Method for characterizing shale pore wettability based on high temperature and high pressure alternate imbibition

By employing a high-temperature and high-pressure alternating percolation method and nuclear magnetic resonance technology, the deviation problem in wettability characterization under normal temperature and pressure was solved, enabling accurate evaluation of multi-scale pore wettability and improving shale oil development efficiency.

CN122409429APending Publication Date: 2026-07-17CHINA UNIV OF PETROLEUM (EAST CHINA)
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
CHINA UNIV OF PETROLEUM (EAST CHINA)
Filing Date
2026-05-15
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing methods for characterizing shale pore wettability are conducted at ambient temperature and pressure, which cannot accurately reflect the high-temperature and high-pressure environment of the formation. This results in large discrepancies between the results and the actual situation, and makes it difficult to distinguish the wettability of different pore regions, thus affecting the efficiency of shale oil development.

Method used

A high-temperature and high-pressure alternating infiltration method was adopted, and the oil and water phases were alternately infiltrated under in-situ formation conditions using nuclear magnetic resonance technology. Combined with the pore size calibration coefficient, the wettability index was calculated to accurately evaluate the wettability changes of multi-scale pores.

Benefits of technology

It enables the accurate reflection of shale wettability evolution under high temperature and high pressure conditions, and precise assessment of wettability changes in multi-scale pore regions, providing precise guidance for shale oil development and improving recovery rate.

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Abstract

本发明公开了基于高温高压交替渗吸表征页岩孔隙润湿性的方法,属于页岩测试技术领域,包括样品准备、双相饱和确定油谱和水谱的孔径标定系数、高温高压下动态交换渗吸确定不同润湿相孔隙的信号分布和计算不同孔隙区间内润湿性指数变化曲线;本发明提供的基于高温高压交替渗吸表征页岩孔隙润湿性的方法,模拟原位条件可真实还原地下储层孔隙结构状态和流体物性,避免常温常压实验带来的孔隙畸变、流体性质偏差,保证实验结果贴合地层实际,还能够准确地表征页岩中多尺度油湿、水湿和混合湿孔隙的孔隙体积变化以及润湿性变化,且具有操作简便、结果可信度高、适用范围广等优点,对页岩储层的开发和提高采收率技术具有重要意义。
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