Conductive microsphere reaction system device

Abstract

The utility model discloses a conductive microsphere reaction system device which comprises a reaction kettle which comprises a top cover and a kettle body; a feed port is formed in the top of the reaction kettle, a discharge port is formed in the bottom of the reaction kettle, and heat preservation ports are formed in two sides of the reaction kettle; the reaction kettle is connected with a stirrer, an ultrasonic generator and a peristaltic pump, and is communicated with the thermostatic bath. According to the reaction kettle disclosed by the utility model, multi-step operations such as reaction, sensitization and activation can be uniformly performed in the kettle body, the stirring motor, the ultrasonic generator and the peristaltic pump are controlled through the processing controller, and the stirring speed, the vibration frequency, the feeding speed, the reaction pH value and the reaction temperature are further controlled in cooperation with the acid-base meter, the thermometer and the thermostatic bath; and after the treatment is finished, the rotary switch at the bottom is used for controlling the discharge port to open and receive the material, so that the reaction efficiency is effectively improved, the prepared conductive microsphere coating is uniform and compact, high in lamination sense and high in conductivity, and the particle size uniformity of a microsphere system is effectively improved.

Description

TECHNICAL FIELD

[0001] The utility model relates to laboratory preparation equipment technical field, concretely relates to a kind of electrically conductive microsphere reaction system device. BACKGROUND

[0002] ‌Electrically conductive microsphere‌It is a spherical particle made of polymer or metal material, which is coated with a conductive polymer or conductive metal layer on its surface, thereby having conductive properties, and is widely used in medical health, electrical communication and other fields. For example, PS conductive nickel ball is composed of polystyrene (PS). A layer of nickel metal is plated on the surface of polystyrene microspheres through a specific process, which has good electrical conductivity, thermal conductivity and corrosion resistance, and gives the PS microspheres conductive properties.

[0003] Currently, when preparing electrically conductive microspheres in the laboratory, the base ball needs to be processed in multiple steps (including reaction, sensitization and activation, etc. During the process, the reaction solution needs to be treated at a specific temperature, pH and ultrasonic frequency). Each step of processing needs to be carried out in an experimental container, so that the experimental equipment such as beaker and filter bottle needs to transfer liquid back and forth, which is complicated and can easily affect the quality and performance of the plating layer. UTILITY MODEL CONTENT

[0004] The utility model aims to solve the above problems, and provides an electrically conductive microsphere reaction system device.

[0005] The utility model realizes the above-mentioned purpose by adopting the following technical solutions, comprising:

[0006] The reaction kettle comprises a top cover and a kettle body;

[0007] The reaction kettle is provided with a feeding port at the top, a discharging port at the bottom, and a heat preservation port at both sides;

[0008] The reaction kettle is connected with a stirrer, an ultrasonic generator and a peristaltic pump, and the reaction kettle and the constant temperature tank are communicated.

[0009] As a further description of the above technical solution, the feeding port comprises a uniform feeding port and a rapid feeding port, the uniform feeding port is used for uniform feeding of materials, and the rapid feeding port is used for rapid feeding of materials.

[0010] As a further description of the above technical solution, the uniform feeding port and the rapid feeding port are provided with an ultrasonic placement port on one side, and the ultrasonic placement port is used for placing an ultrasonic rod;

[0011] The other side of the uniform feeding port and the rapid feeding port is provided with a stirring placement port, and the stirring placement port is used for placing a stirring rod.

[0012] As a further description of the above technical scheme, the stirring placement opening side is provided with an acid-base control opening and a temperature control opening, the acid-base control opening is used for placing an acid-base meter, and the temperature control opening is used for placing a thermometer.

[0013] As a further description of the above technical scheme, the bottom of the discharge opening is provided with a rotary switch for opening and closing the discharge channel.

[0014] As a further description of the above technical scheme, the heat preservation opening comprises a circulating inlet and a circulating outlet, the circulating inlet is arranged at the bottom of one side of the kettle body, and the circulating outlet is arranged at the top of one side of the kettle body.

[0015] As a further description of the above technical scheme, the top cover is installed on the fixed support through a first support frame, and the kettle body is installed on the fixed support through a second support frame.

[0016] As a further description of the above technical scheme, the middle part of the top of the fixed support is provided with a stirring motor, the stirring motor is connected with a stirring rod, and the stirring rod extends into the kettle body through the stirring placement opening;

[0017] One side of the top of the fixed support is provided with an ultrasonic rod, and the ultrasonic rod extends into the kettle body through an ultrasonic placement opening.

[0018] The other side of the top of the fixed support is provided with a treatment controller, and the treatment controller is electrically connected with the stirring motor, the ultrasonic generator and the peristaltic pump.

[0019] As a further description of the above technical scheme, the peristaltic pump and the ultrasonic generator are arranged on the fixed support of one side of the kettle body, and the constant temperature tank is arranged on the fixed support of the other side of the kettle body.

[0020] As a further description of the above technical scheme, the constant temperature tank is provided with a medium inlet and a medium outlet, the medium inlet and the circulating outlet are communicated, the medium outlet and the circulating inlet are communicated, and the constant temperature tank is provided with a constant temperature controller at the top.

[0021] The beneficial effects of the present application are as follows:

[0022] The utility model discloses, the top cover corresponds to set up even -speed feeding mouth, fast feeding mouth, ultrasonic placement mouth, stirring placement mouth, acid -base control mouth and temperature control mouth, can be in the kettle body inside unification carries out reaction, sensitization and activation etc.

[0023] In order to make the purpose, technical scheme and advantage of the embodiments of the utility model more clear, below, the technical scheme in the embodiments of the utility model will be clearly and completely described with the drawings in the embodiments of the utility model. DRAWINGS

[0024] Figure 1 It is the structural schematic diagram of the conductive microsphere reaction system device of the utility model.

[0025] Reference signs:

[0026] 1, reaction kettle;11, top cover;12, kettle body;13, feeding port;131, even -speed feeding mouth;132, fast feeding mouth;133, ultrasonic placement mouth;134, stirring placement mouth;135, acid -base control mouth;136, temperature control mouth;14, discharge port;141, rotary switch;15, heat preservation mouth;151, circulating import;152, circulating export;2, stirrer;21, stirring rod;22, stirring motor;3, ultrasonic generator;31, ultrasonic rod;4, peristaltic pump;5, constant temperature tank;51, medium inlet;52, medium outlet;53, constant temperature controller;6, processing controller;7, first support frame;8, fixed support;9, second support frame. DETAILED DESCRIPTION

[0027] In order to make the purpose, technical scheme and advantage of the embodiments of the utility model more clear, below, the technical scheme in the embodiments of the utility model will be clearly and completely described with the drawings in the embodiments of the utility model.

[0028] As Figure 1 Shown, in an embodiment, a conductive microsphere reaction system device includes: reaction kettle 1, reaction kettle 1 includes top cover 11 and kettle body 12, through top cover 11 covers kettle body 12 and forms enclosed cavity.

[0029] The top cover 11 is installed on the fixed support 8 through the first support frame 7, and the kettle body 12 is installed on the fixed support 8 through the second support frame 9, so that the top cover 11 and the kettle body 12 can be stably connected, and the reaction kettle 1 will not be affected by various mechanical pressures and vibrations generated inside during work.

[0030] Meanwhile, the fixed support 8 on one side of the kettle body 12 is provided with the peristaltic pump 4 and the ultrasonic generator 3, the peristaltic pump 4 is communicated with the top cover 11 through the constant-speed feeding pipe, so that the peristaltic pump 4 can make the liquid in the constant-speed feeding pipe flow into the kettle body 12 uniformly when working, and the fixed support 8 on the other side of the kettle body 12 is provided with the constant-temperature tank 5, so that the circulating medium (such as pure water or heated oil, etc.) in the constant-temperature tank 5 can be circulated and heated through the pipeline, so that the temperature inside the kettle body 12 remains constant.

[0031] Specifically, the reaction kettle 1 is connected with the stirrer 2, the ultrasonic generator 3 and the peristaltic pump 4, the top of the reaction kettle 1 is provided with the feeding port 13 for feeding materials and installing the stirring rod 21 and the ultrasonic rod 31 to stir and vibrate the liquid inside; the reaction kettle 1 is communicated with the constant-temperature tank 5, and the bottom of the reaction kettle 1 is provided with the discharging port 14 for receiving materials after the reaction is completed; the reaction kettle 1 is also provided with the heat preservation port 15 on both sides, so that the circulating medium can be circulated and heated through the pipeline.

[0032] Please continue to refer to Figure 1 In this embodiment, the feeding port 13 includes the constant-speed feeding port 131 and the rapid feeding port 132, the constant-speed feeding port 131 is used for feeding materials at a constant speed, and the rapid feeding port 132 is used for feeding materials rapidly.

[0033] The constant-speed feeding port 131 and the rapid feeding port 132 are provided with the ultrasonic placing port 133 on one side, which is used for placing the ultrasonic rod 31, and the top of the fixed support 8 is provided with the ultrasonic rod 31 on one side, so that the ultrasonic rod 31 can extend into the kettle body 12 through the ultrasonic placing port 133, and the ultrasonic rod 31 is driven by the ultrasonic generator 3 to vibrate the liquid in the kettle body 12.

[0034] Further, the constant-speed feeding port 131 and the rapid feeding port 132 are provided with the stirring placing port 134 on the other side, which is used for placing the stirring rod 21, and the top of the fixed support 8 is provided with the stirring motor 22 in the middle, so that the stirring motor 22 can extend into the kettle body 12 through the stirring placing port 134 after being connected with the stirring rod 21, and the stirring rod 21 is driven by the stirring motor 22 to stir the liquid in the kettle body 12.

[0035] Meanwhile, the stirring placing port 134 is also provided with the acid-base control port 135 and the temperature control port 136 on one side, which are respectively used for placing the acid-base meter and the thermometer, so that the pH value and the temperature inside the kettle body 12 can be checked during the reaction.

[0036] It needs to be specified that the other side of the top of the fixed support 8 is also provided with a processing controller 6, and the processing controller 6 is electrically connected with the stirring motor 22, the ultrasonic generator 3 and the peristaltic pump 4, thereby controlling the stirring rate, the vibration frequency and the feeding speed.

[0037] In addition, the bottom of the discharge port 14 is also provided with a rotary switch 141 for opening and closing the discharge channel, and after the reaction is completed, the discharge port 14 can be opened through the rotary switch 141 to open the receiving channel for receiving materials.

[0038] In addition, the heat preservation port 15 includes a circulating inlet 151 and a circulating outlet 152, wherein the circulating inlet 151 is arranged at the bottom of one side of the kettle body 12, and the circulating outlet 152 is arranged at the top of one side of the kettle body 12; correspondingly, the constant temperature tank 5 is provided with a medium inlet 51 and a medium outlet 52, the medium inlet 51 and the circulating outlet 152 are communicated, and the medium outlet 52 and the circulating inlet are communicated; the circulating medium in the constant temperature tank 5 flows out from the medium outlet 52, enters the kettle body 12 from the circulating inlet, and flows out from the circulating outlet 152 after completing the heat tracing circulation, and then flows back to the constant temperature tank 5 from the medium inlet 51; and the constant temperature controller 53 is arranged at the top of the constant temperature tank 5, the temperature of the circulating medium can be controlled through the constant temperature controller 53, thereby adjusting the temperature inside the kettle body 12.

[0039] Working principle: install and fix the top cover 11 of the reaction kettle 1 on the kettle body 12, connect the uniform feeding pipe and the peristaltic pump 4, then insert the uniform feeding pipe into the uniform feeding port 131, insert the feeding funnel into the rapid feeding port 132, connect the stirring rod 21 and the stirring motor 22, then insert the stirring rod 21 into the kettle body 12 from the stirring placing port 134, insert the ultrasonic rod 31 into the kettle body 12 through the ultrasonic placing port 133, insert the acid-base meter into the acid-base control port 135, and insert the thermometer into the temperature control port 136. Adjust the circulating temperature of the circulating medium through the constant temperature controller 53, control the stirring motor 22, the ultrasonic generator 3 and the peristaltic pump 4 through the processing controller 6, drive the stirring rod 21 to stir through the stirring motor 22, drive the ultrasonic rod 31 to vibrate through the ultrasonic generator 3, and drive the liquid in the uniform feeding pipe through the peristaltic pump 4, then adjust the dripping speed of the feeding funnel according to the reading of the acid-base meter, and adjust the temperature of the constant temperature tank 5 through the thermometer. After the reaction is completed, open the rotary switch 141 at the bottom of the discharge port 14, so that the receiving channel of the discharge port 14 is opened to receive materials.

[0040] Through the technical scheme, the uniform feeding port 131, the rapid feeding port 132, the ultrasonic placing port 133, the stirring placing port 134, the acid-base control port 135 and the temperature control port 136 are correspondingly arranged on the top cover 11, so that the multi-step operations such as reaction, sensitization and activation can be uniformly carried out in the kettle body 12, the stirring motor 22, the ultrasonic generator 3 and the peristaltic pump 4 are controlled by the processing controller 6, and the acid-base meter and the thermometer and the constant-temperature tank 5 are matched, so as to control the stirring speed, the vibration frequency, the feeding rate, the reaction acid-base degree and the reaction temperature, the discharge port 14 is controlled to be opened to receive the material through the rotary switch 141 at the bottom after the processing is completed, the reaction efficiency is effectively improved, the prepared conductive microsphere coating is uniform, dense, high in laminating feeling and strong in conductivity, and the particle size uniformity of the microsphere system is effectively improved.

[0041] The above description of disclosed embodiments enables a person skilled in the art to implement or use the present application. Various modifications to these embodiments will be apparent to those skilled in the art, and the general principles defined herein can be implemented in other embodiments without departing from the spirit or scope of the present application. Therefore, the present application will not be limited to these embodiments shown herein, but will conform to the widest scope consistent with the principles and novel features disclosed herein.

Claims

1. A conductive microsphere reaction system device, characterized in that, Include: The reaction kettle (1) includes a top cover (11) and a kettle body (12); The reaction kettle (1) is provided with a feeding port (13) at the top, a discharging port (14) at the bottom, and a heat preservation port (15) on both sides; The reaction kettle (1) is connected with a stirrer (2), an ultrasonic generator (3) and a peristaltic pump (4), and the reaction kettle (1) is communicated with a constant temperature tank (5).

2. The electrically conductive microsphere reaction system apparatus of claim 1, wherein, The feeding port (13) includes a uniform feeding port (131) and a rapid feeding port (132), the uniform feeding port (131) is used for uniform feeding of materials, and the rapid feeding port (132) is used for rapid feeding of materials.

3. The electrically conductive microsphere reaction system apparatus of claim 2, wherein, The uniform feeding port (131) and the rapid feeding port (132) are provided with an ultrasonic placing port (133) on one side, and the ultrasonic placing port (133) is used for placing an ultrasonic rod (31); The uniform feeding port (131) and the rapid feeding port (132) are provided with a stirring placing port (134) on the other side, and the stirring placing port (134) is used for placing a stirring rod (21).

4. The electrically conductive microsphere reaction system apparatus of claim 3, wherein, The stirring placing port (134) is provided with an acid-base control port (135) and a temperature control port (136) on one side, the acid-base control port (135) is used for placing a pH meter, and the temperature control port (136) is used for placing a thermometer.

5. The conductive microsphere reaction system apparatus of claim 1, wherein, The discharging port (14) is provided with a rotary switch (141) at the bottom, and the rotary switch (141) is used for opening and closing the discharging channel.

6. The electrically conductive microsphere reaction system apparatus of claim 1, wherein, The heat preservation port (15) includes a circulating inlet (151) and a circulating outlet (152), the circulating inlet (151) is arranged at the bottom of one side of the kettle body (12), and the circulating outlet (152) is arranged at the top of one side of the kettle body (12).

7. The electrically conductive microsphere reaction system apparatus of claim 1, wherein The top cover (11) is installed on the fixed support (8) through the first support frame (7), and the kettle body (12) is installed on the fixed support (8) through the second support frame (9).

8. The conductive microsphere reaction system apparatus according to claim 7, wherein The fixed support (8) is provided with a stirring motor (22) at the top and middle, the stirring motor (22) is connected with the stirring rod (21) and extends into the kettle body (12) through the stirring placing port (134); The fixed support (8) is provided with an ultrasonic rod (31) on one side at the top, and the ultrasonic rod (31) extends into the kettle body (12) through the ultrasonic placing port (133); The fixed support (8) is provided with a treatment controller (6) on the other side at the top, and the treatment controller (6) is electrically connected with the stirring motor (22), the ultrasonic generator (3) and the peristaltic pump (4).

9. The conductive microsphere reaction system apparatus of claim 8, wherein, The fixed support (8) on one side of the kettle body (12) is provided with the peristaltic pump (4) and the ultrasonic generator (3), and the fixed support (8) on the other side of the kettle body (12) is provided with the constant temperature tank (5).

10. The conductive microsphere reaction system apparatus of claim 9, wherein, The constant temperature tank (5) is provided with a medium inlet (51) and a medium outlet (52), the medium inlet (51) and the circulating outlet (152) are communicated, the medium outlet (52) and the circulating inlet are communicated, and the constant temperature tank (5) is provided with a constant temperature controller (53) at the top.

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