A water-soluble environmentally friendly DTY oil and its preparation method
By preparing a water-soluble and environmentally friendly DTY oil, the problems of environmental pollution and antistatic instability are solved, and environmentally friendly and efficient fiber processing is achieved, which is suitable for a variety of weaving equipment.
Patent Information
- Application Number
- CN202311766110.4
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2023-12-21
- Publication Date
- 2025-09-05
- Estimated Expiration
- 2043-12-21
AI Technical Summary
Existing DTY oils are not environmentally friendly and have unstable antistatic properties, leading to fiber winding and breakage problems and potentially causing pollution.
It uses water-soluble environmentally friendly DTY oil, an emulsifier composed of ethylene glycol, polyethylene glycol compound, fatty alcohol polyoxyethylene ether and sorbitan ester polyoxyethylene ether, as well as additives such as imidazoline salt and alcohol ether phosphate salt. It is prepared through specific proportions and processes to form a stable emulsion state, thereby improving antistatic properties and smoothness.
The prepared DTY oil is environmentally friendly and harmless, has excellent antistatic performance, reduces fiber breakage, improves production efficiency, meets medium and high-end dyeing requirements, and is suitable for a variety of weaving equipment.
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Abstract
Description
Technical Field
[0001] The invention belongs to the technical field of auxiliary agents in synthetic fiber processing technology, and particularly relates to a method for preparing a water-soluble environmentally friendly DTY oil agent. Background Art
[0002] DTY oil, also known as finished product oil or coning oil, is used in the DTY process of polyester high-speed spinning (POY-DTY) and is used in the yarn finishing process. During the stretching and twisting process, some of the pre-spinning oil is lost, necessitating a post-processing re-apply of oil, often referred to as DTY oil, to ensure smooth unwinding of the yarn from the bobbin and meet the yarn performance requirements of the weaving process.
[0003] DTY oil needs to be suitable for high-speed processing and provide good smoothness, antistatic properties and washability. At the same time, the oil washed out should not contain non-biodegradable harmful substances to ensure the environmental protection of the production process.
[0004] my country's chemical fiber industry has grown rapidly in recent years, particularly with the expansion of the polyester industry. This has led to an increasing demand for DTY finishes, both in terms of variety and quantity. However, current DTY finishes on the market present several challenges. First, they are environmentally unfriendly and may contribute to new pollution. Second, their unstable antistatic properties can lead to fiber entanglement and breakage when used in dry seasons.
[0005] Therefore, it is necessary to find a preparation method of a water-soluble environmentally friendly DTY oil with a new formula, and a preparation method thereof, wherein the prepared DTY oil is green and environmentally friendly and has excellent antistatic and smoothness. Summary of the Invention
[0006] Purpose of the invention: In order to overcome the above shortcomings, the purpose of the present invention is to provide a water-soluble environmentally friendly DTY oil and a preparation method thereof. The formula design is reasonable, the preparation method is simple, the prepared DTY oil is green and environmentally friendly, has excellent antistatic and smoothness, and has broad application prospects.
[0007] The purpose of the present invention is achieved through the following technical solutions:
[0008] A water-soluble environmentally friendly DTY oil agent, comprising the following raw materials in weight fractions:
[0009] 70-90% of the main ingredient, which is a mixture of ethylene glycol and polyethylene glycol, or a mixture of ethylene glycol butyl ether acetate and polyethylene glycol, or a mixture of isomeric alcohol ethers, polyethylene glycol and ethylene glycol;
[0010] 5-15% emulsifier, which is a compound of fatty alcohol polyoxyethylene ether and sorbitan ester polyoxyethylene ether;
[0011] 5-15% of additives, wherein the additives are a two-component or three-component compound, and are selected from at least two of imidazoline salts, alcohol ether phosphate salts, polyethylene glycol esters, and polyoxyethylene ether phosphates;
[0012] The sum of the components is 100%.
[0013] The water-soluble, environmentally friendly DTY finish described in this invention consists of a main ingredient, an emulsifier, and additives. This water-soluble, environmentally friendly DTY finish is primarily used for producing DTY low-stretch yarn on various types of imported and domestic texturing machines. This DTY low-stretch yarn is primarily used for weaving on warp knitting machines, including KS warp knitting machines, circular knitting machines, and water-jet looms. Tests have shown that this water-soluble, environmentally friendly DTY finish achieves normal weaving efficiency, eliminates abnormal end breaks, and exhibits a high decontamination rate, meeting mid- and high-end dyeing requirements. It can replace conventional finishes.
[0014] Furthermore, in the above-mentioned water-soluble environmentally friendly DTY oil, the main ingredient is a compound of ethylene glycol and polyethylene glycol, the emulsifier is a compound of fatty alcohol polyoxyethylene ether and sorbitan ester polyoxyethylene ether; and the additive is a compound of polyethylene glycol ester and polyoxyethylene ether phosphate.
[0015] The formula design of the above-mentioned water-soluble environmentally friendly DTY oil is reasonable. It is made of environmentally friendly ingredients, does not contain harmful substances, is environmentally friendly, and will not pollute the natural environment during use. Fatty alcohol polyoxyethylene ether and dehydrated sorbitan ester polyoxyethylene ether form a two-component emulsifier compound, which can effectively mix the main ingredients and additives to form a stable emulsion state, which is convenient for use and storage. Polyethylene glycol ester and polyoxyethylene ether phosphate form a two-component additive compound, which can improve the viscosity and fluidity of the oil and reduce the surface tension, making the oil easier to apply, penetrate and disperse during the application process. The above-mentioned two-component emulsifier compound and two-component additive compound can improve the stability of the oil, prevent the separation and precipitation of components, extend the service life of the oil, and reduce the number of times new oil needs to be frequently prepared.
[0016] Furthermore, in the above-mentioned water-soluble environmentally friendly DTY oil, the main ingredient is a compound of ethylene glycol and polyethylene glycol, and the mass ratio of the ethylene glycol and polyethylene glycol is 1:4; the emulsifier is a compound of fatty alcohol polyoxyethylene ether AEO-7 and anhydrous sorbitan polyoxyethylene ether T-80, and the mass ratio of the fatty alcohol polyoxyethylene ether AEO-7 and anhydrous sorbitan polyoxyethylene ether T-80 is 1:1; the polyethylene glycol ester in the additive is selected from at least one of polyethylene glycol ester 600MO, polyethylene glycol ester 400MO, and polyethylene glycol ester 400DO, and the polyoxyethylene ether phosphate in the additive is selected from at least one of polyoxyethylene ether phosphate OE-3P and polyoxyethylene ether phosphate OEP-70, and the mass ratio of polyethylene glycol ester and polyoxyethylene ether phosphate in the additive is 3:7.
[0017] Furthermore, in the above-mentioned water-soluble environmentally friendly DTY oil, the main ingredient is a compound of ethylene glycol butyl ether acetate and polyethylene glycol, the emulsifier is a compound of branched fatty alcohol polyoxyethylene ether and sorbitan polyoxyethylene ether; and the additive is a compound of alcohol ether phosphate salt, polyethylene glycol ester, and polyoxyethylene ether phosphate.
[0018] The water-soluble, environmentally friendly DTY oil has a rational formula design. Its two-component main ingredient compound (ethylene glycol butyl ether acetate and polyethylene glycol) of ether ester and polyol exhibits excellent solubility and adhesion. Its two-component emulsifier compound of branched fatty alcohol polyoxyethylene ether and sorbitan ester polyoxyethylene ether allows the oil to mix thoroughly with water to form a stable emulsion. The three-component additive compound of alcohol ether phosphate, polyethylene glycol ester, and polyoxyethylene ether phosphate enhances the oil's wettability and permeability, improving cleaning effectiveness. Furthermore, it is formulated with environmentally friendly ingredients, free of harmful substances, and environmentally friendly.
[0019] Furthermore, the above-mentioned water-soluble environmentally friendly DTY oil agent, the main ingredient is a compound of ethylene glycol butyl ether acetate and polyethylene glycol, the mass ratio of ethylene glycol butyl ether acetate and polyethylene glycol is 1:19; the fatty alcohol polyoxyethylene ether in the emulsifier is selected from at least one of branched fatty alcohol polyoxyethylene ether O-20, branched fatty alcohol polyoxyethylene ether O-23, and branched fatty alcohol polyoxyethylene ether O-25, the anhydrous sorbitan ester polyoxyethylene ether adopts anhydrous sorbitan ester polyoxyethylene ether T-80, and the branched fatty alcohol polyoxyethylene ether in the emulsifier is selected from at least one of branched fatty alcohol polyoxyethylene ether O-20, branched fatty alcohol polyoxyethylene ether O-23, and branched fatty alcohol polyoxyethylene ether O-25. , anhydrous sorbitan ester polyoxyethylene ether is in a mass ratio of 3:2; the polyethylene glycol ester in the additive is selected from at least one of polyethylene glycol ester 600MO, polyethylene glycol ester 400MO, and polyethylene glycol ester 400DO; the polyoxyethylene ether phosphate in the additive is selected from at least one of polyoxyethylene ether phosphate OE-3P and polyoxyethylene ether phosphate OEP-70; the alcohol ether phosphate salt adopts alcohol ether phosphate MAPK; and the mass ratio of alcohol ether phosphate salt, polyethylene glycol ester, and polyoxyethylene ether phosphate in the additive is 3:3:14.
[0020] Furthermore, in the above-mentioned water-soluble environmentally friendly DTY oil, the main ingredient is a compound of isomeric alcohol ethers, polyethylene glycol, and ethylene glycol; the emulsifier is a compound of fatty alcohol polyoxyethylene ether and sorbitan ester polyoxyethylene ether; and the additive is a compound of alcohol ether phosphate salt and polyoxyethylene ether phosphate.
[0021] The water-soluble, environmentally friendly DTY oil has a rational formulation. Its three-component main ingredient compound (isomeric alcohol ethers, polyethylene glycol, and ethylene glycol) of alcohol ether, polyol, and ethylene glycol exhibits excellent lubricity, effectively reducing friction and wear and improving equipment efficiency. The three-component emulsifier compound of sorbitan ester polyoxyethylene ether and fatty alcohol polyoxyethylene ether allows the oil to fully mix with water, forming a stable emulsion that easily separates from the aqueous phase after use, facilitating handling and recycling. The two-component additive compound of alcohol ether phosphate and polyoxyethylene ether phosphate exhibits strong antioxidant properties, effectively preventing oxidation during use and extending the oil's service life. Furthermore, it is formulated with environmentally friendly ingredients, free of harmful substances, and environmentally friendly.
[0022] Furthermore, the above-mentioned water-soluble environmentally friendly DTY oil agent, the main ingredient is a compound of isomeric alcohol ether, polyethylene glycol, and ethylene glycol, the mass ratio of the isomeric alcohol ether, polyethylene glycol, and ethylene glycol is 1:10:9; the fatty alcohol polyoxyethylene ether in the emulsifier includes fatty alcohol polyoxyethylene ether AEO-7 and branched fatty alcohol polyoxyethylene ether, and the branched fatty alcohol polyoxyethylene ether is selected from at least one of branched fatty alcohol polyoxyethylene ether O-20, branched fatty alcohol polyoxyethylene ether O-23, and branched fatty alcohol polyoxyethylene ether O-25, and the dehydrated mountain The sorbitol ester polyoxyethylene ether adopts anhydrous sorbitan ester polyoxyethylene ether T-80, and the mass ratio of fatty alcohol polyoxyethylene ether AEO-7, anhydrous sorbitan ester polyoxyethylene ether, and branched fatty alcohol polyoxyethylene ether in the emulsifier is 3:1:1; the polyoxyethylene ether phosphate in the additive is selected from at least one of polyoxyethylene ether phosphate OE-3P and polyoxyethylene ether phosphate OEP-70, the alcohol ether phosphate salt adopts alcohol ether phosphate ester MAPK, and the mass ratio of alcohol ether phosphate ester and polyoxyethylene ether phosphate in the additive is 3:7.
[0023] The present invention also relates to a method for preparing the water-soluble environmentally friendly DTY oil, comprising the following steps:
[0024] S1: First, the main material is pumped into the reactor, the temperature in the reactor is controlled at 35-40°C, and stirred at a constant speed for 5-15 minutes;
[0025] S2: The emulsifier is then pumped into the reactor, the temperature is raised and controlled at 55-60°C, and stirred at a constant speed for 1-3 hours;
[0026] S3: Finally, the additive is pumped into the reactor, the temperature in the reactor is controlled at 45-50°C, and after uniform stirring for 0.5-2 hours, it is cooled and filtered to produce the finished water-soluble environmentally friendly DTY oil.
[0027] Compared with the prior art, the present invention has the following beneficial effects:
[0028] (1) The water-soluble environmentally friendly DTY oil disclosed in the present invention is composed of a main ingredient, an emulsifier, and an additive. The main ingredient is selected from polyether, ether ester, polyol, and alcohol ether. The emulsifier is selected from fatty alcohol polyoxyethylene ether, branched fatty alcohol polyoxyethylene ether, and sorbitan ester polyoxyethylene ether. The additive is selected from imidazolinium salt, alcohol ether phosphate salt, polyethylene glycol ester, and polyoxyethylene ether phosphate. By optimizing the selection, matching, and content of each component, the DTY oil has green and environmental protection properties, excellent antistatic properties, and smoothness. The water-soluble environmentally friendly DTY oil is mainly used for producing DTY low-stretch yarn on various types of imported and domestic texturing machines. The DTY low-stretch yarn is mainly used for weaving on warp knitting machines, KS warp knitting machines, circular knitting machines, and water-jet looms.
[0029] (2) The preparation method of the water-soluble environmentally friendly DTY oil disclosed in the present invention has reasonable preparation steps, low cost, is suitable for industrial production, and has a wide range of application scenarios. DETAILED DESCRIPTION
[0030] The following examples 1, 2, 3 and comparative examples 1 and 2 are combined with specific experimental data to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative work are within the scope of protection of the present invention.
[0031] The raw materials used in Examples 1, 2 and 3 are all commercially available industrial raw materials.
[0032] The following Examples 1, 2 and 3 provide a water-soluble, environmentally friendly DTY oil and a preparation method thereof.
[0033] Example 1
[0034] The water-soluble environmentally friendly DTY oil of Example 1 comprises the following raw materials in weight fractions:
[0035] 80 kg of two-component main ingredient compound, including 20% ethylene glycol (Shandong Runyue) and 80% polyethylene glycol (BASF PEG-400);
[0036] 7 kg of two-component emulsifier compound, including 50% fatty alcohol polyoxyethylene ether (BASF AEO-7) and 50% sorbitan ester polyoxyethylene ether (T-80);
[0037] 13 kg of two-component additive compound, including 30% polyethylene glycol ester (600MO) and 70% polyoxyethylene ether phosphate (OE-3P);
[0038] A total of 100 kg.
[0039] The preparation of the water-soluble environmentally friendly DTY oil of Example 1 comprises the following steps:
[0040] S1: According to the above formula, firstly, the main ingredients with accurate measurement are pumped into the reactor, the temperature in the reactor is controlled at 35-40°C, and stirred at a constant speed for 10 minutes;
[0041] S2: Then, accurately measure the emulsifier and pump it into the reactor. Heat the reactor and control the temperature at 55-60°C. Stir at a constant speed for 2 hours.
[0042] S3: Finally, accurately measured additives are pumped into the reactor. The temperature in the reactor is controlled at 45-50° C. during the first addition. After uniform stirring for 1 hour, the reactor is cooled and filtered to produce the finished water-soluble environmentally friendly DTY oil of Example 1.
[0043] Example 2
[0044] The water-soluble environmentally friendly DTY oil of Example 2 comprises the following raw materials in weight fractions:
[0045] 82 kg of two-component main ingredient compound, including 5% ethylene glycol butyl ether acetate (Eastman EBAcetate) and 95% polyethylene glycol (BASF PEG-400);
[0046] 7 kg of two-component emulsifier compound, including 60% branched fatty alcohol polyoxyethylene ether (O-23) and 40% sorbitan ester polyoxyethylene ether (T-80);
[0047] 11 kg of a three-component additive mixture, including 15% alcohol ether phosphate (MAPK), 15% polyethylene glycol ester (400MO), and 70% polyoxyethylene ether phosphate (OEP-70);
[0048] A total of 100 kg.
[0049] The preparation of the water-soluble environmentally friendly DTY oil of Example 2 comprises the following steps:
[0050] S1: According to the above formula, firstly, the main ingredients with accurate measurement are pumped into the reactor, the temperature in the reactor is controlled at 35-40°C, and stirred at a constant speed for 10 minutes;
[0051] S2: Then, accurately measure the emulsifier and pump it into the reactor. Heat the reactor and control the temperature at 55-60°C. Stir at a constant speed for 2 hours.
[0052] S3: Finally, accurately measured additives are pumped into the reactor. The temperature in the reactor is controlled at 45-50° C. during the first addition. After uniform stirring for 1 hour, the reactor is cooled and filtered to produce the finished water-soluble environmentally friendly DTY oil of Example 2.
[0053] Example 3
[0054] The water-soluble environmentally friendly DTY oil of Example 3 comprises the following raw materials in weight fractions:
[0055] 85 kg of the three-component main ingredient compound, including 5% isomeric alcohol ether (BASF TO-3), 50% polyethylene glycol (BASF PEG-400), and 45% ethylene glycol (Shandong Runyue);
[0056] 7.5 kg of a three-component emulsifier mixture, including 60% fatty alcohol polyoxyethylene ether (BASF AEO-7), 20% sorbitan ester polyoxyethylene ether (T-80), and 20% branched fatty alcohol polyoxyethylene ether (O-25);
[0057] 7.5 kg of two-component additive compound, including 30% alcohol ether phosphate (MAPK) and 70% polyoxyethylene ether phosphate (OE-3P);
[0058] A total of 100 kg.
[0059] The preparation of the water-soluble environmentally friendly DTY oil of Example 3 comprises the following steps:
[0060] S1: According to the above formula, firstly, the main ingredients with accurate measurement are pumped into the reactor, the temperature in the reactor is controlled at 35-40°C, and stirred at a constant speed for 10 minutes;
[0061] S2: Then, accurately measure the emulsifier and pump it into the reactor. Heat the reactor and control the temperature at 55-60°C. Stir at a constant speed for 2 hours.
[0062] S3: Finally, accurately measured additives are pumped into the reactor. The temperature in the reactor is controlled at 45-50° C. during the first addition. After uniform stirring for 1 hour, the reactor is cooled and filtered to produce the finished product of the water-soluble environmentally friendly DTY oil of Example 3.
[0063] The following Comparative Examples 1 and 2 provide a commercially available DTY oil.
[0064] Comparative Example 1
[0065] Comparative Example 1 is Longfang LF-500A DTY oil produced by Taicang Longfang Oil Co., Ltd.
[0066] Comparative Example 2
[0067] Comparative Example 2 is Longfang LF-500B DTY oil produced by Taicang Longfang Oil Co., Ltd.
[0068] Effect verification
[0069] The performance of the water-soluble environmentally friendly DTY oil prepared in Comparative Example 1, Comparative Example 2, Examples 1, 2, and 3 is tested below. The performance test results of Comparative Example 1, Comparative Example 2, Examples 1, 2, and 3 are shown in Table 1.
[0070] Table 1 Performance test results of Comparative Example 1, Comparative Example 2, Examples 1, 2, and 3
[0071]
[0072] *Calculation is based on:
[0073] .
[0074] As shown in Table 1, the water-soluble, environmentally friendly DTY finishes of Examples 1, 2, and 3, prepared using the technical solution of the present invention, exhibit lower specific resistivity and better antistatic properties than the DTY finishes of Comparative Examples 1 and 2. The water-soluble, environmentally friendly DTY finish of Example 3 is preferred. Based on customer trial feedback, the water-soluble, environmentally friendly DTY finishes of Examples 1, 2, and 3 have not been observed in actual production, effectively resolving the issue of unstable antistatic properties associated with conventional finishes and improving yarn quality.
[0075] Secondly, the water-soluble, environmentally friendly DTY finishes in Examples 1, 2, and 3 exhibited lower residual oil rates than those in Comparative Examples 1 and 2, with Example 3 being the preferred choice. Based on customer trial feedback, the water-soluble, environmentally friendly DTY finishes in Examples 1, 2, and 3 demonstrate strong decontamination rates in actual production, meeting the requirements for mid- to high-end dyeing and serving as a viable alternative to conventional finishes.
[0076] In addition, compared with conventional DTY oils, the preparation method of the water-soluble environmentally friendly DTY oil of the present invention has higher production efficiency and lower energy consumption during the process, meeting the current new requirements for energy conservation and emission reduction.
[0077] The present invention has many specific application paths, and the above is only a preferred embodiment of the present invention. It should be noted that the above embodiments are only used to illustrate the present invention and are not intended to limit the scope of protection of the present invention. For those skilled in the art, several improvements can be made without departing from the principles of the present invention, and these improvements should also be considered as the scope of protection of the present invention.
Claims
1. A water-soluble environmentally friendly DTY oil, characterized in that: The water-soluble environmentally friendly DTY oil comprises the following raw materials by weight: The main ingredient is 70-90%, wherein the main ingredient is a compound of ethylene glycol and polyethylene glycol, or a compound of ethylene glycol butyl ether acetate and polyethylene glycol, or a compound of isomeric alcohol ethers, polyethylene glycol and ethylene glycol; 5-15% emulsifier, wherein the emulsifier is a compound of fatty alcohol polyoxyethylene ether and sorbitan polyoxyethylene ether; 5-15% of additives, wherein the additives are a two-component or three-component compound, and are selected from at least two of imidazoline salts, alcohol ether phosphate salts, polyethylene glycol esters, and polyoxyethylene ether phosphates; The sum of the components is 100%.
2. The water-soluble environmentally friendly DTY oil according to claim 1, characterized in that: The additive is a compound of polyethylene glycol ester and polyoxyethylene ether phosphate.
3. The water-soluble environmentally friendly DTY oil according to claim 2, characterized in that: The main ingredient is a compound of ethylene glycol and polyethylene glycol, and the mass ratio of the ethylene glycol to the polyethylene glycol is 1:4; the emulsifier is a compound of fatty alcohol polyoxyethylene ether AEO-7 and sorbitan polyoxyethylene ether T-80, and the mass ratio of the fatty alcohol polyoxyethylene ether AEO-7 and sorbitan polyoxyethylene ether T-80 is 1:1; the polyethylene glycol ester in the additive is selected from at least one of polyethylene glycol ester 600MO, polyethylene glycol ester 400MO, and polyethylene glycol ester 400DO; the polyoxyethylene ether phosphate in the additive is selected from at least one of polyoxyethylene ether phosphate OE-3P and polyoxyethylene ether phosphate OEP-70, and the mass ratio of the polyethylene glycol ester to the polyoxyethylene ether phosphate in the additive is 3:
7.
4. The water-soluble environmentally friendly DTY oil according to claim 1, characterized in that: The emulsifier is a compound of branched fatty alcohol polyoxyethylene ether and sorbitan ester polyoxyethylene ether; and the additive is a compound of alcohol ether phosphate salt, polyethylene glycol ester and polyoxyethylene ether phosphate.
5. The water-soluble environmentally friendly DTY oil according to claim 4, characterized in that: The main ingredient is a compound of ethylene glycol butyl ether acetate and polyethylene glycol, and the mass ratio of the ethylene glycol butyl ether acetate and the polyethylene glycol is 1:19; the fatty alcohol polyoxyethylene ether in the emulsifier is selected from at least one of branched fatty alcohol polyoxyethylene ether O-20, branched fatty alcohol polyoxyethylene ether O-23, and branched fatty alcohol polyoxyethylene ether O-25, the sorbitan ester polyoxyethylene ether adopts sorbitan ester polyoxyethylene ether T-80, the branched fatty alcohol polyoxyethylene ether, sorbitan ester polyoxyethylene ether in the emulsifier are selected from at least one of branched fatty alcohol polyoxyethylene ether O-20, branched fatty alcohol polyoxyethylene ether O-23, and branched fatty alcohol polyoxyethylene ether O-25, the anhydrous sorbitan ester polyoxyethylene ether adopts anhydrous sorbitan ester polyoxyethylene ether T-80, the branched fatty alcohol polyoxyethylene ether, sorbitan ester polyoxyethylene ether in the emulsifier are selected from at least one of branched fatty alcohol polyoxyethylene ether The mass ratio of the olefin ether is 3:2; the polyethylene glycol ester in the additive is selected from at least one of polyethylene glycol ester 600MO, polyethylene glycol ester 400MO, and polyethylene glycol ester 400DO; the polyoxyethylene ether phosphate in the additive is selected from at least one of polyoxyethylene ether phosphate OE-3P and polyoxyethylene ether phosphate OEP-70; the alcohol ether phosphate salt adopts alcohol ether phosphate MAPK; and the mass ratio of the alcohol ether phosphate salt, polyethylene glycol ester, and polyoxyethylene ether phosphate in the additive is 3:3:
14.
6. The water-soluble environmentally friendly DTY oil according to claim 1, characterized in that: The additive is a compound of alcohol ether phosphate salt and polyoxyethylene ether phosphate.
7. The water-soluble environmentally friendly DTY oil according to claim 6, characterized in that: The main ingredient is a compound of isomeric alcohol ether, polyethylene glycol and ethylene glycol, and the mass ratio of the isomeric alcohol ether, polyethylene glycol and ethylene glycol is 1:10:9; the fatty alcohol polyoxyethylene ether in the emulsifier includes fatty alcohol polyoxyethylene ether AEO-7 and branched fatty alcohol polyoxyethylene ether, and the branched fatty alcohol polyoxyethylene ether is selected from at least one of branched fatty alcohol polyoxyethylene ether O-20, branched fatty alcohol polyoxyethylene ether O-23 and branched fatty alcohol polyoxyethylene ether O-25; the anhydrous sorbitan ester polyoxyethylene ether adopts anhydrous sorbitan ester polyoxyethylene ether. Sorbitan polyoxyethylene ether T-80, the mass ratio of fatty alcohol polyoxyethylene ether AEO-7, anhydrous sorbitan polyoxyethylene ether, and branched fatty alcohol polyoxyethylene ether in the emulsifier is 3:1:1; the polyoxyethylene ether phosphate in the additive is selected from at least one of polyoxyethylene ether phosphate OE-3P and polyoxyethylene ether phosphate OEP-70, the alcohol ether phosphate salt adopts alcohol ether phosphate salt MAPK, and the mass ratio of alcohol ether phosphate salt to polyoxyethylene ether phosphate in the additive is 3:
7.
8. The method for preparing the water-soluble environmentally friendly DTY oil according to any one of claims 1 to 7, characterized in that: The steps include: S1: First, the main material is pumped into the reactor, the temperature in the reactor is controlled at 35-40°C, and stirred at a constant speed for 5-15 minutes; S2: The emulsifier is then pumped into the reactor, the temperature is raised and controlled at 55-60°C, and stirred at a constant speed for 1-3 hours; S3: Finally, the additive is pumped into the reactor, the temperature in the reactor is controlled at 45-50°C, and after uniform stirring for 0.5-2 hours, it is cooled and filtered to produce the finished water-soluble environmentally friendly DTY oil.
Citation Information
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Terylene middle strength filament oil solution and production method thereof
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Compound emulsifier of high-speed spinning polyester low-stretch yarn post-processing oiling agent and preparation method thereof
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