A recycling device for quartz sand pickling liquid
By designing a quartz sand pickling liquid recovery and treatment device including a stirring module and lifting module, the problem of the reaction of fluosilicate filtrate and inorganic alkali solution is solved, and the precipitation rate and recycling and treatment efficiency of fluosilicate crystals are improved.
Patent Information
- Application Number
- CN202411677294.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-11-22
- Publication Date
- 2025-05-09
- Estimated Expiration
- 2044-11-22
AI Technical Summary
In the prior art, the reaction between the fluorosilicate filtrate and the inorganic alkali solution in the quartz sand pickling solution is easily affected by the fluorosilicate crystals precipitated in the sedimentation tank, resulting in a decrease in the crystal precipitation rate.
A recycling and treatment device for quartz sand pickling liquid is designed, including a settlement tank, agitating assembly, a drive assembly, a transmission assembly, a collection assembly and a lifting assembly. The fluorosilicate filtrate reacts with the inorganic alkali solution by rotating the stirring module, and crystals containing fluorosilicate are precipitated, and the crystals are lifted upwards and discharged by lifting the module to avoid affecting the subsequent reaction.
The precipitation rate of the crystals containing fluorosilicate is improved, the influence of reactions in the sedimentation tank is avoided, and the recycling and treatment efficiency of quartz sand pickling liquid is improved.
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Figure CN119176616B_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of silicon dioxide, in particular to a recovery and treatment device for quartz sand pickling liquid. Background Art
[0002] The main component of quartz sand is silicon dioxide. During the purification process of quartz sand, it is necessary to remove some acid-soluble metal oxides and some silicate minerals through pickling. Hydrofluoric acid pickling is mainly used for purification. During the pickling process, hydrofluoric acid reacts with quartz sand to generate fluorosilicic acid. If it is not treated, direct discharge will not only cause serious environmental pollution, but also the fluorosilicates formed by fluorosilicic acid can be usually used for wood preservation, ceramic manufacturing, aluminum and magnesium smelting, agricultural pesticides, optical glass manufacturing, mica formation, and production of ceramic industrial glazes, porcelain paints, enamel products, etc. Failure to recycle and reuse them will cause great waste.
[0003] In the prior art, a search of Chinese patent application CN117049552A discloses a method for recovering fluorosilicate from high-purity quartz sand pickling wastewater; the method comprises the following steps: S1, pickling high-purity quartz sand with hydrofluoric acid (ultrapure); S2, filtering the pickling liquid after pickling to obtain fine quartz sand solid and fluorosilicic acid filtrate; S3, stirring, heating and concentrating the fluorosilicic acid filtrate, and continuously adding an inorganic alkali solution for sedimentation, and stopping adding the inorganic alkali solution when the pH value of the mixed solution is 7.2-7.5; and S4, filtering the mixed solution after sedimentation, collecting the filter cake and drying it to obtain fluorosilicate.
[0004] The above scheme is to place the fluorosilicic acid filtrate obtained after acid washing of quartz sand in a sedimentation tank, stir it, and continuously add an inorganic alkali solution to react with the fluorosilicic acid filtrate to continuously precipitate crystals containing fluorosilicate. However, in the process of continuously adding the inorganic alkali solution into the fluorosilicic acid filtrate, crystals containing fluorosilicate will continuously precipitate inside the sedimentation tank, which will easily affect the reaction of the subsequently added inorganic alkali solution with the fluorosilicic acid filtrate, thereby reducing the precipitation rate of the crystals containing fluorosilicate.
[0005] Currently, no effective solution has been proposed for the problems in the related technologies. Summary of the invention
[0006] 1. Technical issues to be resolved
[0007] In view of the shortcomings of the prior art, the present invention provides a recovery and treatment device for quartz sand pickling liquid, which has the advantages of avoiding affecting the reaction between the subsequently added inorganic alkali solution and the fluorosilicic acid filtrate, thereby improving the precipitation rate of crystals containing fluorosilicates, and solves the problem that the subsequently added inorganic alkali solution is easily affected to react with the fluorosilicic acid filtrate, thereby reducing the precipitation rate of crystals containing fluorosilicates.
[0008] (II) Technical solution
[0009] In order to solve the above technical problem that the inorganic alkali solution added subsequently is easily affected to react with the fluorosilicic acid filtrate, thereby reducing the precipitation rate of crystals containing fluorosilicate, the present invention provides the following technical solution:
[0010] A recycling and processing device for quartz sand pickling liquid comprises a sedimentation tank, a stirring assembly is fixedly installed on the top of the sedimentation tank, a driving assembly is fixedly installed on the top of the stirring assembly, a transmission assembly is fixedly installed on the output end of the driving assembly, a collecting assembly is fixedly installed on the outer surface of the stirring assembly, a lifting assembly is fixedly installed on one side of the collecting assembly, the outer surface of the lifting assembly is fixedly installed with the inside of the transmission assembly, a feeding assembly is arranged on the top of the stirring assembly, and a discharging assembly is fixedly connected to the bottom end of the sedimentation tank.
[0011] Preferably, the stirring assembly includes a cover plate, the bottom end of the cover plate is fixedly mounted on the top end of the sedimentation tank, a rotating shaft is rotatably arranged inside the cover plate, one end of the rotating shaft is fixedly mounted on the output end of the driving assembly, and a reflux stirring blade is fixedly mounted on one end of the rotating shaft.
[0012] Preferably, the stirring assembly also includes a support frame, the top end of the support frame is fixedly installed with the bottom end of the cover plate, one end of the support frame is fixedly connected with a reflux cylinder, the interior of the reflux cylinder is fixedly connected with a limiting frame, and the interior of the limiting frame is rotatably arranged with the outer surface of the rotating shaft.
[0013] Preferably, the driving assembly includes a mounting frame, the bottom end of the mounting frame is fixedly mounted to the top end of the cover plate, a motor is fixedly mounted to the top end of the mounting frame, the output end of the motor is fixedly connected to a mounting seat, the interior of the mounting seat is fixedly mounted to one end of the rotating shaft, and the output end of the motor is fixedly mounted to the interior of the transmission assembly.
[0014] Preferably, the transmission assembly includes a main transmission wheel, the interior of the main transmission wheel is fixedly mounted to the output end of the motor, the inner side of the main transmission wheel is provided with a transmission belt, the inner side of the transmission belt is provided with an auxiliary transmission wheel, and the interior of the auxiliary transmission wheel is fixedly mounted to the outer surface of the lifting assembly.
[0015] Preferably, the collecting assembly comprises a filter plate and a collecting bucket, the interior of the filter plate is fixedly connected to the outer surface of the reflux drum, the interior of the collecting bucket is fixedly mounted to the outer surface of the rotating shaft, a scraper is provided inside the filter plate, and the interior of the scraper is fixedly connected to the outer surface of the rotating shaft.
[0016] Preferably, the lifting assembly includes a fixed cylinder, one side of the fixed cylinder is connected to the interior of the filter plate, a sealing cover is fixedly installed on the top of the fixed cylinder, a connecting shaft is rotatably arranged inside the sealing cover, the outer surface of the connecting shaft is fixedly installed on the inside of the auxiliary transmission wheel, one end of the connecting shaft is fixedly connected to a spiral conveying blade, the outer surface of the spiral conveying blade is fitted with the inner wall of the fixed cylinder, and the outer surface of the fixed cylinder is fixedly connected to a discharge pipe.
[0017] Preferably, the feeding assembly comprises a first feeding pipe and a second feeding pipe, and one end of the first feeding pipe and one end of the second feeding pipe are both fixedly connected to the top end of the cover plate.
[0018] Preferably, the discharge assembly comprises a discharge pipe, one end of which is fixedly connected to the bottom end of the settling tank, and a valve is fixedly installed inside the discharge pipe.
[0019] Preferably, a support leg is fixedly connected to the bottom end of the settling tank, and a mounting plate is fixedly connected to the bottom end of the support leg.
[0020] (III) Beneficial effects
[0021] Compared with the prior art, the present invention provides a recovery and treatment device for quartz sand pickling liquid, which has the following beneficial effects:
[0022] 1. The present invention can drive the stirring component fixedly installed at its output end to rotate by starting the driving component, so that the stirring component can stir the fluorosilicic acid filtrate and the continuously added inorganic alkali solution, so that they can react and precipitate crystals containing fluorosilicate, and then cooperate with the stirring component to push the crystals containing fluorosilicate sunk to the bottom of the sedimentation tank upward and make them fall on the top of the collecting component. Since the outer surface of the collecting component is fixedly installed with the outer surface of the stirring component, when the stirring component rotates, it can drive the collecting component to push the crystals containing fluorosilicate on its surface to one side of the lifting component. At the same time, the driving component can drive the transmission component fixedly installed at its output end to rotate. When the transmission component rotates, it can drive the lifting component fixedly installed inside to rotate. When the lifting component rotates, it can lift and discharge the crystals containing fluorosilicate inside, so as to avoid affecting the reaction of the subsequently added inorganic alkali solution with the fluorosilicic acid filtrate, thereby improving the precipitation rate of the crystals containing fluorosilicate.
[0023] 2. When the auxiliary transmission wheel of the present invention rotates, it can drive the connecting shaft fixedly installed inside it to rotate. When the connecting shaft rotates, it can drive the spiral conveying blade fixedly connected at one end thereof to rotate. When the spiral conveying blade rotates, it can drive the crystals containing fluorosilicate that pass through the filter plate and enter the fixed cylinder to move upward, and can drive them into the inside of the discharge pipe so that they can flow out from one end of the discharge pipe, thereby facilitating the removal of the crystals containing fluorosilicate precipitated inside the sedimentation tank, thereby avoiding affecting the reaction between the subsequently added inorganic alkali solution and the fluorosilicic acid filtrate.
[0024] 3. The present invention can drive the collecting bucket to rotate through the rotation of the rotating shaft, and can intercept the fluorosilicic acid filtrate and the crystals containing fluorosilicates sprayed from the top of the reflux tube. During its rotation, the fluorosilicic acid filtrate and the crystals containing fluorosilicates are driven to fall to the top of the filter plate, so that the fluorosilicic acid filtrate is filtered and the crystals containing fluorosilicates are retained on the top of the filter plate. Then, with the rotation of the rotating shaft, the scraper can be driven to rotate on the top of the filter plate, so that the crystals containing fluorosilicates are concentratedly scraped into the interior of the fixed tube, so that it is convenient to cooperate with the spiral conveying blade to discharge them from the interior of the sedimentation tank, thereby improving the use effect of the quartz sand pickling solution recovery and treatment device. BRIEF DESCRIPTION OF THE DRAWINGS
[0025] Figure 1 It is a schematic diagram of the three-dimensional structure of the present invention;
[0026] Figure 2 It is a schematic diagram of the structure of the present invention from a rear-view perspective;
[0027] Figure 3 For the present invention Figure 2 A magnified schematic diagram of the local structure at point A;
[0028] Figure 4 This is a schematic diagram of the split structure of the stirring assembly of the present invention;
[0029] Figure 5 For the present invention Figure 4 Middle B is an enlarged schematic diagram of the local structure;
[0030] Figure 6 It is a schematic diagram of the internal structure of the lifting assembly of the present invention;
[0031] Figure 7 For the present invention Figure 6 A magnified schematic diagram of the local structure at C in the middle;
[0032] Figure 8 It is a schematic diagram of the structure of the stirring assembly of the present invention when viewed from above.
[0033] In the figure: 1. sedimentation tank; 2. stirring assembly; 201. cover plate; 202. rotating shaft; 203. reflux stirring blade; 204. supporting frame; 205. reflux cylinder; 206. limiting frame; 3. driving assembly; 301. mounting frame; 302. motor; 303. mounting seat; 4. transmission assembly; 401. main transmission wheel; 402. transmission belt; 403. auxiliary transmission wheel; 5. collecting assembly; 501. filter plate; 502. collecting bucket; 503. scraper; 6. lifting assembly; 601. fixing cylinder; 602. sealing cover; 603. connecting shaft; 604. spiral conveying blade; 605. discharge pipe; 7. feeding assembly; 701. first feed pipe; 702. second feed pipe; 8. discharge assembly; 801. discharge pipe; 802. valve; 9. supporting leg; 10. mounting plate. DETAILED DESCRIPTION
[0034] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0035] As introduced in the background technology, in order to solve the deficiencies existing in the prior art and the above technical problems, the present application proposes a recycling and processing device for quartz sand pickling liquid.
[0036] See also Figure 1-Figure 8 A recycling and processing device for quartz sand pickling liquid comprises a settling tank 1, a stirring component 2 is fixedly installed on the top of the settling tank 1, a driving component 3 is fixedly installed on the top of the stirring component 2, a transmission component 4 is fixedly installed on the output end of the driving component 3, a collecting component 5 is fixedly installed on the outer surface of the stirring component 2, a lifting component 6 is fixedly installed on one side of the collecting component 5, the outer surface of the lifting component 6 is fixedly installed with the inside of the transmission component 4, a feeding component 7 is arranged on the top of the stirring component 2, and a discharging component 8 is fixedly connected to the bottom end of the settling tank 1.
[0037] When in use, the feeding component 7 is connected to the fluorosilicic acid filtrate and the inorganic alkali solution through pipelines, so as to facilitate the addition of the fluorosilicic acid filtrate and the inorganic alkali solution into the sedimentation tank 1. The fluorosilicic acid filtrate is added into the sedimentation tank 1 in cooperation with the feeding component 7, and then the driving component 3 is started, which can drive the stirring component 2 fixedly installed at its output end to rotate, so that the stirring component 2 can stir the fluorosilicic acid filtrate, and then the inorganic alkali solution is continuously added into the sedimentation tank 1 through the feeding component 7. When the inorganic alkali solution contacts the fluorosilicic acid filtrate, it can cause a reaction and precipitate crystals containing fluorosilicates. Then, the crystals containing fluorosilicates sunk to the bottom of the sedimentation tank 1 can be pushed upward in cooperation with the stirring component 2 and made to fall on the top of the collecting component 5. Since the outer surface of the collecting component 5 It is fixedly mounted on the outer surface of the stirring component 2, and when the stirring component 2 rotates, it can drive the collecting component 5 to push the crystals containing fluorosilicate on its surface to one side of the lifting component 6 and make them enter the interior of the lifting component 6. Since the outer surface of the lifting component 6 is fixedly mounted on the interior of the transmission component 4, and the interior of the transmission component 4 is fixedly mounted on the output end of the driving component 3, when the driving component 3 is started, it can cooperate with the transmission component 4 to drive the lifting component 6 to rotate. When the lifting component 6 rotates, the crystals containing fluorosilicate that have entered the interior can be lifted upward and made to flow out from the top of the lifting component 6, thereby completing the collection of the crystals containing fluorosilicate, avoiding that they affect the subsequent reaction between the fluorosilicic acid filtrate and the inorganic alkali solution in the sedimentation tank 1.
[0038] The present invention can drive the stirring component 2 fixedly installed at its output end to rotate by starting the driving component 3, so that the stirring component 2 can stir the fluorosilicic acid filtrate and the continuously added inorganic alkali solution, so that they can react and precipitate crystals containing fluorosilicate, and then cooperate with the stirring component 2 to push the crystals containing fluorosilicate sunk to the bottom of the sedimentation tank 1 upward and make them fall on the top of the collecting component 5. Since the outer surface of the collecting component 5 is fixedly installed with the outer surface of the stirring component 2, when the stirring component 2 rotates, the collecting component 5 can be driven to push the crystals containing fluorosilicate on its surface to one side of the lifting component 6. At the same time, the driving component 3 can drive the transmission component 4 fixedly installed at its output end to rotate. When the transmission component 4 rotates, it can drive the lifting component 6 fixedly installed inside it to rotate. When the lifting component 6 rotates, the crystals containing fluorosilicate inside it can be lifted upward and discharged, so as to avoid affecting the reaction of the subsequently added inorganic alkali solution with the fluorosilicic acid filtrate, thereby improving the precipitation rate of the crystals containing fluorosilicate.
[0039] Furthermore, for the above-mentioned stirring component 2, the stirring component 2 includes a cover plate 201, the bottom end of the cover plate 201 is fixedly installed on the top end of the sedimentation tank 1, a rotating shaft 202 is rotatably arranged inside the cover plate 201, one end of the rotating shaft 202 is fixedly installed on the output end of the driving component 3, and a reflux stirring blade 203 is fixedly installed on one end of the rotating shaft 202.
[0040] By starting the driving component 3, the rotating shaft 202 fixedly installed at its output end is driven to rotate. When the rotating shaft 202 rotates, it can drive the reflux stirring blade 203 fixedly installed at one end thereof to rotate. Since the reflux stirring blade 203 is a push-type, it can push the fluorosilicic acid filtrate at the bottom of the sedimentation tank 1 upward, thereby facilitating the stirring thereof.
[0041] Furthermore, for the above-mentioned stirring component 2, the stirring component 2 also includes a support frame 204, the top end of the support frame 204 is fixedly installed with the bottom end of the cover plate 201, one end of the support frame 204 is fixedly connected with a reflux tube 205, the interior of the reflux tube 205 is fixedly connected with a limiting frame 206, and the interior of the limiting frame 206 is rotatably arranged with the outer surface of the rotating shaft 202.
[0042] When the rotating shaft 202 rotates, it can be rotated inside the limiting frame 206, and then it can swing during the rotation, thereby improving the stability of the rotating shaft 202 during the rotation. The setting of the reflux cylinder 205 can facilitate the reflux stirring blade 203 to concentrate the fluorosilicic acid filtrate pushed upward during the rotation process and limit its pushing direction, so that the fluorosilicic acid filtrate can be pushed to the top of the collecting component 5. When the fluorosilicic acid filtrate reacts with the inorganic alkaline solution and precipitates crystals containing fluorosilicate, it can be synchronously pushed to the top of the collecting component 5 and the crystals containing fluorosilicate are collected.
[0043] Furthermore, for the above-mentioned driving component 3, the driving component 3 includes a mounting frame 301, the bottom end of the mounting frame 301 is fixedly installed with the top end of the cover plate 201, the top end of the mounting frame 301 is fixedly installed with a motor 302, the output end of the motor 302 is fixedly connected with a mounting seat 303, the interior of the mounting seat 303 is fixedly installed with one end of the rotating shaft 202, and the output end of the motor 302 is fixedly installed with the interior of the transmission component 4.
[0044] By starting the motor 302, the mounting base 303 fixedly connected to its output end is driven to rotate. When the mounting base 303 rotates, it can drive the rotating shaft 202 fixedly installed inside it to rotate, thereby providing power for the stirring component 2. At the same time, the motor 302 can drive the transmission component 4 fixedly installed at its output end to rotate, thereby providing stable power for the transmission component 4.
[0045] Furthermore, for the above-mentioned transmission component 4, the transmission component 4 includes a main transmission wheel 401, the interior of the main transmission wheel 401 is fixedly installed with the output end of the motor 302, the inner side of the main transmission wheel 401 is provided with a transmission belt 402, the inner side of the transmission belt 402 is provided with a secondary transmission wheel 403, and the interior of the secondary transmission wheel 403 is fixedly installed with the outer surface of the lifting component 6.
[0046] The main transmission wheel 401 fixedly installed at its output end is driven to rotate by starting the motor 302. Since the main transmission wheel 401 and the auxiliary transmission wheel 403 are connected by the transmission belt 402, when the main transmission wheel 401 rotates, it can cooperate with the transmission belt 402 to drive the auxiliary transmission wheel 403 to rotate. When the auxiliary transmission wheel 403 rotates, it can drive the lifting component 6 fixedly installed inside it to operate, thereby providing stable power for the lifting component 6.
[0047] Furthermore, for the above-mentioned collecting component 5, the collecting component 5 includes a filter plate 501 and a collecting bucket 502, the interior of the filter plate 501 is fixedly connected to the outer surface of the reflux tube 205, the interior of the collecting bucket 502 is fixedly installed to the outer surface of the rotating shaft 202, and the interior of the filter plate 501 is provided with a scraper 503, and the interior of the scraper 503 is fixedly connected to the outer surface of the rotating shaft 202.
[0048] When the fluorosilicic acid filtrate and the crystals containing fluorosilicates are sprayed out from the top of the reflux tube 205, they can collide with the inner side of the collecting bucket 502. Since the interior of the collecting bucket 502 and the scraper 503 are fixedly mounted to the outer surface of the rotating shaft 202, when the rotating shaft 202 rotates, it can drive the collecting bucket 502 to rotate, and can block the fluorosilicic acid filtrate and the crystals containing fluorosilicates sprayed out from the top of the reflux tube 205. During its rotation, it drives the fluorosilicic acid filtrate and the crystals containing fluorosilicates to fall to the top of the filter plate 501, so that the fluorosilicic acid filtrate passes through the filter plate 501, and the crystals containing fluorosilicates are retained on the top of the filter plate 501. Then, as the rotating shaft 202 rotates, it can drive the scraper 503 to rotate at the top of the filter plate 501, so that the crystals containing fluorosilicates are concentratedly scraped into the interior of the lifting component 6, which is more convenient.
[0049] Furthermore, for the above-mentioned lifting component 6, the lifting component 6 includes a fixed cylinder 601, one side of the fixed cylinder 601 is connected to the interior of the filter plate 501, a sealing cover 602 is fixedly installed on the top of the fixed cylinder 601, a connecting shaft 603 is rotatably arranged inside the sealing cover 602, the outer surface of the connecting shaft 603 is fixedly installed inside the auxiliary transmission wheel 403, one end of the connecting shaft 603 is fixedly connected to a spiral conveying blade 604, the outer surface of the spiral conveying blade 604 is fitted with the inner wall of the fixed cylinder 601, and the outer surface of the fixed cylinder 601 is fixedly connected to a discharge pipe 605.
[0050] When the auxiliary transmission wheel 403 rotates, it can drive the connecting shaft 603 fixed inside it to rotate. When the connecting shaft 603 rotates, it can drive the spiral conveying blade 604 fixedly connected at one end thereof to rotate. When the spiral conveying blade 604 rotates, it can drive the crystals containing fluorosilicate that pass through the filter plate 501 and enter the fixed cylinder 601 to move upward, and can drive them into the discharge pipe 605 so that they can flow out from one end of the discharge pipe 605, thereby facilitating the scooping out of the crystals containing fluorosilicate precipitated inside the sedimentation tank 1, which is more convenient.
[0051] Furthermore, for the above-mentioned feeding assembly 7, the feeding assembly 7 includes a first feeding pipe 701 and a second feeding pipe 702, and one end of the first feeding pipe 701 and the second feeding pipe 702 are both fixedly connected to the top end of the cover plate 201.
[0052] By flange-connecting the first feed pipe 701 to the fluosilicic acid filtrate pipeline, and flange-connecting the second feed pipe 702 to the inorganic alkali solution pipeline, it is convenient to feed the material into the sedimentation tank 1.
[0053] Furthermore, for the above-mentioned discharge assembly 8, the discharge assembly 8 includes a discharge pipe 801, one end of the discharge pipe 801 is fixedly connected to the bottom end of the sedimentation tank 1, and a valve 802 is fixedly installed inside the discharge pipe 801.
[0054] The arrangement of the discharge pipe 801 and the valve 802 facilitates the discharge of the mixed solution of the fluorosilicic acid filtrate and the inorganic alkali solution after the reaction in the sedimentation tank 1, which is relatively convenient.
[0055] Furthermore, for the above-mentioned sedimentation tank 1 , a support leg 9 is fixedly connected to the bottom end of the sedimentation tank 1 , and a mounting plate 10 is fixedly connected to the bottom end of the support leg 9 .
[0056] The support legs 9 are provided to facilitate supporting the sedimentation tank 1 , and a mounting plate 10 is fixedly connected to the bottom end thereof, and its position can be fixed by bolts, thereby improving the stability of the sedimentation tank 1 .
[0057] Working principle: When in use, the first feed pipe 701 is flange-connected to the fluosilicic acid filtrate pipeline, and the second feed pipe 702 is flange-connected to the inorganic alkali solution pipeline, and then the fluosilicic acid filtrate is poured into the interior of the sedimentation tank 1 in conjunction with the first feed pipe 701, and then the inorganic alkali solution is continuously added in conjunction with the second feed pipe 702, so that it can react with the fluosilicic acid filtrate and precipitate crystals containing fluosilicic acid salts, and then the motor 302 is started to drive the mounting seat 303 fixedly connected to its output end to rotate, and when the mounting seat 303 rotates, it can drive the rotating shaft 202 fixedly installed inside it to rotate, and when the rotating shaft 202 rotates, it can drive one end of it to be fixed The installed reflux stirring blade 203 rotates, so that the fluorosilicic acid filtrate and the crystals containing fluorosilicate at the bottom of the sedimentation tank 1 can be pushed upward together with the reflux tube 205, and are sprayed out from the top of the reflux tube 205. When the fluorosilicic acid filtrate and the crystals containing fluorosilicate are sprayed out from the top of the reflux tube 205, they can collide with the inner side of the collecting bucket 502. Since the interior of the collecting bucket 502 and the scraper 503 are fixedly installed with the outer surface of the rotating shaft 202, when the rotating shaft 202 rotates, the collecting bucket 502 can be driven to rotate, so that the fluorosilicic acid filtrate and the crystals containing fluorosilicate sprayed out from the top of the reflux tube 205 can be blocked, and During its rotation, the fluorosilicic acid filtrate and the crystals containing fluorosilicate are driven to fall to the top of the filter plate 501, so that the fluorosilicic acid filtrate passes through the filter plate 501, and the crystals containing fluorosilicate are retained on the top of the filter plate 501. Then, with the rotation of the rotating shaft 202, the scraper 503 can be driven to rotate on the top of the filter plate 501, so that the crystals containing fluorosilicate are concentratedly scraped into the interior of the fixed cylinder 601. At the same time, the motor 302 can drive the main transmission wheel 401 fixedly installed at its output end to rotate. When the main transmission wheel 401 rotates, it can cooperate with the transmission belt 402 to drive the secondary transmission wheel 403 to rotate, and the secondary transmission wheel 403 rotates. When it rotates, it can drive the connecting shaft 603 fixed inside it to rotate. When the connecting shaft 603 rotates, it can drive the spiral conveying blade 604 fixedly connected at one end thereof to rotate. When the spiral conveying blade 604 rotates, it can drive the crystals containing fluorosilicate that pass through the filter plate 501 and enter the fixed cylinder 601 to move upward, and can drive them into the inside of the discharge pipe 605 so that they can flow out from one end of the discharge pipe 605, thereby facilitating the removal of the crystals containing fluorosilicate precipitated inside the sedimentation tank 1. When the reaction is completed, the mixed liquid inside the sedimentation tank 1 can be discharged through the discharge pipe 801 by opening the valve 802, which is more convenient.
[0058] According to the above technical scheme, 1. by starting the driving component 3, the stirring component 2 fixedly installed at its output end can be driven to rotate, so that the stirring component 2 can stir the fluorosilicic acid filtrate and the continuously added inorganic alkali solution, so that they can react and precipitate crystals containing fluorosilicate, and then the stirring component 2 can push the crystals containing fluorosilicate sunk to the bottom of the sedimentation tank 1 upward and make them fall on the top of the collecting component 5. Since the outer surface of the collecting component 5 is fixedly installed with the outer surface of the stirring component 2, when the stirring component 2 rotates, the collecting component 5 can be driven to push the crystals containing fluorosilicate on its surface to one side of the lifting component 6. At the same time, the driving component 3 can drive the transmission component 4 fixedly installed at its output end to rotate. When the transmission component 4 rotates, it can drive the lifting component 6 fixedly installed inside it to rotate. When the lifting component 6 rotates, the crystals containing fluorosilicate inside it can be lifted upward and discharged, thereby avoiding affecting the reaction of the subsequently added inorganic alkali solution with the fluorosilicic acid filtrate, thereby improving the precipitation rate of the crystals containing fluorosilicate;
[0059] 2. When the secondary transmission wheel 403 rotates, it can drive the connecting shaft 603 fixedly installed inside to rotate. When the connecting shaft 603 rotates, it can drive the spiral conveying blade 604 fixedly connected at one end thereof to rotate. When the spiral conveying blade 604 rotates, it can drive the crystals containing fluorosilicate that pass through the filter plate 501 and enter the fixed cylinder 601 to move upward, and can drive them into the inside of the discharge pipe 605, so that they can flow out from one end of the discharge pipe 605, thereby facilitating the removal of the crystals containing fluorosilicate precipitated inside the sedimentation tank 1, thereby avoiding affecting the reaction between the inorganic alkali solution added subsequently and the fluorosilicic acid filtrate;
[0060] 3. The rotation of the rotating shaft 202 can drive the collecting bucket 502 to rotate, and can block the fluorosilicic acid filtrate and the crystals containing fluorosilicates sprayed from the top of the reflux tube 205. During the rotation, the fluorosilicic acid filtrate and the crystals containing fluorosilicates are driven to fall to the top of the filter plate 501, so that the fluorosilicic acid filtrate passes through the filter plate 501, and the crystals containing fluorosilicates are retained on the top of the filter plate 501. Then, with the rotation of the rotating shaft 202, the scraper 503 can be driven to rotate on the top of the filter plate 501, so that the crystals containing fluorosilicates are concentratedly scraped into the interior of the fixed tube 601, so that it is convenient for it to cooperate with the spiral conveying blade 604 to discharge them from the interior of the sedimentation tank 1, thereby improving the use effect of the quartz sand pickling liquid recovery and treatment device.
[0061] While the embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that many changes, modifications, substitutions and variations can be made to the embodiments without departing from the principles and spirit of the invention.
Claims
1. A quartz sand pickling liquid recovery and treatment device, comprising a settling tank (1), characterized in that: A stirring assembly (2) is fixedly mounted on the top of the settling tank (1), a driving assembly (3) is fixedly mounted on the top of the stirring assembly (2), a transmission assembly (4) is fixedly mounted on the output end of the driving assembly (3), a collecting assembly (5) is fixedly mounted on the outer surface of the stirring assembly (2), a lifting assembly (6) is fixedly mounted on one side of the collecting assembly (5), the outer surface of the lifting assembly (6) is fixedly mounted to the inside of the transmission assembly (4), a feeding assembly (7) is arranged on the top of the stirring assembly (2), and a discharging assembly (8) is fixedly connected to the bottom end of the settling tank (1); The stirring assembly (2) comprises a cover plate (201), the bottom end of the cover plate (201) is fixedly mounted on the top end of the sedimentation tank (1), a rotating shaft (202) is rotatably arranged inside the cover plate (201), one end of the rotating shaft (202) is fixedly mounted on the output end of the driving assembly (3), and a reflux stirring blade (203) is fixedly mounted on one end of the rotating shaft (202); The stirring assembly (2) further comprises a support frame (204), the top end of the support frame (204) being fixedly mounted to the bottom end of the cover plate (201), one end of the support frame (204) being fixedly connected to a reflux cylinder (205), the interior of the reflux cylinder (205) being fixedly connected to a limiting frame (206), the interior of the limiting frame (206) being rotatably arranged with the outer surface of the rotating shaft (202); The driving assembly (3) comprises a mounting frame (301), the bottom end of the mounting frame (301) is fixedly mounted to the top end of the cover plate (201), a motor (302) is fixedly mounted to the top end of the mounting frame (301), an output end of the motor (302) is fixedly connected to a mounting seat (303), the interior of the mounting seat (303) is fixedly mounted to one end of the rotating shaft (202), and the output end of the motor (302) is fixedly mounted to the interior of the transmission assembly (4); The transmission assembly (4) comprises a main transmission wheel (401), the interior of the main transmission wheel (401) is fixedly mounted to the output end of the motor (302), the inner side of the main transmission wheel (401) is provided with a transmission belt (402), the inner side of the transmission belt (402) is provided with an auxiliary transmission wheel (403), and the interior of the auxiliary transmission wheel (403) is fixedly mounted to the outer surface of the lifting assembly (6); The collecting assembly (5) comprises a filter plate (501) and a collecting bucket (502); the interior of the filter plate (501) is fixedly connected to the outer surface of the reflux cylinder (205); the interior of the collecting bucket (502) is fixedly mounted to the outer surface of the rotating shaft (202); a scraper (503) is provided inside the filter plate (501); the interior of the scraper (503) is fixedly connected to the outer surface of the rotating shaft (202); The lifting assembly (6) comprises a fixed cylinder (601), one side of which is in communication with the interior of the filter plate (501), a sealing cover (602) being fixedly mounted on the top of the fixed cylinder (601), a connecting shaft (603) being rotatably arranged inside the sealing cover (602), an outer surface of the connecting shaft (603) being fixedly mounted inside the auxiliary transmission wheel (403), one end of the connecting shaft (603) being fixedly connected to a spiral conveying blade (604), an outer surface of the spiral conveying blade (604) being arranged to fit the inner wall of the fixed cylinder (601), and a discharge pipe (605) being fixedly connected to the outer surface of the fixed cylinder (601).
2. The quartz sand pickling liquid recovery and treatment device according to claim 1, characterized in that: The feeding assembly (7) comprises a first feeding pipe (701) and a second feeding pipe (702), and one end of each of the first feeding pipe (701) and the second feeding pipe (702) is fixedly connected to the top end of the cover plate (201).
3. The recycling and processing device for quartz sand pickling liquid according to claim 1 is characterized in that: The discharge assembly (8) comprises a discharge pipe (801), one end of which is fixedly connected to the bottom end of the settling tank (1), and a valve (802) is fixedly installed inside the discharge pipe (801).
4. The quartz sand pickling liquid recovery and treatment device according to claim 1, characterized in that: The bottom end of the sedimentation tank (1) is fixedly connected to a support leg (9), and the bottom end of the support leg (9) is fixedly connected to a mounting plate (10).
Citation Information
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