Functional additive quantitative adding equipment based on nanoscale stabilization

By combining a stirring assembly, an ultrasonic oscillator, and a peristaltic pump in a nanoscale stabilization functional additive device, the problems of low quantitative accuracy and poor dispersion stability of nanoscale functional additives are solved, achieving high-precision quantitative addition and uniform dispersion, thus ensuring the stabilization of nanomaterials.

CN224252709UActive Publication Date: 2026-05-19HENAN XIONGMU BIOTECHNOLOGY CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
HENAN XIONGMU BIOTECHNOLOGY CO LTD
Filing Date
2025-04-18
Publication Date
2026-05-19

AI Technical Summary

Technical Problem

In existing technologies, the quantitative accuracy of nanoscale functional additives is low and the dispersion stability is poor. Traditional equipment is difficult to achieve high-precision control below the milligram level and uniform dispersion of nanomaterials.

Method used

The pretreatment tank employs a stirring assembly, an ultrasonic oscillator, and a peristaltic pump combined with a PID controller. Quantitative control is achieved through the peristaltic pump, and multiple dispersions are performed using the ultrasonic oscillator and ultrasonic transducer. Combined with a microporous ceramic coating to reduce flow resistance, uniform dispersion and stabilization of nanomaterials are achieved.

Benefits of technology

This method achieves high-precision quantitative addition and uniform dispersion of functional additives, ensuring the stabilization of nanomaterials and improving quantitative accuracy and dispersion stability.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model belongs to the technical field of quantitative adding equipment, and discloses functional additive quantitative adding equipment based on nanoscale stabilization, which comprises a pretreatment tank, a partition plate is fixedly mounted in the pretreatment tank, the pretreatment tank is divided into a pre-mixing cavity and a dispersion cavity by the partition plate, a pretreatment device is mounted in the pre-mixing cavity, and the dispersion cavity is mounted in the pre-mixing cavity. The pretreatment device comprises a stirring assembly and an ultrasonic oscillator, and a dynamic dispersion device is mounted on a partition plate; the quantitative control device comprises a peristaltic pump mounted on the pretreatment tank, a feeding pipe is mounted at the bottom of the peristaltic pump and communicated with the premixing cavity, a storage barrel is mounted at the top of the peristaltic pump, a mass flow meter is mounted on the feeding pipe, a PID (proportion integration differentiation) controller is mounted on the peristaltic pump, and the PID controller is communicated with the premixing cavity. And the peristaltic pump, the mass flow meter and the PID controller are communicated through a CAN bus. According to the utility model, nano materials can be conveniently and uniformly dispersed, the nano steady state of the nano materials can be ensured, and additives can be quantitatively added.
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Description

Technical Field

[0001] This utility model relates to the field of quantitative addition equipment technology, and in particular to a functional additive quantitative addition equipment based on nanoscale stabilization. Background Technology

[0002] The nanoscale stable functional additive quantitative addition equipment is an intelligent device that integrates nanomaterial dispersion, steady-state maintenance, and high-precision metering. It is specifically designed for the atomic-level precise addition and long-term stability control of functional additives (such as nanoparticles, liposomes, quantum dots, etc.) in industrial production.

[0003] Currently, the quantitative addition technology for nanoscale functional additives (such as nanoparticles, carbon nanotubes, quantum dots, etc.) faces the following problems:

[0004] 1) Low quantitative accuracy: Traditional equipment (such as screw extrusion and gravity dripping) is difficult to achieve high-precision control below the milligram level;

[0005] 2) Poor dispersion stability: Nanomaterials are prone to agglomeration due to van der Waals forces or electrostatic effects, resulting in insufficient uniformity of addition. Therefore, we propose a quantitative addition device for functional additives based on nanoscale stabilization. Utility Model Content

[0006] In order to overcome the defects of the prior art mentioned above, the inventors conducted in-depth research and, after a great deal of creative work, completed this utility model.

[0007] Specifically, the technical problem to be solved by this utility model is to provide a functional additive quantitative addition device based on nanoscale stabilization, so as to solve the existing technical problems of low quantitative accuracy and poor dispersion stability.

[0008] To solve the above-mentioned technical problems, the present invention provides the following technical solution:

[0009] A device for quantitative addition of functional additives based on nanoscale stabilization includes a pretreatment tank, a partition fixedly installed inside the pretreatment tank, the pretreatment tank being divided by the partition to form a premixing chamber and a dispersion chamber, a pretreatment device installed in the premixing chamber, the pretreatment device including a stirring assembly and an ultrasonic oscillator, and a dynamic dispersion device installed on the partition.

[0010] A quantitative control device includes a peristaltic pump installed on the pretreatment tank, a feed pipe installed at the bottom of the peristaltic pump and connected to the premixing chamber, a storage cylinder installed at the top of the peristaltic pump, a mass flow meter installed on the feed pipe, and a PID controller installed on the peristaltic pump. The peristaltic pump, the mass flow meter, and the PID controller communicate via a CAN bus.

[0011] As an improved technical solution, the bottom of the pretreatment tank is equipped with a discharge port, and the discharge port is connected to the dispersion chamber.

[0012] As an improved technical solution, the PID controller has a built-in viscosity-pressure mapping table, which can automatically adjust the pumping pressure according to the input viscosity value.

[0013] As an improved technical solution, the stirring assembly includes a stepper motor mounted on the pretreatment tank, a drive shaft vertically and rotatably mounted on the premixing chamber, the drive shaft being drivenly connected to the output shaft of the stepper motor, a stirring blade mounted on the drive shaft, and an ultrasonic oscillator mounted on the drive shaft and coaxially connected to the stirring blade.

[0014] As an improved technical solution, the dynamic dispersion device consists of several ultrasonic transducers installed on the partition plate, a dispersion tube installed on the partition plate, and a microporous ceramic coating coated on the dispersion tube.

[0015] As an improved technical solution, several ultrasonic transducers are equidistantly arranged along the axial / circumferential direction of the pretreatment tank.

[0016] As an improved technical solution, a spiral guide vane is installed on the inner wall of the dispersion tube.

[0017] After adopting the above technical solution, the beneficial effects of this utility model are:

[0018] 1. This utility model involves injecting functional additives into a storage cylinder and then starting a peristaltic pump. The peristaltic pump then injects the functional additives from the storage cylinder into a premixing chamber through a feed pipe. Simultaneously, a mass flow meter monitors the functional additives flowing into the premixing chamber. If the amount reaches a preset threshold, the mass flow meter transmits a signal to a PID controller, which then controls the peristaltic pump to stop operating. This achieves quantitative addition of the functional additives with high accuracy, making it convenient and precise for quantitative addition of functional additives.

[0019] 2. In this invention, by starting a stepper motor, an ultrasonic oscillator, and an ultrasonic transducer, the output shaft of the stepper motor drives the drive shaft to rotate, which in turn drives the stirring blades to rotate, thus dispersing the material at high speed through centrifugation. Simultaneously, the ultrasonic oscillator separates agglomerates, and the ultrasonic transducer further disperses the material. The material then flows into the dispersion chamber through the dispersion tube, where it undergoes a third dispersion by the spiral guide vanes. During this process, the microporous ceramic coating reduces flow resistance, thereby facilitating the uniform dispersion of nanomaterials and ensuring their nanoscale stability. Attached Figure Description

[0020] To more clearly illustrate the technical solutions of the embodiments of this utility model, the drawings used in the description of the embodiments will be briefly introduced below. Obviously, the drawings described below are only some embodiments of this utility model. For those skilled in the art, other drawings can be obtained based on these drawings without creative effort. Among them:

[0021] Figure 1 This is a schematic diagram of the overall main structure of this utility model.

[0022] Figure 2 This is a cross-sectional structural diagram of the present invention.

[0023] Figure 3 For the present utility model Figure 2 Enlarged structural diagram at point A in the middle.

[0024] Explanation of reference numerals in the attached figures:

[0025] In the diagram: 1. Pretreatment tank; 101. Baffle plate; 102. Premixing chamber; 103. Dispersion chamber; 104. Discharge port; 2. Peristaltic pump; 3. Feed pipe; 4. Storage cylinder; 5. Mass flow meter; 6. PID controller; 7. Stepper motor; 8. Drive shaft; 9. Stirring blade; 10. Ultrasonic oscillator; 11. Ultrasonic transducer; 12. Dispersion tube. Detailed Implementation

[0026] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0027] It should be noted that all directional indicators (such as up, down, left, right, front, back, etc.) in this utility model embodiment are only used to explain the relative positional relationship and movement of each component in a certain specific posture (as shown in the figure). If the specific posture changes, the directional indicator will also change accordingly.

[0028] Meanwhile, the meaning of "and / or" or "and / or" appearing throughout the text is that it includes three options. Taking "A and / or B" as an example, it includes option A, option B, or an option that satisfies both A and B.

[0029] Furthermore, in this utility model, descriptions involving "first," "second," etc., are for descriptive purposes only and should not be construed as indicating or implying their relative importance or implicitly specifying the number of technical features indicated. Therefore, a feature defined with "first" or "second" may explicitly or implicitly include at least one of that feature. Additionally, the technical solutions of the various embodiments can be combined with each other, but only on the basis of being achievable by those skilled in the art. When the combination of technical solutions is contradictory or impossible to implement, such a combination of technical solutions should be considered non-existent and not within the scope of protection claimed by this utility model.

[0030] Reference Figures 1-3 A device for quantitatively adding functional additives based on nanoscale stabilization is provided. This device includes a pretreatment tank 1, with a partition 101 fixedly installed inside. The pretreatment tank 1 is divided by the partition 101 to form a premixing chamber 102 and a dispersion chamber 103. A discharge port 104 is installed at the bottom of the pretreatment tank 1 and is connected to the dispersion chamber 103 to facilitate material discharge. A pretreatment device is installed in the premixing chamber 102, which includes a stirring assembly and an ultrasonic oscillator 10. The stirring assembly includes a stepper motor 7 mounted on the pretreatment tank 1, and a drive shaft 8 is vertically and rotatably mounted in the premixing chamber 102. The drive shaft 8 is connected to the output shaft of the stepper motor 7. The drive shaft 8 is equipped with a stirring blade 9. The ultrasonic oscillator 10 is installed on the drive shaft 8 and is coaxially connected with the stirring blade 9. A dynamic dispersion device is installed on the partition 101. The dynamic dispersion device consists of several ultrasonic transducers 11 installed on the partition 101, a dispersion tube 12 installed on the partition 101, and a microporous ceramic coating coated on the dispersion tube 12. Several ultrasonic transducers 11 are equidistantly arranged along the axial / circumferential direction of the pretreatment tank 1. A spiral guide plate is installed on the inner wall of the dispersion tube 12. Through centrifugal-ultrasonic synergistic deagglomeration and eddy current dispersion technology, the nanomaterials can be dispersed multiple times while ensuring nano-stabilization.

[0031] The quantitative control device includes a peristaltic pump 2 installed on the pretreatment tank 1. A feed pipe 3 is installed at the bottom of the peristaltic pump 2 and is connected to the premixing chamber 102. A storage cylinder 4 is installed at the top of the peristaltic pump 2. A mass flow meter 5 is installed on the feed pipe 3. A PID controller 6 is installed on the peristaltic pump 2. The peristaltic pump 2, the mass flow meter 5, and the PID controller 6 communicate via a CAN bus. The PID controller 6 has a built-in viscosity-pressure mapping table and can automatically adjust the pumping pressure according to the input viscosity value. By using the peristaltic pump 2 and the mass flow meter 5 together, precise and quantitative addition can be achieved.

[0032] In practical use, an appropriate amount of nanomaterials is injected into the pretreatment tank 1 through the storage cylinder 4 and the feed pipe 3. Then, functional additives are injected into the storage cylinder 4. The peristaltic pump 2 is then started. At this time, the peristaltic pump 2 injects the functional additives in the storage cylinder 4 into the premixing chamber 102 through the feed pipe 3. At the same time, the mass flow meter 5 monitors the functional additives flowing into the premixing chamber 102. If the amount of additives reaches the preset threshold, the mass flow meter 5 transmits the signal to the PID controller 6, and the PID controller 6 controls the peristaltic pump 2 to stop running, so as to achieve quantitative addition of functional additives with high quantitative accuracy. This facilitates the quantitative addition of functional additives with high quantitative accuracy.

[0033] Simultaneously, by activating the stepper motor 7, ultrasonic oscillator 10, and ultrasonic transducer 11, the output shaft of the stepper motor 7 drives the drive shaft 8 to rotate, which in turn drives the stirring blade 9 to rotate, thus performing a high-speed centrifugal primary dispersion of the material. Simultaneously, the ultrasonic oscillator 10 separates agglomerates, and the ultrasonic transducer 11 performs a secondary dispersion. The material then flows into the dispersion chamber 103 through the dispersion tube 12, where it undergoes a tertiary dispersion by the spiral guide vanes. During this process, the microporous ceramic coating reduces flow resistance, facilitating uniform dispersion of nanomaterials and ensuring their nanoscale stability. This device not only facilitates uniform dispersion of nanomaterials and ensures their nanoscale stability but also allows for the quantitative addition of additives with high precision.

[0034] It should be understood that these embodiments are for illustrative purposes only and are not intended to limit the scope of protection of this utility model. Furthermore, it should be understood that after reading the technical description of this utility model, those skilled in the art can make various alterations, modifications, and / or variations to this utility model, and all such equivalent forms also fall within the scope of protection defined by the appended claims.

Claims

1. A device for quantitatively adding functional additives based on nanoscale steady-state processing, characterized in that: include: A pretreatment tank (1) is fixedly installed inside the pretreatment tank (1). The pretreatment tank (1) is divided by the partition (101) to form a premixing chamber (102) and a dispersion chamber (103). A pretreatment device is installed inside the premixing chamber (102). The pretreatment device includes a stirring assembly and an ultrasonic oscillator (10). A dynamic dispersion device is installed on the partition (101). A quantitative control device is provided, comprising a peristaltic pump (2) installed on the pretreatment tank (1), a feed pipe (3) installed at the bottom of the peristaltic pump (2) and connected to the premixing chamber (102), a storage cylinder (4) installed at the top of the peristaltic pump (2), a mass flow meter (5) installed on the feed pipe (3), and a PID controller (6) installed on the peristaltic pump (2). The peristaltic pump (2), the mass flow meter (5) and the PID controller (6) communicate via a CAN bus.

2. The functional additive quantitative addition device based on nanoscale stabilization according to claim 1, characterized in that: The pretreatment tank (1) is equipped with a discharge port (104) at the bottom, and the discharge port (104) is connected to the dispersion chamber (103).

3. The functional additive quantitative addition device based on nanoscale stabilization according to claim 1, characterized in that: The PID controller (6) has a built-in viscosity-pressure mapping table, which can automatically adjust the pumping pressure according to the input viscosity value.

4. The functional additive quantitative addition device based on nanoscale stabilization according to claim 1, characterized in that: The stirring assembly includes a stepper motor (7) mounted on the pretreatment tank (1), a drive shaft (8) vertically and rotatably mounted on the premixing chamber (102), the drive shaft (8) being connected to the output shaft of the stepper motor (7), a stirring blade (9) mounted on the drive shaft (8), and an ultrasonic oscillator (10) mounted on the drive shaft (8) and coaxially connected to the stirring blade (9).

5. The functional additive quantitative addition device based on nanoscale stabilization according to claim 1, characterized in that: The dynamic dispersion device consists of a plurality of ultrasonic transducers (11) installed on the partition (101), a dispersion tube (12) installed on the partition (101), and a microporous ceramic coating coated on the dispersion tube (12).

6. The functional additive quantitative addition device based on nanoscale stabilization according to claim 5, characterized in that: Several of the ultrasonic transducers (11) are equidistant along the axial / circumferential direction of the pretreatment tank (1).

7. The functional additive quantitative addition device based on nanoscale stabilization according to claim 5, characterized in that: The inner wall of the dispersion tube (12) is equipped with a spiral guide plate.