Multiphase ceramic material with high density and excellent electromagnetic shielding performance and low-temperature sintering preparation method thereof

By combining low-temperature sintering technology with oxide additives, the problem of high-temperature sintering of ultra-high temperature ceramic materials has been solved, realizing multiphase ceramic materials with high density and excellent electromagnetic shielding performance, reducing energy consumption and cost, and expanding their application range.

CN122010574APending Publication Date: 2026-05-12WUHAN UNIV OF TECH
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Patent Information

Application Number
CN202610173252.7
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2026-02-06
Publication Date
2026-05-12

AI Technical Summary

Technical Problem

Existing ultra-high temperature ceramic materials require ultra-high temperature sintering above 2000°C during preparation, resulting in high energy consumption and high cost. Furthermore, they are difficult to combine with carbon fibers, which limits their application in lightweight and high-strength electromagnetic shielding materials.

Method used

Multiphase ceramic materials are prepared at relatively low temperatures (around 1300℃) by using hot pressing sintering or spark plasma sintering technology combined with oxide additives (such as MgO, SiO2, Al2O3). By introducing oxide additives, the densification temperature of ultra-high temperature ceramics is reduced, and high density and excellent electromagnetic shielding performance are achieved at low temperatures.

Benefits of technology

It significantly reduces the energy consumption and cost of material preparation, achieves high density and excellent electromagnetic shielding performance, broadens its application in aerospace, electronic communications and other fields, and provides the possibility of composite with carbon fiber reinforcement.

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Abstract

The invention discloses a multiphase ceramic material with high density and excellent electromagnetic shielding performance and a low-temperature sintering preparation method thereof. The method comprises the following steps: mixing ultra-high-temperature ceramic powder and oxide powder in proportion, carrying out wet ball milling and rotary evaporation drying to obtain uniform powder, and then carrying out thermal insulation for 5-60 minutes under the conditions of 800-1500 DEG C and 10-200 MPa by adopting a hot pressed sintering or spark plasma sintering process to realize low-temperature densification of the ceramic. The relative density of the obtained composite ceramic is greater than or equal to 95%, and the average electromagnetic shielding effectiveness in the X band is greater than or equal to 30 dB. The sintering temperature of the ultrahigh-temperature ceramic is greatly reduced, the energy consumption and the cost are reduced while high density and excellent electromagnetic shielding performance are maintained, and the ultrahigh-temperature ceramic is suitable for electromagnetic shielding, high-temperature thermal protection and light structure-function integrated composite material components.
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