Utilization method of jujube kernel tranquilizing liquid waste residues

Abstract

The invention discloses a method for utilizing waste residues of a jujube kernel tranquilizing liquid, which specifically comprises the following steps of: 1, decocting spina date seeds (fried), salvia miltiorrhiza and vinegar schisandra chinensis generated in a prescription of the jujube kernel tranquilizing liquid for more than two times, then collecting the waste residues, and airing; 2, crushing the waste residues, putting the crushed waste residues into a filter paper tube, putting the filter paper tube into a Soxhlet extraction barrel, adding a petroleum ether solution, and carrying out reflux extraction for more than 4 hours until a soaking solution around the paper tube is basically colorless; 3, evaporating the petroleum ether to dryness in a water bath with the temperature of 60-80 DEG C to obtain jujube kernel tranquilizing essential oil liquid; and 4, detecting the jujube kernel tranquilizing essential oil liquid, and bottling the jujube kernel tranquilizing essential oil liquid. The volatile oil can be obtained from the waste residues, environmental pollution is reduced, meanwhile, the value of the spina date seeds and the value of the schisandra chinensis are brought into full play, and waste is avoided.

Description

Technical Field

[0001] The present invention relates to the technical field of jujube seed processing, and specifically to a method for utilizing the waste residue of jujube seed calming liquid. Background Art

[0002] Insomnia is a common disease. For the treatment of insomnia, although antipsychotic sedative drugs have good effects, their side effects are also obvious, mainly reflected in affecting the mental state the next day after taking the medicine, thus further affecting normal work and life.

[0003] Traditional jujube seed calming preparations include jujube seed calming liquid, jujube seed calming granule, jujube seed calming capsule, etc. The extraction processes include water extraction and alcohol extraction. However, no matter which method is used, waste residue will be left and wasted. Since traditional Chinese medicinal materials contain rich nutrients, the medicinal residues after water extraction and decoction still have a lot of nutritional components. In the past, traditional Chinese medicinal residues were often used as fertilizers or feeds, resulting in the inability to fully utilize the remaining value of the waste, and it is also relatively wasteful. Therefore, improvement is needed. Summary of the Invention

[0004] The purpose of the present invention is to provide a method for utilizing the waste residue of jujube seed calming liquid, so as to solve the problem in the above background art that the waste of the processed products of jujube seed calming preparations is directly used as fertilizer or feed, resulting in the inability to fully utilize the remaining value of the waste and being relatively wasteful.

[0005] To achieve the above purpose, the present invention provides the following technical solution: A method for utilizing the waste residue of jujube seed calming liquid, specifically including the following steps:

[0006] The first step: Fry the wild jujube seeds, salvia miltiorrhiza, and schisandra chinensis var. rubriflora produced in the prescription of jujube seed calming liquid for more than two times, and then collect the waste residue and dry it.

[0007] The second step: Crush the waste residue and place it in a filter paper cylinder, then put it into a Soxhlet extraction cylinder, add petroleum ether solution, and reflux extract for more than 4 hours until the soaking solution around the paper cylinder is basically colorless.

[0008] The third step: Evaporate the petroleum ether in a water bath at 60 - 80 °C to obtain jujube seed calming essential oil liquid.

[0009] The fourth step: Detect the jujube seed calming essential oil liquid and bottle it.

[0010] Preferably, in the first step, fry the wild jujube seeds, salvia miltiorrhiza, and schisandra chinensis var. rubriflora produced in the prescription of jujube seed calming liquid for two times.

[0011] Preferably, during the drying process of the collected waste residue in the first step, ensure that the water content of the final waste residue is controlled at 5% - 10%.

[0012] Preferably, the process of crushing the waste residue in the second step is as follows: First, the waste residue is preliminarily cleaned and dried, then the waste residue is ground using a grinding device, and the ground powder is screened through a sieve or a sorting device to remove impurities and control the particle size of the powder until the required powder fineness is achieved.

[0013] Preferably, the aperture mesh number of the sieve is 8 - 10 meshes.

[0014] Preferably, the decocting time for the collected waste residue in the first step is 2 - 4 h.

[0015] Preferably, in the first step, the collected waste residue is air-dried at a temperature of 20 - 28 °C for natural air-drying.

[0016] Preferably, the reflux extraction time in the second step is 5 hours.

[0017] Preferably, in the third step, petroleum ether is evaporated to dryness in a 70 °C water bath.

[0018] Preferably, after filtering the water generated during cooking in the first step, it can be used as water in the later process of preparing the prescription of Zao Ren Anshen Liquid.

[0019] Compared with the prior art, the beneficial effects of the present invention are as follows: The present invention can obtain volatile oil from the waste residue, reduce environmental pollution, and at the same time give full play to the value of wild jujube seed and schisandra chinensis, avoiding waste. Specific Embodiments

[0020] Next, the technical solutions in the embodiments of the present invention will be clearly and completely described in conjunction with the embodiments of the present invention. Based on the embodiments in the present invention, all other embodiments obtained by those of ordinary skill in the art without making creative efforts shall fall within the protection scope of the present invention.

[0021] Example 1:

[0022] An embodiment provided by the present invention: A method for utilizing the waste residue of Zao Ren Anshen Liquid, specifically including the following steps:

[0023] First step: The wild jujube seed (fried), salvia miltiorrhiza, and schisandra chinensis vinegar produced in the prescription of Zao Ren Anshen Liquid are decocted more than twice, and then the waste residue is collected and air-dried;

[0024] Second step: After crushing the waste residue, it is placed in a filter paper cylinder, then put into a Soxhlet extraction cylinder, petroleum ether solution is added, and reflux extraction is carried out for more than 4 hours until the soaking solution around the paper cylinder is basically colorless;

[0025] Third step: Evaporate petroleum ether to dryness in a 60 - 80 °C water bath to obtain Zao Ren Anshen essential oil liquid;

[0026] Step 4: Detect and bottle the Zao Ren Anshen essential oil liquid.

[0027] Preferably, in the first step, the semen ziziphi spinosae (parched), salvia miltiorrhiza, and schisandra chinensis (vinegar processed) produced in the prescription of Zao Ren Anshen liquid are decocted twice.

[0028] Preferably, during the drying process of the collected waste residue in the first step, ensure that the water content of the final waste residue is controlled at 5%-10%.

[0029] Preferably, the process of pulverizing the waste residue in the second step is as follows: First, wash and dry the waste residue preliminarily, then use grinding equipment to grind the waste residue, and screen the ground powder through a sieve or sorting equipment to remove impurities and control the particle size of the powder until the required powder fineness is achieved.

[0030] Preferably, the aperture mesh number of the sieve is 8-10 meshes.

[0031] Preferably, the decocting time of the collected waste residue in the first step is 2-4 h.

[0032] Preferably, the collected waste residue in the first step is air-dried at a temperature of 20-28°C.

[0033] Preferably, the reflux extraction time in the second step is 5 hours.

[0034] Preferably, in the third step, petroleum ether is evaporated to dryness in a 70°C water bath.

[0035] Preferably, the water produced by cooking in the first step can be used as water in the later production process of the Zao Ren Anshen liquid prescription after filtration.

[0036] Through experiments, it is proved that the finally extracted Zao Ren Anshen essential oil liquid contains 9.7% oleic acid and 6.2% linoleic acid after detection. Considering that linoleic acid is a polyunsaturated fatty acid, it has effects and functions such as reducing cholesterol, anti-inflammatory, promoting cardiovascular health, regulating blood sugar, and maintaining skin health.

[0037] 1. Reducing cholesterol: Linoleic acid can promote cholesterol metabolism, reduce its deposition on the blood vessel wall, and thus help reduce the cholesterol level in the blood.

[0038] 2. Anti-inflammatory effect: Linoleic acid has anti-inflammatory properties, which can help reduce the body's inflammatory response and has a certain auxiliary effect on relieving some inflammatory diseases.

[0039] 3. Cardiovascular health: Linoleic acid helps improve cardiovascular health. It can reduce the risk of cardiovascular diseases and has a positive impact on maintaining heart function.

[0040] 4. Blood sugar regulation: Linoleic acid also helps regulate blood sugar. It can help improve insulin sensitivity and is beneficial to diabetic patients.

[0041] 5. Maintaining skin health: Linoleic acid is an important component of skin cells. It helps keep the skin elastic and moist and has a positive effect on skin health.

[0042] Therefore, the Zao Ren Anshen essential oil liquid obtained by the present invention can be directly applied to the temples for calming the nerves. Thus, the present invention can obtain volatile oil from the waste residue, reducing environmental pollution. At the same time, it gives full play to the value of wild jujube seeds and Schisandra chinensis, avoiding waste.

[0043] Example 2:

[0044] An embodiment provided by the present invention: A method for utilizing the waste residue of Zao Ren Anshen liquid, specifically including the following steps:

[0045] The first step: Fry wild jujube seeds (fried), Salvia miltiorrhiza, and Schisandra chinensis vinegar produced in the prescription of Zao Ren Anshen liquid for more than three times, and then collect the waste residue and dry it.

[0046] The second step: After crushing the waste residue, place it in a filter paper cylinder, then put it into a Soxhlet extraction barrel, add petroleum ether solution, and reflux for more than 6 hours until the soaking solution around the paper cylinder is basically colorless.

[0047] The third step: Evaporate the petroleum ether in a 65°C water bath to obtain Zao Ren Anshen essential oil liquid.

[0048] The fourth step: Detect the Zao Ren Anshen essential oil liquid and bottle it.

[0049] Preferably, during the drying process of the collected waste residue in the first step, ensure that the water content of the final waste residue is controlled at 8%.

[0050] Preferably, the aperture mesh number of the sieve is 9 meshes.

[0051] Preferably, the decocting time of the collected waste residue in the first step is 3h.

[0052] Preferably, in the first step, the collected waste residue is naturally air-dried at a temperature of 25°.

[0053] Example 3:

[0054] An embodiment provided by the present invention: A method for utilizing the waste residue of Zao Ren Anshen liquid, specifically including the following steps:

[0055] Step 1: Fry the prepared wild jujube seeds, salvia miltiorrhiza, and schisandra chinensis in the prescription of Zaoren Anshen Liquid twice, then collect the residue and dry it.

[0056] Step 2: Crush the residue and place it in a filter paper cylinder, then put it into a Soxhlet extraction cylinder, add petroleum ether solution, and reflux for more than 4.5 hours until the soaking solution around the paper cylinder is basically colorless.

[0057] Step 3: Evaporate the petroleum ether in a water bath at 80°C to obtain the essential oil liquid of Zaoren Anshen.

[0058] Step 4: Detect the essential oil liquid of Zaoren Anshen and bottle it.

[0059] Preferably, during the drying process of the collected residue in Step 1, ensure that the water content of the final residue is controlled at 7%.

[0060] Preferably, the process of crushing the residue in Step 2 is as follows: First, wash and dry the residue preliminarily, then use a grinding device to grind the residue, and screen the ground powder through a sieve or sorting device to remove impurities and control the particle size of the powder until the required powder fineness is achieved. The aperture mesh number of the sieve is 8 meshes.

[0061] Preferably, the decocting time of the collected residue in Step 1 is 2.5 h.

[0062] Preferably, the collected residue in Step 1 is dried naturally at a temperature of 26°.

[0063] Example 4:

[0064] An example provided by the present invention: A method for utilizing the residue of Zaoren Anshen Liquid, specifically including the following steps:

[0065] Step 1: Decoct the prepared wild jujube seeds, salvia miltiorrhiza, and schisandra chinensis in the prescription of Zaoren Anshen Liquid twice or more, then collect the residue and dry it.

[0066] Step 2: Crush the residue and place it in a filter paper cylinder, then put it into a Soxhlet extraction cylinder, add petroleum ether solution, and reflux for more than 5.5 hours until the soaking solution around the paper cylinder is basically colorless.

[0067] Step 3: Evaporate the petroleum ether in a water bath at 75°C to obtain the essential oil liquid of Zaoren Anshen.

[0068] Step 4: Detect the essential oil liquid of Zaoren Anshen and bottle it.

[0069] Preferably, in the first step, the semen ziziphi spinosae (fried), salvia miltiorrhiza, and schisandra chinensis vinegar are decocted twice in the prescription of zaoren anshen liquid.

[0070] Preferably, during the drying process of the collected waste residue in the first step, ensure that the water content of the final waste residue is controlled at 9%.

[0071] Preferably, the process of pulverizing the waste residue in the second step is as follows: First, the waste residue is preliminarily cleaned and dried, then the waste residue is ground using a grinding device, and the ground powder is screened through a sieve or sorting device to remove impurities and control the particle size of the powder until the required powder fineness is achieved.

[0072] Preferably, the aperture mesh number of the sieve is 10 mesh.

[0073] Preferably, the decocting time of the collected waste residue in the first step is 4h.

[0074] Preferably, in the first step, the collected waste residue is air-dried at a temperature of 28° for natural air drying.

[0075] Example 5:

[0076] An embodiment provided by the present invention: A method for utilizing the waste residue of zaoren anshen liquid, specifically including the following steps:

[0077] First step: The semen ziziphi spinosae (fried), salvia miltiorrhiza, and schisandra chinensis vinegar generated in the prescription of zaoren anshen liquid are decocted three times, and then the waste residue is collected and dried;

[0078] Second step: After pulverizing the waste residue, it is placed in a filter paper cylinder, then put into a Soxhlet extraction cylinder, petroleum ether solution is added, and reflux extraction is carried out for more than 7 hours until the soaking solution around the paper cylinder is basically colorless;

[0079] Third step: The petroleum ether is evaporated to dryness in a 78°C water bath to obtain zaoren anshen essential oil liquid;

[0080] Fourth step: The zaoren anshen essential oil liquid is detected and bottled.

[0081] Preferably, during the drying process of the collected waste residue in the first step, ensure that the water content of the final waste residue is controlled at 5%.

[0082] Preferably, the process of pulverizing the waste residue in the second step is as follows: First, the waste residue is preliminarily cleaned and dried, then the waste residue is ground using a grinding device, and the ground powder is screened through a sieve or sorting device to remove impurities and control the particle size of the powder until the required powder fineness is achieved, and the aperture mesh number of the sieve is 8 mesh.

[0083] Preferably, the decocting time of the collected waste residue in the first step is 2h.

[0084] Preferably, in the first step, the collected waste residue is air-dried at a temperature of 20°C for natural air-drying.

[0085] The zizyphus jujuba seed calming essential oil liquid obtained by the present invention can be directly applied to the temples for calming the nerves. Therefore, the present invention can obtain volatile oil from the waste residue, reduce environmental pollution, and at the same time give full play to the value of zizyphus jujuba seeds and schisandra chinensis, avoiding waste.

[0086] Although the present invention has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments, or perform equivalent replacements on some of the technical features. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principle of the present invention shall be included in the protection scope of the present invention.

Claims

1. A method for utilizing the waste residue of jujube seed tranquilizing liquid, characterized in that: The specific steps include: The first step is to decoct the Chinese date seeds (fried), salvia miltiorrhiza, and vinegar schisandra chinensis produced in the prescription of the jujube seed tranquilizing liquid for more than two times, and then collect the waste residue and dry it; Step 2: crush the waste residue and place it in a filter paper tube, then put it into a Soxhlet extraction barrel, add petroleum ether solution, and reflux extraction for more than 4 hours until the soaking liquid around the paper tube is basically colorless; Step 3: evaporate the petroleum ether in a 60-80°C water bath to obtain the jujube seed tranquilizing essential oil; Step 4: Test the jujube seed tranquilizing essential oil and bottle it.

2. The method for utilizing the waste residue of the jujube seed tranquilizing liquid according to claim 1, characterized in that: In the first step, the Chinese date seeds (fried), salvia miltiorrhiza and vinegar schisandra chinensis produced in the prescription of Zaoren Anshen Liquid are decocted twice.

3. A method for utilizing the waste residue of the Zao Ren An Shen Liquid according to claim 1 or 2, characterized in that: In the first step, during the drying process of the collected waste residue, the moisture content of the final waste residue is controlled to be 5%-10%.

4. A method for utilizing the waste residue of the Zao Ren An Shen Liquid according to claim 1, 2 or 3, characterized in that: The process of crushing the waste residue in the second step is as follows: first, the waste residue is preliminarily cleaned and dried, then the waste residue is ground using a grinding device, and the ground powder is screened through a screen or a sorting device to remove impurities and control the particle size of the powder until the desired powder fineness is achieved.

5. The method for utilizing the waste residue of the Zao Ren An Shen Liquid according to claim 4, characterized in that: The mesh size of the screen is 8-10 mesh.

6. A method for utilizing the waste residue of the Zao Ren An Shen Liquid according to claim 1, 2 or 3, characterized in that: In the first step, the collected waste residue is boiled for 2 to 4 hours.

7. The method for utilizing the waste residue of the Zao Ren An Shen Liquid according to claim 1, 2 or 3, characterized in that: In the first step, the collected waste residue is dried by natural air drying at a temperature of 20-28°.

8. The method for utilizing the waste residue of the Zao Ren An Shen Liquid according to claim 1, 2 or 3, characterized in that: The extraction time under reflux in the second step was 5 hours.

9. The method for utilizing the waste residue of the Zao Ren An Shen Liquid according to claim 1, 2 or 3, characterized in that: In the third step, the petroleum ether was evaporated in a 70°C water bath.

10. The method for utilizing the waste residue of the Zao Ren An Shen Liquid according to claim 1, 2 or 3, characterized in that: In the first step, the water produced by steaming is filtered and can be used as water in the later preparation process of the Jujube Seed Calming Liquid prescription.