A carboxylated nitrile latex polymerization reactor with precise temperature control
By designing a double-segment pulling assembly and detection assembly in a carboxybutyronitrile latex polymerization reactor, synchronous extraction and viscosity detection of reactants are achieved, and resource redundancy and detection error problems caused by the independent operation of traditional sampling and detection devices is solved, and the accuracy and consistency of experimental data are improved.
Patent Information
- Application Number
- CN202510073065.7
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2025-01-17
- Publication Date
- 2025-04-01
- Estimated Expiration
- 2045-01-17
AI Technical Summary
The traditional sampling and detection device operates independently and lacks unified management, resulting in resource redundancy and potential detection errors, affecting the accuracy and reliability of experimental results.
A precise temperature-controlled carboxylic nitrile latex polymerization reactor is designed, using a dual-segment pulling assembly and detection assembly. Through the coordinated work of the lever and piston, synchronous extraction of reactants and viscosity detection are achieved, and multiple detection devices are coordinated.
Through unified management of detection devices, resources are saved, detection errors are avoided, data accuracy and consistency are improved, and the reliability of experimental results is ensured.
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Figure CN119488860B_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of polymerization reactors, in particular to a carboxyl nitrile latex polymerization reactor with precise temperature control. Background Art
[0002] The precise temperature-controlled carboxy nitrile latex polymerization reactor, as a key equipment in the field of polymer material preparation, is specially designed for efficient and stable polymerization of carboxy nitrile latex. Its core design highlight lies in its excellent temperature control capability. Through the advanced temperature control system, it can achieve precise temperature control during the reaction process to ensure that the polymerization reaction is carried out within the optimal temperature range, thereby greatly improving the reaction efficiency and ensuring the stability and consistency of product quality. Considering the large volume and complex internal environment of the reactor, in order to accurately obtain and monitor the real-time status of the reactants inside it, it is usually necessary to install at least two sampling and detection devices at different positions of the reactor. These sampling and detection devices are like the reactor's "Eyes" can capture the changes of key parameters in the reaction process and provide valuable experimental data for scientific researchers to guide the optimization and adjustment of the reaction. However, in traditional sampling and detection practices, these sampling and detection devices are often designed as independently operated systems, each operating independently and lacking unified management and coordination. This practice not only leads to redundant configuration and waste of resources, but also introduces potential detection errors due to the inherent differences between the sensors of each device. Such errors may mislead scientific researchers' judgment on the reaction process, affect the accuracy and reliability of the experimental results, and may even have an adverse effect on the progress and results of the entire R&D project. For this reason, we propose a carboxyl nitrile latex polymerization reactor with precise temperature control. Summary of the invention
[0003] A technical problem to be solved by the present application is: how to design a configuration and management of an optimized sampling and detection device to improve the accuracy and consistency of data.
[0004] In order to solve the above technical problems, the embodiment of the present application provides a carboxyl nitrile latex polymerization reactor with precise temperature control, including a reactor body, and also including:
[0005] Two injection barrels are longitudinally arranged on the reactor body and communicated with the inner cavity thereof, and pistons are slidably connected in the injection barrels, reactants are extracted when the pistons are moved, and reactants are used to provide resistance to the movement of the pistons;
[0006] A lever is slidably arranged on the reactor body and its two ends are respectively connected to the piston;
[0007] A double-stage pulling assembly is arranged on the reactor body and connected to a lever, and is used to pull the lever to move so as to drive the two pistons to move;
[0008] The detection component is arranged on the reactor body and connected to the lever. When the front section of the double-stage pulling component drives the lever to move, if the two pistons do not move at the same time, the lever will deflect and trigger the detection component, which indicates that the viscosity of the upper and lower layers of the reactants in the reactor body is different.
[0009] When the front section of the double-stage pulling assembly drives the lever to move, and the two pistons move synchronously, this section of the detection assembly will not be triggered. Subsequently, the double-stage pulling assembly continues to work in the rear section and continues to drive the lever to move. At this time, the detection assembly is used to detect the viscosity of the reactants in the two syringes.
[0010] In some embodiments, the two-stage pulling assembly includes a guide rod fixedly connected to the reactor body, a shaft 1 is fixedly connected to the middle of the lever, an H-shaped frame is rotatably connected to the shaft 1, a sliding sleeve is fixedly connected to the side wall of the H-shaped frame, one end of the guide rod slides through the sliding sleeve to guide and limit the movement of the H-shaped frame, and the movement of the H-shaped frame drives the lever to move;
[0011] A U-shaped frame is arranged at one end of the H-shaped frame, a mounting frame is fixedly connected to one end of the guide rod, an electric push rod is fixedly connected to the mounting frame, the electric push rod is fixedly connected to the U-shaped frame, and the electric push rod is started to drive the H-shaped frame to move;
[0012] A conduit is connected between the injection cylinder and the reactor body.
[0013] In some embodiments, one end of the piston is fixedly connected to a push rod, one end of the push rod slides through the injection barrel and is fixedly connected to a U-shaped plate, a second shaft is rotatably connected to the U-shaped plate, and a guide groove is provided at the end of the lever, and the second shaft is located in the guide groove and is slidably connected to its inner wall.
[0014] In some embodiments, the detection assembly includes a tension sensor having one end fixed to a U-shaped frame, and a connector is provided between the U-shaped frame and the H-shaped frame for fixedly connecting the U-shaped frame and the H-shaped frame;
[0015] A rectangular block is fixedly connected to the other end of the tension sensor, a tension spring is fixedly connected to one side of the rectangular block, a pulling member is arranged between the tension spring and the lever, and the tension spring is pulled by the pulling member when the lever is deflected.
[0016] In some embodiments, the pulling member includes a pulling rod slidably connected in an H-shaped frame, one end of the pulling rod is fixedly connected to a tension spring, a deflection plate is fixedly connected to the middle of the lever, one end of the deflection plate is fixedly connected to axis three, and one end of the pulling rod is also fixedly connected to axis three, and a connecting rod is rotatably connected between the two axis threes, which drives the pulling rod to move and pull the tension spring when the lever is deflected.
[0017] In some embodiments, the connecting member includes a hollow cylinder 1 fixedly connected to the U-shaped frame, a hollow cylinder 2 fixedly connected to the H-shaped frame, a latch slidably connected inside the hollow cylinder 1, and one end of the latch is located inside the hollow cylinder 2 to lock the U-shaped frame and the H-shaped frame;
[0018] A rectangular plate is arranged on the mounting frame, one end of the latch is fixedly connected with a cylindrical protrusion, a guide groove is opened on the rectangular plate, one end of the cylindrical protrusion is located in the guide groove, and a locking piece is arranged between the rectangular block and the U-shaped frame. Moving the U-shaped frame drives the cylindrical protrusion to slide along the guide groove to drive the latch to pull out the hollow cylinder 2, and at the same time, the rectangular plate and the H-shaped frame are locked by the locking piece.
[0019] In some embodiments, the guide groove member includes a straight slide groove 1 opened on the rectangular plate, one end of the cylindrical protrusion is located in the straight slide groove 1 and is slidably connected to the inner wall thereof, and when the U-shaped frame is moved, the cylindrical protrusion slides along the straight slide groove 1 to stably connect the U-shaped frame and the H-shaped frame;
[0020] The rectangular plate is provided with an inclined slide groove connected with the straight slide groove 1. In the process of moving the U-shaped frame, the cylindrical protrusion is driven to slide along the inclined slide groove to drive the latch to disengage from the hollow cylinder 2.
[0021] In some embodiments, a second straight slide groove connected to the inclined slide groove is provided on the rectangular plate.
[0022] In some embodiments, the locking member includes two sliding columns symmetrically slidably connected in a rectangular block, a spring is fixedly connected between the two sliding columns, and a sliding column is slidably connected in the hollow cylinder 2. During the process of inserting the pin into the hollow cylinder 2, the sliding column is pushed to move and push the sliding column out of the hollow cylinder 2, and at the same time the spring is compressed to provide it with self-restoring elastic force.
[0023] In some embodiments, two ends of the tension sensor are detachably connected to the U-shaped frame and the rectangular block respectively.
[0024] The present invention has at least the following beneficial effects:
[0025] The device starts the electric push rod and uses the lever to drive the two pistons to move and extract the reactants in the reactor body, and then judges the reaction status of the reactants by the movement of the two pistons, thereby coordinating the operation of multiple detection devices and saving resources.
[0026] This device uses the same tension sensor when detecting the degree of mixing of the upper and lower layers of reactants in the reactor body, as well as when detecting the viscosity of the reactants, which saves resources and avoids the problem of potential detection errors caused by inherent differences between sensors. BRIEF DESCRIPTION OF THE DRAWINGS
[0027] Figure 1 This is a schematic diagram of the overall structure of Embodiment 1 of the present invention;
[0028] Figure 2 For the present invention Figure 1 Schematic diagram of the local cross-section structure;
[0029] Figure 3 For the present invention Figure 2 Schematic diagram of the local cross-section structure;
[0030] Figure 4 For the present invention Figure 3 Schematic diagram of the local cross-section structure;
[0031] Figure 5 For the present invention Figure 4 Schematic diagram of the local cross-section structure;
[0032] Figure 6 For the present invention Figure 5 Schematic diagram of the local cross-section structure;
[0033] Figure 7 For the present invention Figure 6 Schematic diagram of the partial cross-section structure.
[0034] In the figure: 1-reactor body; 2-injection cylinder; 3-piston; 4-lever; 5-double-stage pulling assembly; 6-detection assembly; 51-guide rod; 52-axis one; 53-H-type frame; 54-sliding sleeve; 55-U-type frame; 56-mounting frame; 57-electric push rod; 58-push rod; 59-U-type plate; 61-axis two; 62-guide groove; 63-tension sensor; 64-connector; 65-torque shaped block; 66-tension spring; 67-pulling member; 68-pull rod; 69-deflection plate; 71-axis three; 72-connecting rod; 73-hollow cylinder one; 74-hollow cylinder two; 75-latch pin; 76-rectangular plate; 77-cylindrical convex; 78-guide groove member; 79-locking member; 81-straight slide groove one; 82-oblique slide groove; 83-straight slide groove two; 84-sliding column; 85-spring; 86-sliding column. DETAILED DESCRIPTION
[0035] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0036] Example 1: Please refer to Figure 1-7The present invention provides a technical solution: a carboxyl nitrile latex polymerization reactor with precise temperature control, comprising a reactor body 1, a protective shell fixedly connected to the reactor body 1, and a mechanical structure for protecting the device body, and also comprising:
[0037] Two injection barrels 2 are longitudinally arranged on the reactor body 1 and communicated with the inner cavity thereof, and pistons 3 are slidably connected in the injection barrels 2 to extract reactants and provide resistance to the movement of the pistons 3 when the pistons 3 are moved;
[0038] A lever 4 is slidably disposed on the reactor body 1 and its two ends are respectively connected to the piston 3;
[0039] A double-stage pulling assembly 5 is arranged on the reactor body 1 and connected to the lever 4, and is used to pull the lever 4 to move so as to drive the two pistons 3 to move;
[0040] The detection component 6 is arranged on the reactor body 1 and connected to the lever 4. When the front section of the double-section pulling component 5 drives the lever 4 to move, if the two pistons 3 do not move at the same time, the lever 4 will deflect and trigger the detection component 6, which indicates that the viscosity of the upper and lower layers of the reactants in the reactor body 1 is different;
[0041] When the front section of the two-stage pulling component 5 drives the lever 4 to move, and the two pistons 3 move synchronously, this section of the detection component 6 will not be triggered. Subsequently, the two-stage pulling component 5 continues to work in the rear section and continues to drive the lever 4 to move. At this time, the detection component 6 is used to detect the viscosity of the reactants in the two syringes 2.
[0042] The double-stage pulling assembly 5 includes a guide rod 51 fixedly connected to the reactor body 1, a shaft 52 fixedly connected to the middle of the lever 4, an H-shaped frame 53 rotatably connected to the shaft 52 through a bearing, a sliding sleeve 54 fixedly connected to the side wall of the H-shaped frame 53, one end of the guide rod 51 slides through the sliding sleeve 54 to guide and limit the movement of the H-shaped frame 53, and the H-shaped frame 53 slides on the guide rod 51 to drive the lever 4 to move;
[0043] A U-shaped frame 55 is provided at one end of the H-shaped frame 53, a mounting frame 56 is fixedly connected to one end of the guide rod 51, an electric push rod 57 is fixedly connected to the mounting frame 56, and the extended end of the electric push rod 57 is fixedly connected to the U-shaped frame 55. When the electric push rod 57 is started, the U-shaped frame 55 is driven to move, thereby driving the H-shaped frame 53 to move;
[0044] A conduit is connected between the injection cylinder 2 and the reactor body 1 to balance the air pressure inside the injection cylinder 2 and the reactor body 1 .
[0045] One end of the piston 3 is fixedly connected to a push rod 58, one end of the push rod 58 slides through the injection barrel 2 and is fixedly connected to a U-shaped plate 59, a shaft 61 is rotatably connected to the U-shaped plate 59 through a bearing, and a guide groove 62 is provided at the end of the lever 4, the shaft 61 is located in the guide groove 62 and is slidably connected to the inner wall thereof, and when the lever 4 is moved, the push rod 58 is driven to move, thereby driving the piston 3 to move.
[0046] The detection assembly 6 includes a tension sensor 63 having one end fixed to the U-shaped frame 55, and a connecting member 64 is provided between the U-shaped frame 55 and the H-shaped frame 53 for fixedly connecting the U-shaped frame 55 and the H-shaped frame 53;
[0047] A rectangular block 65 is fixedly connected to the other end of the tension sensor 63, a tension spring 66 is fixedly connected to one side of the rectangular block 65, a pulling member 67 is provided between the tension spring 66 and the lever 4, and when the lever 4 is deflected, the pulling member 67 is used to pull the tension spring 66, thereby providing tension for the tension sensor 63.
[0048] The pulling member 67 includes a pulling rod 68 slidably connected in the H-shaped frame 53, one end of the pulling rod 68 is fixedly connected to the tension spring 66, a deflection plate 69 is fixedly connected to the middle part of the lever 4, one end of the deflection plate 69 is fixedly connected to the shaft three 71, and one end of the pulling rod 68 is also fixedly connected to the shaft three 71, and a connecting rod 72 is rotatably connected between the two shafts three 71 through a bearing. When the lever 4 is deflected, the deflection plate 69 is driven to deflect, and then the connecting rod 72 is driven to move, thereby driving the pulling rod 68 to move and pull the tension spring 66.
[0049] The connecting member 64 includes a hollow cylinder 1 73 fixedly connected to the U-shaped frame 55, a hollow cylinder 2 74 fixedly connected to the H-shaped frame 53, a latch 75 slidably connected inside the hollow cylinder 1 73, and one end of the latch 75 is located inside the hollow cylinder 2 74 to lock the U-shaped frame 55 and the H-shaped frame 53;
[0050] A rectangular plate 76 is fixedly connected to the mounting frame 56, one end of the latch 75 is fixedly connected to a cylindrical protrusion 77, a guide groove 78 is provided on the rectangular plate 76, one end of the cylindrical protrusion 77 is located in the guide groove 78, and a locking member 79 is provided between the rectangular block 65 and the U-shaped frame 55. Moving the U-shaped frame 55 drives the cylindrical protrusion 77 to slide along the guide groove 78, so as to drive the latch 75 to pull out the hollow cylinder 2 74, and at the same time, the locking member 79 is used to lock the rectangular plate 76 and the H-shaped frame 53.
[0051] The guide groove member 78 includes a straight groove 81 formed on the rectangular plate 76. One end of the cylindrical protrusion 77 is located in the straight groove 81 and is slidably connected to the inner wall thereof. When the U-shaped frame 55 is moved, the cylindrical protrusion 77 slides along the straight groove 81 to stably connect the U-shaped frame 55 and the H-shaped frame 53.
[0052] The rectangular plate 76 is provided with an inclined slide groove 82 which is connected to the straight slide groove 1 81 . When the U-shaped frame 55 is moved, the cylindrical protrusion 77 is driven to slide along the inclined slide groove 82 to drive the latch 75 to disengage from the hollow cylinder 2 74 .
[0053] The rectangular plate 76 is provided with a second straight slide groove 83 connected to the oblique slide groove 82 , so that the cylindrical protrusion 77 is driven to slide along the second straight slide groove 83 during the subsequent movement of the U-shaped frame 55 to stabilize the state of the latch 75 being separated from the second hollow cylinder 74 .
[0054] The locking member 79 includes two sliding columns 84 symmetrically slidably connected in the rectangular block 65, a spring 85 is fixedly connected between the two sliding columns 84, and a sliding column 86 is slidably connected in the hollow cylinder 74. When the latch 75 is inserted into the hollow cylinder 74, the sliding column 86 is pushed to move and push the sliding column 84 out of the hollow cylinder 74, and at the same time, the spring 85 is compressed to provide it with self-restoring elastic force.
[0055] Specifically, when the carboxyl nitrile latex reacts in the reactor, the initial step is to mix various raw materials. After the mixing is completed, additives will be further added to allow the reaction to proceed. As the reaction proceeds, the viscosity of the reactants will gradually increase. When the device is in use, the electric push rod 57 is started to drive the U-shaped frame 55 and the H-shaped frame 53 to move synchronously (at this time, because the cylindrical protrusion 77 is located in the straight slide groove 1 81, and the latch 75 is located in the hollow cylindrical second 74 on the H-shaped plate to connect the U-shaped frame 55 and the H-shaped frame 53 into a whole, at this time, one end of the tension sensor 63 is fixed to the U-shaped frame 55 The lever 4 is fixedly connected, and the other end is fixedly connected to the pull rod 68 through the tension spring 66), thereby driving the lever 4 to move, thereby driving the two pistons 3 to move to extract the reactants in the reactor body 1. At this time, two situations may occur. In the first situation, when the upper and lower layers of the reaction substances in the reactor body 1 are not mixed well, or the reaction is uneven, the viscosity of the upper and lower layers of the reaction substances in the reactor is different. Therefore, when the lever 4 drives the two pistons 3 to move, the resistance they encounter is also different, which causes the lever 4 to deflect due to the uneven force at both ends, so as to drive the deflection plate 69 to deflect and pull the connecting rod 72, thereby driving the pull rod 68 to move and pull the tension spring 66, so as to The tension sensor 63 is pulled, and then a signal is sent through the tension sensor 63 to control the electric push rod 57 to reset and push out the reactants in the syringe 2 (indicating that the reaction progress of the reactants in the reactor body 1 is different in different areas, or the mixing is not in place), and at the same time, it indicates that the materials in the reactor body 1 are unevenly mixed or react unevenly, and the reaction should continue and be fully stirred. In the second case, when the viscosity of the upper and lower layers of the reactor is the same, the resistance encountered when the lever 4 drives the two pistons 3 to move is also the same, and then the lever 4 will not deflect. At this time, the tension sensor 63 is not subjected to force, and then the electric push rod 5 is activated. 7 continues to pull, and at the same time drives the cylindrical protrusion 77 to slide along the inclined slide groove 82, thereby driving the latch 75 to pull out the hollow cylinder 2 74, and at the same time the spring 85 resets to drive the sliding column 84 to insert into the hollow cylinder 2 74, thereby fixing one end of the tension sensor 63 to the H-shaped frame 53, and at the same time disconnecting the H-shaped frame 53 from the U-shaped frame 55. At this time, the two ends of the tension sensor 63 are respectively fixed to the U-shaped frame 55, and the other end is fixed to the H-shaped frame 53, so that the tension sensor 63 is used to test the resistance of the two pistons 3, so as to detect the viscosity of the reactants, and then monitor the reaction process of the reactants;
[0056] The device starts the electric push rod 57 and uses the lever 4 to drive the two pistons 3 to move and extract the reactants in the reactor body 1, and then judges the reaction status of the reactants by the movement of the two pistons 3, so that multiple detection devices are operated in a coordinated manner, which is more resource-saving. At the same time, when the mixing degree of the upper and lower layers of the reactants in the reactor body 1 is detected, and when the viscosity of the reactants is detected, the same tension sensor 63 is used, which is more resource-saving and avoids the inherent differences that may exist between sensors, thereby introducing potential detection errors.
[0057] Example 2: Please refer to Figure 1-7 , the present invention provides a technical solution: Example 2 is optimized on the basis of Example 1;
[0058] The two ends of the tension sensor 63 are detachably connected to the U-shaped frame 55 and the rectangular block 65 respectively. The detachable design of the tension sensor 63 facilitates subsequent debugging, disassembly and replacement thereof.
[0059] It should be noted that, in this article, relational terms such as first and second, etc. are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Moreover, the terms "include", "comprise" or any other variants thereof are intended to cover non-exclusive inclusion, so that a process, method, article or device including a series of elements includes not only those elements, but also other elements not explicitly listed, or also includes elements inherent to such process, method, article or device.
[0060] While the embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that many changes, modifications, substitutions and variations can be made to the embodiments without departing from the principles and spirit of the invention.
Claims
1. A carboxyl nitrile latex polymerization reactor with precise temperature control, comprising a reactor body (1), characterized in that: Also included are: Two injection barrels (2) are longitudinally arranged on the reactor body (1) and communicate with the inner cavity thereof, and a piston (3) is slidably connected inside the injection barrel (2). When the piston (3) is moved, reactants are extracted and the reactants are used to provide resistance to the movement of the piston (3); A lever (4) is slidably disposed on the reactor body (1) and has two ends respectively connected to the piston (3); A two-stage pulling assembly (5) is arranged on the reactor body (1) and connected to the lever (4), and is used to pull the lever (4) to move so as to drive the two pistons (3) to move; The detection component (6) is arranged on the reactor body (1) and connected to the lever (4). When the front section of the double-section pulling component (5) drives the lever (4) to move, if the two pistons (3) do not move at the same time, the lever (4) will deflect and trigger the detection component (6), which indicates that the viscosity of the upper and lower layers of the reactants in the reactor body (1) is different; When the front section of the two-stage pulling component (5) drives the lever (4) to move, and the two pistons (3) move synchronously, this section of the detection component (6) will not be triggered. Subsequently, the two-stage pulling component (5) continues to work in the rear section and continues to drive the lever (4) to move. At this time, the detection component (6) is used to detect the viscosity of the reactants in the two syringes (2).
2. The precise temperature-controlled carboxylated nitrile latex polymerization reactor according to claim 1, characterized in that: The two-stage pulling assembly (5) comprises a guide rod (51) fixedly connected to the reactor body (1); a shaft (52) is fixedly connected to the middle of the lever (4); an H-shaped frame (53) is rotatably connected to the shaft (52); a sliding sleeve (54) is fixedly connected to the side wall of the H-shaped frame (53); one end of the guide rod (51) slides through the sliding sleeve (54) to guide and limit the movement of the H-shaped frame (53); and the movement of the H-shaped frame (53) drives the lever (4) to move; A U-shaped frame (55) is provided at one end of the H-shaped frame (53); a mounting frame (56) is fixedly connected to one end of the guide rod (51); an electric push rod (57) is fixedly connected to the mounting frame (56); the electric push rod (57) is fixedly connected to the U-shaped frame (55); when the electric push rod (57) is started, the H-shaped frame (53) is driven to move; A conduit is connected between the injection cylinder (2) and the reactor body (1).
3. The carboxyl nitrile latex polymerization reactor with precise temperature control according to claim 2, characterized in that: One end of the piston (3) is fixedly connected to a push rod (58), one end of the push rod (58) slides through the injection cylinder (2) and is fixedly connected to a U-shaped plate (59), a second shaft (61) is rotatably connected to the U-shaped plate (59), and a guide groove (62) is formed at the end of the lever (4), the second shaft (61) is located in the guide groove (62) and is slidably connected to the inner wall thereof.
4. The carboxyl nitrile latex polymerization reactor with precise temperature control according to claim 3, characterized in that: The detection assembly (6) comprises a tension sensor (63) having one end fixed to the U-shaped frame (55), and a connecting piece (64) is provided between the U-shaped frame (55) and the H-shaped frame (53) for fixedly connecting the U-shaped frame (55) and the H-shaped frame (53); A rectangular block (65) is fixedly connected to the other end of the tension sensor (63), a tension spring (66) is fixedly connected to one side of the rectangular block (65), a pulling member (67) is provided between the tension spring (66) and the lever (4), and the pulling member (67) is used to pull the tension spring (66) when the lever (4) is deflected.
5. The carboxyl nitrile latex polymerization reactor with precise temperature control according to claim 4, characterized in that: The pulling member (67) includes a pulling rod (68) slidably connected in the H-shaped frame (53), one end of the pulling rod (68) is fixedly connected to the tension spring (66), a deflection plate (69) is fixedly connected to the middle of the lever (4), one end of the deflection plate (69) is fixedly connected to the shaft three (71), and one end of the pulling rod (68) is also fixedly connected to the shaft three (71), and a connecting rod (72) is rotatably connected between the two shafts three (71), which drives the pulling rod (68) to move and pull the tension spring (66) when the lever (4) is deflected.
6. The precise temperature-controlled carboxylated nitrile latex polymerization reactor according to claim 5, characterized in that: The connecting member (64) comprises a hollow cylinder 1 (73) fixedly connected to the U-shaped frame (55), a hollow cylinder 2 (74) fixedly connected to the H-shaped frame (53), a latch (75) slidably connected inside the hollow cylinder 1 (73), and one end of the latch (75) is located inside the hollow cylinder 2 (74) to lock the U-shaped frame (55) and the H-shaped frame (53); A rectangular plate (76) is provided on the mounting frame (56), one end of the latch (75) is fixedly connected to a cylindrical protrusion (77), a guide groove (78) is provided on the rectangular plate (76), one end of the cylindrical protrusion (77) is located in the guide groove (78), and a locking member (79) is provided between the rectangular block (65) and the U-shaped frame (55), and the U-shaped frame (55) is moved to drive the cylindrical protrusion (77) to slide along the guide groove (78), so as to drive the latch (75) to pull out the second hollow cylinder (74), and at the same time, the rectangular plate (76) and the H-shaped frame (53) are locked by the locking member (79).
7. The precise temperature-controlled carboxylated nitrile latex polymerization reactor according to claim 6, characterized in that: The guide groove member (78) comprises a straight slide groove (81) formed on the rectangular plate (76); one end of the cylindrical protrusion (77) is located in the straight slide groove (81) and is slidably connected to the inner wall thereof; when the U-shaped frame (55) is moved, the cylindrical protrusion (77) slides along the straight slide groove (81) to stably connect the U-shaped frame (55) and the H-shaped frame (53); The rectangular plate (76) is provided with an inclined slide groove (82) connected to the straight slide groove (81). When the U-shaped frame (55) is moved, the cylindrical protrusion (77) is driven to slide along the inclined slide groove (82) to drive the latch (75) to disengage from the hollow cylinder (74).
8. The precise temperature-controlled carboxylated nitrile latex polymerization reactor according to claim 7, characterized in that: The rectangular plate (76) is provided with a second straight slide groove (83) which is connected to the inclined slide groove (82).
9. The precise temperature-controlled carboxylated nitrile latex polymerization reactor according to claim 8, characterized in that: The locking member (79) comprises two sliding columns (84) symmetrically slidably connected in the rectangular block (65), a spring (85) is fixedly connected between the two sliding columns (84), and a sliding column (86) is slidably connected in the second hollow cylinder (74). When the latch (75) is inserted into the second hollow cylinder (74), the sliding column (86) is pushed to move and push the sliding column (84) out of the second hollow cylinder (74), and at the same time, the spring (85) is compressed to provide a self-restoring elastic force for it.
10. The precise temperature-controlled carboxylated nitrile latex polymerization reactor according to claim 9, characterized in that: Two ends of the tension sensor (63) are respectively detachably connected to the U-shaped frame (55) and the rectangular block (65).
Citation Information
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