A pH value measuring device in chemical synthesis process

Abstract

The invention discloses a pH value measuring device in a chemical synthesis process, and relates to the field of chemical technology. The pH value measuring device in a chemical synthesis process comprises a main body box, a cover plate is fixedly connected to the top of the main body box, a back plate is fixedly connected to the back of the main body box, a heat sink is fixedly connected to the left side of the main body box, a temperature conduction box is fixedly connected to the left side of the heat sink box, a stirring mechanism is fixedly connected to the inside of the main body box, a measuring component is fixedly connected to the bottom of the stirring mechanism, a suction mechanism is arranged on the left side of the main body box, and a temperature control component is arranged on the outer wall of the stirring mechanism inside the main body box. The pH value measuring device in a chemical synthesis process uses a suction mechanism to take solutions of different depths for measurement, a stirring mechanism stirs the inflowing liquid to allow the liquid to be fully mixed and evenly measured, and a temperature control component is used to cool the liquid to be measured to measure a more accurate pH.

Description

Technical Field

[0001] The invention relates to the technical field of chemical engineering, in particular to a pH value measuring device in a chemical synthesis process. Background Art

[0002] In the process of chemical synthesis, the pH control of the synthesis liquid plays a key role in the yield and quality of the product. The device for effectively monitoring the pH of the synthesis liquid is one of the problems that should be solved when chemical products move from the laboratory to industrialization.

[0003] Citing patent number "CN105203597A", ​​the patent proposes a pH value measuring device in a chemical synthesis process, including a fixed frame and a pH tester and a detection container arranged on the fixed frame, the pH tester is a digital pH meter, and the digital pH meter is connected to a pH electrode; the digital pH meter and the detection container are respectively arranged on the upper and middle layers of the fixed frame, and the lower layer of the fixed frame is provided with a lifting pump; an overflow trough is provided inside the detection container, and the bottom below the overflow trough is connected to a vent pipe, and a vent valve is provided on the vent pipe; a conveying pipeline is connected between the lifting pump and the overflow trough; the inlet of the lifting pump and the bottom of the detection container are both connected with a fixed pipeline, and the other end of the fixed pipeline is set as a threaded end.

[0004] Although this patent can measure pH, the extraction range is limited, and there is a deviation between the local measured value and the actual pH value. At the same time, in the actual process, when the temperature increases, the ion product constant of water will also change. The pH value at this time cannot represent the acidity and alkalinity. The measured pH value at this time deviates from the actual pH value of water, which is not conducive to the quality of the products obtained by chemical synthesis. Summary of the invention

[0005] In view of the deficiencies of the prior art, the present invention provides a device for measuring pH value in a chemical synthesis process to solve the problems raised in the above background technology.

[0006] To achieve the above purpose, the present invention is implemented through the following technical solutions: A pH value measuring device in a chemical synthesis process, comprising a main body box, a cover plate fixedly connected to the top of the main body box, a back plate fixedly connected to the back of the main body box, a heat sink fixedly connected to the left side of the main body box, a temperature conduction box fixedly connected to the left side of the heat sink box, a stirring mechanism fixedly connected to the inside of the main body box, a measuring component fixedly connected to the bottom of the stirring mechanism, a suction mechanism arranged on the left side of the main body box, and a temperature control component arranged on the outer wall of the stirring mechanism inside the main body box;

[0007] The stirring mechanism includes:

[0008] A fixed bottom plate, the fixed bottom plate is fixedly connected to the bottom of the main box;

[0009] A mixing box, the mixing box is movably connected to the top of the fixed bottom plate;

[0010] A fixed top frame, wherein the fixed top frame is fixedly connected to the bottom of the cover plate and movably connected to the top of the mixing box;

[0011] The suction mechanism includes:

[0012] A heat conducting pipe, which is fixedly connected to the top of the mixing box, and the material of the portion where the heat conducting pipe is connected to other components has good thermal conductivity;

[0013] Hose 1, the hose 1 is fixedly connected to the left side of the temperature conducting pipe;

[0014] A connector is fixedly connected to a bottom of the hose.

[0015] Preferably, a movable column is movably connected to the bottom of the connector, a cavity is movably connected to the outer wall of the movable column, and an outer arm of the movable column is located at the bottom of the cavity and fixedly connected to a fan blade.

[0016] Preferably, the outer wall of the movable column is provided with teeth at the top of the cavity, the top of the cavity is fixedly connected to a fixing frame, the inside of the fixing frame is fixedly connected to a gear motor, the gear motor is movably connected to the movable column through the teeth of the gear meshing movable column arranged at the bottom, the top of the cavity is fixedly connected to a counterweight block, and the counterweight block is located on the opposite side of the gear motor with respect to the movable column.

[0017] Preferably, a rotating column is movably connected inside the mixing box, four baffle plates are movably connected to the outer wall of the rotating column, and the baffle plates are fixedly connected to the inner wall of the mixing box, four stirring blades are fixedly connected to the outer wall of the rotating column at the top of the baffle plate, and each baffle plate has four stirring blades on the top, for a total of sixteen stirring blades.

[0018] Preferably, a bevel gear is provided on the top of the rotating column, and a bevel gear motor is fixedly connected to the top of the mixing box. The bevel gear provided on the top of the bevel gear motor meshes with the bevel gear on the top of the rotating column, and the bevel gear motor is movably connected to the rotating column through the bevel gear provided on the top.

[0019] Preferably, the measuring component includes a test box, which is fixedly connected to the bottom of the main box, the back of the test box is connected to the bottom of the mixing box through a pipe, the outer wall of the mixing box is fixedly connected to a fixing ring, the outer wall of the fixing ring is located on the front of the mixing box and is fixedly connected to a tester, the bottom of the tester is fixedly connected to a test head, and the test head is fixedly connected to the inside of the test box, the bottom of the main box is fixedly connected to a gas-liquid mixing pump, and the right side of the gas-liquid mixing pump is connected to the left side of the test box through a pipe.

[0020] Preferably, the temperature control component includes a heat pipe, which is fixedly connected to the left side of the gas-liquid mixing pump, part of the heat pipe is movably connected to the outer wall of the gas-liquid mixing pump, and part of the heat pipe is movably connected to the outer wall of the bevel gear motor.

[0021] Preferably, the outer wall of the temperature conducting pipe is fixedly connected to a temperature conducting block, and the temperature conducting block is fixedly connected to the inside of the temperature conducting box, part of the heat conducting pipe is fixedly connected to the inside of the temperature conducting block, the outer wall of the temperature conducting pipe is fixedly connected to a heat sink group on the right side of the temperature conducting block, and a fan is fixedly connected to the top of the heat sink group.

[0022] Preferably, a second hose is fixedly connected to the left side of the heat conducting pipe, and an outlet head is fixedly connected to the right side of the second hose.

[0023] The present invention provides a device for measuring pH value in a chemical synthesis process. It has the following beneficial effects:

[0024] 1. The pH value measuring device in the chemical synthesis process drives the movable column to rotate intermittently through the gear motor through the suction mechanism, thereby driving the fan blades to rotate, so that the movable column absorbs solutions of different depths to increase the number of samples to increase the accuracy of pH value determination, thereby improving the quality of products obtained from chemical synthesis.

[0025] 2. The pH value measuring device in the chemical synthesis process uses the bevel gear motor of the stirring mechanism to drive the rotating column through the meshing bevel gear to use the stirring blade to fully stir and mix the extracted solution to make the measurement structure more accurate. During the stirring and rotating process, the inclined structure of the stirring blade will produce a slight pump-like effect, thereby reducing the working pressure of the gas-liquid mixing pump, thereby improving the quality of the products obtained from the chemical synthesis.

[0026] 3. The pH value measuring device in the chemical synthesis process reduces the temperature of the inhaled liquid to be tested through the temperature control component, reduces the influence of the pH ionized by water at high temperature on the measured pH, and measures the measured pH. The measured solution is heated up and then put back into the liquid to reduce the excessive influence of the liquid on the original solution after the measurement.

[0027] 4. The pH value measuring device in the chemical synthesis process uses the heat generated by the bevel gear motor of the stirring component to cooperate with the heat pipe of the temperature control component to absorb the heat generated by the bevel gear motor to heat up the liquid to be measured, while cooling the motor, and absorbing the heat generated by the motor inside the gas-liquid mixing pump. BRIEF DESCRIPTION OF THE DRAWINGS

[0028] Figure 1 It is a schematic diagram of the main stereoscopic structure of the present invention;

[0029] Figure 2 for Figure 1 Schematic diagram of the cross-section structure;

[0030] Figure 3 It is a schematic diagram of the back three-dimensional structure of the present invention;

[0031] Figure 4 This is a schematic diagram of the internal front three-dimensional structure of the present invention;

[0032] Figure 5 for Figure 4 Schematic diagram of the cross-section structure;

[0033] Figure 6 for Figure 5 A schematic diagram of the enlarged structure of the middle part A;

[0034] Figure 7 This is a schematic diagram of the three-dimensional structure of the back of the present invention;

[0035] Figure 8 for Figure 7 Schematic diagram of the cross-section structure;

[0036] Fig. 9 It is a schematic diagram of the main structure of the suction mechanism of the present invention;

[0037] Fig.10 for Fig. 9 Schematic diagram of the cross-section structure.

[0038] In the figure: 1. main box; 12. cover plate; 13. back plate; 14. heat sink; 15. temperature conduction box; 2. suction mechanism; 21. cavity; 22. movable column; 23. connector; 24. hose one; 25. counterweight; 26. gear motor; 27. fixed frame; 28. fan blade; 29. ​​temperature conduction pipe; 3. stirring mechanism; 31. fixed bottom plate; 32. stirring box; 33. bevel gear motor; 34. rotating column; 35. fixed top frame; 36. stirring blade; 37. baffle plate; 4. measuring component; 41. test box; 42. test head; 43. tester; 44. gas-liquid mixing pump; 45. fixed ring; 5. temperature control component; 51. heat conduction pipe; 52. temperature conduction block; 53. heat sink group; 54. fan; 55. hose two; 56. outflow head. DETAILED DESCRIPTION

[0039] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.

[0040] Examples of the embodiments are shown in the accompanying drawings, wherein the same or similar reference numerals throughout represent the same or similar elements or elements having the same or similar functions. The embodiments described below with reference to the accompanying drawings are exemplary and are intended to be used to explain the present invention, and should not be construed as limiting the present invention.

[0041] See also Figure 1-10 The present invention provides a technical solution: a pH value measuring device in a chemical synthesis process, comprising a main body box 1, a cover plate 12 is fixedly connected to the top of the main body box 1, a back plate 13 is fixedly connected to the back of the main body box 1, a heat dissipation box 14 is fixedly connected to the left side of the main body box 1, a temperature conduction box 15 is fixedly connected to the left side of the heat dissipation box 14, a stirring mechanism 3 is fixedly connected inside the main body box 1, a measuring component 4 is fixedly connected to the bottom of the stirring mechanism 3, a suction mechanism 2 is arranged on the left side of the main body box 1, and a temperature control component 5 is arranged on the outer wall of the stirring mechanism 3 inside the main body box 1;

[0042] The stirring mechanism 3 comprises:

[0043] A fixed bottom plate 31, wherein the fixed bottom plate 31 is fixedly connected to the bottom of the main box 1;

[0044] A mixing box 32, wherein the mixing box 32 is movably connected to the top of the fixed bottom plate 31;

[0045] A fixed top frame 35, wherein the fixed top frame 35 is fixedly connected to the bottom of the cover plate 12, and the fixed top frame 35 is movably connected to the top of the mixing box 32;

[0046] The interior of the mixing box 32 is movably connected to a rotating column 34, and the outer wall of the rotating column 34 is movably connected to four blocking plates 37, and the blocking plates 37 are fixedly connected to the inner wall of the mixing box 32. The outer wall of the rotating column 34 is located on the top of the blocking plates 37 and is fixedly connected to four stirring blades 36, and each of the blocking plates 37 has four stirring blades 36 on the top, for a total of sixteen stirring blades 36.

[0047] A bevel gear is provided on the top of the rotating column 34, and a bevel gear motor 33 is fixedly connected to the top of the mixing box 32. The bevel gear provided on the top of the bevel gear motor 33 meshes with the bevel gear on the top of the rotating column 34, and the bevel gear motor 33 is movably connected to the rotating column 34 through the bevel gear provided on the top.

[0048] The suction mechanism 2 comprises:

[0049] A temperature conducting pipe 29, wherein the temperature conducting pipe 29 is fixedly connected to the top of the mixing box 32;

[0050] A hose 24, wherein the hose 24 is fixedly connected to the left side of the temperature conducting pipe 29;

[0051] A connector 23 is fixedly connected to the bottom of a hose 24.

[0052] The bottom of the connector 23 is movably connected to a movable column 22 , the outer wall of the movable column 22 is movably connected to the cavity 21 , and the outer arm of the movable column 22 is located at the bottom of the cavity 21 and is fixedly connected to a fan blade 28 .

[0053] The outer wall of the movable column 22 is located at the top of the cavity 21 and is provided with teeth. A fixing frame 27 is fixedly connected to the top of the cavity 21. A gear motor 26 is fixedly connected inside the fixing frame 27. The gear motor 26 is movably connected to the movable column 22 through the teeth of the gear-engaged movable column 22 arranged at the bottom. A counterweight block 25 is fixedly connected to the top of the cavity 21, and the counterweight block 25 is located on the opposite side of the gear motor 26 with respect to the movable column 22.

[0054] The measuring component 4 includes a test box 41, which is fixedly connected to the bottom of the main box 1. The back of the test box 41 is connected to the bottom of the mixing box 32 through a pipeline. A fixing ring 45 is fixedly connected to the outer wall of the mixing box 32. The outer wall of the fixing ring 45 is located on the front of the mixing box 32 and is fixedly connected to a tester 43. A test head 42 is fixedly connected to the bottom of the tester 43, and the test head 42 is fixedly connected to the inside of the test box 41. A gas-liquid mixing pump 44 is fixedly connected to the bottom of the main box 1, and the right side of the gas-liquid mixing pump 44 is connected to the left side of the test box 41 through a pipeline.

[0055] The temperature control component 5 includes a heat pipe 51, which is fixedly connected to the left side of the gas-liquid mixing pump 44, and part of the heat pipe 51 is movably connected to the outer wall of the gas-liquid mixing pump 44, and part of the heat pipe 51 is movably connected to the outer wall of the bevel gear motor 33.

[0056] The outer wall of the heat conducting pipe 29 is fixedly connected to a heat conducting block 52, and the heat conducting block 52 is fixedly connected to the inside of the heat conducting box 15. Part of the heat conducting pipe 51 is fixedly connected to the inside of the heat conducting block 52. The outer wall of the heat conducting pipe 29 is located on the right side of the heat conducting block 52 and is fixedly connected to a heat sink group 53. The top of the heat sink group 53 is fixedly connected to a fan 54.

[0057] A second hose 55 is fixedly connected to the left side of the heat conducting pipe 51 , and an outlet head 56 is fixedly connected to the right side of the second hose 55 .

[0058] When in use, the cavity 21 is placed on the liquid to be tested. Due to the action of the cavity 21, the bevel gear motor 33 attached to the surface of the liquid drives the rotating column 34 to start rotating, and the gas-liquid mixing pump 44 starts to operate. The liquid to be tested is sucked in through the bottom of the movable column 22. At the same time, the gear motor 26 intermittently drives the movable column 22 to move up and down, so that the movable column 22 absorbs the liquid to be tested at different depths. The sucked liquid flows into the temperature conducting tube 29 and transmits the temperature to the temperature conducting tube 29. When passing through the heat sink group 53, the fan 54 drives the air flow to blow through the heat sink group 53 to cool the liquid to be tested inside. The liquid flows into the stirring box 32, and is stirred by the stirring blade 36 driven by the rotating rotating column 34. During the rotation of the stirring blade 36, the inclined structure of the stirring blade 36 will produce a slight pump-like effect, thereby reducing the work of the gas-liquid mixing pump 44. The liquid to be tested flows into the test box 41 through the pipe at the bottom of the stirring box 32 after being fully stirred. The liquid to be tested flows through the test head 42 and the pH value is detected and displayed by the tester 43. The tested liquid is pumped into the heat pipe 51 by the gas-liquid mixing pump 44 during the flow inside the heat pipe 51. During the flow inside the heat pipe 51, the liquid to be tested can absorb the heat generated by the motor in the gas-liquid mixing pump 44 and the heat generated by the bevel gear motor 33 to heat the tested liquid. At the same time, the bevel gear motor 33 and the gas-liquid mixing pump 44 can be cooled. When passing through the temperature conducting block 52, the temperature conducting block 52 transfers the temperature of the newly inhaled liquid to the tested liquid, thereby achieving the effect of cooling the liquid to be tested and heating the tested liquid at the same time. Then the tested liquid flows into the hose 2 55 and flows out from the outflow head 56 into the original liquid.

[0059] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.

Claims

1. A pH value measuring device in a chemical synthesis process, comprising a main box (1), characterized in that: The top of the main box (1) is fixedly connected to a cover plate (12), the back of the main box (1) is fixedly connected to a back plate (13), the left side of the main box (1) is fixedly connected to a heat dissipation box (14), the left side of the heat dissipation box (14) is fixedly connected to a temperature conduction box (15), the inside of the main box (1) is fixedly connected to a stirring mechanism (3), the bottom of the stirring mechanism (3) is fixedly connected to a measuring component (4), the left side of the main box (1) is provided with a suction mechanism (2), and the inside of the main box (1) is provided with a temperature control component (5) on the outer wall of the stirring mechanism (3); The stirring mechanism (3) comprises: A fixed bottom plate (31), the fixed bottom plate (31) being fixedly connected to the inner bottom of the main box (1); A stirring box (32), wherein the stirring box (32) is movably connected to the top of the fixed bottom plate (31); A fixed top frame (35), wherein the fixed top frame (35) is fixedly connected to the bottom of the cover plate (12), and the fixed top frame (35) is movably connected to the top of the mixing box (32); The suction mechanism (2) comprises: A temperature conducting pipe (29), wherein the temperature conducting pipe (29) is fixedly connected to the top of the stirring box (32); Hose 1 (24), the hose 1 (24) is fixedly connected to the left side of the temperature conducting tube (29); A connector (23), the connector (23) being fixedly connected to the bottom of the hose 1 (24); The bottom of the connector (23) is movably connected to a movable column (22), the outer wall of the movable column (22) is movably connected to a cavity (21), and the outer arm of the movable column (22) is located at the bottom of the cavity (21) and is fixedly connected to a fan blade (28); The stirring box (32) is movably connected to a rotating column (34), and the outer wall of the rotating column (34) is movably connected to four blocking plates (37), and the blocking plates (37) are fixedly connected to the inner wall of the stirring box (32). The outer wall of the rotating column (34) is located on the top of the blocking plates (37) and is fixedly connected to four stirring blades (36), and each of the blocking plates (37) has four stirring blades (36) on the top, for a total of sixteen stirring blades (36); A bevel gear is arranged on the top of the rotating column (34), a bevel gear motor (33) is fixedly connected to the top of the mixing box (32), the bevel gear arranged on the top of the bevel gear motor (33) and the bevel gear on the top of the rotating column (34) are meshed with each other, and the bevel gear motor (33) is movably connected to the rotating column (34) via the bevel gear arranged on the top; The temperature control component (5) comprises a heat conducting pipe (51), the heat conducting pipe (51) is fixedly connected to the left side of the gas-liquid mixing pump (44), part of the heat conducting pipe (51) is movably connected to the outer wall of the gas-liquid mixing pump (44), and part of the heat conducting pipe (51) is movably connected to the outer wall of the bevel gear motor (33); The outer wall of the heat conducting pipe (29) is fixedly connected to a heat conducting block (52), and the heat conducting block (52) is fixedly connected to the inside of the heat conducting box (15); a portion of the heat conducting pipe (51) is fixedly connected to the inside of the heat conducting block (52); the outer wall of the heat conducting pipe (29) is located on the right side of the heat conducting block (52) and is fixedly connected to a heat sink group (53); and a fan (54) is fixedly connected to the top of the heat sink group (53).

2. The pH value measuring device in a chemical synthesis process according to claim 1, characterized in that: The outer wall of the movable column (22) is provided with teeth at the top of the cavity (21); a fixing frame (27) is fixedly connected to the top of the cavity (21); a gear motor (26) is fixedly connected inside the fixing frame (27); the gear motor (26) is movably connected to the movable column (22) by meshing the teeth of the movable column (22) with a gear provided at the bottom; a counterweight (25) is fixedly connected to the top of the cavity (21), and the counterweight (25) is located on the opposite side of the gear motor (26) with respect to the movable column (22).

3. The pH value measuring device in a chemical synthesis process according to claim 1, characterized in that: The measuring assembly (4) comprises a test box (41), the test box (41) being fixedly connected to the bottom of the main box (1), the back of the test box (41) being connected to the bottom of the mixing box (32) via a pipeline, a fixing ring (45) being fixedly connected to the outer wall of the mixing box (32), a tester (43) being fixedly connected to the outer wall of the fixing ring (45) located at the front of the mixing box (32), a test head (42) being fixedly connected to the bottom of the tester (43), and the test head (42) being fixedly connected to the inside of the test box (41), a gas-liquid mixing pump (44) being fixedly connected to the bottom of the main box (1), and the right side of the gas-liquid mixing pump (44) being connected to the left side of the test box (41) via a pipeline.

4. The pH value measuring device in a chemical synthesis process according to claim 1, characterized in that: A second hose (55) is fixedly connected to the left side of the heat conducting pipe (51), and an outlet head (56) is fixedly connected to the right side of the second hose (55).

Images