Distillation extraction device for detecting peat phenol value in peat malt

Abstract

The utility model relates to the field of malt physicochemical index detection, and discloses a distillation extraction device for detecting peat phenol value in peat malt, which comprises a support II, a support I and an electric jacket, the outer side of the support II is fixedly connected with a bottom support, the middle part of the bottom support is provided with a condenser pipe, the inside of the condenser pipe is fixedly connected with a coiled pipe, and the coiled pipe is fixedly connected with the support I; a distiller is installed on the outer side of the first support through a chain clamp, a distiller cover is installed on the top of the distiller, a water outlet and a water inlet are sequentially and fixedly connected to the outer side of the condensation pipe from top to bottom, and a conical flask is arranged under the coiled pipe. According to the utility model, the technical scheme of a distillation condensation mode is adopted, so that total phenols in malt can be continuously and uniformly collected. According to the scheme, the whole collection process does not exceed 20 minutes, and the distillation water can be continuously supplemented, so that the efficiency is greatly improved. Compared with the problems of low collection efficiency and complex operation in the prior art, the scheme greatly simplifies the experimental process and improves the overall working efficiency.

Description

TECHNICAL FIELD

[0001] The utility model relates to the malt physical and chemical index detection field especially relates to a kind of distillation extraction device for detecting peat phenol value in peat malt. BACKGROUND

[0002] With the rapid growth of domestic whiskey market, especially the peat whiskey with unique flavor becomes the important subcategory of market, and the quality control demand of peat malt is increasing. The present application provides a kind of distillation extraction device for detecting peat phenol value in peat malt, which can efficiently and stably extract volatile phenol in peat malt and carry out quantitative analysis. The device is mainly applied to whiskey distillery, food detection agency and scientific research laboratory, and can monitor the change of phenol content during the process of malt harvesting, storage and use, so as to reasonably adjust the addition amount of peat malt and ensure the stable flavor of whiskey products.

[0003] At present, there is no device for determining the phenol content in peat malt in China, and the related detection mainly relies on the data provided by imported malt suppliers. However, due to the volatility of phenol, its content may be affected by transportation, storage and environmental conditions, resulting in unstable data. In addition, the existing general distillation detection method is low in efficiency and easy to be affected by the experience of operator, and the repeatability of detection results is poor. Some laboratories use traditional steam distillation method, but it is difficult to ensure the stable transmission of gas during collection, which affects the determination accuracy. Therefore, an efficient, stable and special device suitable for laboratory and distillery on-site detection is urgently needed to fill the technical gap and improve the accuracy of peat malt detection.

[0004] Therefore, a kind of distillation extraction device for detecting peat phenol value in peat malt is proposed to solve the above problems. UTILITY MODEL CONTENT

[0005] In order to make up for the above shortcomings, the utility model provides a kind of distillation extraction device for detecting peat phenol value in peat malt, which aims at improving the problems of low collection efficiency, complicated operation and insufficient data accuracy in the prior art.

[0006] In order to achieve the above purpose, the utility model adopts the following technical scheme: a kind of distillation extraction device for detecting peat phenol value in peat malt, including support two, support one and electric heating jacket, the bottom support is fixedly connected on the outer side of support two, the condenser is installed in the middle part of bottom support, the serpentine pipe is fixedly connected in the inside of condenser, the retort is installed on the outer side of support one by chain clamp, and the retort cover is installed on the top of retort.

[0007] As a further description of the above technical scheme:

[0008] The water outlet and the water inlet are sequentially fixed and connected to the outside of the condenser tube from top to bottom, and a conical flask is arranged directly below the serpentine tube.

[0009] As a further description of the above technical solution:

[0010] The distiller is fixedly connected with a plurality of limiting plates on the inner wall, the top of the limiting plate is provided with a storage net, the outer side of the distiller is fixedly connected with an air inlet, and the top of the distiller cover is fixedly connected with an air outlet one.

[0011] As a further description of the above technical solution:

[0012] The sealing gasket is installed between the distiller cover and the distiller.

[0013] As a further description of the above technical solution:

[0014] The top of the electric heating jacket is fixedly connected with an air outlet two, a silica gel hose two is inserted into the outside of the air outlet two, and one end of the silica gel hose two away from the air outlet two is inserted into the outside of the air inlet.

[0015] As a further description of the above technical solution:

[0016] The silica gel hose one is inserted into the outside of the air outlet one, and one end of the silica gel hose one away from the air outlet one is inserted into the top of the serpentine tube.

[0017] As a further description of the above technical solution:

[0018] The storage net is slidably connected in the distiller, and the air inlet is located below the storage net.

[0019] As a further description of the above technical solution:

[0020] The distiller and the distiller cover are both provided with a heat insulation jacket outside.

[0021] The utility model has the following beneficial effects:

[0022] 1、The utility model discloses a distillation and condensation mode technical scheme can continuously and uniformly collect total phenol in malt.

[0023] 2. The utility model discloses fill the blank of peat phenol value detection device, have independent test function. Through the technical scheme, can accurately determine the phenol content in malt, when comparing with EBC standard malt, the detection Z value of phenol content is less than 2, and the accuracy is higher. Compared with prior art, the accuracy of the scheme is higher, and the reliability is stronger, effectively solve the problem of big data deviation of traditional method.

[0024] 3. The utility model discloses designed economic and practical instrument, is applicable to the peat phenol value test of laboratory scale. Compared with the expensive, complex operation equipment on the market, the scheme reduces the instrument cost, so that the laboratory can more conveniently carry out the large -scale test, solves the problem that the current market equipment is high and leads to the problem of being unable to popularize.

[0025] 4. The utility model discloses have higher popularization value in whiskey distillery goods inspection. Through this special device, the distillery can quickly, accurately detect the phenol content in peat malt, and ensure the stability of malt quality. Compared with the equipment that can not provide real -time accurate detection in the prior art, the scheme provides more efficient, more reliable detection tool for the distillery, and helps to improve product quality control. DRAWINGS

[0026] Figure 1 A stereogram of a distillation extraction device for detecting peat phenol value in peat malt is provided for the utility model;

[0027] Figure 2 A structure diagram of a distillation device section of a distillation extraction device for detecting peat phenol value in peat malt is provided for the utility model;

[0028] Figure 3 A structure diagram of a condenser section of a distillation extraction device for detecting peat phenol value in peat malt is provided for the utility model.

[0029] LEGEND:

[0030] 1, silicone hose one;2, air outlet one;3, distillation device cover;4, distillation device;5, air outlet two;6, electric heating jacket;7, support one;8, chain clamp;9, conical flask;10, support two;11, bottom support;12, water inlet;13, condenser;14, serpentine pipe;15, gasket;16, storage net;17, limit plate;18, air inlet;19, silicone hose two;20, water outlet. DETAILED DESCRIPTION

[0031] The technical solutions in the embodiments of the utility model will be clearly and completely described below with reference to the drawings in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, rather than all the embodiments. Based on the embodiments of the utility model, all other embodiments obtained by those skilled in the art without creative labor fall within the scope of the utility model.

[0032] With reference to Figure 1 - Figure 3 The utility model provides an embodiment: a kind of distillation extraction device for detecting peat coal phenol value in peat coal malt, including support two 10, support one 7 and electric heating jacket 6, support two 10 outside is fixedly connected with bottom support 11, bottom support 11 middle part is equipped with condenser pipe 13, condenser pipe 13 inside is fixedly connected with serpentine pipe 14, support one 7 outside is equipped with distilling apparatus 4 by chain clamp 8, distilling apparatus 4 top is equipped with distilling apparatus cover 3, distilling apparatus 4 and distilling apparatus cover 3 outside are all set with heat insulation jacket, sealing washer 15 is installed between distilling apparatus cover 3 and distilling apparatus 4, condenser pipe 13 outside is sequentially fixedly connected with water outlet 20 and water inlet 12 from top to bottom, serpentine pipe 14 is provided with conical flask 9 directly below.

[0033] Support two 10 provides support for the whole device, ensures the stability of each part, avoids displacement or shaking of equipment during operation.Support one 7 is fixedly connected distilling apparatus 4 by chain clamp 8, provides support and position fixation for distilling apparatus 4.Electric heating jacket 6 provides heat source, for heating peat coal malt, so that it releases volatile substance during heating process.Bottom support 11 is fixedly installed on the outside of support two 10, to ensure the stability of the device, especially the fixing of the installation position of condenser pipe 13.Condenser pipe 13 condenses the evaporated volatile substance back to liquid through the serpentine pipe 14 inside it for collection and analysis.The outside of condenser pipe 13 is sequentially fixedly connected with water outlet 20 and water inlet 12, water inlet 12 is used to introduce cooling water, and water outlet 20 is used to discharge cooled water flow.Distilling apparatus 4 is sealedly connected with distilling apparatus cover 3, to ensure the sealing property during distillation process, avoid gas leakage, and ensure the efficiency and accuracy of distillation process.Distilling apparatus cover 3 and distilling apparatus 4 outside are all set with heat insulation jacket, effectively reduce heat loss, maintain high temperature environment during distillation process.Sealing washer 15 is installed between distilling apparatus cover 3 and distilling apparatus 4, to ensure sealing effect and avoid steam leakage.Serpentine pipe 14 is provided with conical flask 9 directly below, as a container for receiving distillation liquid, to ensure effective collection of liquid and facilitate subsequent analysis.

[0034] With reference to Figure 1 - Figure 3Multiple limiting plates 17 are fixedly connected to the inner wall of the distiller 4. A storage net 16 is provided on the top of the limiting plate 17. An air inlet 18 is fixedly connected to the outer side of the distiller 4. An air outlet 2 is fixedly connected to the top of the distiller cover 3. An air outlet 5 is fixedly connected to the top of the electric heating sleeve 6. A silicone hose 19 is inserted into the outer side of the air outlet 5. The end of the silicone hose 19 away from the air outlet 5 is inserted into the outer side of the air inlet 18. A silicone hose 1 is inserted into the outer side of the air outlet 2. The end of the silicone hose 1 away from the air outlet 2 is inserted into the top of the serpentine tube 14. The storage net 16 is slidably connected inside the distiller 4. The air inlet 18 is located below the storage net 16.

[0035] Multiple limiting plates 17 are fixedly connected to the inner wall of the still 4. The function of the limiting plates 17 is to prevent the malt net 16 from moving or deforming during the distillation process, ensuring that the malt is evenly distributed on the malt net 16, thereby ensuring the uniformity of distillation. The malt net 16 is slidably connected inside the still 4, and its position can be adjusted when needed, making it convenient to place and remove the malt, while ensuring that the malt is evenly heated during the distillation process.

[0036] An air inlet 18 is fixedly connected to the outside of the still 4. The air inlet 18 is used by the heating mantle 6 to heat the peat malt in the still 4, causing it to release volatile substances during heating. These volatile substances enter the serpentine tube 14 through the silicone hose 1 for condensation, and the condensed substances fall into the conical flask 9. A silicone hose 19 is inserted into the outside of the outlet 2 5. The end of the silicone hose 19 furthest from the outlet 2 5 is inserted into the outside of the air inlet 18 to guide and transport gas to the air inlet 18, ensuring a stable gas flow and heating the peat malt in the still 4. A silicone hose 1 is inserted into the outside of the outlet 2 5. The end of the silicone hose 1 furthest from the outlet 2 is inserted into the top of the serpentine tube 14 to guide the volatile gas released from the peat malt during distillation into the serpentine tube 14 for condensation and collection.

[0037] Working Principle: When detecting the phenol content in peat malt, firstly, open the distiller lid 3, evenly place the peat malt on the storage net 16, then seal the distiller 4 and cover it with a heat-insulating jacket. Start the electric heating mantle 6, transferring heat to the peat malt in the distiller 4 through the air inlet 18. At high temperatures, the peat malt releases volatile substances (such as phenol). The evaporated volatile substances enter the silicone tubing 1 from the air outlet 2 of the distiller 4, and are then transported to the serpentine tube 14. Simultaneously, condensate enters from the water inlet 12 and flows out from the water outlet 20, condensing the serpentine tube 14. Here, the evaporated substances are cooled and converted into liquid. The condensed liquid flows through the condenser tube 13 into the conical flask 9 below for collection.

[0038] The collected liquid can be further analyzed for phenol content to provide important quality control information for whiskey production.

[0039] Finally, it should be noted that the above is only the preferred embodiments of the present application, and is not intended to limit the present application, although the foregoing embodiments of the present application are described in detail, for those skilled in the art, it still can be modified, or part of the technical features of the equivalent replacement, within the spirit and principles of the present application, any modification, equivalent replacement, improvement, etc., should be included in the scope of the present application.

Claims

1. A distillation extraction apparatus for detecting peat phenol value in peat malt comprising a support two (10), a support one (7) and a heating mantle (6), characterized in that: The support two (10) outside fixedly connected with the bottom (11), the bottom (11) in the middle of the installation of condenser pipe (13), the condenser pipe (13) inside fixedly connected with the serpentine pipe (14), the support one (7) outside through the chain clamp (8) installed distiller (4), the distiller (4) top installed distiller cover (3).

2. A distillation extraction apparatus for detecting the value of peat phenol in peat malt according to claim 1, characterized in that: The condenser pipe (13) outside from top to bottom fixedly connected with the water outlet (20) and water inlet (12) in turn, the serpentine pipe (14) below provided with the conical flask (9).

3. A distillation extraction apparatus for detecting the value of peat phenol in peat malt according to claim 1, characterized in that: The distiller (4) inner wall fixedly connected with a plurality of limiting plate (17), the limiting plate (17) top provided with the article net (16), the distiller (4) outside fixedly connected with the air inlet (18), the distiller cover (3) top fixedly connected with the air outlet one (2).

4. A distillation extraction apparatus for detecting the value of peat phenol in peat malt according to claim 1, characterized in that: The distiller cover (3) and the distiller (4) between the installation of sealing pad (15).

5. A distillation extraction apparatus for detecting the value of peat phenol in peat malt according to claim 3, characterized in that: The electric heating jacket (6) top fixedly connected with the air outlet two (5), the air outlet two (5) outside inserted with silica gel hose two (19), the silica gel hose two (19) far from the air outlet two (5) one end inserted in the air inlet (18) outside.

6. A distillation extraction apparatus for detecting the value of peat phenol in peat malt according to claim 3, characterized in that: The air outlet one (2) outside inserted with silica gel hose one (1), the silica gel hose one (1) far from the air outlet one (2) one end inserted in the serpentine pipe (14) top.

7. A distillation extraction apparatus for detecting the value of peat phenol in peat malt according to claim 3, characterized in that: The article net (16) slidingly connected in the distiller (4) inside, the air inlet (18) below the article net (16).

8. A distillation extraction apparatus for detecting the value of peat phenol in peat malt according to claim 1, characterized in that: The distiller (4) and the distiller cover (3) outside are all set with heat insulation cover.

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