A continuous acidification device and acidification process for fatty acid production
By designing a continuous acidification equipment and process for fatty acid production, using a dual-axis motor to drive the reciprocating movement of the mixing rod and the cross plate, the quantitative discharge and full mixing of acidifiers and materials is achieved, and the problem of insufficient or excessive acidification of fatty acid reactions in the prior art is solved, and the purity and quality of the product are improved.
Patent Information
- Application Number
- CN202510252809.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2025-03-05
- Publication Date
- 2025-05-02
- Estimated Expiration
- 2045-03-05
AI Technical Summary
In the prior art, by pouring the material, acidifying agent and water into a container to stir, the fatty acid reaction is insufficient or excessive acidification, which affects the purity and quality of the product.
A continuous acidification equipment and acidification process for fatty acid production are designed, including an acidification box, a quantitative component, a hopper and a linkage assembly. The reciprocating movement of the mixing rod and the cross plate is driven by a dual-axis motor to realize the quantitative discharge and full mixing of the acidifier and material.
It improves the purity and quality of fatty acids, avoids the problems of insufficient reaction or excessive acidification, and ensures the stability and efficient production of the product.
Smart Images

Figure CN119733467B_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of fatty acid production, and in particular to continuous acidification equipment and an acidification process for fatty acid production. Background Art
[0002] Fatty acids are organic substances with long aliphatic hydrocarbon chains containing a carboxyl group at one end. They are the simplest type of fat and can be divided into saturated fatty acids and unsaturated fatty acids. They participate in many physiological processes in organisms, such as energy storage and the formation of biological membranes. They can be used in industry to produce many products such as soaps, lubricants, and coatings.
[0003] In a Chinese patent with application number CN201820872281.3, a fatty acid continuous acidification tank is disclosed. This device realizes two process effects of acidification and separation. The reaction chamber and the separation chamber are separated by a partition to ensure the stability of the separation of the fatty acid phase and the water phase; the waste acid guide pipe is arranged in a U shape to ensure that the fatty acid phase and the water phase are separated by gravity under pressureless conditions.
[0004] In the above patent, for the production of fatty acids, the general method is to pour all the materials, acidulants and water into a container for stirring reaction. However, this method will cause the fatty acids to react insufficiently, resulting in incomplete acidification or over-acidification of the fatty acids, which will affect the purity and quality of the product.
[0005] Therefore, we proposed a continuous acidification equipment and acidification process for fatty acid production. Summary of the invention
[0006] The object of the present invention is to provide a continuous acidification device and an acidification process for fatty acid production, which solves the problem in the background technology that the material, acidulant and water are all poured into a container for stirring, which may affect the purity and quality of the product.
[0007] To achieve the above object, the present invention provides the following technical solution: A continuous acidification device and an acidification process for fatty acid production, comprising an acidification box, a quantitative component for quantitative feeding is fixedly installed on the upper surface of the acidification box, a feeding hopper is fixedly installed on the upper surface of the acidification box, the feeding hopper (3) is located on one side of the quantitative component, and the feeding hopper is connected to the acidification box;
[0008] The quantitative component includes an outer box fixedly mounted on the upper surface of the acidification box, a liquid storage box fixedly mounted inside the outer box, the liquid storage box, a lifting assembly arranged inside the acidification box for accelerating the stirring speed, a linkage assembly arranged inside the outer box for driving the liquid storage box and the lifting assembly to operate, a double-shaft motor fixedly mounted on the upper surface of the acidification box, the double-shaft motor is located inside the outer box, a stirring assembly fixedly mounted on one of the output ends of the double-shaft motor for stirring, a pinion is sleeved on the outer surface of the other output end of the double-shaft motor, the linkage assembly meshes with the pinion, a horizontal plate is also arranged inside the outer box, a C-shaped plate is fixedly mounted on one side of the horizontal plate, an inclined groove is opened on the upper surface of the C-shaped plate, an inclined block is slidably arranged inside the inclined groove, a baffle is fixedly mounted on the upper surface of the inclined block, and the baffle is slidably connected to the inside of the feeding hopper;
[0009] The linkage assembly includes a disc arranged inside the outer box, a column and a clamping column fixedly mounted on the upper surface of the disc, the column is located at the center point of the disc, two groups of clamping columns are arranged, and the two groups of clamping columns are symmetrically distributed on both sides of the disc, a large gear is fixedly mounted on the lower surface of the disc, the large gear is meshed with the small gear, one end of the column is movably connected to the top of the outer box, a short column and a T-block are fixedly mounted on the upper surface of the horizontal plate, a bottom groove is opened on the lower surface of the horizontal plate, a connecting column is fixedly mounted on the inner wall of the bottom groove, a side plate is fixedly mounted on one side of the horizontal plate, two groups of side plates are arranged, rollers are arranged between the two groups of side plates, a V-plate is arranged above the horizontal plate, a fixed column is fixedly mounted inside the V-plate, one end of the fixed column is movably connected to the top of the outer box, a vertical groove is opened at one end of the V-plate, the short column is slidably connected to the vertical groove, and the lower surfaces of the V-plate and the T-block are both in contact with the upper surface of the disc.
[0010] Furthermore, a plate groove and a fine groove are provided on one side of the outer box, the plate groove is matched with the baffle plate, and the fine groove is matched with the C-shaped plate.
[0011] Furthermore, the stirring assembly includes a drive shaft fixedly mounted on one of the output ends of the dual-shaft motor, the drive shaft passes through the top of the acidification box, a connecting plate is arranged at one end of the drive shaft, the connecting plate is located inside the acidification box, a stirring rod is fixedly mounted on the lower surface of the connecting plate, and the stirring rod is located at the center of the lifting assembly.
[0012] Furthermore, the lifting assembly includes a circular frame arranged inside the acidizing box, a circular hole opened on the upper surface of the circular frame, a limit rod movably arranged inside the circular hole, one end of the limit rod is fixedly connected to the top of the acidizing box, and a T-shaped arc groove is opened on one side of the inner wall of the circular frame.
[0013] Furthermore, a lever is movably sleeved on the outer surface of the connecting column, a center column is arranged inside the lever, a T-plate is fixedly installed on one end of the lever, the T-plate is slidably connected to the T-shaped arc groove, a flip hole is opened on the upper surface of the acidizing box, the lever is movably connected to the inner wall of the flip hole through the center column, one end of the lever is located inside the outer box, and the other end of the lever is located inside the acidizing box.
[0014] Furthermore, a pipeline and a spring rod are fixedly installed on a side of the liquid storage tank close to the linkage assembly, a liquid outlet pipe is fixedly installed on the lower surface of the liquid storage tank and is connected with the interior of the liquid storage tank, a pressure valve is fixedly installed inside the liquid outlet pipe, two groups of spring rods are provided, one end of the two groups of spring rods are fixedly installed with inclined plates, a pressure plate is fixedly installed between the inclined plates, a groove is provided on one side of the pressure plate, the groove and the pipeline are on the same horizontal line and correspond to each other, a fixing rod is fixedly installed on the inner wall of the groove, one end of the fixing rod is located inside the liquid storage tank, a push plate is fixedly installed on one end of the fixing rod, the push plate is located inside the liquid storage tank, the push plate is slidably connected to the inside of the liquid storage tank, a liquid inlet pipe is fixedly installed on the side of the liquid storage tank away from the linkage assembly, one end of the liquid inlet pipe is externally connected to a water pump, a one-way valve is fixedly installed inside the liquid inlet pipe, and one side of the pressure plate and the inclined plate are both in contact with the roller.
[0015] Furthermore, a heating chamber is provided inside the acidification box, and a plurality of heating plates are fixedly installed on the inner wall of the heating chamber. The heating chamber is at the same height as the stirring rod. A sewage outlet is provided on the side of the acidification box away from the liquid storage tank. A conical opening is provided at the bottom of the acidification box, and the conical opening is located below the filter assembly. A liquid discharge pipe is fixedly installed at the bottom of the conical opening. A feed discharge port is provided on the upper surface of the acidification box, and the feed discharge port is adapted to the feeding hopper. A water inlet is provided on the inner wall of the acidification box, and a temporary storage box is fixedly installed on the inner wall of the acidification box, and the temporary storage box is located below the stirring rod. A filter assembly for filtering liquid is fixedly installed inside the acidification box, and the filter assembly is located below the temporary storage box.
[0016] Furthermore, a leakage groove is provided on the upper surface of the temporary storage box, a storage groove is provided on the inner wall of the leakage groove, an electric retractable plate is arranged inside the storage groove, a liquid storage cavity is provided inside the temporary storage box, the liquid storage cavity is connected with the leakage groove, a V-groove is provided at the bottom of the liquid storage cavity, a drainage port is provided at the bottom of the V-groove, a drainage pipe is provided on the lower surface of the temporary storage box, the drainage pipe is connected with the drainage port, the upper surface of the temporary storage box is inclined, and a quantitative valve is arranged inside the drainage pipe.
[0017] Further, the filtering assembly includes a fixed frame fixedly mounted on the inner wall of the acidification box, a side box fixedly mounted on one side of the acidification box, an electric telescopic rod fixedly mounted on the inner wall of the side box, a scraper fixedly mounted on one end of the electric telescopic rod, the fixed frame is located below the temporary storage box, a filter membrane fixedly mounted on the inner wall of the fixed frame, the upper surfaces of the fixed frame and the filter membrane are both in contact with the lower surface of the scraper, a magnet A embedded in one side of the fixed frame, and a flip plate arranged inside the sewage outlet, and the magnet A is opposite to the flip plate;
[0018] A magnet B is fixedly installed on one side of the flip plate close to the magnet A, and the magnet B is magnetically attracted to the magnet A. A tension spring is fixedly installed on the other side of the flip plate, and one end of the tension spring is fixedly connected to the top of the sewage outlet. A long rod is provided at one end of the flip plate, and both ends of the long rod are fixedly connected to the inner wall of the sewage outlet.
[0019] Another technical solution proposed by the present invention is an acidification process for continuous acidification for fatty acid production, comprising the following steps:
[0020] S1: After the required water source is added into the acidification tank through the water inlet, the water source will be located on the upper surface of the temporary storage tank because the electric telescopic plate blocks the drain groove. Then, the materials for making fatty acids are added into the hopper, and the acidulant needs to be added into the liquid storage tank. Then, the dual-axis motor can be started to start stirring the stirring rod;
[0021] S2: As the dual-axis motor starts, one set of small gears will drive the large gear to rotate, and the rotating large gear will drive the disc and the clamping column to rotate together. One set of rotating clamping columns will drive the T block to move, and the T block will drive the cross plate to move to one end until the clamping column and the T block are separated. At this time, the other set of clamping columns will contact one end of the V plate, causing the V plate to rotate counterclockwise, thereby driving the cross plate to move to the other end, allowing the cross plate to move back and forth;
[0022] S3: As the horizontal plate reciprocates, the roller will reciprocate to squeeze the inclined plate and the pressure plate, and the moving inclined plate and the pressure plate will also move together with the fixed rod and the push plate, so that the push plate squeezes the acidifier inside the liquid storage tank into the liquid outlet pipe, and finally flows into the water source that has been added in advance through the liquid outlet pipe. Since the C-shaped plate is fixedly connected to the horizontal plate and the C-shaped plate moves inside the fine groove, the reciprocating C-shaped plate allows the inclined block to reciprocate along the inclined groove, so that the material inside the hopper is discharged together with the acidifier. At this time, the acidifier and the material will be added to the water source for mixing and stirring. When the horizontal plate reciprocates, the lever will swing back and forth with the central column as the center, thereby driving the circular frame to rise and fall back and forth, further increasing the speed of stirring and mixing;
[0023] S4: When the liquid mixing is completed, the dual-axis motor is stopped, and the electric telescopic plate is turned on to allow the liquid to enter the liquid storage chamber, and then discharged to the surface of the filter membrane through the quantitative valve. At this time, the speed of the liquid descent will decrease, and the total amount of liquid will also decrease, which can prevent the impact caused by the liquid discharge from causing the filter membrane to rupture. When all the liquid enters the liquid storage chamber, the next round of mixing can be carried out, and the liquid that falls on the surface of the filter membrane will be filtered, and the activated carbon, sodium fatty acid, sodium sulfate crystals and other substances in the liquid will be filtered, so that only fatty acids fall to the cone mouth, and the scraper will slide out the impurities on the surface of the filter membrane, and finally discharge from the sewage outlet.
[0024] Compared with the prior art, the present invention has the following beneficial effects:
[0025] The present invention provides a continuous acidification device and an acidification process for fatty acid production. When fatty acids need to be produced, materials are added into a hopper. At this time, a baffle blocks the materials in the hopper. Then, water is added into an acidification tank through a water inlet. A double-shaft motor is started to rotate a disc with a pinion. The rotating disc allows a transverse plate to reciprocate through a clamping column on the surface. The reciprocating transverse plate reciprocates to squeeze a pressing plate, allowing the pressing plate to discharge the liquid in a liquid storage tank with a fixed rod and a push plate. The baffle also reciprocates due to an inclined groove and an inclined block, allowing the materials in the hopper to be discharged. At this time, the double-shaft motor stirs the liquid. While the transverse plate reciprocates, a lever also reciprocates to swing, causing a circular frame to reciprocate. The reciprocating movement of the transverse plate drives the quantitative discharge of materials and an acidulant. The reciprocating reciprocating circular frame is used to improve the purity and quality of the fatty acids. BRIEF DESCRIPTION OF THE DRAWINGS
[0026] Figure 1 This is a schematic diagram of the overall structure of the continuous acidification equipment for fatty acid production of the present invention;
[0027] Figure 2 This is a schematic cross-sectional view of the overall structure of the continuous acidification equipment for fatty acid production of the present invention;
[0028] Figure 3 This is a schematic diagram of the overall structure of the continuous acidification equipment for fatty acid production of the present invention;
[0029] Figure 4 It is a schematic exploded cross-sectional view of the linkage assembly structure of the continuous acidification equipment for fatty acid production of the present invention;
[0030] Figure 5 This is a schematic cross-sectional view of the lifting assembly structure of the continuous acidification equipment for fatty acid production of the present invention;
[0031] Figure 6 It is a partial cross-sectional schematic diagram of the liquid storage tank structure of the continuous acidification equipment for fatty acid production of the present invention;
[0032] Figure 7 This is a schematic diagram of the structure of the stirring assembly of the continuous acidification equipment for fatty acid production of the present invention;
[0033] Figure 8 The present invention is a schematic cross-sectional view of the filtering assembly and temporary storage box structure of the continuous acidification equipment for fatty acid production.
[0034] In the figure: 1, acidification box; 11, heating chamber; 111, heating plate; 12, sewage outlet; 13, cone mouth; 14, liquid discharge pipe; 15, flip hole; 16, feed port; 17, water inlet; 2, quantitative component; 21, outer box; 211, plate groove; 212, fine groove; 22, liquid storage box; 221, pipeline; 222, spring rod; 223, liquid outlet pipe; 224, inclined plate; 225, pressure plate; 226, concave slot; 227, fixed rod; 228, push plate; 229, liquid inlet pipe; 23, lifting assembly; 231, circular frame; 232, round hole; 233, limit rod; 234, T-shaped arc slot; 24, linkage assembly; 241, disc; 2411, column; 2412, clamping column; 2413, large gear; 242, C-shaped plate; 2421, inclined slot; 2422, baffle; 243, horizontal plate; 2431, short column; 2432, T block; 2433, bottom groove; 2434, side plate; 2435, roller; 2436, V plate; 2437, fixed column; 2438, vertical groove; 244, connecting column; 2441, center column; 2442, lever; 2443, T plate; 25, stirring assembly; 251, driving shaft; 252, connecting plate; 253, stirring rod; 26, dual-axis motor; 261, small gear; 3. Feeding hopper; 4. Filter assembly; 41. Side box; 42. Electric telescopic rod; 43. Scraper; 44. Fixed frame; 45. Magnet A; 46. Flip plate; 461. Magnet B; 462. Tension spring; 463. Long rod; 47. Filter membrane; 5. Temporary storage box; 51. Leakage trough; 52. Storage trough; 53. Electric telescopic plate; 54. Liquid storage chamber; 55. V-groove; 56. Drain port; 57. Drain pipe. DETAILED DESCRIPTION
[0035] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0036] In order to solve the technical problems of how to improve the purity and quality of fatty acids, such as Figure 1-Figure 8 As shown, the following preferred technical solutions are provided:
[0037] A continuous acidification device and an acidification process for fatty acid production, comprising an acidification box 1, a quantitative component 2 for quantitative feeding is fixedly installed on the upper surface of the acidification box 1, a feeding hopper 3 is fixedly installed on the upper surface of the acidification box 1, the feeding hopper 3 is located on one side of the quantitative component 2, and the feeding hopper 3 is connected to the acidification box 1;
[0038] The quantitative component 2 includes an outer box 21 fixedly mounted on the upper surface of the acidification box 1, a liquid storage box 22 fixedly mounted inside the outer box 21, a lifting assembly 23 arranged inside the acidification box 1 for accelerating the stirring speed, a linkage assembly 24 arranged inside the outer box 21 for driving the liquid storage box 22 and the lifting assembly 23 to operate, a double-axis motor 26 fixedly mounted on the upper surface of the acidification box 1, the double-axis motor 26 is located inside the outer box 21, and one of the output shafts of the double-axis motor 26 is fixedly mounted on the output shaft 26. The stirring assembly 25 at the output end is used for stirring, and the outer surface of the other output end of the dual-axis motor 26 is sleeved with a small gear 261, and the linkage assembly 24 is meshed with the small gear 261. A horizontal plate 243 is also arranged inside the outer box 21, and a C-shaped plate 242 is fixedly installed on one side of the horizontal plate 243. An inclined groove 2421 is opened on the upper surface of the C-shaped plate 242, and an inclined block is slidably arranged inside the inclined groove 2421. A baffle 2422 is fixedly installed on the upper surface of the inclined block, and the baffle 2422 is slidably connected to the inside of the feeding hopper 3;
[0039] The linkage assembly 24 includes a disc 241 arranged inside the outer box 21, a column 2411 and a clamping column 2412 fixedly installed on the upper surface of the disc 241, the column 2411 is located at the center point of the disc 241, two groups of clamping columns 2412 are provided, and the two groups of clamping columns 2412 are symmetrically distributed on both sides of the disc 241, a large gear 2413 is fixedly installed on the lower surface of the disc 241, the large gear 2413 is meshed with the small gear 261, one end of the column 2411 is movably connected to the top of the outer box 21, a short column 2431 and a T block 2432 are fixedly installed on the upper surface of the cross plate 243, a bottom groove 2433 is opened on the lower surface of the cross plate 243, and a connecting column is fixedly installed on the inner wall of the bottom groove 2433 244, a side plate 2434 is fixedly installed on one side of the horizontal plate 243, and the side plate 2434 is provided with two groups, and a roller 2435 is provided between the two groups of side plates 2434, and a V-plate 2436 is provided above the horizontal plate 243, and a fixed column 2437 is fixedly installed inside the V-plate 2436, and one end of the fixed column 2437 is movably connected to the top of the outer box 21, and a vertical groove 2438 is opened at one end of the V-plate 2436, and the short column 2431 is slidably connected to the vertical groove 2438, and the lower surfaces of the V-plate 2436 and the T block 2432 are both in contact with the upper surface of the disc 241, and through the rotation of the disc 241, one group of the clamping columns 2412 is allowed to move with the T block 2432, and the T block 2432 will move with When the clamping column 2412 is separated from the T block 2432, the other set of clamping columns 2412 will contact one end of the V plate 2436, causing the V plate 2436 to rotate counterclockwise. The counterclockwise rotating V plate 2436 will move with the short column 2431 inside the other end. Since the short column 2431 and the cross plate 243 are fixedly connected, the V plate 2436 will move with the cross plate 243 in the opposite direction. When the other set of clamping columns 2412 is separated from the V plate 2436, it will contact the T block 2432 and move with the T block 2432. At this point, the cross plate 243 will reciprocate. When the cross plate 243 moves back and forth, the roller 2435 will continuously squeeze the liquid storage. Box 22, so that the acidulant inside the storage box 22 can be discharged. Since the baffle 2422 on the surface of the C-shaped plate 242 moves along the inclined groove 2421 through the inclined block, and the C-shaped plate 242 follows the horizontal plate 243 in the outer box 21, when the horizontal plate 243 moves to the inner wall on one side of the outer box 21, the baffle 2422 will move along the inclined groove 2421, thereby opening the discharge port of the hopper 3, so that the material inside the hopper 3 can move to the acidulant box 1. On the contrary, when the horizontal plate 243 moves to the inner wall on the other side of the outer box, the baffle 243 will block the discharge port of the hopper 3, so that the material inside the hopper 3 stops adding, and the material inside the hopper 3 and the acidulant will be discharged together.
[0040] A plate groove 211 and a fine groove 212 are provided on one side of the outer box 21. The plate groove 211 is matched with the baffle 2422, and the fine groove 212 is matched with the C-shaped plate 242. The baffle 2422 can be completely accommodated through the plate groove 211, and the C-shaped plate 242 can have space to move through the fine groove 212.
[0041] The stirring assembly 25 includes a driving shaft 251 fixedly mounted on one of the output ends of the dual-axis motor 26. The driving shaft 251 passes through the top of the acidification tank 1. A connecting plate 252 is arranged at one end of the driving shaft 251. The connecting plate 252 is located inside the acidification tank 1. A stirring rod 253 is fixedly mounted on the lower surface of the connecting plate 252. The stirring rod 253 is located at the center of the lifting assembly 23. The driving shaft 251 with a small gear 261 drives the rotation of the disc 241 through the drive of the dual-axis motor 26. Since the large gear 2413 is larger than the small gear 261, the rotation speed of the disc 241 is slower than that of the driving shaft 251.
[0042] The lifting assembly 23 includes a circular frame 231 arranged inside the acidification box 1, a circular hole 232 opened on the upper surface of the circular frame 231, a limiting rod 233 movably arranged inside the circular hole 232, one end of the limiting rod 233 is fixedly connected to the top of the acidification box 1, and a T-shaped arc groove 234 is opened on one side of the inner wall of the circular frame 231. The circular frame 231 can further improve the stirring effect and speed when the stirring assembly 25 stirs, and the limiting rod 233 can improve the stability of the circular frame 231.
[0043] A lever 2442 is movably sleeved on the outer surface of the connecting column 244, a center column 2441 is arranged inside the lever 2442, a T-disc 2443 is fixedly mounted on one end of the lever 2442, the T-disc 2443 is slidably connected to the T-shaped arc groove 234, a flip hole 15 is opened on the upper surface of the acidification box 1, the lever 2442 is movably connected to the inner wall of the flip hole 15 through the center column 2441, one end of the lever 2442 is located inside the outer box 21, and the other end of the lever 2442 is located inside the acidification box 1, and the swinging lever 2442 can drive the circular frame 231 to rise and fall, thereby increasing the speed of stirring and mixing the fatty acids.
[0044] A pipe 221 and a spring rod 222 are fixedly installed on one side of the liquid storage tank 22 close to the linkage assembly 24, a liquid outlet pipe 223 is fixedly installed on the lower surface of the liquid storage tank 22, and is connected to the interior of the liquid storage tank 22, a pressure valve is fixedly installed inside the liquid outlet pipe 223, two groups of spring rods 222 are provided, one end of the two groups of spring rods 222 are fixedly installed with an inclined plate 224, a pressing plate 225 is fixedly installed between the inclined plates 224, a groove 226 is opened on one side of the pressing plate 225, the groove 226 and the pipe 221 are on the same horizontal line and correspond to each other, a fixing rod 227 is fixedly installed on the inner wall of the groove 226, one end of the fixing rod 227 is located inside the liquid storage tank 22, and a push plate 228 is fixedly installed on one end of the fixing rod 227, the push plate 228 is located inside the liquid storage tank 22, the push plate 228 is slidably connected to the inside of the liquid storage tank 22, and the liquid storage tank 22 is away from the linkage assembly 24. A liquid inlet pipe 229 is fixedly installed on one side of the moving component 24. One end of the liquid inlet pipe 229 is externally connected to a water pump. A one-way valve is fixedly installed inside the liquid inlet pipe 229. One side of the pressing plate 225 and the inclined plate 224 are both in contact with the roller 2435. When the roller 2435 moves back and forth, the pressing plate 225 pushes the pushing plate 228 through the fixed rod 227 to squeeze the acidifier in the liquid storage tank 22 to the liquid outlet pipe 223. At the same time, the liquid inlet pipe 229 continuously replenishes the acidifier to ensure the continuity of liquid discharge. When the roller 2435 moves to the inclined plate 224, since the inclined plate 224 is in an inclined state, the pressure on the pressing plate 225 will be reduced at this time, and the spring rod 222 will bring the inclined plate 224 and the pressing plate 225 to reset, so that when the roller 2435 squeezes the pressing plate 225 again, the acidifier in the liquid storage tank 22 can be squeezed into the acidification tank 1 again.
[0045] A heating chamber 11 is provided inside the acidification tank 1, and a plurality of heating plates 111 are fixedly installed on the inner wall of the heating chamber 11. The heating chamber 11 is at the same height as the stirring rod 253. A sewage outlet 12 is provided on the side of the acidification tank 1 away from the liquid storage tank 22. A conical opening 13 is provided at the bottom of the acidification tank 1. The conical opening 13 is located below the filter assembly 4. A liquid discharge pipe 14 is fixedly installed at the bottom of the conical opening 13. A feed opening 16 is provided on the upper surface of the acidification tank 1. The feed opening 16 is adapted to the feeding hopper 3. A water inlet 17 is provided on the wall, a temporary storage box 5 is fixedly installed on the inner wall of the acidification box 1, and the temporary storage box 5 is located below the stirring rod 253. A filter component 4 for filtering liquid is fixedly installed inside the acidification box 1, and the filter component 4 is located below the temporary storage box 5. The raw material is added into the acidification box 1 through the feed port 16, and then the water source is added into the acidification box 1 through the water inlet 17, the fatty acid is discharged through the liquid discharge pipe 14, and finally the impurities on the surface of the filter component 4 are discharged through the sewage outlet 12.
[0046] A leakage groove 51 is provided on the upper surface of the temporary storage box 5, and a storage groove 52 is provided on the inner wall of the leakage groove 51. An electric telescopic plate 53 is arranged inside the storage groove 52. A liquid storage chamber 54 is provided inside the temporary storage box 5, and the liquid storage chamber 54 is connected with the leakage groove 51. A V-groove 55 is provided at the bottom of the liquid storage chamber 54, and a drainage port 56 is provided at the bottom of the V-groove 55. A drainage pipe 57 is provided on the lower surface of the temporary storage box 5, and the drainage pipe 57 is connected with the drainage port 56. The upper surface of the temporary storage box 5 is inclined, and a quantitative valve is arranged inside the drainage pipe 57. Through the inclined state of the upper surface of the temporary storage box 5, the liquid can be guided to the leakage groove 51. At this time, the electric telescopic plate 53 is started to move the electric telescopic plate 53 to the inside of the storage groove 52, so that the liquid enters the liquid storage chamber 54. Finally, the liquid in the liquid storage chamber 54 can be quantitatively dropped onto the surface of the filter component 4 through the quantitative valve.
[0047] The filter assembly 4 includes a fixed frame 44 fixedly mounted on the inner wall of the acidification box 1, a side box 41 fixedly mounted on one side of the acidification box 1, an electric telescopic rod 42 fixedly mounted on the inner wall of the side box 41, a scraper 43 fixedly mounted on one end of the electric telescopic rod 42, the fixed frame 44 is located below the temporary storage box 5, a filter membrane 47 fixedly mounted on the inner wall of the fixed frame 44, the upper surfaces of the fixed frame 44 and the filter membrane 47 are both in contact with the lower surface of the scraper 43, a magnet A45 embedded on one side of the fixed frame 44, and a flip plate 46 arranged inside the sewage outlet 12, and the magnet A45 is opposite to the flip plate 46;
[0048] A magnet B461 is fixedly installed on one side of the flip plate 46 close to the magnet A45, and the magnet B461 is magnetically attracted to the magnet A45. A tension spring 462 is fixedly installed on the other side of the flip plate 46, and one end of the tension spring 462 is fixedly connected to the top of the sewage outlet 12. A long rod 463 is provided at one end of the flip plate 46, and both ends of the long rod 463 are fixedly connected to the inner wall of the sewage outlet 12. The magnets A45 and the magnet B461 can ensure that the water falling on the surface of the filter membrane 47 will not flow out, and then the activated carbon, sodium fatty acid, sodium sulfate crystals and other substances in the liquid are isolated by the filter membrane 47, and the fatty acids are allowed to fall into the inside of the cone mouth 13 and then discharged from the liquid discharge pipe 14. Finally, the substances on the surface of the filter membrane 47 are scraped off by the scraper 43, and finally the flip plate 46 is pushed open to discharge the substances.
[0049] Another technical solution proposed by the present invention is an acidification process for continuous acidification for fatty acid production, comprising the following steps:
[0050] S1: After the required water source is added into the acidification tank 1 through the water inlet 17, the water source will be located on the upper surface of the temporary storage tank 5 because the electric telescopic plate 53 blocks the drain groove 51. Then, the material for making fatty acids is added into the hopper 3, and the acidulant needs to be added into the liquid storage tank 22. Then, the dual-axis motor 26 can be started to allow the stirring rod 253 to start stirring;
[0051] S2: With the start of the dual-axis motor 26, one group of small gears 261 will drive the large gear 2413 to rotate, and the rotating large gear 2413 will drive the disc 241 and the clamping column 2412 to rotate together, and one group of rotating clamping columns 2412 will drive the T block 2432 to rotate, and the T block 2432 will drive the horizontal plate 243 to move to one end until the clamping column 2412 and the T block 2432 are separated, at which time the other group of clamping columns 2412 will contact the V plate 2436, causing the V plate 2436 to rotate counterclockwise, thereby driving the horizontal plate 243 to move to the other end, and causing the horizontal plate 243 to move back and forth;
[0052] S3: With the reciprocating movement of the horizontal plate 243, the roller 2435 will reciprocate and squeeze the inclined plate 224 and the pressure plate 225. The moving inclined plate 224 and the pressure plate 225 will also move together with the fixed rod 227 and the push plate 228, so that the push plate 228 squeezes the acidifier inside the liquid storage tank 22 into the inside of the liquid outlet pipe 223, and finally flows into the water source added in advance through the liquid outlet pipe 223. Since the C-shaped plate 242 is fixedly connected to the horizontal plate 243, and the C-shaped plate 242 is located inside the fine groove 212 and moves, the reciprocating C-shaped plate 242 allows the inclined block to reciprocate along the inclined groove 2421, so that the material inside the hopper 3 is discharged together with the acidifier. At this time, the acidifier and the material will be added to the water source for mixing and stirring. When the horizontal plate 243 reciprocates, the lever 2442 will swing back and forth with the central column 2441 as the center, thereby driving the circular frame 231 to rise and fall back and forth, further improving the stirring and mixing speed;
[0053] S4: When the liquid mixing is completed, the dual-axis motor 26 is stopped, and the electric telescopic plate 53 is turned on to allow the liquid to enter the liquid storage chamber 54, and then discharged to the surface of the filter membrane 47 through the quantitative valve. At this time, the speed at which the liquid descends will decrease, and the total amount of the liquid will also decrease, which can prevent the filter membrane 47 from rupturing. After all the liquid enters the liquid storage chamber 54, the next round of mixing can be carried out, and the liquid that falls on the surface of the filter membrane 47 will be filtered, and the activated carbon, sodium fatty acid, sodium sulfate crystals and other substances in the liquid will be filtered, so that only the fatty acid falls to the cone mouth 13, and the scraper 43 will slide out the impurities on the surface of the filter membrane 47, and finally discharged from the sewage outlet 12.
[0054] Specifically, when fatty acids need to be produced, materials are added into the hopper 3, acidulant is added into the liquid storage tank 22, and then water is added into the acidification tank 1. At this time, the materials in the hopper 3 will be blocked by the baffle 2422. At this time, the dual-axis motor 26 is started to rotate the drive shaft 251, and the drive shaft 251 with the small gear 261 will drive the large gear 2413 to rotate together. The rotating large gear 2413 will drive the disc 241 and the clamping column 2412 to rotate together. At this time, one group of clamping columns 2412 will contact one side of the T block 2432, so that the T block 2432 moves to one end with the cross plate 243. When the clamping column 2412 is separated from the T block 2432, the other group of clamping columns 2412 will contact the V plate 2 436, thereby rotating the V-plate 2436 counterclockwise. Since a short column 2431 is provided inside the vertical slot 2438 at the other end of the V-plate 2436, and the short column 2431 is fixedly connected to the cross plate 243, the counterclockwise rotating V-plate 2436 will move the cross plate 243 to the other end. When the other set of clamping columns 2412 are separated from one end of the V-plate 2436, they will contact the T block 2432, allowing the T block 2432 to continue to move the cross plate 243. At this time, the rotation of the disc 241 drives the reciprocating movement of the cross plate 243. Due to the reciprocating movement of the cross plate 243, the roller 2435 located on one side of the cross plate 243 will reciprocately squeeze the pressure plate 225 and the inclined plate 224. Since a spring rod 222 is fixedly installed on one side of the inclined plate 224, the squeezed The pressing plate 225 will move with the fixed rod 227, so that the fixed rod 227 and the push plate 228 squeeze the acidifier in the liquid storage tank 22 into the liquid outlet pipe 223, so that the acidifier in the liquid outlet pipe 223 flows into the acidification tank 1. When the roller 2435 moves to the inclined plate 224, the spring rod 222 will reset the inclined plate 224 and the pressing plate 225 to prepare for the next squeezing. At the same time as the liquid storage tank 22 is squeezed, the baffle 2422 will also reciprocate due to the inclined block and the inclined groove 2421, so that the material in the hopper 3 is also indirectly discharged into the acidification tank 1. At this time, the material and the acidifier will be indirectly discharged to ensure that the material and the acidifier are fully and evenly mixed and reacted. When the liquid is stirred, the lever 2442 located in the bottom groove 2433 will swing back and forth with the central column 2441 as the center. Since the T-disc 2443 at one end of the lever 2442 is located in the T-shaped arc groove 234 and the circular frame 231 can only move vertically, the reciprocating horizontal plate 243 will also drive the circular frame 231 to rise and fall back and forth, further improving the stirring efficiency. When the liquid is stirred, the electric telescopic plate 53 is opened to allow the liquid to enter the liquid storage chamber 54, and then the quantitative valve inside the discharge pipe 57 is used to indirectly allow the liquid to fall onto the surface of the filter membrane 47 for filtration. The indirect discharge of the liquid can prevent the impact force of the liquid from tearing the filter membrane 47. After all the liquid enters the liquid storage chamber 54, the liquid can be stirred again.When the liquid production is completed, the electric telescopic rod 42 is started, and the electric telescopic rod 42 and the scraper 43 are used to scrape the impurities isolated from the surface of the filter membrane 47. Finally, the scraper 43 pushes the flip plate 46 open, and the impurities are discharged through the sewage outlet 12. The reciprocating movement of the horizontal plate 243 drives the quantitative discharge of the material and the acidifier, and the reciprocating lifting and lowering circular frame 231 is equipped, thereby improving the purity and quality of the fatty acid.
[0055] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.
Claims
1. A continuous acidification device for fatty acid production, comprising an acidification tank (1), characterized in that: A quantitative component (2) for quantitative feeding is fixedly mounted on the upper surface of the acidification box (1), and a feeding hopper (3) is fixedly mounted on the upper surface of the acidification box (1). The feeding hopper (3) is located on one side of the quantitative component (2), and the feeding hopper (3) is connected to the acidification box (1); The quantitative component (2) comprises an outer box (21) fixedly mounted on the upper surface of the acidification box (1), a liquid storage box (22) fixedly mounted inside the outer box (21), a lifting assembly (23) disposed inside the acidification box (1) for accelerating the stirring speed, a linkage assembly (24) disposed inside the outer box (21) for driving the liquid storage box (22) and the lifting assembly (23) to operate, and a double-axis motor (26) fixedly mounted on the upper surface of the acidification box (1). The double-axis motor (26) is located inside the outer box (21), and one of the output ends of the double-axis motor (26) is fixedly mounted for A stirring assembly (25) for stirring the raw materials; a pinion (261) is sleeved on the outer surface of the other output end of the dual-axis motor (26); the linkage assembly (24) meshes with the pinion (261); a transverse plate (243) is further arranged inside the outer box (21); a C-shaped plate (242) is fixedly mounted on one side of the transverse plate (243); an inclined groove (2421) is provided on the upper surface of the C-shaped plate (242); an inclined block is slidably arranged inside the inclined groove (2421); a baffle (2422) is fixedly mounted on the upper surface of the inclined block; and one side of the baffle (2422) is movably arranged inside the feeding hopper (3); The linkage assembly (24) comprises a disk (241) arranged inside the outer box (21), a column (2411) and a clamping column (2412) fixedly mounted on the upper surface of the disk (241), the column (2411) being located at the center point of the disk (241), two groups of clamping columns (2412) being arranged, and the two groups of clamping columns (2412) being symmetrically distributed on both sides of the disk (241), a large gear (2413) being fixedly mounted on the lower surface of the disk (241), the large gear (2413) being meshed with a small gear (261), one end of the column (2411) being movably connected to the top of the outer box (21), a short column (2431) and a T block (2432) being fixedly mounted on the upper surface of the horizontal plate (243), and a bottom groove being provided on the lower surface of the horizontal plate (243) (2433), a connecting column (244) is fixedly installed on the inner wall of the bottom groove (2433), a side plate (2434) is fixedly installed on one side of the horizontal plate (243), two groups of side plates (2434) are provided, and a roller (2435) is provided between the two groups of side plates (2434), a V-plate (2436) is provided above the horizontal plate (243), a fixing column (2437) is fixedly installed inside the V-plate (2436), one end of the fixing column (2437) is movably connected to the top of the outer box (21), one end of the V-plate (2436) is provided with a vertical groove (2438), the short column (2431) is slidably connected to the vertical groove (2438), and the lower surfaces of the V-plate (2436) and the T-block (2432) are both in contact with the upper surface of the disc (241).
2. A continuous acidification device for fatty acid production as claimed in claim 1, characterized in that: A plate groove (211) and a thin groove (212) are provided on one side of the outer box (21); the plate groove (211) is matched with the baffle plate (2422), and the thin groove (212) is matched with the C-shaped plate (242).
3. A continuous acidification device for fatty acid production as claimed in claim 2, characterized in that: The stirring assembly (25) comprises a driving shaft (251) fixedly mounted on one of the output ends of the dual-shaft motor (26), the driving shaft (251) passing through the top of the acidification box (1), a connecting plate (252) arranged at one end of the driving shaft (251), the connecting plate (252) being located inside the acidification box (1), a stirring rod (253) being fixedly mounted on the lower surface of the connecting plate (252), and the stirring rod (253) being located at the center of the lifting assembly (23).
4. A continuous acidification device for fatty acid production as claimed in claim 1, characterized in that: The lifting assembly (23) comprises a circular frame (231) arranged inside the acidification box (1), a circular hole (232) provided on the upper surface of the circular frame (231), a limiting rod (233) movably arranged inside the circular hole (232), one end of the limiting rod (233) being fixedly connected to the top of the acidification box (1), and a T-shaped arc groove (234) provided on one side of the inner wall of the circular frame (231).
5. A continuous acidification device for fatty acid production as claimed in claim 4, characterized in that: The outer surface of the connecting column (244) is movably sleeved with a lever (2442), a central column (2441) is arranged inside the lever (2442), a T-disc (2443) is fixedly mounted on one end of the lever (2442), the T-disc (2443) is slidably connected to the T-shaped arc groove (234), a flip hole (15) is provided on the upper surface of the acidification box (1), the lever (2442) is movably connected to the inner wall of the flip hole (15) through the central column (2441), one end of the lever (2442) is located inside the outer box (21), and the other end of the lever (2442) is located inside the acidification box (1).
6. A continuous acidification device for fatty acid production as claimed in claim 1, characterized in that: A pipe (221) and a spring rod (222) are fixedly mounted on one side of the liquid storage tank (22) close to the linkage assembly (24); a liquid outlet pipe (223) is fixedly mounted on the lower surface of the liquid storage tank (22) and is in communication with the interior of the liquid storage tank (22); a pressure valve is fixedly mounted inside the liquid outlet pipe (223); two groups of spring rods (222) are provided; inclined plates (224) are fixedly mounted on one end of the two groups of spring rods (222); a pressure plate (225) is fixedly mounted between the inclined plates (224); a groove (226) is provided on one side of the pressure plate (225); the groove (226) and the pipe (221) are on the same horizontal line and are mutually opposite. Correspondingly, a fixing rod (227) is fixedly installed on the inner wall of the groove (226), one end of the fixing rod (227) is located inside the liquid storage box (22), one end of the fixing rod (227) is fixedly installed with a push plate (228), the push plate (228) is located inside the liquid storage box (22), the push plate (228) is slidably connected to the inside of the liquid storage box (22), a liquid inlet pipe (229) is fixedly installed on the side of the liquid storage box (22) away from the linkage assembly (24), one end of the liquid inlet pipe (229) is externally connected to a water pump, a one-way valve is fixedly installed inside the liquid inlet pipe (229), and one side of the pressure plate (225) and the inclined plate (224) are both in contact with the roller (2435).
7. A continuous acidification device for fatty acid production as claimed in claim 5, characterized in that: The acidification box (1) has a heating chamber (11) formed inside, and a plurality of heating plates (111) are fixedly mounted on the inner wall of the heating chamber (11). The heating chamber (11) is at the same height as the stirring rod (253). A sewage outlet (12) is formed on the side of the acidification box (1) away from the liquid storage tank (22). A conical opening (13) is formed at the bottom of the acidification box (1), and the conical opening (13) is located below the filter assembly (4). A liquid discharge pipe (14) is fixedly mounted at the bottom of the conical opening (13). A material discharge port (16) is formed on the upper surface of the acidification box (1), and the material discharge port (16) is adapted to the feeding hopper (3). A water inlet (17) is formed on the inner wall of the acidification box (1). A temporary storage box (5) is fixedly mounted on the inner wall of the acidification box (1), and the temporary storage box (5) is located below the stirring rod (253). A filter assembly (4) for filtering liquid is fixedly mounted inside the acidification box (1), and the filter assembly (4) is located below the temporary storage box (5).
8. A continuous acidification device for fatty acid production as claimed in claim 7, characterized in that: The temporary storage box (5) has a drain groove (51) on its upper surface, a storage groove (52) on its inner wall, an electric telescopic plate (53) arranged inside the storage groove (52), a liquid storage chamber (54) arranged inside the temporary storage box (5), the liquid storage chamber (54) being connected to the drain groove (51), a V-groove (55) arranged at the bottom of the liquid storage chamber (54), a liquid discharge port (56) arranged at the bottom of the V-groove (55), a liquid discharge pipe (57) arranged at the lower surface of the temporary storage box (5), the liquid discharge pipe (57) being connected to the liquid discharge port (56), the upper surface of the temporary storage box (5) being inclined, and a quantitative valve arranged inside the liquid discharge pipe (57).
9. A continuous acidification device for fatty acid production as claimed in claim 8, characterized in that: The filtering assembly (4) comprises a fixing frame (44) fixedly mounted on the inner wall of the acidification box (1), a side box (41) fixedly mounted on one side of the acidification box (1), an electric telescopic rod (42) fixedly mounted on the inner wall of the side box (41), and a scraper (43) fixedly mounted on one end of the electric telescopic rod (42); the fixing frame (44) is located below the temporary storage box (5); a filtering membrane (47) fixedly mounted on the inner wall of the fixing frame (44); the upper surfaces of the fixing frame (44) and the filtering membrane (47) are both in contact with the lower surface of the scraper (43); a magnet A (45) is embedded on one side of the fixing frame (44); and a flip plate (46) is arranged inside the sewage outlet (12); the magnet A (45) and the flip plate (46) are opposite to each other; A magnet B (461) is fixedly mounted on one side of the flip plate (46) close to the magnet A (45), and the magnet B (461) and the magnet A (45) are magnetically attracted to each other. A tension spring (462) is fixedly mounted on the other side of the flip plate (46), and one end of the tension spring (462) is fixedly connected to the top of the sewage outlet (12). A long rod (463) is provided at one end of the flip plate (46), and both ends of the long rod (463) are fixedly connected to the inner wall of the sewage outlet (12).
10. An acidification process of the continuous acidification equipment for fatty acid production according to any one of claims 1 to 9, characterized in that: The following steps are involved: S1: After the required water source is added into the acidification tank (1) through the water inlet (17), the drain groove (51) is blocked by the electric telescopic plate (53), and the water source is located on the upper surface of the temporary storage tank (5). Then, the material for making fatty acids is added into the hopper (3), and the acidulant is added into the liquid storage tank (22). Then, the dual-axis motor (26) can be started to start stirring the stirring rod (253); S2: As the dual-axis motor (26) is started, the small gear (261) drives the large gear (2413) to rotate, and the rotating large gear (2413) drives the disk (241) and the clamping column (2412) to rotate together, and one set of rotating clamping columns (2412) drives the T block (2432) to move, and the T block (2432) drives the horizontal plate (243) to move to one end until the clamping column (2412) and the T block (2432) are separated, at which time another set of clamping columns (2412) contacts one end of the V plate (2436), causing the V plate (2436) to rotate counterclockwise, thereby driving the horizontal plate (243) to move to the other end, causing the horizontal plate (243) to move back and forth; S3: As the horizontal plate (243) moves back and forth, the roller (2435) will reciprocate and squeeze the inclined plate (224) and the pressure plate (225). The moving inclined plate (224) and the pressure plate (225) will also move together with the fixed rod (227) and the push plate (228), so that the push plate (228) can squeeze the acidifier inside the liquid storage tank (22) into the liquid outlet pipe (223), and finally flow through the liquid outlet pipe (223) to the water source that has been added in advance. Due to the fixed connection between the C-shaped plate (242) and the horizontal plate (243), , and the C-shaped plate (242) is located inside the narrow groove (212) and moves, so the reciprocating C-shaped plate (242) allows the inclined block to reciprocate along the inclined groove (2421), so that the material inside the hopper (3) is discharged together with the acidifier. At this time, the acidifier and the material are added to the water source for mixing and stirring. When the horizontal plate (243) reciprocates, the lever (2442) reciprocates with the center column (2441) as the center, thereby driving the circular frame (231) to reciprocate and rise and fall, further improving the stirring and mixing speed; S4: When the liquid mixing is completed, the dual-axis motor (26) is stopped, and the electric telescopic plate (53) is turned on to allow the liquid to enter the liquid storage chamber (54), and then discharged to the surface of the filter membrane (47) through the quantitative valve. At this time, the speed of the liquid falling will be reduced, and the total amount of the liquid will also be reduced, which can prevent the problem of the filter membrane (47) being broken due to the impact generated when the liquid is discharged. When all the liquid enters the liquid storage chamber (54), the next round of mixing can be carried out, and the liquid that falls on the surface of the filter membrane (47) will be filtered to filter the activated carbon, sodium fatty acid, sodium sulfate crystals and other substances in the liquid, so that only the fatty acid falls to the cone mouth (13), and the scraper (43) will slide out the impurities on the surface of the filter membrane (47), and finally discharged from the sewage outlet (12).
Citation Information
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