Cascade reaction device for synthesizing methyltetrahydrofolic acid from carbon dioxide under photocatalysis condition
By using a cascade reaction device under photocatalytic conditions, aurora columns and LED light-emitting chips are used to catalyze the reaction of carbon dioxide and water to produce methyltetrahydrofolate, which solves the problem of high carbon emissions in existing technologies and achieves low-carbon preparation and high-efficiency production.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2025-03-20
- Publication Date
- 2026-03-31
AI Technical Summary
Existing technologies generate significant carbon emissions during the preparation of methyltetrahydrofolic acid, making it difficult to achieve low-carbon production.
A cascade reaction device was designed under photocatalytic conditions, including a catalytic tank, a biosynthesis tank, and a non-polar column filter tank. The device utilizes an aurora column and an LED light-emitting chip to catalyze the reaction of carbon dioxide and water to produce methyltetrahydrofolate, and the reaction products are transported and filtered through a stirring shaft and a pump.
The low-carbon preparation of methyltetrahydrofolate has been achieved, which improves the conversion rate and processing efficiency and reduces production pollution.
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Figure CN224057328U_ABST
Abstract
Description
Technical Field
[0001] This invention relates to the field of methyltetrahydrofolate preparation, and more particularly to a cascade reaction apparatus for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalytic conditions. Background Technology
[0002] Methyltetrahydrofolate is a nitrogen-containing organic compound that promotes nucleic acid synthesis, protects DNA, and helps prevent neural tube defects in the human body. A deficiency of folic acid during pregnancy can lead to congenital malformations in the fetus. Therefore, many pregnant women supplement their diets with folic acid to improve their condition.
[0003] There are many ways to synthesize methyltetrahydrofolate, but in actual preparation, carbon emissions are high and pollution is generated. Utility Model Content
[0004] The purpose of this invention is to address the shortcomings of existing technologies by proposing a cascade reaction device for the synthesis of methyltetrahydrofolate from carbon dioxide under photocatalytic conditions.
[0005] To achieve the above objectives, the present invention adopts the following technical solution: a cascade reaction device for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalytic conditions, comprising a base, four support frames arranged side by side from left to right on the base, and a catalytic tank, a biosynthesis tank, a non-polar column filter tank, and a collection tank arranged sequentially from left to right within the support frames. A gas supply pipe is provided at the bottom of the catalytic tank, and a transparent cover is vertically installed in the middle of the catalytic tank. An aurora column is provided inside the transparent cover, and LED light-emitting chips are evenly distributed on the aurora column. A stirring shaft is rotatably connected inside the biosynthesis tank, and a feed pipe is provided at the top of the biosynthesis tank. One side of the bottom of the biosynthesis tank is connected to the top of the non-polar column filter tank via a first pipe. A light-shielding cover is provided outside the biosynthesis tank, and a heating plate is provided at the bottom of the biosynthesis tank.
[0006] As a further description of the above technical solution:
[0007] A first pump body is installed on the first pipeline, and the first pump body is located at the top of the non-polar column filter tank.
[0008] As a further description of the above technical solution:
[0009] One side of the liquid outlet at the bottom of the non-polar column filter tank is connected to the bottom of one side of the collection tank via a third pipe, and a second pump body is installed on the third pipe.
[0010] As a further description of the above technical solution:
[0011] The bottom end of the stirring shaft penetrates the bottom wall of the biosynthesis tank and is connected to the output end of a speed reducer. The speed reducer is installed inside the base, and the input end of the speed reducer is connected to a motor, which is also installed inside the base.
[0012] As a further description of the above technical solution:
[0013] A water pipe is installed on the top of the catalytic tank.
[0014] As a further description of the above technical solution:
[0015] An oxygen pipe is installed on one side of the top of the catalytic tank.
[0016] As a further description of the above technical solution:
[0017] The collection tank is equipped with a lid on top.
[0018] As a further description of the above technical solution:
[0019] The bottom of the biosynthesis tank is connected to the bottom of the catalytic tank via a second pipe, and a third pump is installed on the second pipe.
[0020] This utility model has the following beneficial effects:
[0021] In this invention, carbon dioxide is directly catalyzed by a catalytic tank, and combined with a biosynthesis tank, low-carbon preparation of methyltetrahydrofolate can be achieved while ensuring a good conversion rate. During the preparation of methyltetrahydrofolate, a non-polar column filter tank can filter and collect methyltetrahydrofolate in real time, which improves the processing efficiency of methyltetrahydrofolate, reduces pollution in the production of methyltetrahydrofolate, and reduces carbon emissions. Attached Figure Description
[0022] Figure 1 This is a three-dimensional view of a cascade reaction apparatus for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalytic conditions, as proposed in this utility model.
[0023] Figure 2 This is a partial cross-sectional view of a cascade reaction apparatus for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalytic conditions, as proposed in this utility model.
[0024] Figure 3 This is a cross-sectional view of the transparent cover of a cascade reaction apparatus for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalytic conditions, as proposed in this utility model.
[0025] Legend:
[0026] 1. Base; 2. Collection tank; 3. Non-polar column filter tank; 4. Light shield; 5. Biosynthesis tank; 6. Feed pipe; 7. First pump body; 8. First pipeline; 9. Catalytic tank; 10. Second pump body; 11. Second pipeline; 12. Third pump body; 13. Third pipeline; 14. Support frame; 15. Water pipe; 16. Transparent cover; 17. Gas supply pipe; 18. Motor; 19. Stirring shaft; 20. Aurora column; 21. Oxygen pipe; 22. Heating plate. Detailed Implementation
[0027] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.
[0028] Reference Figure 1-3 This utility model provides an embodiment of a cascade reaction device for the synthesis of methyltetrahydrofolate from carbon dioxide under photocatalytic conditions. The device includes a base 1, with four support frames 14 arranged side-by-side from left to right. Within each support frame 14, from left to right, are arranged a catalytic tank 9, a biosynthesis tank 5, a non-polar column filter tank 3, and a collection tank 2. This constitutes a complete process for the production of methyltetrahydrofolate. A gas supply pipe 17 is installed at the bottom of the catalytic tank 9 to supply carbon dioxide. A transparent cover 16 is vertically installed in the middle of the catalytic tank 9, and an aurora column 20 is arranged inside the transparent cover 16, with the aurora column 20 having a uniform surface... The biosynthesis tank 5 is equipped with evenly distributed LED light-emitting chips. The light catalyzes the reaction of carbon dioxide and water to produce methyltetrahydrofolate. A stirring shaft 19 is rotatably connected inside the biosynthesis tank 5 to promote the synthesis of methyltetrahydrofolate. A feed pipe 6 is provided at the top of the biosynthesis tank 5. The bottom side of the biosynthesis tank 5 is connected to the top of the first pipe 8 and the non-polar column filter tank 3. A light shield 4 is provided on the outside of the biosynthesis tank 5. Methyltetrahydrofolate is easily decomposed by light, so the reaction is protected from light. A heating plate 22 is provided at the bottom of the biosynthesis tank 5. The heating plate 22 can heat the solution inside the biosynthesis tank 5 to ensure that the enzyme reaction is carried out under mild conditions.
[0029] A first pump body 7 is installed on the first pipe 8. The first pump body 7 is located at the top of the non-polar column filter tank 3. One side of the liquid outlet end of the bottom of the non-polar column filter tank 3 is connected to the bottom side of the collection tank 2 through the third pipe 13 for easy pumping. A second pump body 10 is installed on the third pipe 13. The bottom end of the stirring shaft 19 penetrates the bottom wall of the biosynthesis tank 5 and is connected to the output end of the reducer. The reducer is located inside the base 1. The input end of the reducer is connected to the motor 18. The motor 18 drives the stirring shaft 19 to rotate through the reducer, making the methyltetrahydrofolate reaction more uniform and rapid. The motor 18 is located inside the base 1. A water pipe 15 is installed at the top of the catalytic tank 9. An oxygen pipe 21 is installed on one side of the top of the catalytic tank 9, through which the oxygen generated by the reaction flows out. A cover is installed at the top of the collection tank 2. The bottom of the biosynthesis tank 5 is connected to the bottom of the catalytic tank 9 through the second pipe 11. A third pump body 12 is installed on the second pipe 11.
[0030] Working principle: In the actual production of methyltetrahydrofolate, firstly, pure water is introduced into the catalytic tank 9 through water pipe 15, and carbon dioxide gas is introduced into the catalytic tank 9 through gas supply pipe 17. At this time, the aurora column 20 emits light, and carbon dioxide and water react to produce methyltetrahydrofolate. Then, the third pump body 12 introduces liquid methyltetrahydrofolate into the biosynthesis tank 5 through the second pipe 11. The protein ligand of the catalytic protease is introduced into the biosynthesis tank 5 through the feed pipe 6 to promote the further reaction of carbon dioxide and water to produce methyltetrahydrofolate. At the same time, the motor 18 drives the stirring shaft 19 to rotate through the reducer to make the reaction of methyltetrahydrofolate more uniform and rapid. Then, the first pump body 7 introduces the mixed liquid containing methyltetrahydrofolate into the non-polar column filter tank 3 through the first pipe 8 for filtration. The filtered methyltetrahydrofolate then enters the light-shielded collection tank 2 through the third pipe 13 and the second pump body 10, and then proceeds to the next solid purification process.
[0031] Finally, it should be noted that the above description is only a preferred embodiment of the present utility model and is not intended to limit the present utility model. Although the present utility model has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments or make equivalent substitutions for some of the technical features. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present utility model should be included within the protection scope of the present utility model.
Claims
1. A cascade reaction device for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalytic conditions, comprising a base (1), characterized in that: The base (1) is provided with four support frames (14) side by side from left to right, the support frames (14) are sequentially provided with a catalytic tank (9), a biosynthesis tank (5), a non-polar column filter tank (3) and a collection tank (2) from left to right, the catalytic tank (9) is provided with a gas supply pipe (17) at the bottom, a transparent cover (16) is vertically installed in the middle of the catalytic tank (9), the transparent cover (16) is provided with a polar column (20) and the polar column (20) is uniformly distributed with LED light emitting chips, the biosynthesis tank (5) is rotatably connected with a stirring shaft (19), the biosynthesis tank (5) is provided with a feed pipe (6) at the top, one side of the bottom of the biosynthesis tank (5) is connected with the top of the non-polar column filter tank (3) through a first pipeline (8), the biosynthesis tank (5) is provided with a light shield (4) outside, and the bottom of the biosynthesis tank (5) is provided with a heating plate (22).
2. The cascade reaction device for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalysis according to claim 1, characterized in that: The first pipeline (8) is provided with a first pump body (7), and the first pump body (7) is arranged at the top of the non-polar column filter tank (3).
3. The cascade reaction device for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalysis according to claim 1, characterized in that: One side of the liquid outlet end of the bottom of the non-polar column filter tank (3) is connected with one side of the bottom of the collection tank (2) through a third pipeline (13), and the third pipeline (13) is provided with a second pump body (10).
4. The cascade reaction device for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalysis according to claim 1, characterized in that: The bottom end of the stirring shaft (19) penetrates the bottom wall of the biosynthesis tank (5) and is connected with the output end of a speed reducer, the speed reducer is arranged in the base (1), the input end of the speed reducer is connected with a motor (18), and the motor (18) is arranged in the base (1).
5. The cascade reaction device for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalysis according to claim 1, characterized in that: The catalytic tank (9) is provided with a water pipe (15) at the top.
6. The cascade reaction device for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalysis according to claim 1, characterized in that: One side of the top of the catalytic tank (9) is provided with an oxygen pipe (21).
7. The cascade reaction device for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalysis according to claim 1, characterized in that: The top of the collection tank (2) is provided with a cover.
8. The cascade reaction device for synthesizing methyltetrahydrofolate from carbon dioxide under photocatalysis according to claim 1, characterized in that: The bottom of the biosynthesis tank (5) is connected with the bottom of the catalytic tank (9) through a second pipeline (11), and the second pipeline (11) is provided with a third pump body (12).