liquid to vibrate and stir violently without mechanical contact with the liquid. This effectively reduces the interference with the liquid elements and greatly ensures the purity of the extracted organic phase.

Claims

1. An organic phase purification apparatus, comprising a body and a cooling device disposed within the body, a collection component for collecting the organic phase, and a storage component for storing waste liquid, wherein one end of the cooling device is connected to the storage component and the other end is connected to the collection component, and a distillation device is provided between the storage component and the cooling device, characterized in that: The distillation apparatus includes a distillation cup that is sealed to a cooling device. An ultrasonic device is provided at the bottom of the distillation cup. The distillation cup is in communication with a liquid storage component. A negative pressure device is provided between the cooling device and the liquid storage component.

2. The organic phase purification apparatus according to claim 1, characterized in that: The negative pressure device includes a negative pressure pump installed inside the machine body. A negative pressure bottle is fixedly installed on one side of the negative pressure pump, and the negative pressure pump is connected to the collection component.

3. The organic phase purification apparatus according to claim 2, characterized in that: The collection component includes a sealed bottle for collecting organic phase. The sealed bottle is connected to a cooling device and a negative pressure pump. The sealed bottle is equipped with a weighing component for measuring the weight of the sealed bottle. An outer cylinder is provided on one side of the machine body and is connected to the sealed bottle. When the weighing component reaches the set weight, the organic phase in the sealed bottle is discharged into the outer cylinder.

4. The organic phase purification apparatus according to claim 3, characterized in that: The weighing assembly includes a balance set at the bottom of the sealed bottle, a control system is provided on one side of the machine body, the balance is electrically connected to the control system, and an opening and closing valve is provided on one side of the sealed bottle, the control system being able to control the opening and closing of the opening and closing valve.

5. An organic phase purification apparatus according to claim 1, characterized in that: The liquid storage assembly includes a waste container connected to a distillation cup, and a liquid addition pump is provided between the waste container and the distillation cup.

6. The organic phase purification apparatus according to claim 5, characterized in that: The cooling device includes a condenser bottle that is sealed to a distillation cup. The body of the device is equipped with a liquid storage tank for storing cold water. A cold water circulator is provided on one side of the condenser bottle to control the circulation of the cold water. One end of the cold water circulator is connected to the condenser bottle and the other end is connected to the liquid storage tank.

7. An organic phase purification apparatus according to claim 6, characterized in that: The distillation apparatus includes a heater disposed around the periphery of the distillation cup, and a temperature controller is provided on one side of the apparatus body, the temperature controller being electrically connected to the control system.

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