Separator in epoxiconazole purification process

Abstract

The utility model belongs to the field of separation, in particular relates to a separator in an epoxiconazole purification process, and aims to solve the problems that particulate impurities on a first filter screen are inconvenient to clean in the existing filtering process, so that the filtering of the first filter screen is influenced by the particulate impurities, the filtering efficiency of the first filter screen is reduced, and the filtering efficiency of the first filter screen is reduced. According to the scheme, the device comprises a bottom plate, a fixing frame is fixedly arranged at the top of the bottom plate, and a mixing tank is fixedly arranged on the inner wall of the fixing frame; the cleaning mechanism is arranged at the bottom of the mixing tank and is used for cleaning the surface of the filter screen; the mixing mechanism is arranged on the mixing tank and is used for mixing and dissolving the mixture. When the filter screen is used, particle impurities on the filter screen can be shoveled and collected, so that the effect of cleaning the filter screen is achieved, the influence of the particle impurities on the filtering of the filter screen is avoided, and the filtering efficiency of the filter screen is improved.

Description

Technical Field

[0001] The utility model relates to the technical field of separation, in particular to a separator in a flutriafol purification process. Background Art

[0002] Flutriafol, with its mechanism of action as an inhibitor of C-14 demethylase in sterol biosynthesis, has both protective and therapeutic effects. Suitable crops include wheat, barley, rice, sugar beet, rapeseed, leguminous crops, vegetables, grapes, apples, etc. When producing flutriafol chemically, a separator in the flutriafol purification process is often required;

[0003] After retrieval, the patent with the authorization announcement number CN219399126U proposes a 6-chloronicotinic acid separation and purification device, aiming to solve the problem in the prior art that it is difficult to remove the dissolved chemical substances in the mixed solution, resulting in poor purification effect of 6-chloronicotinic acid. The key points of its technical solution are: a 6-chloronicotinic acid separation and purification device, including a frame, on which a mixing tank, a condensation tank and a separation tank are arranged in sequence. The top of the mixing tank is provided with a feed inlet. A partition plate is horizontally arranged in the mixing tank, and the inner part of the mixing tank is divided into an upper chamber and a lower chamber by the partition plate. A stirring component is arranged in the upper chamber, and a first filter screen is vertically arranged in the lower chamber. In the 6-chloronicotinic acid separation and purification device of the utility model, the large particulate impurities in the mixed solution are first screened out by the first filter screen, and then the 6-chloronicotinic acid crystals are precipitated by condensation and the chemical impurities dissolved in the mixed solution are filtered out by the second filter screen. Through two filtration processes, the impurities in the mixed solution are effectively removed, ensuring the purification and separation effect of 6-chloronicotinic acid. The following problems exist in this technical solution:

[0004] During use, the particulate impurities in the mixed solution can be filtered out by the first filter screen. Since it is not convenient to clean the particulate impurities on the first filter screen during the filtration process, the particulate impurities will affect the filtration of the first filter screen and reduce the filtration efficiency of the first filter screen, making it inconvenient to use;

[0005] In view of the above problems, the present utility model document proposes a separator in a flutriafol purification process. Summary of the Utility Model

[0006] The utility model provides a separator in a flutriafol purification process, which solves the disadvantages in the prior art that due to the inconvenience of cleaning the particulate impurities on the first filter screen during the filtration process, the particulate impurities will affect the filtration of the first filter screen and reduce the filtration efficiency of the first filter screen, making it inconvenient to use.

[0007] The utility model provides the following technical solutions:

[0008] A separator in a flutriafol purification process, comprising:

[0009] A bottom plate, a fixing frame is fixedly arranged at the top of the bottom plate, a mixing tank is fixedly arranged on the inner wall of the fixing frame, a storage tank corresponding to the mixing tank is arranged at the top of the bottom plate, a filter screen is fixedly installed on the inner wall of the storage tank, a drain pipe is communicated with the bottom of the mixing tank, and a solenoid valve is arranged on the outer wall of the drain pipe;

[0010] A cleaning mechanism is arranged at the bottom of the mixing tank for cleaning the surface of the filter screen;

[0011] A mixing mechanism is arranged on the mixing tank for mixing and dissolving the mixture.

[0012] In a possible design, the cleaning mechanism includes a second motor, the second motor is fixedly installed at the bottom of the mixing tank, the output end of the second motor is fixedly provided with a round block through a coupling, an installation block is fixedly arranged on the outer wall of the round block, and two clamping grooves are opened at the top of the installation block.

[0013] In a possible design, clamping blocks are clamped and installed inside both of the two clamping grooves, the same collecting filter frame is fixedly arranged on one side of the two clamping blocks, and a plurality of filter holes are opened on one side of the collecting filter frame.

[0014] In a possible design, the mixing mechanism includes a first motor, the output end of the first motor penetrates through the top of the mixing tank and extends into the mixing tank, the output end of the first motor is fixedly provided with a stirring rod through a coupling, a plurality of stirring blades are fixedly arranged on the outer wall of the stirring rod, an installation groove is opened inside the mixing tank, and a heating plate is fixedly installed inside the installation groove.

[0015] In a possible design, a separation box is arranged at the top of the bottom plate, a condensation box is arranged at the top of the separation box, a suction pump is fixedly installed on one side of the fixing frame, the liquid inlet and the liquid outlet of the suction pump are respectively communicated with a liquid inlet pipe and a liquid outlet pipe, the end of the liquid inlet pipe far away from the suction pump penetrates through the outer wall of the storage tank and extends into the storage tank, the end of the liquid outlet pipe far away from the suction pump is communicated with the condensation box, and a connecting pipe corresponding to the separation box is communicated with one side of the condensation box far away from the liquid outlet pipe.

[0016] In a possible design, a filter frame is arranged inside the separation box, placing blocks are fixedly arranged on both sides of the filter frame, handles are fixedly arranged on the tops of the two placing blocks, a drain pipe is communicated with one side of the separation box, and a valve is arranged on the outer wall of the drain pipe.

[0017] In this application, during use, first, the epoxiconazole raw material is put into the mixing tank and dissolved in an appropriate solvent in the mixing tank. Then, the first motor is turned on and runs. The stirring rod and stirring blades are driven by the first motor to stir and mix the solution and the epoxiconazole raw material. At the same time, the heating plate in the installation slot is turned on and runs. The heating plate can heat the solution and the epoxiconazole mixed raw material. Thus, in cooperation with stirring, the epoxiconazole raw material can be quickly dissolved, making the dissolved mixed liquid more uniform. This not only enhances the processing efficiency but also improves the quality of epoxiconazole production. After the mixed liquid is heated and mixed to a certain extent, the solenoid valve is opened, and the mixed liquid is discharged into the storage tank through the drain pipe. At the same time, it will pass through a filter screen for filtration. The filter screen can filter out the particles that are not completely dissolved in the mixed liquid and the internal impurities. During this filtration process, the second motor is turned on and runs. The second motor drives the round block to rotate, and the round block drives the outer mounting block and the collection filter frame to rotate. The rotation of the collection filter frame can shovel the particulate impurities on the filter screen for collection. At the same time, the liquid shoveled in will be discharged through the filter holes on one side of the collection filter frame, achieving the effect of cleaning the filter screen and preventing particulate impurities from affecting the filtration of the filter screen, thereby improving the filtration efficiency of the filter screen. When cleaning the inside of the collection filter frame, the clamping connection between the clamping block fixed on one side of the collection filter frame and the clamping groove on the mounting block can be used to achieve the effect of convenient installation and disassembly of the collection filter frame, improving the convenience;

[0018] After all the mixed liquid is filtered into the storage tank, the suction pump is turned on and runs. The suction pump can suck the mixed liquid in the storage tank into the condensing pipe in the condensing box through the liquid outlet tank. After the mixed liquid undergoes a condensing effect in the condensing box, epoxiconazole can gradually crystallize out, achieving high-purity crystallization of epoxiconazole. Subsequently, the epoxiconazole crystals and the generated wastewater will enter the separation box through the connecting pipe. At the same time, the filter frame in the separation box can be used for further filtration, enabling the filtered wastewater to enter the separation box, while the epoxiconazole crystals will remain in the filter frame, achieving the effect of separating the epoxiconazole crystals from the wastewater. Thus, it is convenient to obtain pure epoxiconazole crystals, improving the applicability. After the purification is completed, by lifting the handle, it is convenient to remove the filter frame, which is beneficial for extracting the epoxiconazole crystals. Moreover, by using the placing blocks on both sides of the filter frame, it can be easily clamped to the top side wall of the separation box, facilitating the convenient installation of the filter frame. Finally, the wastewater is discharged through the drain pipe connected to one side of the separation box, and the valve on the outer wall of the drain pipe is convenient to control, improving the usage effect.

[0019] In this utility model, for the separator in an epoxiconazole purification process, the cleaning mechanism can shovel and collect the particulate impurities on the filter screen, achieving the effect of cleaning the filter screen. At the same time, it also realizes the effect of convenient installation and disassembly of the collection filter frame, improving the convenience;

[0020] In the present utility model, the separator in a flutriafol purification process can quickly dissolve the flutriafol raw materials through a mixing mechanism, making the dissolved mixture relatively uniform, which not only enhances the processing efficiency but also improves the quality of flutriafol production.

[0021] In the present utility model, the particulate impurities on the filter screen can be shoveled and collected to achieve the effect of cleaning the filter screen, avoiding the influence of particulate impurities on the filtration of the filter screen and improving the filtration efficiency of the filter screen. BRIEF DESCRIPTION OF THE DRAWINGS

[0022] Figure 1 FIG. 1 is one of the front view structural diagrams of a separator in a flutriafol purification process provided by an embodiment of the present utility model;

[0023] Figure 2 FIG. 2 is another front view structural diagram of a separator in a flutriafol purification process provided by an embodiment of the present utility model;

[0024] Figure 3 FIG. 3 is a sectional view structural diagram of a mixing tank of a separator in a flutriafol purification process provided by an embodiment of the present utility model;

[0025] Figure 4 FIG. 4 is a split structural diagram of a collection filter frame of a separator in a flutriafol purification process provided by an embodiment of the present utility model;

[0026] Figure 5 FIG. 5 is a split structural diagram of a filter frame of a separator in a flutriafol purification process provided by an embodiment of the present utility model.

[0027] REFERENCE NUMERALS:

[0028] 1, bottom plate; 2, fixing frame; 3, mixing tank; 4, first motor; 5, stirring rod; 6, stirring blade; 7, heating plate; 8, filter frame; 9, placing block; 10, handle; 11, storage tank; 12, filter screen; 13, second motor; 14, round block; 15, mounting block; 16, card slot; 17, clamping block; 18, collection filter frame; 19, suction pump; 20, separation box; 21, condensation box; 22, connecting pipe. DETAILED DESCRIPTION OF THE EMBODIMENTS

[0029] The following will clearly and completely describe the technical solutions in the embodiments of the present utility model with reference to the accompanying drawings in the embodiments of the present utility model. Obviously, the described embodiments are only a part of the embodiments of the present utility model, rather than all of the embodiments.

[0030] Embodiment 1

[0031] Please refer to Figures 1-5 , a separator, comprising:

[0032] Base plate 1, a fixing frame 2 is fixedly arranged on the top of the base plate 1, a mixing tank 3 is fixedly arranged on the inner wall of the fixing frame 2, a storage tank 11 corresponding to the mixing tank 3 is arranged on the top of the base plate 1, a filter screen 12 is fixedly installed on the inner wall of the storage tank 11, a drain pipe is communicated with the bottom of the mixing tank 3, a solenoid valve is arranged on the outer wall of the drain pipe. After the liquid is heated and mixed to a certain degree, the solenoid valve is opened, so that the mixed liquid is discharged into the storage tank 11 through the drain pipe, and at the same time, it will pass through the filter screen 12 for filtration. Through the filter screen 12, the particles that are not completely dissolved in the mixed liquid and the internal sundries can be filtered out.

[0033] A cleaning mechanism is arranged at the bottom of the mixing tank 3 for cleaning the surface of the filter screen 12. The cleaning mechanism includes a second motor 13, the second motor 13 is fixedly installed at the bottom of the mixing tank 3, the output end of the second motor 13 is fixedly provided with a round block 14 through a coupling, an installation block 15 is fixedly arranged on the outer wall of the round block 14, two clamping grooves 16 are opened at the top of the installation block 15, two clamping blocks 17 are clamped and installed in the two clamping grooves 16 respectively, and the same collection filter frame 18 is fixedly arranged on one side of the two clamping blocks 17. A plurality of filter holes are opened on one side of the collection filter frame 18.

[0034] The second motor 13 drives the round block 14 to rotate, the round block 14 drives the outer installation block 15 and the collection filter frame 18 to rotate, so that the particulate impurities on the filter screen 12 can be shoveled and collected. At the same time, the filter holes on one side of the collection filter frame 18 will discharge the shoveled liquid, achieving the effect of cleaning the filter screen 12, avoiding the influence of particulate impurities on the filtration of the filter screen 12, improving the filtration efficiency of the filter screen 12, and realizing the effect of convenient installation and disassembly of the collection filter frame 18 by using the clamping connection between the clamping blocks 17 fixed on one side of the collection filter frame 18 and the clamping grooves 16 on the installation block 15, improving the convenience.

[0035] A mixing mechanism is arranged on the mixing tank 3 for mixing and dissolving the mixture. The mixing mechanism includes a first motor 4, the output end of the first motor 4 penetrates through the top of the mixing tank 3 and extends into the mixing tank 3, the output end of the first motor 4 is fixedly provided with a stirring rod 5 through a coupling, a plurality of stirring blades 6 are fixedly arranged on the outer wall of the stirring rod 5, an installation groove is opened inside the mixing tank 3, and a heating plate 7 is fixedly installed inside the installation groove. By driving the stirring rod 5 and the stirring blades 6 by the first motor 4, the solution and the fluxapyroxad raw material can be stirred and mixed. At the same time, the heating plate 7 in the installation groove is turned on to operate, and the heating plate 7 can heat the solution and the fluxapyroxad mixed raw material. Then, in cooperation with stirring, the fluxapyroxad raw material can be quickly dissolved, making the dissolved mixed liquid more uniform, not only enhancing the processing efficiency, but also improving the quality of fluxapyroxad production.

[0036] A separation box 20 is provided on the top of the bottom plate 1, a condensation box 21 is provided on the top of the separation box 20, a suction pump 19 is fixedly installed on one side of the fixing frame 2, a liquid inlet pipe and a liquid outlet pipe are respectively communicated with the liquid inlet and the liquid outlet of the suction pump 19, one end of the liquid inlet pipe away from the suction pump 19 penetrates through the outer wall of the storage tank 11 and extends into the interior of the storage tank 11, and one end of the liquid outlet pipe away from the suction pump 19 is communicated with the condensation box 21. A connecting pipe 22 corresponding to the separation box 20 is communicated on one side of the condensation box 21 away from the liquid outlet pipe. Through the suction pump 19, the mixed liquid in the storage tank 11 can be sucked into the condensation pipe in the condensation box 21 through the liquid outlet tank. After the mixed liquid is condensed in the condensation box 21, the epoxiconazole can gradually crystallize out, realizing the high-purity crystallization of epoxiconazole. Subsequently, the epoxiconazole crystals and the generated wastewater will enter the separation box 20 through the connecting pipe 22 to achieve the separation effect.

[0037] This application can be used in the field of epoxiconazole purification and separation, and can also be used in other fields applicable to this application.

[0038] Among them, the suction pump 19 and the condensation box 21 are the same as the suction pump 15 and the condensation box 3 mentioned in the Chinese Patent Authorization Publication No. CN219399126U, and their structures and mechanisms will not be elaborated here.

[0039] Embodiment 2

[0040] Reference Figure 5 , on the basis of Embodiment 1, an improvement is made: a separator in an epoxiconazole purification process, which is applied to the field of epoxiconazole purification and separation;

[0041] A filter frame 8 is arranged inside the separation box 20. Placing blocks 9 are fixedly arranged on both sides of the filter frame 8, and handles 10 are fixedly arranged on the tops of the two placing blocks 9. A drain pipe is communicated on one side of the separation box 20, and a valve is arranged on the outer wall of the drain pipe. The filter frame 8 in the separation box 20 can be used for further filtration, so that the filtered wastewater enters the separation box 20, while the epoxiconazole crystals will stay in the filter frame 8, realizing the separation effect of epoxiconazole crystals and wastewater. By lifting the handle 10, it is convenient to remove the filter frame 8, which is beneficial to extracting the epoxiconazole crystals. Moreover, by using the placing blocks 9 on both sides of the filter frame 8, it can be conveniently clamped to the top side wall of the separation box 20 to achieve the effect of convenient installation of the filter frame 8. Finally, the wastewater is discharged through the drain pipe communicated on one side of the separation box 20, and the valve on the outer wall of the drain pipe is convenient to control, improving the use effect.

[0042] However, as is well known to those skilled in the art, the working principles and wiring methods of the first motor 4, the heating plate 7, the second motor 13, the suction pump 19 and the condensation box 21 devices are common knowledge, and they all belong to conventional means or well-known common sense, so they will not be elaborated here. Those skilled in the art can make arbitrary selections according to their needs or convenience.

[0043] The above are only the specific embodiments of the present utility model, but the protection scope of the present utility model is not limited thereto. Any person skilled in the art within the technical scope disclosed by the present utility model can easily think of changes or substitutions, which should all be covered within the protection scope of the present utility model; without conflict, the embodiments of the present utility model and the features in the embodiments can be combined with each other. Therefore, the protection scope of the present utility model shall be subject to the protection scope of the claims.

Claims

1. A separator in a process for purifying epoxiconazole, characterized in that: include: A bottom plate (1), a fixing frame (2) is fixedly arranged on the top of the bottom plate (1), a mixing tank (3) is fixedly arranged on the inner wall of the fixing frame (2), a storage tank (11) corresponding to the mixing tank (3) is arranged on the top of the bottom plate (1), a filter screen (12) is fixedly installed on the inner wall of the storage tank (11), a drain pipe is connected to the bottom of the mixing tank (3), and a solenoid valve is arranged on the outer wall of the drain pipe; A cleaning mechanism, which is arranged at the bottom of the mixing tank (3) and is used to clean the surface of the filter screen (12); A mixing mechanism is arranged on the mixing tank (3) and is used to mix and dissolve the mixture.

2. The separator in the process for purifying epoxiconazole according to claim 1, characterized in that: The cleaning mechanism comprises a second motor (13), the second motor (13) is fixedly mounted on the bottom of the mixing tank (3), a round block (14) is fixedly mounted on the output end of the second motor (13) via a coupling, a mounting block (15) is fixedly mounted on the outer wall of the round block (14), and two slots (16) are provided on the top of the mounting block (15).

3. The separator in the process for purifying epoxiconazole according to claim 2, characterized in that: A clamping block (17) is clamped and installed inside the two clamping slots (16), and a same collecting filter frame (18) is fixedly arranged on one side of the two clamping blocks (17), and a plurality of filter holes are opened on one side of the collecting filter frame (18).

4. The separator in the process for purifying epoxiconazole according to claim 1, characterized in that: The mixing mechanism comprises a first motor (4), the output end of the first motor (4) passes through the top of the mixing tank (3) and extends into the interior of the mixing tank (3), the output end of the first motor (4) is fixedly provided with a stirring rod (5) via a coupling, the outer wall of the stirring rod (5) is fixedly provided with a plurality of stirring blades (6), the interior of the mixing tank (3) is provided with a mounting groove, and a heating plate (7) is fixedly installed in the interior of the mounting groove.

5. The separator in the process for purifying epoxiconazole according to claim 1, characterized in that: A separation box (20) is arranged on the top of the bottom plate (1), and a condensation box (21) is arranged on the top of the separation box (20). A suction pump (19) is fixedly mounted on one side of the fixed frame (2), and a liquid inlet and a liquid outlet of the suction pump (19) are respectively connected to a liquid inlet pipe and a liquid outlet pipe, and an end of the liquid inlet pipe away from the suction pump (19) penetrates the outer wall of the storage tank (11) and extends to the interior of the storage tank (11), and an end of the liquid outlet pipe away from the suction pump (19) is connected to the condensation box (21), and a side of the condensation box (21) away from the liquid outlet pipe is connected to a connecting pipe (22) corresponding to the separation box (20).

6. The separator in the process for purifying epoxiconazole according to claim 5, characterized in that: A filter frame (8) is provided inside the separation box (20), placement blocks (9) are fixedly provided on both sides of the filter frame (8), handles (10) are fixedly provided on the tops of the two placement blocks (9), and a drain pipe is connected to one side of the separation box (20), and a valve is provided on the outer wall of the drain pipe.

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