Synthesis system for metal-organic structures for supercapacitor electrodes and multifunctional nanocomposite compositions containing MXene

Abstract

This invention provides a synthesis system for metal-organic structures for supercapacitor electrodes and multifunctional nanocomposite compositions containing MXene. [Solution] The system 100 is configured as a structurally unified device incorporating a rigid structural frame 102, a precursor encapsulation assembly 104, a controlled discharge assembly 106, a sealed reaction chamber assembly 108, a mechanical stirring assembly 110, a delamination assembly 112 based on a rotor-stator configuration, a temperature control assembly 114, a pressure control element, and a composite recovery device. It operates through coordinated electromechanical interactions to ensure controlled supply of precursor material, uniform mixing, effective delamination of the layered MXene structure, and maintenance of predetermined thermal and pressure conditions. The integration of these hardware elements enables consistent formation of nanocomposite materials with improved structural uniformity, surface properties, and electrochemical performance.

Description

Technical Field

[0001] The present invention relates to the field of advanced material synthesis systems, and more specifically, to a mechanically integrated device for the controlled synthesis of multifunctional nanocomposite compositions containing metal-organic framework materials and MXene structures, which are used in high-performance supercapacitor electrodes. The present invention particularly addresses the aspects of structural, mechanical, and thermodynamic control required to produce hybrid nanomaterials with improved electrochemical properties in a scalable and reproducible manner.

Background Art

[0002] The development of highly efficient energy storage devices has become essential for exploring hybrid nanocomposite materials that combine a large specific surface area of metals and adjustable porosity. Conventional synthesis methods are prone to problems such as low reproducibility, insufficient control of material morphology, non-uniform mixing, and insufficient delamination of layered structures. Furthermore, existing laboratory-scale methods lack the mechanical integrity and scalability required for industrial production. Therefore, there is a need for a structurally robust and mechanically controlled system that can synthesize such nanocomposite materials under precisely controlled conditions of mixing, shearing, temperature, and pressure.

[0003] With the rapid advancement of portable electronic devices, electric vehicles, and grid-level energy storage systems, there is a significant increase in demand for high-performance energy storage devices with high power density, long lifespan, and rapid charge / discharge characteristics. Among the various available technologies, supercapacitors have emerged as a promising solution due to their ability to bridge the gap between conventional dielectric capacitors and electrochemical batteries. However, the performance of supercapacitors is primarily dependent on the properties of the electrode material. Electrode materials require a high specific surface area, excellent conductivity, chemical stability, and efficient ion transport pathways. Against this backdrop, hybrid nanocomposites combining metal-organic structures and two-dimensional MXene materials have emerged. In-situ growth is a method that directly grows metal-organic structures on the surface of MXene sheets to improve interfacial bonding and dispersibility. While this method enhances the interaction between the two components, insufficient control of nucleation and growth rates makes it prone to coating non-uniformity and morphological variability of the composite material. Furthermore, these methods are often highly dependent on chemical conditions such as pH, solvent composition, and precursor concentration, making it difficult to ensure consistent reproducibility in large-scale production environments.

[0004] Another common method combines ultrasonic treatment with mechanical mixing, where pre-synthesized metal-organic structure particles and MXene sheets are physically mixed in a liquid medium. Ultrasonic treatment is used to promote dispersion and partial delamination of the MXene layer. However, this method has inherent limitations, such as insufficient control of mixing uniformity and shear force. Ultrasonic treatment can cause localized cavitation effects, which may impair the structural integrity of both the metal-organic structure and the MXene component. Furthermore, insufficient control of shear conditions often results in incomplete delamination of the MXene layer, leading to aggregation and reduced electrochemical performance.

[0005] Spray drying and freeze-drying methods have also been investigated for the fabrication of composite materials of metal-organic structures and MXene. These methods aim to form porous structures by rapidly removing the solvent from the precursor suspension. Although these methods have some scalability, they cannot adequately control the formation of the internal microstructure, and the resulting composite materials often exhibit irregular morphologies and suffer from weak interfacial bonding between constituent components. Furthermore, these processes usually require post-treatment steps such as annealing and chemical modification, which further increases complexity and energy consumption.

[0006] From a mechanical and systems perspective, many existing solutions feature fragmented processing steps that are not integrated into a single, unified system. Synthesis processes often involve multiple independent stages, such as precursor preparation, mixing, reaction, exfoliation, and recovery, each performed using separate equipment. This lack of integration leads to inefficiency, increased contamination risks, and variability in product quality.

[0007] Furthermore, the inability to control critical parameters such as temperature, pressure, shear rate, and mixing dynamics in real time limits the ability to consistently produce reproducible material properties.

[0008] Therefore, despite significant progress in the development of metal-organic structure-MXene nanocomposites, existing synthesis methods face limitations in process integration, control precision, scalability, and material uniformity. These challenges highlight the need for a mechanically integrated system that can control and synchronize all critical synthesis steps, including precursor handling, mixing, exfoliation, thermal management, pressure regulation, and product recovery. Such a system would not only improve reproducibility and efficiency but also enable large-scale production of high-quality nanocomposite materials suitable for advanced supercapacitor applications. [Overview of the project] [Problems that the invention aims to solve]

[0009] This invention provides a mechanically engineered synthesis system configured as an integrated device consisting of interconnected structural and functional assemblies designed to facilitate the controlled preparation of nanocomposite compositions comprising metal-organic structures and MXene materials. The system integrates precursor storage, precise dispensing, controlled mixing, mechanical exfoliation, temperature control, pressure management, and final recovery within a single, robust structural framework, thereby ensuring consistency, scalability, and enhanced material properties suitable for supercapacitor electrode applications. The invention described herein is based on the system architecture disclosed in the appended claims.

[0010] The primary objective of this invention is to provide a mechanically integrated system for synthesizing multifunctional nanocomposite compositions containing metal-organic structures and MXene materials for application in supercapacitor electrodes. This system is configured as a structurally unified apparatus capable of handling precursors, controlled mixing, exfoliation, reaction, and recovery within a single, coordinated framework. This invention aims to overcome the limitations of conventional fragmented and multi-step synthesis techniques by enabling all essential processes to be performed continuously and synchronously, thereby improving reproducibility, efficiency, and material uniformity.

[0011] A further objective of this invention is to provide a structurally robust and vibration-isolated system framework that can maintain mechanical stability during high-speed stirring and peeling operations, thereby reducing wear, minimizing energy loss, and increasing operational reliability.

[0012] Another objective of this invention is to achieve scalability in nanocomposite synthesis by providing a system architecture that supports continuous or semi-continuous operation, thereby bridging the gap between laboratory-scale experimentation and industrial-scale production of advanced electrode materials.

[0013] Furthermore, the objective of this invention is to enable the synthesis of nanocomposite materials with increased specific surface area, improved conductivity, and optimized structural form through precise mechanical and thermodynamic control during the synthesis process, thereby improving the electrochemical performance of supercapacitor electrodes. [Means for solving the problem]

[0014] To solve the above problems, the present invention provides a synthesis system for a multifunctional nanocomposite composition containing a metal-organic structure for supercapacitor electrodes and MXene, comprising: a rigid structural frame configured to support a plurality of mechanical assemblies connected to one another; a precursor encapsulation assembly comprising a plurality of sealed material reservoirs configured to store precursor materials corresponding to the components of the metal-organic structure and the MXene material; a controlled dispensing assembly mechanically connected to the precursor encapsulation assembly, the controlled dispensing assembly comprising a precision metering valve, a linear actuator, and a flow control conduit configured to perform controlled dispensing of the precursor material; and a reaction chamber assembly comprising a mechanically sealed housing mounted on the rigid structural frame and defining an internal mixing cavity formed from a chemically inert material. A composite recovery assembly comprising: a mechanical stirring assembly functionally connected to the reaction chamber assembly, the mechanical stirring assembly comprising a rotating shaft, a gear transmission, and a variable-speed drive motor configured to generate a controlled stirring force within an internal mixing cavity; a delamination assembly mechanically connected to the reaction chamber assembly, comprising a rotor-stator configuration configured to induce structural separation of the laminated MXene material; a temperature control assembly comprising a thermally conductive jacket positioned around the reaction chamber assembly and a connected heat exchange unit configured to maintain predetermined thermal conditions; a pressure control assembly comprising a sealed pressure vessel configuration integrated with a mechanical pressure control valve and a pressure sensing interface; and a composite recovery assembly comprising a discharge conduit and a mechanically operated outlet valve configured to transfer the nanocomposite material to a storage container, wherein the precursor encapsulation assembly further comprises a mechanically stirred storage container comprising an internal impeller driven by a dedicated electric motor configured to maintain a uniform distribution of metal-organic skeleton precursor components, wherein the control discharge assembly further comprises a cam-operated metering mechanism coupled with a rotary position encoder configured to provide synchronous volumetric discharge. [Effects of the Invention]

[0015] The present invention relates to a synthesis system for a multifunctional nanocomposite composition containing a metal-organic structure and MXene for use in supercapacitor electrodes. The system is configured as a structurally unified apparatus incorporating a rigid structural frame, a precursor encapsulation assembly, a controlled dispensing assembly, a sealed reaction chamber assembly, a mechanical stirring assembly, a delamination assembly based on a rotor-stator configuration, a temperature control assembly, a pressure control element, and a composite recovery device. The system operates through coordinated electromechanical interactions to ensure controlled supply of precursor materials, uniform mixing, effective delamination of the layered MXene structure, and maintenance of predetermined thermal and pressure conditions. The integration of these hardware elements enables the consistent formation of nanocomposite materials with improved structural uniformity, surface properties, and electrochemical performance. [Brief explanation of the drawing]

[0016] These features, aspects, and advantages of the present invention, as well as other features, aspects, and advantages, will be better understood by reading the following detailed description in conjunction with the accompanying drawings. In the drawings, the same symbol indicates the same part throughout all drawings.

[0017] Figure 1 shows a block diagram of a synthesis system for producing a nanocomposite composition consisting of a metal-organic structure and MXene for use as a supercapacitor electrode.

[0018] Furthermore, those skilled in the art will understand that elements in the drawings are shown for simplification and are not necessarily drawn to actual size. For example, flowcharts illustrate the method with respect to the most prominent steps involved to aid in understanding aspects of the disclosure. Also, with respect to the configuration of the apparatus, one or more components of the apparatus may be represented in the drawings by conventional symbols, and the drawings may show only certain details relevant to understanding embodiments of the disclosure so as not to obscure the drawings with details that are easily understood by those skilled in the art who enjoy the description herein. [Modes for carrying out the invention]

[0019] For the purpose of facilitating the understanding of the principles of the invention, the embodiments shown in the drawings will be referenced and specific terminology will be used in describing them. However, this is not intended to limit the scope of the invention, and it should be understood that any modifications or further improvements to the illustrated system, and further applications of the principles of the invention shown therein, are within the realm of what a person skilled in the art would ordinarily conceive.

[0020] Those skilled in the art will understand that the above-mentioned general description and the following detailed description are for illustrative purposes only and are not intended to limit the present invention.

[0021] Throughout this specification, the phrases “one aspect,” “another aspect,” or similar expressions mean that a particular function, structure, or feature described in relation to an example is included in at least one example. Therefore, the occurrence of phrases “in one example,” “in another example,” and similar expressions throughout this specification does not necessarily refer to the same example.

[0022] The expressions “includes,” “is included,” or other similar expressions are intended to be non-exclusive, and a process or method containing a list of steps does not include only those steps, but may include other steps not expressly stated or inherent in the process or method. Similarly, one or more devices, subsystems, elements, structures, or components preceding “includes…” does not, unless further restricted, exclude the existence of other devices, other subsystems, other elements, other structures, other components, additional devices, additional subsystems, additional elements, additional structures, or additional components.

[0023] Unless otherwise defined, all technical and scientific terms used herein have the same meanings as those commonly understood by those skilled in the art to which this invention pertains. The systems, methods, and embodiments described herein are illustrative and not intended to be limiting.

[0024] Examples of this specification will be described in detail below with reference to the accompanying drawings. Referring to FIG. 1, a block diagram of a mechanical synthesis system for manufacturing a nanocomposite composition including a metal organic structure and MXene used for a supercapacitor electrode is shown. System 100 consists of the following components: a rigid structure frame (102) configured to support a plurality of interconnected mechanical assemblies; a precursor encapsulation assembly (104) including a plurality of sealed material reservoirs configured to store precursor substances corresponding to the components of the metal organic structure and the MXen material; a control discharge assembly (106) mechanically connected to the precursor encapsulation assembly. This control discharge assembly includes a precision metering valve, a linear actuator, and a flow adjustment conduit configured to perform a controlled discharge of the precursor substance; a reaction chamber assembly (108) including a mechanically sealed housing mounted on the rigid structure frame and defining an internal mixing cavity formed of a chemically inert material; a mechanical stirring assembly (110) functionally connected to the reaction chamber assembly. This mechanical stirring assembly includes a rotating shaft, a gear transmission, and a variable speed drive motor configured to generate a controlled stirring force within the internal mixing cavity; a delamination assembly (112) having a rotor-stator configuration mechanically connected to the reaction chamber assembly and configured to induce a structural separation of the laminated MXene material; a temperature adjustment assembly (114) including a thermally conductive jacket disposed around the reaction chamber assembly and an associated heat exchange unit configured to maintain a predetermined thermal condition; a pressure adjustment assembly (116) including a sealed pressure vessel configuration integrated with a mechanical pressure control valve and a pressure sensing interface; and a composite material recovery assembly (118) including a discharge conduit configured to transfer the nanocomposite material to a storage container and a mechanically actuated discharge valve.

[0025] In one embodiment, the precursor encapsulation assembly (104) further comprises a mechanically stirred storage container with an internal impeller driven by a dedicated electric motor configured to maintain a uniform distribution of the metal-organic framework precursor component.

[0026] In one embodiment, the controlled dispensing assembly (106) further comprises a cam-operated metering mechanism coupled with a rotary position encoder configured to effect synchronous volumetric dispensing.

[0027] In one embodiment, the reaction chamber assembly (108) is composed of a double-walled housing made of a corrosion-resistant alloy material and lined with polytetrafluoroethylene to withstand the chemical interaction with the metal-organic framework precursor and the MXene material.

[0028] In one embodiment, the mechanical agitation device (110) comprises a multi-stage impeller configuration including an axial flow impeller and a radial flow impeller arranged along a common axis to generate a multi-directional flow field.

[0029] In one embodiment, the delamination assembly (112) comprises a mechanically adjustable rotor-stator gap configured to control the shear strength applied to the MXene material.

[0030] In one embodiment, the temperature regulation assembly (114) further comprises a closed-loop circulation device including a pump, a heat exchanger, and an integrated flow path network provided within a thermally conductive jacket.

[0031] In one embodiment, the pressure regulation assembly further comprises a spring-loaded relief valve and a diaphragm-type pressure sensing element integrally formed within a sealed pressure vessel structure. In one embodiment, the composite recovery assembly further comprises a filtration unit including a porous membrane configured to adjust the particle size distribution of the nanocomposite composition.

[0032] In one embodiment, the rigid structural frame further includes vibration-damping elements configured to minimize the transmission of mechanical vibrations generated by the mechanical stirring assembly.

[0033] In one embodiment, the peeling assembly (112) further comprises a high-torque drive motor connected via a reduction gearbox configured to maintain the continuous shear conditions necessary for the separation of the MXene layer.

[0034] In one embodiment, the reaction chamber assembly further comprises an internal baffle arrangement configured to enhance mixing uniformity and prevent localized concentration gradients within the nanocomposite composition.

[0035] This system is fully realized by physical and electromechanical components configured to perform defined operations without relying on abstract or non-physical concepts. The structural frame, reaction chamber, storage tank, piping, valves, shafts, gears, impeller, rotor / stator mechanism, and filtration elements are all manufactured from industrial materials and assembled to form a functional device. Measurement and control are performed using discrete sensing devices such as pressure transducers, temperature probes, and position encoders that generate electrical signals directly from physical states. These signals are processed by an electronic control circuit consisting of wired controllers, analog-to-digital converters, and drive circuits that drive motors, pumps, and linear actuators through physical electrical connections. Material flow is controlled by mechanically operated valves and metering mechanisms, and mixing and separation are performed by rotating shafts and drive assemblies that apply force within the reaction chamber. Thermal control is performed through a heat exchange structure with fluid circulation paths, and pressure control is maintained using mechanical relief valves and sealed container structures. Therefore, since each function of the system is performed by identifiable hardware elements that work together through electrical and mechanical interactions, direct implementation and reproducible operation in industrial environments are possible.

[0036] This invention provides a mechanically integrated system for synthesizing multifunctional nanocomposite compositions comprising metal-organic structures and MXene materials. The system's operation is controlled by coordinated control techniques implemented through electromechanical drives, sensing feedback, and synchronized sequences of mechanical assemblies. These techniques are configured to coordinate a series of interdependent functions, including precursor storage, dispensing, mixing, exfoliation, heat treatment, pressure stabilization, and composite material recovery, thereby ensuring controlled synthesis conditions and reproducible material properties, as disclosed in the system architecture.

[0037] In the initial stages of operation, the technology initiates a precursor preparation sequence and activates the precursor encapsulation assembly to maintain a uniform distribution of the stored material. An internal impeller within a sealed reservoir is driven at a predetermined rotational speed determined based on the viscosity and density parameters of the precursor material. The technology continuously evaluates rotational resistance and torque feedback to ensure that sedimentation and phase separation do not occur, thereby preparing the precursor for controlled discharge. Simultaneously, environmental parameters such as ambient temperature and initial chamber conditions are evaluated to establish baseline operating conditions for subsequent stages.

[0038] After precursor preparation, the technology transitions to a synchronized dispensing phase, activating the controlled dispensing assembly. A cam-driven metering mechanism works in conjunction with a rotary position encoder to achieve precise volumetric dispensing of the precursor material into the reaction chamber assembly. The technology calculates the required flow rate based on predefined stoichiometric ratios and dynamically adjusts the displacement of the linear actuator and the valve opening profile to maintain consistency. Feedback signals from the flow control piping and position encoder are processed in real time, and deviations are corrected to ensure that the introduction of the metal-organic structure components and MXene material is carried out in a controlled and repeatable manner.

[0039] Once the discharge process is complete, the technology initiates the reaction and mixing sequence within the reaction chamber assembly. A mechanical stirring assembly is activated, and a variable-speed drive motor rotates a multi-stage impeller configuration to generate a multi-directional flow field. The technology adjusts the rotational speed, torque, and operating state of the impeller configuration based on real-time feedback from internal sensors that measure viscosity, shear resistance, and mixing uniformity. The internal baffle arrangement within the chamber interacts with the induced fluid pattern to eliminate stagnant areas, and the technology continuously evaluates mixing efficiency by analyzing variations in mechanical load and hydrodynamics. This closed-loop control ensures uniform dispersion of precursor materials and promotes consistent nucleation of metal-organic structures.

[0040] Simultaneously, this technology coordinates the operation of a delamination assembly mechanically connected to the reaction chamber. The rotor-stator configuration is activated, applying the controlled shear force necessary for interlaminar delamination of the layered MXene material. This technology adjusts the gap between the rotor and stator via a mechanical actuator, thereby controlling the shear intensity in response to feedback signals indicating particle size distribution and shear stress levels. A high-torque drive motor, coupled to a reduction gearbox, is controlled to maintain continuous and stable shear conditions. By dynamically balancing shear force and exposure time, this technology ensures that delamination occurs without excessive fracturing or structural degradation.

[0041] Temperature control is achieved through continuous interaction between the technology and a temperature control device. A circulating heat exchange fluid is supplied to a thermally conductive jacket surrounding the reaction chamber, and the technology monitors the temperature gradient throughout the reaction chamber using distributed sensing elements. Based on these measurements, the technology adjusts the pump speed, the operating status of the heat exchanger, and the fluid distribution within the internal channel network to maintain a predefined thermal profile. This controlled thermal environment is essential for regulating the reaction rate and ensuring uniform crystal growth within the nanocomposite structure.

[0042] In parallel, the pressure regulation assembly is controlled by this technology to maintain safe and optimal pressure conditions within the reaction chamber. Pressure data obtained from the diaphragm sensing element is continuously analyzed, and this technology activates the mechanical pressure control valve to adjust the internal pressure level. If pressure fluctuations exceed a preset threshold occur, a spring-loaded relief valve automatically activates to prevent structural stress and system failure. This technology integrates pressure data with temperature and mixing parameters to ensure that all thermodynamic conditions remain within the desired operating range.

[0043] As the synthesis process progresses toward completion, the technology evaluates key indicators such as mixing stability, shear consistency, thermal equilibrium, and pressure uniformity to determine the reaction's termination point. Once predefined completion criteria are met, the system moves to a controlled discharge phase. The composite material recovery assembly is activated, and a mechanically operated discharge valve opens in a controlled manner, transferring the synthesized nanocomposite material through the discharge pipe. This technology ensures a constant discharge flow rate and prevents clogging and pressure fluctuations during material transfer.

[0044] During the discharge process, a filtration unit integrated into the composite recovery assembly operates to adjust the particle size distribution. This technology monitors the flow resistance at both ends of the porous membrane and adjusts the discharge pressure accordingly, maintaining efficient filtration while preventing membrane fouling. As a result, a nanocomposite composition with controlled morphology and uniform structural properties is recovered into the storage container.

[0045] This technology maintains synchronization between all mechanical assemblies throughout the entire operating cycle through continuous feedback and adaptive control. A robust structural frame with vibration isolation elements provides a stable foundation that minimizes mechanical disturbances, and the technology compensates for residual vibrations by adjusting motor rotation speed and actuator response. This integrated control strategy ensures that all stages of the synthesis process operate in harmony, resulting in improved process reliability and product uniformity.

[0046] The coordinated interaction of the mechanical components described above enables precise control of key synthesis parameters such as precursor ratio, mixing strength, shear force, temperature distribution, and pressure conditions. By integrating these parameters into a unified control framework, this system achieves highly reproducible synthesis of multifunctional nanocomposite materials with optimized electrochemical properties suitable for supercapacitor electrode applications.

[0047] This system consists of a rigid frame that serves as the foundational support structure for all mechanical and functional assemblies. This frame is designed to maintain dimensional stability and alignment during operation. The frame also incorporates vibration damping elements to reduce mechanical vibrations generated during high-speed stirring and peeling processes, thereby ensuring operational stability and extending component life.

[0048] The structural frame is fitted with a precursor containment assembly consisting of multiple sealed reservoirs configured to store precursor materials related to the formation of metal-organic structures and the preparation of MXene materials. Each reservoir is designed from chemically compatible materials and may feature an internal impeller driven by a dedicated motor to maintain a uniform suspension of the precursor components and prevent sedimentation. This containment assembly is mechanically connected to a control discharge assembly consisting of precision metering valves, linear actuators, and flow control piping. The discharge assembly is configured to deliver the precursor material to the reaction chamber in a synchronized and volume-controlled manner, with a cam drive mechanism and rotary position encoders enabling accurate and repeatable discharge cycles.

[0049] The reaction chamber assembly is located in the center of the system and consists of a mechanically sealed enclosure that forms an internal mixing cavity. This enclosure is preferably made of a corrosion-resistant alloy and lined with polytetrafluoroethylene to withstand the reaction with chemically corrosive precursors. Furthermore, the chamber is equipped with internal baffles configured to disrupt the flow pattern and eliminate dead zones, thereby promoting a uniform distribution of reactants.

[0050] The mechanical agitator is functionally connected to the reaction chamber and comprises a rotating shaft supported by a bearing structure, a gear transmission mechanism, and a variable-speed drive motor. A multi-stage impeller configuration, combining axial and radial flow impellers, is attached to this shaft, and together these elements generate a complex, multi-directional flow field within the mixing chamber. This configuration ensures uniform mixing and promotes the nucleation and growth of metal-organic structures in the presence of MXene material.

[0051] The delamination apparatus is mechanically integrated with the reaction chamber and features a rotor-stator configuration designed to generate the high shear force necessary for delaminating the layered MXene structure. The gap between the rotor and stator is mechanically adjustable, allowing for precise control of the shear strength and thus the degree of delamination. The apparatus is driven by a high-torque motor connected via a reduction gearbox, maintaining stable shear conditions even during continuous operation.

[0052] Furthermore, the system includes a temperature control assembly consisting of a thermally conductive jacket surrounding the reaction chamber. This jacket is integrated with a closed-loop circulation system that includes a pump, heat exchanger, and internal flow channels. This configuration allows for the precise maintenance of the thermal conditions necessary for a controlled synthetic reaction, which in turn affects the crystallinity and structural integrity of the resulting nanocomposite.

[0053] The pressure regulation assembly is incorporated as part of a sealed pressure vessel configuration, integrating a mechanical pressure control valve and a sensing interface. This assembly includes a spring-loaded relief valve and a diaphragm-type pressure sensor, which monitor and regulate the pressure in the reaction chamber in real time to prevent overpressure and ensure safe operation.

[0054] Once the synthesis process is complete, the nanocomposite material is transported through a composite recovery system consisting of an exhaust pipe and a mechanically operated exhaust valve. This system may further include a filtration unit with a porous membrane configured to adjust the particle size distribution and remove unwanted aggregates, thereby ensuring consistency in the final composition of the nanocomposite material.

[0055] The integrated operation of this system enables the controlled synthesis of multifunctional nanocomposite materials with improved specific surface area, conductivity, and electrochemical properties, and the resulting materials are particularly suitable for application as electrodes for high-efficiency supercapacitors.

[0056] This system provides a highly scalable and mechanically robust solution for the industrial production of advanced nanocomposite materials. Its precise control over mixing, delamination, thermal conditions, and pressure makes it ideally suited for the manufacture of next-generation energy storage materials, including supercapacitors, where performance stability and material quality are critical.

[0057] The drawings and the preceding description illustrate examples of embodiments. Those skilled in the art will understand that it is possible to integrate one or more of the described elements into a single functional element. Alternatively, it is possible to divide a particular element into multiple functional elements. It is also possible to add elements of one embodiment to another. For example, the order of processes described herein is changeable and is not limited to the methods described herein. Furthermore, the operations in any flowchart do not need to be implemented in the order shown, and not all operations necessarily need to be performed. Operations that do not depend on other operations may be performed in parallel with other operations. The scope of embodiments is by no means limited by these specific examples. Numerous variations are possible, whether or not they are explicitly stated in the specification, including differences in structure, dimensions, and use of materials. The scope of embodiments is at least equivalent to, or broader than, the scope given by the following claims.

[0058] The advantages, other merits, and solutions to problems of the specific embodiments described above have been explained. However, these advantages, merits, solutions to problems, and the components that bring them about or enhance their effects should not be construed as definitive, essential, or indispensable features or components in any or all of the claims.

Claims

1. A synthesis system for a multifunctional nanocomposite composition containing a metal-organic structure for supercapacitor electrodes and MXene, A rigid structural frame configured to support multiple mechanical assemblies connected to one another; A precursor encapsulation assembly comprising multiple sealed material reservoirs configured to store precursor materials corresponding to the components of a metal-organic structure and MXene material; A controlled dispensing assembly mechanically connected to the precursor-filling assembly, the controlled dispensing assembly comprising a precision metering valve, a linear actuator, and a flow-regulating conduit configured to perform controlled dispensing of the precursor material; A reaction chamber assembly including a mechanically sealed housing mounted on the rigid structural frame and defining an internal mixing cavity formed from a chemically inert material; A mechanical stirring assembly functionally connected to the reaction chamber assembly, the mechanical stirring assembly includes a rotating shaft, a gear transmission, and a variable-speed drive motor configured to generate a controlled stirring force within the internal mixing cavity; A delamination assembly mechanically connected to the reaction chamber assembly, comprising a rotor-stator configuration configured to induce structural separation of the laminated MXene material; A temperature control assembly comprising a heat-conductive jacket positioned around the reaction chamber assembly and connected heat exchange units configured to maintain predetermined thermal conditions; A pressure regulating assembly comprising a sealed pressure vessel configuration integrated with a mechanical pressure control valve and a pressure sensing interface; and A composite recovery assembly comprising a discharge conduit and a mechanically operated outlet valve configured to transfer nanocomposite materials to a storage container, Here, the precursor encapsulation assembly further includes a mechanically agitated storage container equipped with an internal impeller driven by a dedicated electric motor configured to maintain a uniform distribution of the metal-organic skeleton precursor component, A synthesis system for metal-organic structures for supercapacitor electrodes and multifunctional nanocomposite compositions containing MXene, characterized in that the control dispensing assembly further includes a cam-operated metering mechanism coupled with a rotary position encoder configured to provide synchronous volume dispensing.

2. The synthesis system for a multifunctional nanocomposite composition containing a metal-organic structure and MXene for supercapacitor electrodes according to claim 1, characterized in that the reaction chamber assembly includes a double-walled housing made from a corrosion-resistant alloy material and lined with polytetrafluoroethylene to withstand chemical interactions with the metal-organic structure precursor and the MXene material.

3. The mechanical stirring assembly has a multi-stage impeller configuration including an axial flow impeller and a radial flow impeller arranged along a common axis to generate a multi-directional flow field. The peeling assembly has a mechanically adjustable rotor-stator gap configured to control the shear strength acting on the MXene material, The temperature control assembly further includes a closed-loop circulation device comprising a pump, a heat exchanger, and a flow path network integrated within a heat-conducting jacket. The synthesis system for a metal-organic structure for a supercapacitor electrode and a multifunctional nanocomposite composition containing MXene, characterized in that the pressure adjustment assembly further includes a spring-loaded relief valve and a diaphragm-type pressure sensing element integrated into a sealed pressure vessel configuration, as described in claim 1.

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