Massage essential oil and preparation method thereof
By pretreating xanthan gum and hyaluronic acid and mixing them with base oil and isopropyl myristate, the problem of uneven distribution of massage oil components was solved, and the stability and uniformity of massage oil during long-term storage were achieved.
Patent Information
- Application Number
- CN202511141375.4
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-08-15
- Publication Date
- 2025-11-07
AI Technical Summary
When blending multiple single essential oils, differences in density and miscibility can lead to uneven distribution of components in massage oils after prolonged standing, affecting their effectiveness.
Xanthan gum and hyaluronic acid are pretreated with single essential oils to form intermolecular forces. Then, they are mixed with base oil and isopropyl myristate. Through specific stirring and settling steps, the components are ensured to be evenly dispersed, thus preparing a stable massage essential oil.
The components remain stable and evenly distributed during long-term storage, avoiding unevenness in the direction of gravity of the massage oil and ensuring the stability of the effect.
Abstract
Description
TECHNICAL FIELD
[0001] The present application relates to the technical field of essential oils, in particular to a massage essential oil and a preparation method thereof. BACKGROUND
[0002] Massage essential oil is essential oil for massage, which can play the role of lubrication, nerve soothing, etc. Massage essential oil is usually a compound essential oil, which is generally mixed by “single essential oil + base oil”. The base oil and the single essential oil constitute the core components of the massage essential oil. Among them, the base oil as the base of the massage essential oil can usually play the role of lubrication, and also can nourish the skin and provide protection; the single essential oil as the key ingredient in the massage essential oil can bring diverse health effects. By reasonably selecting and compounding multiple single essential oils, the nerve pressure can be relieved, the nervous and muscle tension and pain can be relaxed, and various discomfort and pain can be quickly relieved. It is helpful for blood to flow more smoothly, reduces the discomfort and pain caused by the tension, swelling and blockage between the human body and the muscle and lymph, and quickly helps to relieve the symptoms of edema and swelling caused by metabolic imbalance.
[0003] However, when multiple single essential oils are compounded, due to the density difference and mutual solubility difference between different single essential oils or between the single essential oil and the base oil, after the massage essential oil is placed for a long time, part of the components will sink, and part of the components will float. Although it may not be obvious stratification, it will cause the uneven distribution of the components of the massage essential oil in the direction of gravity. When the massage essential oil is poured out for use, the components of the massage essential oil poured out at different times are unstable, which affects the use effect of the massage essential oil. SUMMARY
[0004] In view of the deficiencies of the prior art, the first object of the present application is to provide a preparation method of massage essential oil, which can obtain massage essential oil with stable and uniform component distribution during long-term storage.
[0005] The second object of the present application is to provide massage essential oil prepared by the above preparation method.
[0006] To achieve the first object of the present application, the present application provides a preparation method of massage essential oil, which comprises the following steps: step one: preparing raw materials, wherein the raw materials comprise 500 parts by mass of base oil, 13-16 parts by mass of single essential oil, 1-2 parts by mass of xanthan gum, 0.5-1 part by mass of hyaluronic acid and 1-3 parts by mass of isopropyl myristate; wherein the base oil is a mixture of coconut oil, jojoba oil and sweet almond oil, and the single essential oil is a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil; step two: stirring the single essential oil, xanthan gum and hyaluronic acid at a first rotating speed under heating conditions, then stirring at a second rotating speed at room temperature, and then standing under cooling conditions, and stirring at a third rotating speed after returning to room temperature to obtain an essential oil mixture; the second rotating speed is less than the first rotating speed, and the third rotating speed is less than the second rotating speed; and step three: stirring the essential oil mixture, the base oil and the isopropyl myristate at a fourth rotating speed at room temperature to obtain massage essential oil; the fourth rotating speed is less than the third rotating speed.
[0007] In some embodiments of the present application, the raw materials comprise 500 parts by mass of base oil, 13-15 parts by mass of single essential oil, 1-1.5 parts by mass of xanthan gum, 0.5-0.6 parts by mass of hyaluronic acid and 2-3 parts by mass of isopropyl myristate.
[0008] In some embodiments of the present application, in the base oil, the mass ratio of the coconut oil, the jojoba oil and the sweet almond oil is 1:(2-3):(4-5).
[0009] In some embodiments of the present application, in the single essential oil, the mass ratio of the coffee essential oil, the sandalwood essential oil, the frankincense essential oil and the cedar essential oil is 1:(0.5-1):(0.3-0.5):(0.3-0.5).
[0010] In some embodiments of the present application, in the step two, the single essential oil, xanthan gum and hyaluronic acid are stirred at a rotating speed of 300-500 rpm for 5-10 min at 40-50 DEG C, then stirred at a rotating speed of 200-300 rpm for 30-60 min at room temperature, then stand at 0-5 DEG C for 1-2 h, and then stirred at a rotating speed of 100-200 rpm for 10-20 min after returning to room temperature to obtain the essential oil mixture.
[0011] In some embodiments of the present application, in the step two, the single essential oil, xanthan gum and hyaluronic acid are stirred at a rotating speed of 300-400 rpm for 6-8 min at 40-45 DEG C, then stirred at a rotating speed of 200-250 rpm for 40-60 min at room temperature, then stand at 0-5 DEG C for 1-1.5 h, and then stirred at a rotating speed of 100-150 rpm for 10-15 min after returning to room temperature to obtain the essential oil mixture.
[0012] In some embodiments of the present application, in the step three, the essential oil mixture, the base oil and the isopropyl myristate are stirred at room temperature at a third rotating speed for 20-30 min, to obtain the massage essential oil.
[0013] In some embodiments of the present application, in the step three, the essential oil mixture, the base oil and the isopropyl myristate are stirred at room temperature at a third rotating speed for 20-30 min, to obtain the massage essential oil.
[0014] In some embodiments of the present application, in the step three, the essential oil mixture, the base oil and the isopropyl myristate are stirred at room temperature at a third rotating speed, and then the obtained product is placed at room temperature for 1-1.5 h, and then filtered through a 40-80 mesh filter screen, to obtain the massage essential oil.
[0015] To achieve the second object of the present application, the present application provides a massage essential oil prepared by the preparation method.
[0016] Compared with the prior art, the present application can achieve the following beneficial effects: The preparation method of the massage essential oil of the present application first pretreats single essential oil through the cooperation of xanthan gum and hyaluronic acid in a specific step, so that multiple single essential oils directly form intermolecular forces with xanthan gum and hyaluronic acid, and then the obtained mixture containing single essential oil is mixed with base oil and isopropyl myristate to dilute and disperse the mixture of single essential oil under specific mixing conditions, to prepare massage essential oil. The single essential oil can be stably and uniformly dispersed in the base oil, and the component ratio of the massage essential oil in the direction of gravity can remain basically constant during long-term storage of the massage essential oil, which is conducive to maintaining the stable efficacy of the massage essential oil. DETAILED DESCRIPTION
[0017] The embodiments of the present application provide a preparation method of massage essential oil, which can obtain massage essential oil with stable and uniform component distribution during long-term storage. The preparation method of massage essential oil of the present embodiment is especially suitable for the preparation of massage essential oil with mixed base oil and mixed single essential oil, which can avoid the problem of uneven distribution of components caused by sinking or floating of different components when essential oil components with different densities and different mutual solubilities are mixed.
[0018] Specifically, the preparation method of the present embodiment includes the following steps: Step one: prepare raw materials, including base oil 500 parts by mass, single essential oil 13-16 parts by mass, xanthan gum 1-2 parts by mass, hyaluronic acid 0.5-1 parts by mass, isopropyl myristate 1-3 parts by mass; wherein the base oil is a mixture of coconut oil, jojoba oil and sweet almond oil, and the single essential oil is a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil; Step two: stir the single essential oil, xanthan gum and hyaluronic acid under heating conditions at a first rotation speed, then stir at a second rotation speed at room temperature, and then stand under cooling conditions, and after returning to room temperature, stir at a third rotation speed to obtain an essential oil mixture; the second rotation speed is less than the first rotation speed, and the third rotation speed is less than the second rotation speed; Step three: stir the essential oil mixture, base oil and isopropyl myristate at room temperature at a fourth rotation speed to obtain a massage essential oil; the fourth rotation speed is less than the third rotation speed.
[0019] In step one, the mixture of coconut oil, jojoba oil and sweet almond oil is used as the base oil as the basic carrier of the massage essential oil, with the highest proportion, mainly to dilute the single essential oil, reduce the irritation of the single essential oil, at the same time, provide nourishment and moisturizing for the skin, enhance the spreadability of the essential oil, facilitate the application and push during massage, and also help the penetration of nutrients into the skin. The mixture of the three oils can combine the characteristics of easy absorption of coconut oil, strong stability of jojoba oil and mild and skin-friendly sweet almond oil.
[0020] The single essential oil adopts a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil, which is the functional core component of the massage essential oil. Coffee essential oil can refresh the mind, promote blood circulation and boost mood; sandalwood essential oil can calm, anti-inflammatory, antibacterial and promote skin healing; frankincense essential oil can calm and pacify the nerves, promote healing, soothe inflamed skin and fight acne bacteria; cedar essential oil can calm, reduce pressure, promote lymph circulation and improve edema. The above single essential oil combined with massage techniques can have the effects of calming, reducing swelling, reducing redness, detoxifying, unblocking lymph and the like.
[0021] The combination of xanthan gum and hyaluronic acid can play a stabilizing role, forming intermolecular forces with each single essential oil component, preventing stratification of each component, making the composition of essential oil more uniform, and enhancing the stability of the formula.
[0022] Isopropyl myristate has lubricating and penetration promoting effects, can reduce the gel feeling of essential oil, promote the spread of essential oil, and at the same time help the base oil and single essential oil to penetrate the skin better, enhance the absorption efficiency.
[0023] Step two, the single essential oil, xanthan gum, hyaluronic acid are first heated and stirred rapidly, so that the single essential oil is fully dispersed and mixed evenly with other ingredients, then stirred at room temperature, which is conducive to the full contact of xanthan gum and hyaluronic acid with the single essential oil and the formation of intermolecular forces, and enhances the compatibility. Subsequent low-temperature standing can make the intermolecular interaction more stable.
[0024] Step three, the essential oil mixture is stirred with base oil and isopropyl myristate at low speed, so that all components are fully integrated. The base oil serves as the main body to disperse other ingredients, and the isopropyl myristate adjusts the overall texture, finally forming a uniform, stable and suitable viscosity essential oil product. Low-speed stirring can avoid damaging the stable structure formed in the early stage, ensuring the long-term stability of the product.
[0025] In some examples, the raw materials include 500 parts by mass of base oil, 13-15 parts by mass of single essential oil, 1-1.5 parts by mass of xanthan gum, 0.5-0.6 parts by mass of hyaluronic acid, and 2-3 parts by mass of isopropyl myristate. When each component is within the above range, the uniformity and stability of the massage essential oil can be further improved.
[0026] In some examples, in the base oil, the mass ratio of coconut oil, jojoba oil and sweet almond oil is 1:(2-3):(4-5) to obtain the desired spreadability and delicate feel.
[0027] In some examples, in the single essential oil, the mass ratio of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil is 1:(0.5-1):(0.3-0.5):(0.3-0.5) to obtain the desired efficacy.
[0028] In some examples, in step two, the single essential oil, xanthan gum and hyaluronic acid are stirred at 40-50°C at a speed of 300-500 rpm for 5-10 min, then stirred at room temperature at a speed of 200-300 rpm for 30-60 min, then placed at 0-5°C for 1-2 h, and then stirred at 100-200 rpm for 10-20 min after returning to room temperature to obtain the essential oil mixture.
[0029] In some examples, in step two, the single essential oil, xanthan gum and hyaluronic acid are stirred at 40-45°C at a speed of 300-400 rpm for 6-8 min, then stirred at room temperature at a speed of 200-250 rpm for 40-60 min, then placed at 0-5°C for 1-1.5 h, and then stirred at 100-150 rpm for 10-15 min after returning to room temperature to obtain the essential oil mixture.
[0030] In some examples, in step three, the essential oil mixture, base oil and isopropyl myristate are stirred at room temperature at a rotation speed of 50-100 rpm for 20-30 min to obtain the massage essential oil.
[0031] In some examples, in step three, the essential oil mixture, base oil and isopropyl myristate are stirred at room temperature at a rotation speed of 80-100 rpm for 20-25 min to obtain the massage essential oil.
[0032] In some examples, in step three, after the essential oil mixture, base oil and isopropyl myristate are stirred at room temperature at the third rotation speed, the obtained product is further placed at room temperature for 1-1.5 h, and then filtered with a 40-80 mesh filter screen to remove a small amount of insoluble substances to obtain the massage essential oil.
[0033] In some examples, the embodiment also provides the massage essential oil prepared by the above-mentioned scheme.
[0034] The technical solutions of the present application will be further described in detail through specific examples.
[0035] Example 1 The preparation method steps of the massage essential oil of the present embodiment are as follows: Step one: prepare raw materials, which include base oil 500 parts by mass, single essential oil 13 parts by mass, xanthan gum 1 part by mass, hyaluronic acid 0.5 parts by mass, and isopropyl myristate 2 parts by mass; wherein the base oil is a mixture of coconut oil, jojoba oil and sweet almond oil, and the mass ratio of coconut oil, jojoba oil and sweet almond oil is 1:2:4; the single essential oil is a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil, and the mass ratio of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil is 1:0.5:0.3:0.3.
[0036] Step two: in step two, the single essential oil, xanthan gum and hyaluronic acid are stirred at a rotation speed of 300 rpm at 40°C for 6 min, then stirred at a rotation speed of 200 rpm at room temperature for 40 min, then placed at 0°C for 1 h, and after returning to room temperature, stirred at a rotation speed of 100 rpm for 10 min to obtain the essential oil mixture.
[0037] Step three: the essential oil mixture, base oil and isopropyl myristate are stirred at room temperature at a rotation speed of 80 rpm for 20 min, the obtained product is placed at room temperature for 1 h, and then filtered with a 40 mesh filter screen to obtain the massage essential oil.
[0038] Example 2 The preparation method steps of the massage essential oil of the present embodiment are as follows: Step one: prepare raw materials, the raw materials include base oil 500 parts by mass, single essential oil 15 parts by mass, xanthan gum 1.5 parts by mass, hyaluronic acid 0.6 parts by mass, isopropyl myristate 3 parts by mass; wherein the base oil is a mixture of coconut oil, jojoba oil and sweet almond oil, the mass ratio of coconut oil, jojoba oil and sweet almond oil is 1:3:5; the single essential oil is a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil, the mass ratio of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil is 1:1:0.5:0.5.
[0039] Step two: in step two, the single essential oil, xanthan gum and hyaluronic acid are stirred at 45℃ for 8min at a speed of 400rpm, then stirred at room temperature for 60min at a speed of 250rpm, then placed at 5℃ for 1.5h, after returning to room temperature, stirred at 150rpm for 15min, to obtain an essential oil mixture.
[0040] Step three: the essential oil mixture, base oil and isopropyl myristate are stirred at room temperature at a speed of 100rpm for 25min, the obtained product is placed at room temperature for 1.5h, then filtered with a 80 mesh filter screen, to obtain a massage essential oil.
[0041] Example 3 The preparation method steps of the massage essential oil of the present example are as follows: Step one: prepare raw materials, the raw materials include base oil 500 parts by mass, single essential oil 15 parts by mass, xanthan gum 1.5 parts by mass, hyaluronic acid 0.6 parts by mass, isopropyl myristate 3 parts by mass; wherein the base oil is a mixture of coconut oil, jojoba oil and sweet almond oil, the mass ratio of coconut oil, jojoba oil and sweet almond oil is 1:3:5; the single essential oil is a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil, the mass ratio of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil is 1:1:0.5:0.5.
[0042] Step two: in step two, the single essential oil, xanthan gum and hyaluronic acid are stirred at 45℃ for 8min at a speed of 400rpm, then stirred at room temperature for 60min at a speed of 250rpm, then placed at 5℃ for 1.5h, after returning to room temperature, stirred at 150rpm for 15min, to obtain an essential oil mixture.
[0043] Step three: the essential oil mixture, base oil and isopropyl myristate are stirred at room temperature at a speed of 100rpm for 25min, the obtained product is placed at room temperature for 1.5h, then filtered with a 80 mesh filter screen, to obtain a massage essential oil.
[0044] Example 4 The preparation method steps of the massage essential oil of the present example are as follows: Step one: preparing raw materials, the raw materials include base oil 500 parts by mass, single essential oil 13 parts by mass, xanthan gum 1 part by mass, hyaluronic acid 0.5 parts by mass, isopropyl myristate 1 part by mass; wherein the base oil is a mixture of coconut oil, jojoba oil and sweet almond oil, and the mass ratio of coconut oil, jojoba oil and sweet almond oil is 1:2:4; the single essential oil is a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil, and the mass ratio of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil is 1:1:0.5:0.5.
[0045] Step two: in step two, the single essential oil, xanthan gum and hyaluronic acid are stirred at 40℃ for 6min at a speed of 300rpm, then stirred at room temperature for 40min at a speed of 200rpm, then placed at 0℃ for 1h, and then stirred at 100rpm for 10min after returning to room temperature to obtain an essential oil mixture.
[0046] Step three: the essential oil mixture, base oil and isopropyl myristate are stirred at room temperature for 20min at a speed of 80rpm, the obtained product is placed at room temperature for 1h, and then filtered with a 100 mesh screen to obtain a massage essential oil.
[0047] Comparative example 1 The preparation method steps of the massage essential oil of the present comparative example are as follows: Step one: preparing raw materials, the raw materials include base oil 500 parts by mass, single essential oil 13 parts by mass.
[0048] Step two: the single essential oil, base oil and isopropyl myristate are stirred at room temperature for 20min at a speed of 80rpm to obtain a massage essential oil.
[0049] Comparative example 2 The preparation method steps of the massage essential oil of the present comparative example are as follows: Step one: preparing raw materials, the raw materials include base oil 500 parts by mass, single essential oil 13 parts by mass, xanthan gum 1 part by mass, hyaluronic acid 0.5 parts by mass; wherein the base oil is a mixture of coconut oil, jojoba oil and sweet almond oil, and the mass ratio of coconut oil, jojoba oil and sweet almond oil is 1:2:4; the single essential oil is a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil, and the mass ratio of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil is 1:0.5:0.3:0.3.
[0050] Step two: in step two, the single essential oil, xanthan gum and hyaluronic acid are stirred at 40℃ for 6min at a speed of 300rpm, then stirred at room temperature for 40min at a speed of 200rpm, then placed at 0℃ for 1h, and then stirred at 100rpm for 10min after returning to room temperature to obtain an essential oil mixture.
[0051] Step three: the mixture of essential oil, base oil at room temperature with 80 rpm stirring 20 min, the product obtained at room temperature for 1 h, and then with 40 mesh filter, massage essential oil.
[0052] Comparative example 3 The preparation method steps of the massage essential oil of the present comparative example are as follows: Step one: preparing raw materials, raw materials including base oil 500 parts by mass, single essential oil 13 parts by mass, xanthan gum 1 part by mass, hyaluronic acid 0.5 parts by mass, capric acid triglyceride 2 parts by mass; wherein the base oil is a mixture of coconut oil, jojoba oil and sweet almond oil, the mass ratio of coconut oil, jojoba oil and sweet almond oil is 1:2:4; single essential oil is a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil, the mass ratio of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil is 1:0.5:0.3:0.3.
[0053] Step two: in step two, the single essential oil, xanthan gum and hyaluronic acid are stirred at 40℃ with 300 rpm for 6 min, then stirred at room temperature with 200 rpm for 40 min, then placed at 0℃ for 1 h, after returning to room temperature, stirred with 100 rpm for 10 min, to obtain the essential oil mixture.
[0054] Step three: the mixture of essential oil, base oil and capric acid triglyceride at room temperature with 80 rpm stirring 20 min, the product obtained at room temperature for 1 h, and then with 40 mesh filter, massage essential oil.
[0055] Comparative example 4 The preparation method steps of the massage essential oil of the present comparative example are as follows: Step one: preparing raw materials, raw materials including base oil 500 parts by mass, single essential oil 13 parts by mass, xanthan gum 5 parts by mass, hyaluronic acid 3 parts by mass, isopropyl myristate 5 parts by mass; wherein the base oil is a mixture of coconut oil, jojoba oil and sweet almond oil, the mass ratio of coconut oil, jojoba oil and sweet almond oil is 1:2:4; single essential oil is a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil, the mass ratio of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil is 1:0.5:0.3:0.3.
[0056] Step two: in step two, the single essential oil, xanthan gum and hyaluronic acid are stirred at 40℃ with 300 rpm for 6 min, then stirred at room temperature with 200 rpm for 40 min, then placed at 0℃ for 1 h, after returning to room temperature, stirred with 100 rpm for 10 min, to obtain the essential oil mixture.
[0057] Step three: the mixture of essential oil, base oil and isopropyl myristate were stirred at room temperature for 20 min at 80 rpm, the resulting product was left to stand at room temperature for 1 h, and then filtered with a 40 mesh filter to obtain the massage essential oil.
[0058] Comparative Example 5 The preparation method of the massage essential oil of the present comparative example is as follows: Step one: the raw materials were prepared, including 500 parts by mass of base oil, 13 parts by mass of single essential oil, 1.5 parts by mass of xanthan gum, and 2 parts by mass of isopropyl myristate; wherein the base oil was a mixture of coconut oil, jojoba oil and sweet almond oil, and the mass ratio of coconut oil, jojoba oil and sweet almond oil was 1:2:4; the single essential oil was a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil, and the mass ratio of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil was 1:0.5:0.3:0.3.
[0059] Step two: in step two, the single essential oil and the xanthan gum were stirred at 40°C for 6 min at 300 rpm, then stirred at room temperature for 40 min at 200 rpm, then left to stand at 0°C for 1 h, and then stirred at 100 rpm for 10 min after returning to room temperature to obtain the mixture of essential oil.
[0060] Step three: the mixture of essential oil, base oil and isopropyl myristate were stirred at room temperature for 20 min at 80 rpm, the resulting product was left to stand at room temperature for 1 h, and then filtered with a 40 mesh filter to obtain the massage essential oil.
[0061] Comparative Example 6 The preparation method of the massage essential oil of the present comparative example is as follows: Step one: the raw materials were prepared, including 500 parts by mass of base oil, 13 parts by mass of single essential oil, 1.5 parts by mass of xanthan gum, and 2 parts by mass of isopropyl myristate; wherein the base oil was a mixture of coconut oil, jojoba oil and sweet almond oil, and the mass ratio of coconut oil, jojoba oil and sweet almond oil was 1:2:4; the single essential oil was a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil, and the mass ratio of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil was 1:0.5:0.3:0.3.
[0062] Step two: in step two, the single essential oil and the xanthan gum were stirred at 40°C for 6 min at 300 rpm, then stirred at room temperature for 40 min at 200 rpm, then left to stand at 0°C for 1 h, and then stirred at 100 rpm for 10 min after returning to room temperature to obtain the mixture of essential oil.
[0063] Step three: the mixture of essential oil, base oil and isopropyl myristate are stirred at room temperature for 20 min at 80 rpm, the product is left to stand at room temperature for 1 h, then filtered through a 40 mesh screen to obtain the massage essential oil.
[0064] The massage essential oils obtained in the above examples and comparative examples are prepared in bottles of 500 ml each, and are left to stand at room temperature. Samples are taken at the beginning, 3 months, 6 months and 12 months, and the upper 100 ml and lower 100 ml of each sample bottle are tested for density. The results are shown in Table 1.
[0065] Table 1 Test results Example 1 Example 2 Example 3 Example 4 Comparative Example 1 Comparative Example 2 Comparative Example 3 Comparative Example 4 Comparative Example 5 Comparative Example 6 Initial Upper layer 0.895 0.918 0.923 0.905 0.863 0.899 0.894 0.954 0.893 0.901 Lower layer 0.893 0.920 0.922 0.906 0.865 0.901 0.895 0.958 0.895 0.905 3 months Upper layer 0.893 0.917 0.920 0.903 0.821 0.875 0.882 0.931 0.879 0.893 Lower layer 0.896 0.921 0.923 0.907 0.892 0.920 0.904 0.967 0.900 0.912 6 months Upper layer 0.892 0.917 0.918 0.898 0.765 0.856 0.867 0.920 0.863 0.886 Lower layer 0.896 0.922 0.926 0.910 0.913 0.928 0.921 0.969 0.918 0.923 12 months Upper layer 0.892 0.916 0.911 0.893 0.733 0.845 0.855 0.912 0.851 0.875 Lower layer 0.898 0.923 0.930 0.912 0.922 0.935 0.930 0.973 0.924 0.935 As can be seen from the above, the massage essential oils obtained in the examples of the present application have small changes in density between the upper and lower layers during long-term storage, reflecting that the composition of the massage essential oil is uniformly and stably distributed in the direction of gravity. The comparative examples which are not prepared using the method of the present application have large changes in density, and the composition becomes non-uniform during long-term storage.
[0066] Finally, it should be emphasized that the above description is only of the preferred embodiments of the present application, and is not intended to limit the present application. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present application should be included in the scope of protection of the present application.
Claims
1. A method of preparing a massage essential oil, characterized by The method comprises the following steps: Step 1: preparing raw materials, the raw materials comprising 500 parts by mass of base oil, 13-16 parts by mass of single essential oil, 1-2 parts by mass of xanthan gum, 0.5-1 part by mass of hyaluronic acid, and 1-3 parts by mass of isopropyl myristate; wherein the base oil is a mixture of coconut oil, jojoba oil and sweet almond oil, and the single essential oil is a mixture of coffee essential oil, sandalwood essential oil, frankincense essential oil and cedar essential oil; Step 2: stirring the single essential oil, xanthan gum and hyaluronic acid at a first rotating speed under heating, then stirring at a second rotating speed at room temperature, and then standing at a cooling condition, and stirring at a third rotating speed after returning to room temperature to obtain an essential oil mixture; the second rotating speed is less than the first rotating speed, and the third rotating speed is less than the second rotating speed; Step 3: stirring the essential oil mixture, the base oil and the isopropyl myristate at a fourth rotating speed at room temperature to obtain a massage essential oil; the fourth rotating speed is less than or equal to the third rotating speed.
2. The method of claim 1, wherein The raw materials comprise 500 parts by mass of base oil, 13-15 parts by mass of single essential oil, 1-1.5 parts by mass of xanthan gum, 0.5-0.6 parts by mass of hyaluronic acid, and 2-3 parts by mass of isopropyl myristate.
3. A method of preparing a massage essential oil according to claim 1 or 2, characterized in that In the base oil, the mass ratio of the coconut oil, the jojoba oil and the sweet almond oil is 1:(2-3):(4-5).
4. The method of claim 1 or 2, wherein In the single essential oil, the mass ratio of the coffee essential oil, the sandalwood essential oil, the frankincense essential oil and the cedar essential oil is 1:(0.5-1):(0.3-0.5):(0.3-0.5).
5. The method of claim 1 or 2, wherein In the step 2, the single essential oil, xanthan gum and hyaluronic acid are stirred at a rotating speed of 300-500 rpm at 40-50℃ for 5-10 min, then stirred at a rotating speed of 200-300 rpm at room temperature for 30-60 min, then stood at 0-5℃ for 1-2 h, and stirred at a rotating speed of 100-200 rpm after returning to room temperature for 10-20 min to obtain the essential oil mixture.
6. The method of claim 5, wherein In the step 2, the single essential oil, xanthan gum and hyaluronic acid are stirred at a rotating speed of 300-400 rpm at 40-45℃ for 6-8 min, then stirred at a rotating speed of 200-250 rpm at room temperature for 40-60 min, then stood at 0-5℃ for 1-1.5 h, and stirred at a rotating speed of 100-150 rpm after returning to room temperature for 10-15 min to obtain the essential oil mixture.
7. The method of claim 1 or 2, wherein In the step 3, the essential oil mixture, the base oil and the isopropyl myristate are stirred at a rotating speed of 50-100 rpm at room temperature for 20-30 min to obtain the massage essential oil.
8. A method of preparing a massage essential oil according to claim 7, characterized in that In the step 3, the essential oil mixture, the base oil and the isopropyl myristate are stirred at a rotating speed of 80-100 rpm at room temperature for 20-25 min to obtain the massage essential oil.
9. The method of claim 1 or 2, wherein In the step 3, after the essential oil mixture, the base oil and the isopropyl myristate are stirred at the third rotating speed at room temperature, the obtained product is further stood at room temperature for 1-1.5 h, then filtered through a filter screen with a mesh size of 40-80 to obtain the massage essential oil.
10. A massage essential oil, characterized by obtained by the production process according to any one of claims 1 to 9.