Anti-wrinkle poppy seed oil moisturizing cream and production method thereof

Abstract

The invention discloses anti-wrinkle poppy seed oil moisturizing cream and a production method thereof. The invention relates to a skin care cream, which is prepared from caprylic / capric triglyceride, nicotinamide, hexyldecanol, glyceryl stearate, polydimethylsiloxane, glyceryl stearate citrate, tocopheryl acetate, potassium cetyl phosphate, hydrogenated palm oil glyceride, N-palmitoyl hydroxyproline cetyl ester, disodium EDTA (Ethylene Diamine Tetraacetic Acid), cetostearyl alcohol, deionized water, propylene glycol, butanediol, glycerol and panthenol. The anti-aging agent is prepared from p-hydroxyacetophenone, 1, 2-hexanediol, polyacrylamide, poppy seed oil, 4-tert-butyl cyclohexanol, hyaluronic acid, sodium hydroxide and dipotassium glycyrrhizinate. The anti-wrinkle poppy seed oil moisturizing cream combines various moisturizing, moistening, anti-oxidation, anti-inflammatory and soothing components, can comprehensively improve the problems of skin dryness, water shortage and the like, and particularly, due to the addition of poppy seed oil, the skin is kept in a moisturized, soft and healthy state; meanwhile, the whitening and anti-aging effects are achieved, and the requirements of different skin types can be met.

Description

Technical Field

[0001] The invention belongs to the field of royal rice oil cosmetics, and particularly relates to an anti-wrinkle royal rice oil moisturizing cream and a production method thereof. Background Art

[0002] Royal rice oil is a pure natural product made from rare poppy seeds that have been inactivated and refined. It has extremely high nutritional value and contains extremely high complex medicinal and health care ingredients. According to the inspection reports of the National Grain and Oil Quality Supervision and Inspection Center and the Beijing Center for Disease Control and Prevention, Royal rice oil contains a variety of fatty acids and more than ten kinds of amino acids necessary for normal human growth, as well as a variety of trace elements such as copper, selenium, magnesium, iron, zinc, and manganese. Among them, polyunsaturated fatty acids such as linoleic acid (content as high as 68% or more) and linolenic acid are essential fatty acids that the human body needs but cannot synthesize on its own.

[0003] At present, royal rice oil is generally used as vegetable oil in food. However, according to research, royal rice oil can clean up oxygen free radicals in the human body, increase cell activity, improve immunity, resist radiation, lighten and prevent skin spots, improve facial microcirculation, smooth wrinkles, and whiten and beautify. Therefore, the application potential of royal rice oil in cosmetics needs to be explored urgently. Summary of the invention

[0004] The purpose of the present invention is to provide an anti-wrinkle royal rice oil moisturizing cream and a production method thereof, and the royal rice oil is applied to the design of moisturizing cream skin care products, and combined with a variety of moisturizing, nourishing, anti-oxidant, anti-inflammatory and soothing ingredients, which can comprehensively improve the problems of dry skin, dehydration, etc., and keep the skin hydrated, soft and healthy; at the same time, it also has the effects of whitening, anti-aging and the like, and can meet the needs of different skin types.

[0005] In order to achieve the above object, the present invention adopts the following technical solution.

[0006] In a first aspect, the present invention provides an anti-wrinkle rice oil moisturizing cream, comprising the following components in percentage by mass: Phase A: Caprylic / capric triglyceride 3.5-4.5%, Niacinamide 1.8-2.2%, Hexyldecanol 1.8-2.2%, Glyceryl stearate 1.2-1.8%, Dimethicone 0.8-1.2%, Glyceryl stearate citrate 0.8-1.2%, Tocopheryl acetate 0.8-1.2%, Cetyl phosphate potassium 0.4-0.6%, Hydrogenated palm glycerides 0.18-0.22%, N-palmitoyl hydroxyproline cetyl ester 0.18-0.22%, Disodium EDTA 0.11-0.13%, Cetearyl alcohol 3-5%; Phase B: deionized water 46.38-69.44%, propylene glycol 2-4%, butylene glycol 1-2%, glycerin 1-3%, panthenol 0.3-0.6%, p-hydroxyacetophenone 0.4-0.6%, 1,2-hexanediol 0.4-0.6%, polyacrylamide 0.11-0.13%; Phase C: Royal Rice Oil 10-20%, 4-tert-butyl cyclohexanol 0.5-1.5%, hyaluronic acid 0.1-0.3%, sodium hydroxide 0.1-0.3%, dipotassium glycyrrhizinate 0.08-0.12%; The sum of the mass percentages of the raw materials of phase A, phase B and phase C is 100%.

[0007] Furthermore, the anti-wrinkle rice oil moisturizing cream comprises the following components in percentage by mass: Phase A: Caprylic / capric triglyceride 4%, niacinamide 2%, hexyldecanol 2%, glyceryl stearate 1.5%, dimethicone 1%, glyceryl stearate citrate 1%, tocopheryl acetate 1%, potassium cetyl phosphate 0.5%, hydrogenated palm glycerides 0.2%, cetyl N-palmitoyl hydroxyproline 0.2%, disodium EDTA 0.12%, cetearyl alcohol 4%; Phase B: deionized water 58.36%, propylene glycol 3%, butylene glycol 1.5%, glycerin 1.5%, panthenol 0.5%, p-hydroxyacetophenone 0.5%, 1,2-hexanediol 0.5%, polyacrylamide 0.12%; Phase C: 15% royal rice oil, 1% 4-tert-butyl cyclohexanol, 0.2% hyaluronic acid, 0.2% sodium hydroxide, and 0.1% dipotassium glycyrrhizinate.

[0008] Furthermore, the royal rice oil in phase C is obtained by using inactivated poppy seeds as raw materials, which are subjected to solid-state fermentation treatment after being crushed, and then cold-pressed, deacidified, decolorized and deodorized.

[0009] Preferably, the pulverizing is to grind the inactivated poppy seeds into 60-100 meshes using a food grinder to obtain inactivated poppy seed granular powder.

[0010] Preferably, the solid-state fermentation is to obtain the inactivated poppy seed fermentation product by solid-state fermentation of inactivated poppy seed granule powder with a mixed bacterial agent of Bacillus natto and Bifidobacterium.

[0011] More preferably, the inoculation amount of the mixed bacterial agent is 6-8% of the mass of the inactivated poppy seed granule powder, the mass ratio of Bacillus natto to Bifidobacterium in the mixed bacterial agent is 2:1-3, and the live bacteria content of Bacillus natto is 1×10 10 ~1×10 12 CFU / g, the content of live bifidobacteria is 1×10 10 ~1×10 12 CFU / g.

[0012] More preferably, the fermentation temperature of the solid-state fermentation is 28-32° C., and the fermentation time is 60-84 h.

[0013] Preferably, the cold pressing is to use inactivated poppy seed fermentation material with a water content of 7-8wt%, send it into an oil press to squeeze out oil, control the inactivated poppy seed fermentation material feed temperature to 15°C-25°C, and the oil outlet temperature is not higher than 45°C.

[0014] In a second aspect, the present invention provides a method for producing the above-mentioned anti-wrinkle rice oil moisturizing cream, comprising: (1) Weigh deionized water, propylene glycol, butylene glycol, glycerin, panthenol, p-hydroxyacetophenone, 1,2-hexanediol, and polyacrylamide, and add them into the first stirring tank in sequence, control the stirring speed to 500-600 rpm, and the stirring time to 20-30 min to obtain a phase B mixture; weigh caprylic / capric triglyceride, niacinamide, hexyldecyl alcohol, glyceryl stearate, polydimethylsiloxane, glyceryl stearate citrate, tocopheryl acetate, potassium cetyl phosphate, hydrogenated palm oil glyceride, N- Palmitoyl hydroxyproline cetyl ester, disodium EDTA, and cetearyl alcohol are sequentially added to the second stirred tank, the stirring speed is controlled to be 800-1000 rpm, and the stirring time is 20-40 min to obtain a phase A mixture; royal rice oil, 4-tert-butyl cyclohexanol, hyaluronic acid, dipotassium glycyrrhizate, and sodium hydroxide are weighed, and sequentially added to the third stirred tank, the stirring speed is controlled to be 1200-1500 rpm, the temperature is 45-50° C., and the stirring time is 30-40 min to obtain a phase C mixture; (2) The phase A mixture and the phase B mixture are fed into the fourth stirring tank, the stirring speed is controlled to 1500-2000 rpm, the temperature is raised to 50-55°C, and the mixture is homogenized for 5-10 min. The phase C mixture is fed into the fourth stirring tank, the stirring speed is kept unchanged, the temperature is lowered to 40-50°C, and the mixture is homogenized for 5-10 min to obtain an anti-wrinkle rice oil moisturizing cream.

[0015] Due to the adoption of the above technical solution, the beneficial technical effects of the present invention are: The anti-wrinkle rice oil moisturizing cream of the present invention combines a variety of moisturizing, nourishing, anti-oxidant, anti-inflammatory and soothing ingredients, and can comprehensively improve the problems of dry skin, dehydration, etc., especially the addition of rice oil can keep the skin moisturized, soft and healthy; at the same time, it also has whitening, anti-aging and other effects, and can meet the needs of different skin types. Among them, the caprylic / capric triglyceride used has strong permeability and can quickly penetrate into the deep layer of the skin to provide a lasting moisturizing effect. As a moisturizing factor, it can effectively lock the moisture of the skin and keep the skin moisturized. At the same time, it has a good moisturizing effect and helps to improve the problem of dry skin; niacinamide has a whitening effect, can inhibit the activation and pigmentation of melanocytes, reduce the formation of spots, is anti-oxidant, can remove free radicals, delay the skin aging process, promote the renewal of epidermal cells, help smooth fine lines and wrinkles, make the skin smoother, increase the water content of the stratum corneum, improve its thickness and stability, and protect the skin; hexyldecyl Alcohol regulates the consistency and taste of cosmetics, softens the stratum corneum, promotes cell renewal, improves skin texture, has antibacterial and antiseptic functions, and increases the shelf life of products; glyceryl stearate can absorb moisture on the skin surface to form a moisturizing film to prevent moisture loss, mix oil and water molecules together, provide sufficient moisture and nutrition for the skin, and protect the skin from damage by ultraviolet rays and environmental pollution; polydimethylsiloxane forms a protective film on the skin surface to reduce water evaporation, play a moisturizing role, reduce the friction coefficient between fibers, make the skin feel smoother, improve skin texture, and make the skin more even and smooth. ; Glyceryl stearate citrate has excellent skin feel and eye affinity; Tocopherol acetate can eliminate free radicals in the body, reduce the damage of ultraviolet rays to the human body, nourish the skin, and maintain skin elasticity and luster; Potassium cetyl phosphate, hydrogenated palm oil glycerides, N-palmitoyl hydroxyproline cetyl ester, and cetearyl alcohol help to improve the texture and stability of the product while moisturizing the skin; Disodium EDTA, as a chelating agent, can chelate metal ions to prevent the adverse effects of metal ions on product stability; Propylene glycol, butylene glycol, and glycerin can absorb and retain skin moisture, improving the texture and touch of the product; Pan- Alcohol has a deep moisturizing effect and promotes skin repair and regeneration; parahydroxyacetophenone and 1,2-hexanediol can prevent microbial contamination; polyacrylamide improves the consistency and stability of the product; royal rice oil is rich in various nutrients, such as vitamins, minerals, etc., which help moisturize and nourish the skin; 4-tert-butyl cyclohexanol has anti-inflammatory effects and can relieve skin inflammation and redness; hyaluronic acid is a powerful moisturizing ingredient that can absorb and retain a large amount of water to keep the skin hydrated; sodium hydroxide adjusts the pH value of the product to make it more suitable for the skin; dipotassium glycyrrhizinate has a soothing effect and can relieve skin discomfort and sensitivity. DETAILED DESCRIPTION

[0016] In order to make the purpose, technical solution and advantages of the present invention more clearly understood, the present invention is further described in detail below in conjunction with the embodiments. It should be understood that the specific embodiments described herein are only used to explain the present invention and are not used to limit the present invention.

[0017] Example 1 Preparation of royal rice oil: inactivated poppy seeds are used as raw materials, crushed to 40 meshes by a food grinder to obtain inactivated poppy seed granular powder; the inactivated poppy seed granular powder and a mixed bacterial agent of natto Bacillus and bifidobacterium are subjected to solid-state fermentation to obtain inactivated poppy seed fermentation product, wherein the inoculation amount of the mixed bacterial agent is 3% of the mass of the inactivated poppy seed granular powder, the mass ratio of natto Bacillus and bifidobacterium in the mixed bacterial agent is 2:1, and the live bacterial content of natto Bacillus is 1×10 10 CFU / g, the content of live bifidobacteria is 1×10 10 CFU / g, the fermentation temperature of solid-state fermentation is 28°C, and the fermentation time is 84h; the inactivated poppy seed fermentation material with a water content of 6wt% is sent to the oil press to extract oil, the feeding temperature of the inactivated poppy seed fermentation material is controlled to be 15°C, and the oil outlet temperature is 45°C; the cold-pressed oil is deacidified, decolorized and deodorized to obtain royal rice oil.

[0018] Ingredients for Anti-Wrinkle Rice Oil Moisturizing Cream: Phase A: Caprylic / capric triglyceride 3.5%, niacinamide 1.8%, hexyldecanol 1.8%, glyceryl stearate 1.2%, dimethicone 0.8%, glyceryl stearate citrate 0.8%, tocopheryl acetate 0.8%, cetyl phosphate potassium 0.4%, hydrogenated palm glycerides 0.18%, N-palmitoyl hydroxyproline cetyl ester 0.18%, disodium EDTA 0.11%, cetearyl alcohol 3%; Phase B: deionized water 69.44%, propylene glycol 2%, butylene glycol 1%, glycerin 1%, panthenol 0.3%, p-hydroxyacetophenone 0.4%, 1,2-hexanediol 0.4%, polyacrylamide 0.11%; Phase C: 10% royal rice oil, 0.5% 4-tert-butyl cyclohexanol, 0.1% hyaluronic acid, 0.1% sodium hydroxide, and 0.08% dipotassium glycyrrhizate.

[0019] Preparation of Anti-Wrinkle Rice Oil Moisturizing Cream: (1) Weigh deionized water, propylene glycol, butylene glycol, glycerin, panthenol, p-hydroxyacetophenone, 1,2-hexanediol, and polyacrylamide, and add them to the first stirring tank in sequence, control the stirring speed to 500 rpm, and the stirring time to 20 min to obtain a phase B mixture; weigh caprylic / capric triglyceride, niacinamide, hexyldecyl alcohol, glyceryl stearate, polydimethylsiloxane, glyceryl stearate citrate, tocopheryl acetate, potassium cetyl phosphate, hydrogenated palm oil glyceride, N-palmitoyl hydroxyproline cetyl ester, disodium EDTA, and cetearyl alcohol, and add them to the second stirring tank in sequence, control the stirring speed to 800 rpm, and the stirring time to 20 min to obtain a phase A mixture; weigh royal rice oil, 4-tert-butyl cyclohexanol, hyaluronic acid, dipotassium glycyrrhizate, and sodium hydroxide, and add them to the third stirring tank in sequence, control the stirring speed to 1200 rpm, the temperature to 45°C, and the stirring time to 30 min to obtain a phase C mixture; (2) The phase A mixture and the phase B mixture are fed into the fourth stirring tank, the stirring speed is controlled to 1500 rpm, the temperature is raised to 50°C, and homogenized for 5 minutes. The phase C mixture is fed into the fourth stirring tank, the stirring speed is kept unchanged, the temperature is lowered to 40°C, and homogenized for 5 minutes to obtain the anti-wrinkle rice oil moisturizing cream.

[0020] Example 2 Preparation of royal rice oil: inactivated poppy seeds are used as raw materials, crushed to 80 meshes by a food grinder to obtain inactivated poppy seed granular powder; the inactivated poppy seed granular powder and a mixed bacterial agent of natto Bacillus and bifidobacterium are subjected to solid-state fermentation to obtain inactivated poppy seed fermentation product, wherein the inoculation amount of the mixed bacterial agent is 10% of the mass of the inactivated poppy seed granular powder, the mass ratio of natto Bacillus and bifidobacterium in the mixed bacterial agent is 2:3, and the live bacterial content of natto Bacillus is 1×10 12 CFU / g, the content of live bifidobacteria is 1×10 12 CFU / g, the fermentation temperature of solid-state fermentation is 32°C, and the fermentation time is 60h; the inactivated poppy seed fermentation material with a water content of 9wt% is sent to an oil press to extract oil, and the feed temperature of the inactivated poppy seed fermentation material is controlled to be 25°C, and the oil outlet temperature is 40°C; the cold-pressed oil is deacidified, decolorized, and deodorized to obtain royal rice oil.

[0021] Ingredients for Anti-Wrinkle Rice Oil Moisturizing Cream: Phase A: Caprylic / capric triglyceride 4.5%, niacinamide 2.2%, hexyldecanol 2.2%, glyceryl stearate 1.8%, dimethicone 1.2%, glyceryl stearate citrate 1.2%, tocopheryl acetate 1.2%, cetyl phosphate potassium 0.6%, hydrogenated palm glycerides 0.22%, cetyl N-palmitoyl hydroxyproline 0.22%, disodium EDTA 0.13%, cetearyl alcohol 5%; Phase B: deionized water 46.38%, propylene glycol 4%, butylene glycol 2%, glycerin 3%, panthenol 0.6%, p-hydroxyacetophenone 0.6%, 1,2-hexanediol 0.6%, polyacrylamide 0.13%; Phase C: 20% royal rice oil, 1.5% 4-tert-butyl cyclohexanol, 0.3% hyaluronic acid, 0.3% sodium hydroxide, and 0.12% dipotassium glycyrrhizinate.

[0022] Preparation of Anti-Wrinkle Rice Oil Moisturizing Cream: (1) Weigh deionized water, propylene glycol, butylene glycol, glycerin, panthenol, p-hydroxyacetophenone, 1,2-hexanediol, and polyacrylamide, and add them to the first stirring tank in sequence, control the stirring speed to 600 rpm, and the stirring time to 30 min to obtain a phase B mixture; weigh caprylic / capric triglyceride, niacinamide, hexyldecyl alcohol, glyceryl stearate, polydimethylsiloxane, glyceryl stearate citrate, tocopheryl acetate, potassium cetyl phosphate, hydrogenated palm oil glyceride, N-palmitoyl hydroxyproline cetyl ester, disodium EDTA, and cetearyl alcohol, and add them to the second stirring tank in sequence, control the stirring speed to 1000 rpm, and the stirring time to 40 min to obtain a phase A mixture; weigh royal rice oil, 4-tert-butyl cyclohexanol, hyaluronic acid, dipotassium glycyrrhizate, and sodium hydroxide, and add them to the third stirring tank in sequence, control the stirring speed to 1500 rpm, the temperature to 50°C, and the stirring time to 40 min to obtain a phase C mixture; (2) The phase A mixture and the phase B mixture are fed into the fourth stirring tank, the stirring speed is controlled to 2000 rpm, the temperature is raised to 55°C, and homogenized for 10 min. The phase C mixture is fed into the fourth stirring tank, the stirring speed is kept unchanged, the temperature is lowered to 50°C, and homogenized for 10 min to obtain the anti-wrinkle rice oil moisturizing cream.

[0023] Example 3 Preparation of royal rice oil: inactivated poppy seeds are used as raw materials, crushed to 40-80 meshes by a food grinder to obtain inactivated poppy seed granular powder; the inactivated poppy seed granular powder and a mixed bacterial agent of natto Bacillus and bifidobacterium are subjected to solid-state fermentation to obtain inactivated poppy seed fermentation product, wherein the inoculation amount of the mixed bacterial agent is 6.5% of the mass of the inactivated poppy seed granular powder, the mass ratio of natto Bacillus and bifidobacterium in the mixed bacterial agent is 1:1, and the live bacterial content of natto Bacillus is 1×10 11 CFU / g, the content of live bifidobacteria is 1×10 11 CFU / g, the fermentation temperature of solid-state fermentation is 30°C, and the fermentation time is 72h; the inactivated poppy seed fermentation material with a water content of 7.5wt% is sent to an oil press to extract oil, and the feed temperature of the inactivated poppy seed fermentation material is controlled to be 20°C, and the oil outlet temperature is 35°C; the cold-pressed oil is deacidified, decolorized, and deodorized to obtain royal rice oil.

[0024] Ingredients for Anti-Wrinkle Rice Oil Moisturizing Cream: Phase A: Caprylic / capric triglyceride 4%, niacinamide 2%, hexyldecanol 2%, glyceryl stearate 1.5%, dimethicone 1%, glyceryl stearate citrate 1%, tocopheryl acetate 1%, potassium cetyl phosphate 0.5%, hydrogenated palm glycerides 0.2%, cetyl N-palmitoyl hydroxyproline 0.2%, disodium EDTA 0.12%, cetearyl alcohol 4%; Phase B: deionized water 58.36%, propylene glycol 3%, butylene glycol 1.5%, glycerin 1.5%, panthenol 0.5%, p-hydroxyacetophenone 0.5%, 1,2-hexanediol 0.5%, polyacrylamide 0.12%; Phase C: 15% royal rice oil, 1% 4-tert-butyl cyclohexanol, 0.2% hyaluronic acid, 0.2% sodium hydroxide, and 0.1% dipotassium glycyrrhizinate.

[0025] Preparation of Anti-Wrinkle Rice Oil Moisturizing Cream: (1) Weigh deionized water, propylene glycol, butylene glycol, glycerin, panthenol, p-hydroxyacetophenone, 1,2-hexanediol, and polyacrylamide, and add them to the first stirring tank in sequence, control the stirring speed to 550 rpm, and the stirring time to 25 min to obtain a phase B mixture; weigh caprylic / capric triglyceride, niacinamide, hexyldecyl alcohol, glyceryl stearate, polydimethylsiloxane, glyceryl stearate citrate, tocopheryl acetate, potassium cetyl phosphate, hydrogenated palm oil glyceride, N-palmitoyl hydroxyproline cetyl ester, disodium EDTA, and cetearyl alcohol, and add them to the second stirring tank in sequence, control the stirring speed to 900 rpm, and the stirring time to 30 min to obtain a phase A mixture; weigh royal rice oil, 4-tert-butyl cyclohexanol, hyaluronic acid, dipotassium glycyrrhizate, and sodium hydroxide, and add them to the third stirring tank in sequence, control the stirring speed to 1350 rpm, the temperature to 48°C, and the stirring time to 35 min to obtain a phase C mixture; (2) The phase A mixture and the phase B mixture are fed into the fourth stirring tank, the stirring speed is controlled to 1800 rpm, the temperature is raised to 52.5°C, and homogenized for 8 minutes. The phase C mixture is fed into the fourth stirring tank, the stirring speed is kept unchanged, the temperature is lowered to 45°C, and homogenized for 8 minutes to obtain the anti-wrinkle rice oil moisturizing cream.

[0026] Example 4 Preparation of royal rice oil: inactivated poppy seeds are used as raw materials, crushed to 60 meshes by a food grinder to obtain inactivated poppy seed granular powder; the inactivated poppy seed granular powder and a mixed bacterial agent of natto Bacillus and bifidobacterium are subjected to solid-state fermentation to obtain inactivated poppy seed fermentation product, wherein the inoculation amount of the mixed bacterial agent is 6.5% of the mass of the inactivated poppy seed granular powder, the mass ratio of natto Bacillus and bifidobacterium in the mixed bacterial agent is 1:1, and the live bacterial content of natto Bacillus is 1×10 11CFU / g, the content of live bifidobacteria is 1×10 11 CFU / g, the fermentation temperature of solid-state fermentation is 30°C, and the fermentation time is 72h; the inactivated poppy seed fermentation material with a water content of 7.5wt% is sent to an oil press to extract oil, and the feed temperature of the inactivated poppy seed fermentation material is controlled to be 20°C, and the oil outlet temperature is 35°C; the cold-pressed oil is deacidified, decolorized, and deodorized to obtain royal rice oil.

[0027] Ingredients for Anti-Wrinkle Rice Oil Moisturizing Cream: Phase A: Caprylic / capric triglyceride 3.5%, niacinamide 1.8%, hexyldecanol 1.8%, glyceryl stearate 1.2%, dimethicone 0.8%, glyceryl stearate citrate 0.8%, tocopheryl acetate 0.8%, cetyl phosphate potassium 0.4%, hydrogenated palm glycerides 0.18%, N-palmitoyl hydroxyproline cetyl ester 0.18%, disodium EDTA 0.11%, cetearyl alcohol 3%; Phase B: deionized water 58.69%, propylene glycol 4%, butylene glycol 2%, glycerin 3%, panthenol 0.6%, p-hydroxyacetophenone 0.6%, 1,2-hexanediol 0.6%, polyacrylamide 0.13%; Phase C: 15% royal rice oil, 0.5% 4-tert-butyl cyclohexanol, 0.1% hyaluronic acid, 0.11% sodium hydroxide, and 0.1% dipotassium glycyrrhizinate.

[0028] Preparation of Anti-Wrinkle Rice Oil Moisturizing Cream: (1) Weigh deionized water, propylene glycol, butylene glycol, glycerin, panthenol, p-hydroxyacetophenone, 1,2-hexanediol, and polyacrylamide, and add them to the first stirring tank in sequence, control the stirring speed to 550 rpm, and the stirring time to 25 min to obtain a phase B mixture; weigh caprylic / capric triglyceride, niacinamide, hexyldecyl alcohol, glyceryl stearate, polydimethylsiloxane, glyceryl stearate citrate, tocopheryl acetate, potassium cetyl phosphate, hydrogenated palm oil glyceride, N-palmitoyl hydroxyproline cetyl ester, disodium EDTA, and cetearyl alcohol, and add them to the second stirring tank in sequence, control the stirring speed to 900 rpm, and the stirring time to 30 min to obtain a phase A mixture; weigh royal rice oil, 4-tert-butyl cyclohexanol, hyaluronic acid, dipotassium glycyrrhizate, and sodium hydroxide, and add them to the third stirring tank in sequence, control the stirring speed to 1350 rpm, the temperature to 48°C, and the stirring time to 35 min to obtain a phase C mixture; (2) The phase A mixture and the phase B mixture are fed into the fourth stirring tank, the stirring speed is controlled to 1800 rpm, the temperature is raised to 52.5°C, and homogenized for 8 minutes. The phase C mixture is fed into the fourth stirring tank, the stirring speed is kept unchanged, the temperature is lowered to 45°C, and homogenized for 8 minutes to obtain the anti-wrinkle rice oil moisturizing cream.

[0029] Example 5 Preparation of royal rice oil: inactivated poppy seeds are used as raw materials, crushed to 60 meshes by a food grinder to obtain inactivated poppy seed granular powder; the inactivated poppy seed granular powder and a mixed bacterial agent of natto Bacillus and bifidobacterium are subjected to solid-state fermentation to obtain inactivated poppy seed fermentation product, wherein the inoculation amount of the mixed bacterial agent is 6.5% of the mass of the inactivated poppy seed granular powder, the mass ratio of natto Bacillus and bifidobacterium in the mixed bacterial agent is 1:1, and the live bacterial content of natto Bacillus is 1×10 11 CFU / g, the content of live bifidobacteria is 1×10 11 CFU / g, the fermentation temperature of solid-state fermentation is 30°C, and the fermentation time is 72h; the inactivated poppy seed fermentation material with a water content of 7.5wt% is sent to an oil press to extract oil, and the feed temperature of the inactivated poppy seed fermentation material is controlled to be 20°C, and the oil outlet temperature is 35°C; the cold-pressed oil is deacidified, decolorized, and deodorized to obtain royal rice oil.

[0030] Ingredients for Anti-Wrinkle Rice Oil Moisturizing Cream: Phase A: Caprylic / capric triglyceride 4.5%, niacinamide 2.2%, hexyldecanol 2.2%, glyceryl stearate 1.8%, dimethicone 1.2%, glyceryl stearate citrate 1.2%, tocopheryl acetate 1.2%, cetyl phosphate potassium 0.6%, hydrogenated palm glycerides 0.22%, cetyl N-palmitoyl hydroxyproline 0.22%, disodium EDTA 0.13%, cetearyl alcohol 5%; Phase B: deionized water 57.2%, propylene glycol 2%, butylene glycol 1%, glycerin 1%, panthenol 0.3%, p-hydroxyacetophenone 0.4%, 1,2-hexanediol 0.4%, polyacrylamide 0.11%; Phase C: 15% royal rice oil, 1.5% 4-tert-butyl cyclohexanol, 0.3% hyaluronic acid, 0.2% sodium hydroxide, and 0.12% dipotassium glycyrrhizinate.

[0031] Preparation of Anti-Wrinkle Rice Oil Moisturizing Cream: (1) Weigh deionized water, propylene glycol, butylene glycol, glycerin, panthenol, p-hydroxyacetophenone, 1,2-hexanediol, and polyacrylamide, and add them to the first stirring tank in sequence, control the stirring speed to 550 rpm, and the stirring time to 25 min to obtain a phase B mixture; weigh caprylic / capric triglyceride, niacinamide, hexyldecyl alcohol, glyceryl stearate, polydimethylsiloxane, glyceryl stearate citrate, tocopheryl acetate, potassium cetyl phosphate, hydrogenated palm oil glyceride, N-palmitoyl hydroxyproline cetyl ester, disodium EDTA, and cetearyl alcohol, and add them to the second stirring tank in sequence, control the stirring speed to 900 rpm, and the stirring time to 30 min to obtain a phase A mixture; weigh royal rice oil, 4-tert-butyl cyclohexanol, hyaluronic acid, dipotassium glycyrrhizate, and sodium hydroxide, and add them to the third stirring tank in sequence, control the stirring speed to 1350 rpm, the temperature to 48°C, and the stirring time to 35 min to obtain a phase C mixture; (2) The phase A mixture and the phase B mixture are fed into the fourth stirring tank, the stirring speed is controlled to 1800 rpm, the temperature is raised to 52.5°C, and homogenized for 8 minutes. The phase C mixture is fed into the fourth stirring tank, the stirring speed is kept unchanged, the temperature is lowered to 45°C, and homogenized for 8 minutes to obtain the anti-wrinkle rice oil moisturizing cream.

[0032] Comparative Example 1 A moisturizing face cream, the raw materials of which are as follows by weight percentage: Phase A: Caprylic / capric triglyceride 3.5%, niacinamide 1.8%, hexyldecanol 1.8%, glyceryl stearate 1.2%, dimethicone 0.8%, glyceryl stearate citrate 0.8%, tocopheryl acetate 0.8%, cetyl phosphate potassium 0.4%, hydrogenated palm glycerides 0.18%, N-palmitoyl hydroxyproline cetyl ester 0.18%, disodium EDTA 0.11%, cetearyl alcohol 3%; Phase B: deionized water 73.69%, propylene glycol 4%, butylene glycol 2%, glycerin 3%, panthenol 0.6%, p-hydroxyacetophenone 0.6%, 1,2-hexanediol 0.6%, polyacrylamide 0.13%; Phase C: 4-tert-butyl cyclohexanol 0.5%, hyaluronic acid 0.1%, sodium hydroxide 0.11%, dipotassium glycyrrhizinate 0.1%.

[0033] Preparation of Moisturizing Cream: (1) Weigh deionized water, propylene glycol, butylene glycol, glycerin, panthenol, p-hydroxyacetophenone, 1,2-hexanediol, and polyacrylamide, and add them to the first stirring tank in sequence, control the stirring speed to 550 rpm, and the stirring time to 25 min to obtain a phase B mixture; weigh caprylic / capric triglyceride, niacinamide, hexyldecyl alcohol, glyceryl stearate, polydimethylsiloxane, glyceryl stearate citrate, tocopheryl acetate, potassium cetyl phosphate, hydrogenated palm oil glyceride, N-palmitoyl hydroxyproline cetyl ester, disodium EDTA, and cetearyl alcohol, and add them to the second stirring tank in sequence, control the stirring speed to 900 rpm, and the stirring time to 30 min to obtain a phase A mixture; weigh 4-tert-butyl cyclohexanol, hyaluronic acid, dipotassium glycyrrhizate, and sodium hydroxide, and add them to the third stirring tank in sequence, control the stirring speed to 1350 rpm, the temperature to 48°C, and the stirring time to 35 min to obtain a phase C mixture; (2) Add the phase A mixture and the phase B mixture to the fourth stirring tank, control the stirring speed to 1800 rpm, raise the temperature to 52.5°C, and homogenize for 8 minutes. Add the phase C mixture to the fourth stirring tank, keep the stirring speed unchanged, cool to 45°C, and homogenize for 8 minutes to obtain a moisturizing cream.

[0034] Comparative Example 2 A moisturizing face cream, the raw materials of which are as follows by weight percentage: Phase A: Caprylic / capric triglyceride 3.5%, niacinamide 1.8%, hexyldecanol 1.8%, glyceryl stearate 1.2%, dimethicone 0.8%, glyceryl stearate citrate 0.8%, tocopheryl acetate 0.8%, cetyl phosphate potassium 0.4%, hydrogenated palm glycerides 0.18%, N-palmitoyl hydroxyproline cetyl ester 0.18%, disodium EDTA 0.11%, cetearyl alcohol 3%; Phase B: deionized water 58.69%, propylene glycol 4%, butylene glycol 2%, glycerin 3%, panthenol 0.6%, p-hydroxyacetophenone 0.6%, 1,2-hexanediol 0.6%, polyacrylamide 0.13%; Phase C: 15% coconut oil, 0.5% 4-tert-butyl cyclohexanol, 0.1% hyaluronic acid, 0.11% sodium hydroxide, and 0.1% dipotassium glycyrrhizate.

[0035] Preparation of Moisturizing Cream: (1) Weigh deionized water, propylene glycol, butylene glycol, glycerin, panthenol, p-hydroxyacetophenone, 1,2-hexanediol, and polyacrylamide, and add them to the first stirring tank in sequence, control the stirring speed to 550 rpm, and the stirring time to 25 min to obtain a phase B mixture; weigh caprylic / capric triglyceride, niacinamide, hexyldecyl alcohol, glyceryl stearate, polydimethylsiloxane, glyceryl stearate citrate, tocopheryl acetate, potassium cetyl phosphate, hydrogenated palm oil glyceride, N-palmitoyl hydroxyproline cetyl ester, disodium EDTA, and cetearyl alcohol, and add them to the second stirring tank in sequence, control the stirring speed to 900 rpm, and the stirring time to 30 min to obtain a phase A mixture; weigh 4-tert-butyl cyclohexanol, hyaluronic acid, dipotassium glycyrrhizate, and sodium hydroxide, and add them to the third stirring tank in sequence, control the stirring speed to 1350 rpm, the temperature to 48°C, and the stirring time to 35 min to obtain a phase C mixture; (2) Add the phase A mixture and the phase B mixture to the fourth stirring tank, control the stirring speed to 1800 rpm, raise the temperature to 52.5°C, and homogenize for 8 minutes. Add the phase C mixture to the fourth stirring tank, keep the stirring speed unchanged, cool to 45°C, and homogenize for 8 minutes to obtain a moisturizing cream.

[0036] Test example: Skin stratum corneum moisture content test According to QB_T 4256-2011 "Guidelines for Evaluation of Moisturizing Efficacy of Cosmetics", the capacitance method is used to measure the moisture content of the skin stratum corneum.

[0037] 70 female volunteers aged 18-65 were selected. The volunteers were healthy, had no history of allergies, had not used hormone drugs and immunosuppressants in the past month, and had not participated in other clinical trials in the past three months. They were randomly divided into 7 groups, and the moisturizing creams of Examples 1 to 5 and Comparative Examples 1 to 2 were used respectively. Test site: The inner forearm of the subject, the test area was 3 cm 2 ×3cm 2 , according to (2.0±0.1) mg / cm 2 The amount of application was covered with a latex fingertip to cover the entire test area. The test was conducted using a skin moisture meter, corneometer, and the test results are shown in the following table.

[0038] 30min 60min 90min 120min 180min 240min Example 1 61.05 59.48 57.84 55.76 55.14 54.56 Example 2 62.30 60.92 59.13 58.37 57.75 56.01 Example 3 62.17 60.14 58.01 57.53 56.62 55.31 Example 4 61.31 59.32 58.11 57.85 56.21 54.81 Example 5 61.45 60.44 58.76 57.24 56.63 55.23 Comparative Example 1 51.10 45.25 40.19 38.57 35.66 34.61 Comparative Example 2 61.40 58.32 57.14 56.62 54.58 52.22 By comparing the test results, it can be seen that the moisture content of the stratum corneum of the skin of Examples 1-5 is high, and the water loss rate in the later period is low, and the moisturizing performance is high; Comparative Example 1 has a high deionized water content due to the absence of Royal Rice Oil, and the water loss rate of the stratum corneum of the skin in the test area of ​​the subject is high, and the moisturizing performance is low. Comparative Example 2 does not use Royal Rice Oil, but uses coconut oil. Although the water loss rate of the stratum corneum in the test area of ​​the subject is lower than that of Comparative Example 1, it is still slightly lower than that of Examples 1-5. It can be seen that the moisturizing cream of the present invention has a relatively better moisturizing effect due to the combination of Royal Rice Oil and other ingredients.

[0039] The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention. Any modifications, equivalent substitutions and improvements made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. An anti-wrinkle rice oil moisturizing cream, characterized in that: The following components are included in percentage by mass: Phase A: Caprylic / capric triglyceride 3.5-4.5%, Niacinamide 1.8-2.2%, Hexyldecanol 1.8-2.2%, Glyceryl stearate 1.2-1.8%, Dimethicone 0.8-1.2%, Glyceryl stearate citrate 0.8-1.2%, Tocopheryl acetate 0.8-1.2%, Cetyl phosphate potassium 0.4-0.6%, Hydrogenated palm glycerides 0.18-0.22%, N-palmitoyl hydroxyproline cetyl ester 0.18-0.22%, Disodium EDTA 0.11-0.13%, Cetearyl alcohol 3-5%; Phase B: deionized water 46.38-69.44%, propylene glycol 2-4%, butylene glycol 1-2%, glycerin 1-3%, panthenol 0.3-0.6%, p-hydroxyacetophenone 0.4-0.6%, 1,2-hexanediol 0.4-0.6%, polyacrylamide 0.11-0.13%; Phase C: Royal Rice Oil 10-20%, 4-tert-butyl cyclohexanol 0.5-1.5%, hyaluronic acid 0.1-0.3%, sodium hydroxide 0.1-0.3%, dipotassium glycyrrhizinate 0.08-0.12%; The sum of the mass percentages of the raw materials of phase A, phase B and phase C is 100%.

2. The anti-wrinkle rice oil moisturizing cream according to claim 1, characterized in that: The following components are expressed in percentage by mass: Phase A: Caprylic / capric triglyceride 4%, niacinamide 2%, hexyldecanol 2%, glyceryl stearate 1.5%, dimethicone 1%, glyceryl stearate citrate 1%, tocopheryl acetate 1%, potassium cetyl phosphate 0.5%, hydrogenated palm glycerides 0.2%, cetyl N-palmitoyl hydroxyproline 0.2%, disodium EDTA 0.12%, cetearyl alcohol 4%; Phase B: deionized water 58.36%, propylene glycol 3%, butylene glycol 1.5%, glycerin 1.5%, panthenol 0.5%, p-hydroxyacetophenone 0.5%, 1,2-hexanediol 0.5%, polyacrylamide 0.12%; Phase C: 15% royal rice oil, 1% 4-tert-butyl cyclohexanol, 0.2% hyaluronic acid, 0.2% sodium hydroxide, and 0.1% dipotassium glycyrrhizinate.

3. The anti-wrinkle rice oil moisturizing cream according to claim 1, characterized in that: The royal rice oil in phase C is made from inactivated poppy seeds, which are solid-state fermented after being crushed, and then cold-pressed, deacidified, decolorized and deodorized.

4. The anti-wrinkle rice oil moisturizing cream according to claim 3, characterized in that: The crushing process comprises crushing the inactivated poppy seeds to 60-100 meshes by using a food crusher to obtain inactivated poppy seed granule powder.

5. The anti-wrinkle rice oil moisturizing cream according to claim 4, characterized in that: The solid-state fermentation is to obtain the inactivated poppy seed fermentation product by solid-state fermentation of inactivated poppy seed granule powder and a mixed bacterial agent of natto bacillus and bifidobacterium.

6. The anti-wrinkle rice oil moisturizing cream according to claim 5, characterized in that: The inoculation amount of the mixed bacterial agent is 6-8% of the mass of the inactivated poppy seed granule powder, the mass ratio of Bacillus natto to Bifidobacterium in the mixed bacterial agent is 2:1-3, and the live bacteria content of Bacillus natto is 1×10 10 ~1×10 12 CFU / g, the content of live bifidobacteria is 1×10 10 ~1×10 12 CFU / g.

7. The anti-wrinkle rice oil moisturizing cream according to claim 6, characterized in that: The fermentation temperature of the solid-state fermentation is 28-32° C., and the fermentation time is 60-84 hours.

8. The anti-wrinkle rice oil moisturizing cream according to claim 7, characterized in that: The cold pressing method uses inactivated poppy seed fermentation products with a water content of 7-8wt%, feeds them into an oil press to extract oil, controls the feed temperature of the inactivated poppy seed fermentation products to be 15-25°C, and the oil outlet temperature is not higher than 45°C.

9. The method for producing the anti-wrinkle rice oil moisturizing cream according to claims 1-8, characterized in that: include: (1) Weigh deionized water, propylene glycol, butylene glycol, glycerin, panthenol, p-hydroxyacetophenone, 1,2-hexanediol, and polyacrylamide, and add them into the first stirring tank in sequence, control the stirring speed to 500-600 rpm, and the stirring time to 20-30 min to obtain a phase B mixture; weigh caprylic / capric triglyceride, niacinamide, hexyldecyl alcohol, glyceryl stearate, polydimethylsiloxane, glyceryl stearate citrate, tocopheryl acetate, potassium cetyl phosphate, hydrogenated palm oil glyceride, N- Palmitoyl hydroxyproline cetyl ester, disodium EDTA, and cetearyl alcohol are sequentially added to the second stirred tank, the stirring speed is controlled to be 800-1000 rpm, and the stirring time is 20-40 min to obtain a phase A mixture; royal rice oil, 4-tert-butyl cyclohexanol, hyaluronic acid, dipotassium glycyrrhizate, and sodium hydroxide are weighed, and sequentially added to the third stirred tank, the stirring speed is controlled to be 1200-1500 rpm, the temperature is 45-50° C., and the stirring time is 30-40 min to obtain a phase C mixture; (2) The phase A mixture and the phase B mixture are fed into the fourth stirring tank, the stirring speed is controlled to 1500-2000 rpm, the temperature is raised to 50-55°C, and the mixture is homogenized for 5-10 min. The phase C mixture is fed into the fourth stirring tank, the stirring speed is kept unchanged, the temperature is lowered to 40-50°C, and the mixture is homogenized for 5-10 min to obtain an anti-wrinkle rice oil moisturizing cream.