Distillation device for synthesizing sanshool

Abstract

The utility model discloses a distillation device for synthesizing sanshool, which relates to the technical field of distillation equipment and comprises a working table, a first storage cabinet and a second storage cabinet are respectively arranged at the bottom of the working table, and two groups of distillation components for distilling sanshool are arranged at the top of the working table. The device disclosed by the utility model has the beneficial effects that due to the arrangement of the first storage cabinet and the second storage cabinet, distillation equipment can be stored, and due to the arrangement of the two groups of distillation components, the distillation efficiency of the device on sanshool can be improved; the support, the settling bottle and the liquid conveying pipe can effectively settle the sanshool, and the water storage tank and the cooling assembly can cool the settling bottle, so that the purification efficiency of the device on the sanshool is improved, and the problem that when an existing distillation device is used for purifying the sanshool, due to the limitation of heating and condensing efficiency, the purification efficiency of the sanshool is influenced is solved. The purification efficiency of the sanshool is reduced.

Description

Technical Field

[0001] This utility model relates to the field of distillation equipment technology, and in particular to a distillation apparatus for the synthesis of sanshool. Background Technology

[0002] Sanshool is a natural compound mainly extracted from plants such as Sichuan pepper. Its chemical components include lactic acid and terpenoids. Sanshool can inhibit the generation of free radicals, reduce oxidative damage to the skin, maintain skin health, reduce melanin production, inhibit the formation of age spots, increase skin moisture content, and improve dry and rough skin. It also has anti-inflammatory and analgesic effects, relieving skin inflammation, especially having a good soothing effect on sensitive skin. Sanshool can also promote fibroblast proliferation, inhibit matrix metalloproteinase expression, and induce autophagy, making it an important component in the fight against photodamage.

[0003] Sanshool, as an important bioactive component, has wide applications in food, spices, medicine, and skincare products. To improve the purification efficiency of sanshool and ensure its purity and stability, a distillation apparatus for sanshool synthesis is needed. However, existing distillation apparatuses for sanshool synthesis often require a long time to complete the entire process due to limitations in heating and condensation efficiency, thus reducing the purification efficiency. Furthermore, existing distillation apparatuses for sanshool synthesis lack gas purification devices during the distillation process, which means that the apparatus cannot treat the gases generated during the purification process, leading to environmental pollution and compromising the safety of laboratory personnel. Utility Model Content

[0004] The purpose of this section is to outline some aspects of embodiments of the present invention and to briefly describe some preferred embodiments. Simplifications or omissions may be made in this section, as well as in the abstract and title of this application, to avoid obscuring the purpose of these documents; however, such simplifications or omissions should not be construed as limiting the scope of the present invention.

[0005] To solve the above-mentioned technical problems, this utility model provides the following technical solution:

[0006] A distillation apparatus for the synthesis of sanshool includes a workbench, with a first storage cabinet and a second storage cabinet respectively installed at the bottom of the workbench. Two sets of distillation components for distilling sanshool are installed on the top of the workbench, with gas guide pipes connected to the top of each set of distillation components. Two sets of exhaust pipes are installed on the top of the workbench, with the inner walls of each exhaust pipe connected to one end of the gas guide pipe. Activated carbon adsorption rings are installed on the outer sides of the two exhaust pipes. A support is installed on the top of the workbench, and a settling bottle is installed above the support. Two sets of infusion pipes are connected to the top of the settling bottle. A water tank is installed below the workbench, and a cooling assembly is installed on the top of the water tank.

[0007] The distillation assembly includes two sets of fixing frames disposed on the top of the workbench. A heat-conducting film is disposed on the top of each set of fixing frames. A distillation flask is disposed on the top of the heat-conducting film. The inner wall of the distillation flask is connected to one end of the infusion tube. An alcohol lamp is disposed below the heat-conducting film. A regulating valve is disposed on the top of the distillation flask, and the inner wall of the regulating valve is connected to one end of the gas delivery tube.

[0008] The cooling assembly includes a water pump located on top of the water tank, with a water supply pipe connected to the outlet of the water pump. An outer frame is provided on the outside of the settling bottle, and an annular pipe is provided inside the outer frame. The inner wall of the annular pipe is connected to one end of the water supply pipe, and a return pipe is connected to the inner wall of the annular pipe. One end of the return pipe is connected to the inner wall of the water tank.

[0009] As a preferred embodiment of the distillation apparatus for synthesizing sanshool according to the present invention, the top of the fixed frame is fixed with two limiting blocks, the inner walls of the two limiting blocks are slidably connected with sliding rods, one side of the two limiting blocks is fixed with a first spring arranged horizontally, and one end of the first spring is fixed with a first clamping plate.

[0010] In a preferred embodiment of the distillation apparatus for synthesizing sanshool according to the present invention, the support has two sets of collars on its outer side, and the inner walls of the two sets of collars are threaded with lead screws. One end of the lead screw is fixed with a turntable, and the other end of the lead screw is rotatably connected to a second clamping plate.

[0011] In a preferred embodiment of the distillation apparatus for synthesizing sanshool according to the present invention, the inner wall of the first storage cabinet is fixed with a horizontally arranged partition, and a support plate for supporting the water tank is fixed on one side of the first storage cabinet.

[0012] In a preferred embodiment of the distillation apparatus for synthesizing sanshool according to the present invention, the top of the water storage tank is connected to a vertically arranged water inlet pipe, and one side of the water storage tank is connected to a horizontally arranged drain pipe.

[0013] In a preferred embodiment of the distillation apparatus for the synthesis of sanshool according to the present invention, the inner wall of the second storage cabinet is slidably connected to three sets of drawers, the interior of the three sets of drawers is provided with a first baffle, and the inner wall of the first baffle is slidably connected to a second baffle.

[0014] In a preferred embodiment of the distillation apparatus for synthesizing sanshool according to the present invention, the inner wall of the drawer is fixed with a limiting frame, the inner wall of the limiting frame is fixed with a second spring arranged horizontally, and one end of the second spring is fixed with a snap-fit ​​plate for snapping into the first baffle.

[0015] The beneficial effects of this utility model are as follows:

[0016] 1. The first and second storage cabinets can store the distillation equipment. The two sets of distillation components can improve the distillation efficiency of the device for sanshool. The support, settling bottle and delivery tube can effectively settle sanshool. The water tank and cooling components can cool the settling bottle. Thus, the purification efficiency of sanshool by this device is improved, avoiding the reduction in the purification efficiency of sanshool caused by the limited heating and condensation efficiency of existing distillation devices.

[0017] 2. The fixed frame supports the heat-conducting film, which in turn supports the distillation flask. The heat-conducting film ensures that the distillation flask is heated evenly. The multi-mouth design of the distillation flask allows for the purification of the sanshool raw material. The alcohol lamp heats the distillation flask, and the regulating valve adjusts the internal pressure of the distillation flask while also allowing harmful gases to be discharged.

[0018] 3. The water pump and water delivery pipe can transport cooling water from the storage tank. The outer frame can protect the annular pipe. The annular pipe can cool the sedimentation bottle from different angles, thereby improving the purification efficiency of sanshool. The return pipe can transport the cooling water back to the storage tank, realizing the purpose of water circulation and saving water resources. Attached Figure Description

[0019] To more clearly illustrate the technical solutions of the embodiments of this utility model, the drawings used in the description of the embodiments will be briefly introduced below. Obviously, the drawings described below are only some embodiments of this utility model. For those skilled in the art, other drawings can be obtained based on these drawings without creative effort. Among them:

[0020] Figure 1 This is a schematic diagram of the overall structure of the distillation apparatus used for the synthesis of sanshool.

[0021] Figure 2This is a structural diagram of the overall distillation components of a distillation apparatus used for the synthesis of sanshool.

[0022] Figure 3 This is a structural diagram of the cooling components of a distillation apparatus used for the synthesis of sanshool.

[0023] Figure 4 This is a structural diagram of the workbench of a distillation apparatus used for the synthesis of sanshool.

[0024] Figure 5 This is a diagram of the drawer structure of a distillation apparatus used for the synthesis of sanshool.

[0025] Figure 6 This is a structural diagram of the sedimentation flask in a distillation apparatus used for the synthesis of sanshool.

[0026] Numbered in the diagram: 1. Workbench; 2. First storage cabinet; 3. Second storage cabinet; 4. Distillation assembly; 41. Fixing frame; 42. Thermal conductive film; 43. Distillation flask; 44. Alcohol lamp; 45. Regulating valve; 5. Gas delivery pipe; 6. Exhaust pipe; 7. Activated carbon adsorption ring; 8. Support; 9. Settling bottle; 10. Infusion tube; 11. Water tank; 12. Cooling assembly; 121. Water pump; 122. Water delivery pipe; 123. Outer frame ; 124. Ring pipe; 125. Return pipe; 13. Limiting block; 14. Slide rod; 15. First spring; 16. First clamping plate; 17. Collar; 18. Lead screw; 19. Turntable; 20. Second clamping plate; 21. Partition plate; 22. Support plate; 23. Water inlet pipe; 24. Drain pipe; 25. Drawer; 26. First baffle; 27. Second baffle; 28. Limiting frame; 29. ​​Second spring; 30. Snap-fit ​​plate. Detailed Implementation

[0027] To make the above-mentioned objectives, features and advantages of this utility model more apparent and understandable, the specific embodiments of this utility model will be described in detail below with reference to the accompanying drawings.

[0028] Many specific details are set forth in the following description in order to provide a full understanding of the present invention. However, the present invention may also be implemented in other ways different from those described herein. Those skilled in the art can make similar extensions without departing from the spirit of the present invention. Therefore, the present invention is not limited to the specific embodiments disclosed below.

[0029] Secondly, the term "an embodiment" or "embodiment" as used herein refers to a specific feature, structure, or characteristic that may be included in at least one implementation of the present invention. The phrase "in one embodiment" appearing in different places in this specification does not necessarily refer to the same embodiment, nor is it a single or selective embodiment that excludes other embodiments.

[0030] Example 1:

[0031] Reference Figures 1-6 This is the first embodiment of the present invention. This embodiment provides a distillation apparatus for the synthesis of sanshool, including a workbench 1. The bottom of the workbench 1 is respectively provided with a first storage cabinet 2 and a second storage cabinet 3. The top of the workbench 1 is provided with two sets of distillation components 4 for distilling sanshool. The top of the two sets of distillation components 4 are connected to gas guide pipes 5. The top of the workbench 1 is provided with two sets of exhaust pipes 6, and the inner wall of the two sets of exhaust pipes 6 is connected to one end of the gas guide pipes 5. Activated carbon adsorption rings 7 are provided on the outer side of the two sets of exhaust pipes 6. The top of the workbench 1 is provided with a support 8. The top of the support 8 is provided with a sedimentation bottle 9. The top of the sedimentation bottle 9 is connected to two sets of infusion pipes 10. The bottom of the workbench 1 is provided with a water storage tank 11. The top of the water storage tank 11 is provided with a cooling component 12.

[0032] The workbench 1 facilitates the placement of the distillation equipment. The first storage cabinet 2 and the second storage cabinet 3 facilitate the storage of the distillation equipment. The distillation assembly 4 facilitates the distillation of sanshool raw materials. The gas guide pipe 5 facilitates the delivery of the gas generated during the distillation of sanshool raw materials to the exhaust pipe 6. The exhaust pipe 6 facilitates the discharge of the gas generated during the distillation of sanshool raw materials. The activated carbon adsorption ring 7 facilitates the purification of the gas generated during the distillation of sanshool raw materials. The support 8 facilitates the support of the settling bottle 9 and the outer frame 123. The settling bottle 9 facilitates the settling of sanshool. The infusion pipe 10 facilitates the delivery of the distilled sanshool to the settling bottle 9. The water tank 11 facilitates the supply of water to the cooling assembly 12. The cooling assembly 12 facilitates the cooling of the distilled sanshool.

[0033] The distillation assembly 4 includes two sets of fixing brackets 41 set on the top of the workbench 1. Each set of fixing brackets 41 is provided with a heat-conducting film 42 on its top. A distillation flask 43 is provided on the top of the heat-conducting film 42. The inner wall of the distillation flask 43 is connected to one end of the infusion tube 10. An alcohol lamp 44 is provided below the heat-conducting film 42. A regulating valve 45 is provided on the top of the distillation flask 43. The inner wall of the regulating valve 45 is connected to one end of the gas delivery tube 5.

[0034] By setting the fixing frame 41, the heat-conducting film 42 can be easily supported. By setting the heat-conducting film 42, the distillation flask 43 can be easily heated evenly. By setting the distillation flask 43, the sanshool raw material can be easily distilled. By setting the alcohol lamp 44, the distillation flask 43 can be easily heated. By setting the regulating valve 45, the gas pressure in the distillation flask 43 can be easily regulated, and the gas generated during the distillation of the sanshool raw material can be easily discharged into the gas guide tube 5.

[0035] The cooling assembly 12 includes a water pump 121 disposed on the top of the water storage tank 11. The outlet end of the water pump 121 is connected to a water supply pipe 122. An outer frame 123 is disposed on the outside of the settling bottle 9. An annular pipe 124 is disposed inside the outer frame 123. The inner wall of the annular pipe 124 is connected to one end of the water supply pipe 122. A return pipe 125 is connected to the inner wall of the annular pipe 124. One end of the return pipe 125 is connected to the inner wall of the water storage tank 11.

[0036] By setting up a water pump 121, water in the water storage tank 11 can be easily transported to the water delivery pipe 122. By setting up the water delivery pipe 122, water can be easily transported to the annular pipe 124. By setting up an outer frame 123, the annular pipe 124 can be easily protected. By setting up the annular pipe 124, the settling bottle 9 can be easily cooled. By setting up a return pipe 125, water can be easily transported to the water storage tank 11.

[0037] Example 2:

[0038] This is the second embodiment of the present invention, which is based on the previous embodiment.

[0039] Specifically, two limiting blocks 13 are fixed to the top of the fixing frame 41, and a sliding rod 14 is slidably connected to the inner wall of the two limiting blocks 13. A first spring 15 arranged horizontally is fixed to one side of the two limiting blocks 13, and a first clamping plate 16 is fixed to one end of the first spring 15.

[0040] By setting the limiting block 13, the slide bar 14 can be easily limited. By setting the slide bar 14, the first clamping plate 16 can be easily fixed. By setting the first spring 15, the first clamping plate 16 can be easily fixed to the distillation flask 43 by the reverse force.

[0041] Specifically, the outer side of the bracket 8 is provided with two sets of collars 17, and the inner walls of the two sets of collars 17 are threaded with lead screws 18. One end of the lead screw 18 is fixed with a turntable 19, and the other end of the lead screw 18 is rotatably connected to a second clamping plate 20.

[0042] By setting the collar 17, it is easy to limit the screw 18 and to fix the outer frame 123 and the settling bottle 9. By setting the screw 18, it is easy to drive the second clamping plate 20 to fix the collar 17. By setting the turntable 19, it is easy to drive the screw 18 to rotate.

[0043] Example 3:

[0044] This is the third embodiment of the present invention, which is based on the first two embodiments.

[0045] Specifically, the inner wall of the first storage cabinet 2 is fixed with a horizontally arranged partition 21, and a support plate 22 for supporting the water tank 11 is fixed on one side of the first storage cabinet 2.

[0046] By setting up the partition 21, the internal space of the first storage cabinet 2 can be easily divided, and by setting up the support plate 22, the water tank 11 can be easily supported.

[0047] Specifically, the top of the water storage tank 11 is connected to a vertically arranged water inlet pipe 23, and one side of the water storage tank 11 is connected to a horizontally arranged drain pipe 24.

[0048] By setting up the water inlet pipe 23, it is easy to pour cooling water into the water storage tank 11, and by setting up the drain pipe 24, it is easy to drain the water in the water storage tank 11.

[0049] Specifically, the inner wall of the second storage cabinet 3 is slidably connected to three sets of drawers 25, the interior of the three sets of drawers 25 is provided with a first baffle 26, and the inner wall of the first baffle 26 is slidably connected to a second baffle 27.

[0050] By setting up drawer 25, it is convenient to store distillation equipment. By setting up first baffle 26 and second baffle 27, it is convenient to divide the internal space of drawer 25, so that distillation equipment can be stored in categories.

[0051] Specifically, a limit frame 28 is fixed to the inner wall of drawer 25, and a second spring 29 is fixed to the inner wall of the limit frame 28. One end of the second spring 29 is fixed to a snap-fit ​​plate 30 for snapping into the first baffle 26.

[0052] By setting the limiting frame 28, the first baffle 26 can be easily limited. By setting the second spring 29, the snap-fit ​​plate 30 can be easily moved by the reverse force. By setting the snap-fit ​​plate 30, the first baffle 26 can be easily fixed.

[0053] In use, first pull the first clamping plate 16, then place the distillation flask 43 on the heat-conducting film 42. Then release the first clamping plate 16, which will clamp the distillation flask 43 through the reverse force of the first spring 15. Next, rotate the turntable 19, which drives the lead screw 18 to rotate. The lead screw 18 then moves the second clamping plate 20, which fixes the outer frame 123 and the settling bottle 9 to the support 8. Then, connect the distillation flask 43 and the settling bottle 9 through the infusion tube 10. Next, put the sanshool raw material into the distillation flask 43, and then heat the distillation flask 43 using an alcohol lamp 44. Simultaneously, the heat-conducting film 42 heats the distillation flask 43. 3. The sorbitol vapor is fully heated and enters the settling bottle 9 through the infusion pipe 10. Then, the water pump 121 is started, and the water pump 121 delivers the cooling water in the water storage tank 11 to the water delivery pipe 122. The water delivery pipe 122 delivers the cooling water to the ring pipe 124, thereby cooling the settling bottle 9. The distilled sorbitol falls into the measuring cylinder below due to gravity, thus completing the purpose of sorbitol distillation. During the distillation of sorbitol raw material, the gas generated by the sorbitol raw material is delivered to the gas guide pipe 5 by controlling the regulating valve 45. The gas is then delivered to the exhaust pipe 6 through the gas guide pipe 5. The gas is purified by the activated carbon adsorption ring 7 and finally discharged through the exhaust pipe 6.

[0054] It should be noted that the above embodiments are only used to illustrate the technical solution of this utility model and are not intended to limit it. Although this utility model has been described in detail with reference to preferred embodiments, those skilled in the art should understand that modifications or equivalent substitutions can be made to the technical solution of this utility model without departing from the spirit and scope of the technical solution of this utility model, and all such modifications or substitutions should be covered within the scope of the claims of this utility model.

Claims

1. A distillation apparatus for the synthesis of capsaicin comprising a workbench (1), characterized by: The bottom of the workbench (1) is respectively provided with a first storage cabinet (2) and a second storage cabinet (3), the top of the workbench (1) is provided with two groups of distillation assemblies (4) for distilling sanshool, the top of the two groups of distillation assemblies (4) is communicated with a gas guide pipe (5), the top of the workbench (1) is provided with two groups of exhaust pipes (6), the inner wall of the two groups of exhaust pipes (6) is communicated with one end of the gas guide pipe (5), the outer side of the two groups of exhaust pipes (6) is provided with an activated carbon adsorption ring (7), the top of the workbench (1) is provided with a support (8), the upper side of the support (8) is provided with a settling bottle (9), the top of the settling bottle (9) is communicated with two groups of infusion tubes (10), the lower side of the workbench (1) is provided with a water storage tank (11), the top of the water storage tank (11) is provided with a cooling assembly (12). The distillation assembly (4) comprises two groups of fixing frames (41) arranged on the top of the workbench (1), the top of the two groups of fixing frames (41) is provided with a heat-conducting film (42), the top of the heat-conducting film (42) is provided with a distillation bottle (43), the inner wall of the distillation bottle (43) is communicated with one end of the infusion tube (10), the lower side of the heat-conducting film (42) is provided with an alcohol lamp (44), the top of the distillation bottle (43) is provided with an adjusting valve (45), and the inner wall of the adjusting valve (45) is communicated with one end of the gas guide pipe (5). The cooling assembly (12) comprises a water pump (121) arranged on the top of the water storage tank (11), the water outlet end of the water pump (121) is communicated with a water delivery pipe (122), the outer side of the settling bottle (9) is provided with an outer frame (123), the inner side of the outer frame (123) is provided with an annular pipe (124), the inner wall of the annular pipe (124) is communicated with one end of the water delivery pipe (122), and the inner wall of the annular pipe (124) is communicated with a return pipe (125), and one end of the return pipe (125) is communicated with the inner wall of the water storage tank (11).

2. The distillation apparatus for synthesis of shogaol according to claim 1, characterized by: The top of the fixing frame (41) is fixed with two limiting blocks (13), the inner wall of the two limiting blocks (13) is slidably connected with a sliding rod (14), one side of the two limiting blocks (13) is fixed with a first spring (15) arranged transversely, and one end of the first spring (15) is fixed with a first clamping plate (16).

3. The distillation apparatus for synthesis of shogaol according to claim 1, characterized by: The outer side of the support (8) is provided with two groups of sleeve rings (17), the inner wall of the two groups of sleeve rings (17) is threadedly connected with a lead screw (18), one end of the lead screw (18) is fixed with a rotating disc (19), and the other end of the lead screw (18) is rotatably connected with a second clamping plate (20).

4. The distillation apparatus for synthesis of shogaol according to claim 1, characterized by: The inner wall of the first storage cabinet (2) is fixed with a transversely arranged partition plate (21), and one side of the first storage cabinet (2) is fixed with a supporting plate (22) for supporting the water storage tank (11).

5. The distillation apparatus for synthesis of shogaol according to Claim 1, characterized by: The top of the water storage tank (11) is communicated with a vertically arranged water inlet pipe (23), and one side of the water storage tank (11) is communicated with a transversely arranged water outlet pipe (24).

6. The distillation apparatus for synthesis of shogaol according to Claim 1, characterized by: The inner wall of the second storage cabinet (3) is slidably connected with three groups of drawers (25), the interiors of the three groups of drawers (25) are provided with first baffles (26), and the inner wall of the first baffle (26) is slidably connected with a second baffle (27).

7. The distillation apparatus for synthesis of shogaol according to claim 6, characterized by: The inner wall of the drawer (25) is fixedly connected with a limiting frame (28), the inner wall of the limiting frame (28) is fixedly connected with a transversely arranged second spring (29), one end of the second spring (29) is fixedly connected with a clamping plate (30) for clamping the first baffle (26).

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