Electrolysis reactor for preparing pentane

Abstract

The invention relates to the technical field of electrolytic reaction of organic compounds, in particular to an electrolytic reactor for preparing pentane, which comprises a bottom plate, a reaction device for processing electrolytic materials is fixedly arranged on the bottom plate, the reaction device comprises positioning columns fixedly arranged on the bottom plate, the positioning columns are arranged in parallel, and the positioning columns are arranged on the bottom plate. A positioning column is fixedly arranged on the base, a carrying plate is fixedly arranged on the positioning column, a shell is fixedly arranged on the carrying plate, a rotating shaft is rotationally arranged on the carrying plate, a motor is fixedly arranged at the lower end of the carrying plate, and the output end of the motor is fixedly connected with the rotating shaft; the electrolyzer arranged on the peripheral surface of the rotating shaft controls the transmission mechanism at one end of the electrolyzer, so that a worker moves the device to a proper position when using the device and then fixes and positions the device, and then the device is fixed through the arc-shaped groove formed in the inner wall of the shell. The stirring rods can be driven to rotate to stir a solution in the device in the rotating process of the rotating shaft.

Description

Technical Field

[0001] The invention relates to the technical field of electrolytic reaction of organic compounds, in particular to an electrolytic reactor for preparing pentane. Background Art

[0002] The synthesis steps of decafluoro-3-methoxy-2-trifluoromethylpentane include dissolving perfluorohexanone in a suitable solvent (such as diethylene glycol dimethyl ether), and then slowly adding dimethyl sulfate and potassium fluoride. The reaction mixture is stirred at room temperature for several hours (such as 5 hours). After the reaction is completed, a series of post-treatment steps, such as extraction, drying, filtration, concentration and separation and purification, can be used to obtain the target product decafluoro-3-methoxy-2-trifluoromethylpentane. The potassium fluoride is prepared by an electrolytic reactor, and the potassium fluoride undergoes an oxidation-reduction reaction in an aqueous solution or a molten state by the action of an electric current in an electrolytic cell by electrolysis, thereby precipitating the desired product on the cathode and anode respectively. Among them, the boiling point during the electrolytic reaction is very high, and a large amount of heat energy generated during the reaction lacks a collection device, resulting in a waste of resources. Summary of the invention

[0003] Based on the above problems existing in the prior art, the technical solution adopted in the present application is: an electrolytic reactor for preparing pentane, comprising a bottom plate, on which a reaction device for processing electrolytic materials is fixedly arranged; The reaction device comprises positioning posts fixedly arranged on the bottom plate, each of the positioning posts is arranged parallel to each other, a carrier plate is fixedly arranged on the positioning posts, a housing is fixedly arranged on the carrier plate, a rotating shaft is rotatably arranged on the carrier plate, a motor is fixedly arranged on the lower end of the carrier plate, an output end of the motor is fixedly connected to the rotating shaft, and an electrolyzer is slidably arranged on the outer peripheral surface of the rotating shaft; The electrolyzer comprises a positioner slidably arranged on the rotating shaft, a stirring shaft is fixedly arranged on the outer circumference of the positioner, reaction blades are fixedly arranged on the outer circumference of the stirring shaft, and a transmission mechanism for controlling the axial rotation of the reaction blades is arranged on the rotating shaft.

[0004] Preferably, four mutually parallel support columns are fixedly arranged on the bottom plate, and the four support columns are evenly distributed at each corner of the bottom plate, and an anti-skid plate is fixedly arranged on the bottom end of each support column.

[0005] Preferably, a circular groove coaxially arranged therewith is provided at the axis center of the rotating shaft, and two mutually parallel sliding grooves are provided on the outer circumferential surface of the rotating shaft. A slide plate is slidably arranged in the slide groove, and the slide plate is fixedly connected to the positioner. A connecting shaft is rotatably arranged on the slide plate, and a positioning plate is fixedly arranged on the other end of the connecting shaft, and the positioning plate is slidably connected to the other slide groove.

[0006] Preferably, the transmission mechanism includes an arc-shaped groove opened on the inner wall of the outer shell, the stirring shaft is slidably connected to the arc-shaped groove, a plurality of connecting rods parallel to each other are fixedly provided on the positioning plate, a positioning plate is fixedly provided on the other end of the plurality of connecting rods, and a tooth pattern is opened on one end of the positioning plate facing the stirring shaft, and a gear meshing with the tooth pattern is fixedly provided on the outer peripheral surface of the stirring shaft.

[0007] Preferably, the height difference on the vertical surface of the arc-shaped groove is equal to the length of the sliding groove.

[0008] Preferably, a liquid storage tank is fixedly arranged on the bottom plate, a heat dissipation pipe is fixedly arranged in the liquid storage tank, and the heat dissipation pipe is fixedly connected to the outer shell.

[0009] Preferably, a sleeve is fixedly provided on the outer peripheral surface of the shell, an air suction blade is rotatably provided in the sleeve, and a control unit for controlling the rotation of the air suction blade is provided on the positioning plate.

[0010] Preferably, the control unit includes a long plate fixedly mounted on the positioning plate, a guide plate fixedly mounted on the end of the long plate, a guide groove being formed on the guide plate, a long rod fixedly mounted on the suction fan blade, one end of the long rod being movably connected to the guide groove, and the other end of the long rod being fixedly connected to the axis of the suction fan blade.

[0011] Preferably, the outer end of the sleeve is funnel-shaped with one end being small and the other end being large.

[0012] Preferably, a water pump is fixedly provided at the bottom end of the liquid storage tank, a connecting pipe is fixedly provided on the water pump, and the other end of the connecting pipe is fixedly connected to the outer shell.

[0013] The beneficial effects of the present application are as follows: an electrolytic reactor for preparing pentane provided by the present application controls a transmission mechanism at one end of the electrolyzer by means of an electrolyzer arranged on the outer peripheral surface of a rotating shaft, so that when using the device, the staff first moves the device to a suitable position, then fixes it in a fixed position, and then, by providing an arc groove on the inner wall of the outer shell, drives the stirring rod to rotate and stir the solution inside the device during the rotation of the rotating shaft, and in the process of the electrolyzer moving up and down, the long plate controls the guide plate to drive the long rod to rotate, thereby controlling the rotation of the suction fan blades, and the heat generated by the electrolytic reaction in the device is sucked into the liquid storage tank through the suction fan blades for heat conversion.

[0014] In addition to the above-described purposes, features and advantages, the present application also has other purposes, features and advantages. The present application will be further described in detail below with reference to the drawings. BRIEF DESCRIPTION OF THE DRAWINGS

[0015] Figure 1 It is a schematic diagram of the overall structure of the present invention; Figure 2 It is a schematic diagram of the internal structure of the present invention; Figure 3 It is a schematic diagram of the structure of the electrolyzer of the present invention; Figure 4 For the present invention Figure 3 The enlarged structural diagram at A in the middle; Figure 5 It is a schematic diagram of the local structure of the present invention Figure 1 ; Figure 6 It is a schematic diagram of the internal structure of the liquid storage tank of the present invention; Figure 7 It is a schematic diagram of the local structure of the present invention Figure 2 ; Figure 8 It is a schematic diagram of the rotating shaft structure of the present invention.

[0016] In the figure: 1, bottom plate; 11, support column; 12, anti-skid plate; 2, positioning column; 3, loading plate; 31, housing; 32, rotating shaft; 321, circular groove; 322, slide groove; 323, slide plate; 324, connecting shaft; 325, positioning plate; 33, motor; 4, electrolyzer; 41, positioner; 42, stirring shaft; 43, reaction blade; 5, arc groove; 51, connecting rod; 52, positioning plate; 53, gear; 6, liquid storage tank; 61, heat pipe; 7, sleeve; 71, suction fan blade; 8, long board; 81, guide plate; 82, guide groove; 83, long rod; 9, water pump; 91, connecting pipe. DETAILED DESCRIPTION

[0017] It should be noted that, in the absence of conflict, the embodiments and features in the embodiments of the present application can be combined with each other. The present application will be described in detail below with reference to the accompanying drawings and in combination with the embodiments.

[0018] In order to enable those skilled in the art to better understand the solution of the present application, the technical solution in the embodiments of the present application will be clearly and completely described below in conjunction with the drawings in the embodiments of the present application. Obviously, the described embodiments are only part of the embodiments of the present application, not all of the embodiments. Based on the embodiments in the present application, all other embodiments obtained by ordinary technicians in this field without creative work should fall within the scope of protection of the present application.

[0019] Reference Figure 1-Figure 3 , an electrolytic reactor for preparing pentane, comprising a bottom plate 1, on which a reaction device for processing electrolytic materials is fixedly arranged; The reaction device includes positioning columns 2 fixedly arranged on a bottom plate 1, each positioning column 2 is arranged parallel to each other, a loading plate 3 is fixedly arranged on the positioning column 2, a housing 31 is fixedly arranged on the loading plate 3, a rotating shaft 32 is rotatably arranged on the loading plate 3, and a motor 33 is fixedly arranged on the lower end of the loading plate 3, an output end of the motor 33 is fixedly connected to the rotating shaft 32, and an electrolyzer 4 is slidably arranged on the outer peripheral surface of the rotating shaft 32; The electrolyzer 4 includes a positioner 41 slidably disposed on the rotating shaft 32 , a stirring shaft 42 is fixedly disposed on the outer circumference of the positioner 41 , a reaction blade 43 is fixedly disposed on the outer circumference of the stirring shaft 42 , and a transmission mechanism for controlling the axial rotation of the reaction blade 43 is provided on the rotating shaft 32 .

[0020] Reference Figure 2-Figure 4 Four mutually parallel support columns 11 are fixedly arranged on the base plate 1, and the four support columns 11 are evenly distributed at the corners of the base plate 1, and an anti-skid plate 12 is fixedly arranged on the bottom end of each support column 11. The four support columns 11 arranged on the base plate 1 realize the support function of the entire device. At the same time, each support column 11 is arranged at the corner of the base plate 1 so that each support column 11 can be evenly stressed during the support process of the device, thereby avoiding damage to the support column 11 due to uneven force during the support process. At the same time, the anti-skid plate 12 arranged on the bottom end of the support column 11 can increase the friction between the device and the ground, thereby avoiding the device from slipping during use.

[0021] Reference Figure 3-Figure 5 A circular groove 321 coaxially arranged therewith is provided at the axis center of the rotating shaft 32, and two mutually parallel sliding grooves 322 are provided on the outer circumference of the rotating shaft 32. A slide plate 323 is slidably provided in the sliding groove 322, and the slide plate 323 is fixedly connected to the positioner 41. A connecting shaft 324 is rotatably provided on the slide plate 323, and a positioning plate 325 is fixedly provided on the other end of the connecting shaft 324. The positioning plate 325 is slidably connected to another sliding groove 322. By means of the circular groove 321 provided on the rotating shaft 32 and the sliding groove 322 provided on the outer circumference of the rotating shaft 32, it is achieved that when the rotating shaft 32 rotates, the slide plate 323 can be driven to move up and down along the sliding groove 322.

[0022] Reference Figure 6-Figure 8The transmission mechanism includes an arc groove 5 provided on the inner wall of the shell 31, and the stirring shaft 42 is slidably connected to the arc groove 5. A plurality of connecting rods 51 parallel to each other are fixedly provided on the positioning plate 325, and a positioning disk 52 is fixedly provided on the other end of the plurality of connecting rods 51, and a tooth pattern is provided on the end of the positioning disk 52 facing the stirring shaft 42, and a gear 53 meshing with the tooth pattern is fixedly provided on the outer peripheral surface of the stirring shaft 42. Through the tooth pattern provided on the positioning disk 52, when the lower section rotating shaft 32 rotates, the locator 41 rotates, and drives the stirring shaft 42 rotatably connected thereto to rotate, and during the rotation process, the gear 53 meshes with the tooth pattern and rotates, thereby driving the stirring shaft 42 to rotate axially, stirring the reaction solution in the device, and improving the reaction efficiency.

[0023] Reference Figure 2-Figure 4 The height difference on the vertical surface of the arc groove 5 is equal to the length of the slide groove 322. By setting the relationship between the upper and lower height difference of the arc groove 5 and the length of the slide groove 322, the device can be prevented from getting stuck during use.

[0024] Reference Figure 5-Figure 7 A liquid storage tank 6 is fixedly arranged on the bottom plate 1, a heat dissipation pipe 61 is fixedly arranged in the liquid storage tank 6, and the heat dissipation pipe 61 is fixedly connected to the outer shell 31. By setting the liquid storage tank 6 on the bottom plate 1, the staff can fill the liquid storage tank 6 with solution when using the device, and when reacting inside the device, the heat can be converted and stored to improve the utilization efficiency of resources.

[0025] Reference Figure 2-Figure 4 A sleeve 7 is fixedly arranged on the outer circumferential surface of the shell 31, and an air suction fan blade 71 is rotatably arranged in the sleeve 7. A control unit for controlling the rotation of the air suction fan blade 71 is provided on the positioning plate 325. The heat generated during the reaction in the shell 31 is converted by the sleeve 7 arranged on the shell 31 and the air suction fan blade 71 rotatably arranged in the sleeve 7.

[0026] Reference Figure 3-Figure 5 The control unit includes a long plate 8 fixedly arranged on the positioning plate 325, a guide plate 81 fixedly arranged on the end of the long plate 8, a guide groove 82 is opened on the guide plate 81, and a long rod 83 is fixedly arranged on the suction fan blade 71. One end of the long rod 83 is movably connected to the guide groove 82, and the other end of the long rod 83 is fixedly connected to the axis of the suction fan blade 71. By setting the long plate 8 on the positioning plate 325, the suction fan blade 71 is driven to rotate when the positioning plate 325 moves up and down at any time, so as to adsorb the internal hot air flow into the liquid storage tank 6 and realize the conversion and storage of heat.

[0027] Reference Figure 1-Figure 3The outer end of the sleeve 7 is funnel-shaped with one end small and the other end large. By setting the sleeve 7 to be funnel-shaped with one end small and the other end large, when the suction fan blade 71 absorbs the airflow, part of the airflow will condense into beads inside the sleeve 7 and finally fall into the inside of the device.

[0028] Reference Figure 6-Figure 8 A water pump 9 is fixedly arranged at the bottom end of the liquid storage tank 6, and a connecting pipe 91 is fixedly arranged on the water pump 9. The other end of the connecting pipe 91 is fixedly connected to the outer shell 31. By using the water pump 9 arranged at the bottom end of the liquid storage tank 6, the extraction and use of the solution inside the liquid storage tank 6 is realized, which is simple and convenient.

[0029] The specific scheme is as follows: when using the device, the staff first moves the device to a suitable position, and realizes the support function of the entire device by setting four support columns 11 on the bottom plate 1. At the same time, each support column 11 is set at the corner of the bottom plate 1 so that each support column 11 can be evenly stressed during the support process, thereby avoiding damage to the support column 11 due to uneven stress during the support process. At the same time, the anti-skid plate 12 set on the bottom end of the support column 11 can increase the friction between the device and the ground, thereby avoiding the device from slipping during use. By setting the teeth on the positioning plate 52, when the lower section of the rotating shaft 32 rotates, the positioner 41 rotates, and drives the stirring shaft 42 connected to it to rotate, and during the rotation, the gear 53 meshes with the teeth and rotates, thereby driving the stirring shaft 42 to rotate axially, stirring the reaction solution in the device and improving the reaction rate. The liquid storage tank 6 set on the bottom plate 1 enables the staff to fill the liquid storage tank 6 with solution when using the device, and when the device reacts inside, it can improve the utilization efficiency of resources by converting and storing heat.

[0030] A person skilled in the art should understand that the discussion of any of the above embodiments is only exemplary, and within the spirit of the present invention, the technical features in the above embodiments or in different embodiments may be combined, the steps may be implemented in any order, and there are many other variations of the different aspects of the present invention as described above, which are not provided in detail for the sake of simplicity.

[0031] The present invention is intended to cover all such substitutions, modifications and variations that fall within the broad scope of the appended claims. Therefore, any omissions, modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the scope of protection of the present invention.

Claims

1. An electrolytic reactor for preparing pentane, comprising a bottom plate (1), characterized in that: A reaction device for processing electrolytic materials is fixedly arranged on the bottom plate (1); The reaction device comprises a positioning column (2) fixedly arranged on the bottom plate (1), each of the positioning columns (2) being arranged parallel to each other, a carrier plate (3) being fixedly arranged on the positioning column (2), a shell (31) being fixedly arranged on the carrier plate (3), a rotating shaft (32) being rotatably arranged on the carrier plate (3), the rotating shaft (32) being composed of two sections, and the two sections of the rotating shaft (32) being rotatably arranged between each other, the upper section of the rotating shaft (32) being fixedly connected to the shell (31), a motor (33) being fixedly arranged on the lower end of the carrier plate (3), an output end of the motor (33) being fixedly connected to the lower section of the rotating shaft (32), and an electrolyzer (4) being slidably arranged on the outer peripheral surface of the rotating shaft (32); The electrolyzer (4) comprises a positioner (41) slidably arranged on the rotating shaft (32), a stirring shaft (42) is fixedly arranged on the outer peripheral surface of the positioner (41), a reaction blade (43) is fixedly arranged on the outer peripheral surface of the stirring shaft (42), and a transmission mechanism for controlling the axial rotation of the reaction blade (43) is provided on the rotating shaft (32).

2. The electrolytic reactor for preparing pentane according to claim 1, characterized in that: Four mutually parallel support columns (11) are fixedly arranged on the bottom plate (1), and the four support columns (11) are evenly distributed at each corner of the bottom plate (1), and an anti-slip plate (12) is fixedly arranged on the bottom end of each support column (11).

3. The electrolytic reactor for preparing pentane according to claim 1, characterized in that: A circular groove (321) coaxially arranged therewith is provided at the axis center of the rotating shaft (32), two mutually parallel slide grooves (322) are provided on the outer peripheral surface of the rotating shaft (32), a slide plate (323) is slidably arranged in the slide groove (322), the slide plate (323) is fixedly connected to the positioner (41), a connecting shaft (324) is rotatably arranged on the slide plate (323), a positioning plate (325) is fixedly arranged on the other end of the connecting shaft (324), and the positioning plate (325) is slidably connected to the other slide groove (322).

4. The electrolytic reactor for preparing pentane according to claim 3, characterized in that: The transmission mechanism comprises an arcuate groove (5) formed on the inner wall of the housing (31); the stirring shaft (42) is slidably connected to the arcuate groove (5); a plurality of mutually parallel connecting rods (51) are fixedly provided on the positioning plate (325); a positioning plate (52) is fixedly provided on the other end of the plurality of connecting rods (51); and a tooth pattern is formed on one end of the positioning plate (52) facing the stirring shaft (42); and a gear (53) meshing with the tooth pattern is fixedly provided on the outer peripheral surface of the stirring shaft (42).

5. The electrolytic reactor for preparing pentane according to claim 4, characterized in that: The height difference on the vertical plane of the arc-shaped groove (5) is equal to the length of the sliding groove (322).

6. The electrolytic reactor for preparing pentane according to claim 1, characterized in that: A liquid storage tank (6) is fixedly arranged on the bottom plate (1), a heat dissipation pipe (61) is fixedly arranged inside the liquid storage tank (6), and the heat dissipation pipe (61) is fixedly connected to the outer shell (31).

7. The electrolytic reactor for preparing pentane according to claim 4, characterized in that: A sleeve (7) is fixedly arranged on the outer peripheral surface of the housing (31), an air suction blade (71) is rotatably arranged inside the sleeve (7), and a control unit for controlling the rotation of the air suction blade (71) is provided on the positioning plate (325).

8. An electrolytic reactor for preparing pentane according to claim 7, characterized in that: The control unit comprises a long plate (8) fixedly arranged on the positioning plate (325), a guide plate (81) fixedly arranged on the end of the long plate (8), a guide groove (82) being provided on the guide plate (81), a long rod (83) fixedly arranged on the suction fan blade (71), one end of the long rod (83) being movably connected to the guide groove (82), and the other end of the long rod (83) being fixedly connected to the axis of the suction fan blade (71).

9. The electrolytic reactor for preparing pentane according to claim 7, characterized in that: The outer end of the sleeve (7) is arranged in a funnel shape with one end being small and the other end being large.

10. The electrolytic reactor for preparing pentane according to claim 6, characterized in that: A water pump (9) is fixedly arranged at the bottom end of the liquid storage tank (6), a connecting pipe (91) is fixedly arranged on the water pump (9), and the other end of the connecting pipe (91) is fixedly connected to the outer shell (31).

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