An extraction separation device for fine chemical production
By integrating extraction and solid-liquid separation functions, the problem of forced dehydration of materials after extraction in existing technologies has been solved, achieving efficient extraction and solid-liquid separation, and reducing equipment costs and plant area.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- ZIBO KERUN CHEMICAL TECHNOLOGY CO LTD
- Filing Date
- 2025-05-13
- Publication Date
- 2026-06-09
AI Technical Summary
In current fine chemical production, the material cannot be forcibly dehydrated after extraction, which leads to increased equipment purchases, higher costs, and larger plant area. At the same time, the material is easily contaminated during transportation, affecting the utilization value of the product.
Design a device that integrates extraction and solid-liquid separation functions. The device uses a rotating rod to drive the material placement assembly to rotate for extraction and centrifugal separation, thereby achieving efficient solid-liquid separation of materials and reducing equipment procurement costs and plant area requirements.
It achieves improved extraction efficiency and integrated solid-liquid separation, reduces equipment procurement costs and plant area, and avoids pollution during material transfer.
Smart Images
Figure CN224331552U_ABST
Abstract
Description
Technical Field
[0001] This application belongs to the technical field of extraction and separation equipment, specifically relating to an extraction and separation device for fine chemical production. Background Technology
[0002] In the production of fine chemical products, it is often necessary to extract natural products through extraction methods, such as extracting fragrances, natural pigments, or effective components of traditional Chinese medicine from plants. This is usually done using extraction equipment.
[0003] Chinese patent publication CN222829102U discloses a low-temperature extraction device for traditional Chinese herbal plant juices. This device includes a tank with two positioning frames fixedly connected inside. An extraction tank is fixedly installed between the two positioning frames. A filter plate is fixedly connected to the bottom of the inner side of the extraction tank, and a docking groove is provided at the bottom of the extraction tank, with the top of the docking groove extending to the bottom of the filter plate. After the extraction process is completed, the material inside the extraction tank cannot be forcibly dehydrated, and the material still contains a certain amount of water. Furthermore, the concentration of extracts in this water is relatively high, requiring transfer to a separation device for solid-liquid separation. This not only increases the equipment purchase quantity and cost but also increases the plant area occupied, reducing the economic value per unit area of the plant. Simultaneously, the material is easily contaminated during transfer, rendering the separated liquid unusable. Utility Model Content
[0004] The technical problem to be solved by this application is to overcome the shortcomings of the prior art and provide an extraction and separation device for fine chemical production. This application integrates the two functions of extraction and solid-liquid separation, and performs centrifugal separation directly after extraction, thereby reducing the procurement cost of the entire production line and the plant area occupied.
[0005] The technical solution adopted by this application to solve its existing problems is:
[0006] An extraction and separation device for fine chemical production includes a tank, the top of which is provided with a material inlet and a drive device.
[0007] The tank body is equipped with a rotating rod coaxially inside, and a material placement assembly is connected to the rotating rod. The driving device drives the rotating rod to rotate.
[0008] The bottom of the tank is connected to a drain pipe.
[0009] Preferably, the rotating rod includes a rod body, the top of which extends to the outer side of the upper part of the tank and is connected to a driven gear, and a limit rod is coaxially connected to the lower part of the rod body, the limit rod driving the material placement assembly to rotate.
[0010] The output of the drive device drives the driven gear to rotate.
[0011] Preferably, the output shaft of the drive device is connected to a drive gear, which meshes with or is connected to a driven gear via a transmission belt.
[0012] Preferably, the horizontal cross-sectional shape of the limiting rod is polygonal.
[0013] The material placement assembly includes a sleeve that is fitted onto a limiting rod. The inner cavity of the sleeve has the same shape as the horizontal cross-sectional shape of the limiting rod. Several material cylinders are connected to the circumference of the sleeve via a connecting plate.
[0014] The material cylinder has an open top and several through holes on its surface.
[0015] Preferably, a baffle plate is provided on the outer side of the circumferential surface of the material cylinder.
[0016] Preferably, a slide bar is coaxially arranged above the driven gear.
[0017] The sleeve has several vertically arranged tie rods above it. The upper end of the tie rod passes through the driven gear. A sliding sleeve is fixed to the top of the tie rod and is sleeved on the sliding rod.
[0018] The top of the tank is fixed with a lifting drive assembly, which controls the sliding sleeve to move up and down.
[0019] Preferably, the lifting drive assembly includes a vertically arranged electric linear module, and the sliding part of the electric linear module is fixed with a semi-circular sleeve through a connecting rod, wherein the semi-circular sleeve is rotatably connected to the sliding sleeve.
[0020] Preferably, the bottom of the rotating rod is inserted into the support shaft, and the support shaft is rotatably connected to the bottom of the tank.
[0021] Preferably, the bottom of the tank is provided with a bearing hole, and a support shaft is connected inside the bearing hole through a bearing. Several drainage holes are arranged in a ring array around the bearing hole.
[0022] The bottom of the tank is equipped with a liquid collection tank, which is located directly below the drain hole, and the drain pipe is connected to the liquid collection tank.
[0023] Preferably, the material inlet at the top of the tank is covered with a removable cover.
[0024] Compared with the prior art, the beneficial effects of this application are as follows:
[0025] (1) The height of the material cylinder can be changed, thereby realizing the adjustment of the appropriate height of the material cylinder in the extraction operation and the material handling operation, which is more suitable for two different working conditions.
[0026] (2) By changing the rotation speed of the material placement assembly, the liquid stirring during the extraction process and the solid-liquid separation after the extraction are completed can be achieved. This can optimize the extraction efficiency and integrate the solid-liquid separation function, making one machine for two purposes and reducing the equipment purchase cost and the plant area occupied. Attached Figure Description
[0027] The present application will be further described below with reference to the accompanying drawings and embodiments.
[0028] Figure 1 This is a structural diagram of an extraction and separation device for fine chemical production according to this application.
[0029] Figure 2 This is a cross-sectional view of an extraction and separation device for fine chemical production according to this application.
[0030] Figure 3 for Figure 2 Enlarged view of a portion of point A in the middle.
[0031] Figure 4 This is a structural diagram of the rotating rod in an extraction and separation device for fine chemical production according to this application.
[0032] Figure 5 This is a structural diagram of the material placement assembly in an extraction and separation device for fine chemical production according to this application.
[0033] Figure 6 This is a structural diagram of a semi-circular ferrule in an extraction and separation device for fine chemical production according to this application.
[0034] Figure 7 This is a cross-sectional view of the support shaft in an extraction and separation device for fine chemical production according to this application.
[0035] In the diagram: 1-Tank body, 101-Drain hole, 2-Collection tank, 3-Drain pipe, 4-Removable cover plate, 5-Drive device, 6-Drive gear, 7-Rotating rod, 701-Rod body, 702-Driven gear, 703-Slide rod, 704-Limiting rod, 8-Material placement assembly, 801-Sleeve, 802-Connecting plate, 803-Material cylinder, 804-Break plate, 805-Pull rod, 806-Sliding sleeve, 9-Semi-circular ferrule, 901-Connecting rod, 10-Electric linear module, 11-Support shaft, 1101-Insertion hole, 1102-Limiting plate. Detailed Implementation
[0036] The attached figure shows the preferred embodiment of an extraction and separation device for fine chemical production. The following is a more detailed description of this application in conjunction with the attached figure.
[0037] Depend on Figures 1 to 7As shown, an extraction and separation device for fine chemical production includes a tank body 1. The top of the tank body 1 is provided with a material inlet / outlet and a drive device 5. A removable cover plate 4 is provided on the material inlet / outlet, and the drive device 5 is an electric motor. A drain pipe 3 is connected to the bottom of the tank body 1, and an electric shut-off valve is connected in series on the drain pipe 3.
[0038] The tank body 1 is equipped with a rotating rod 7 coaxially inside, and a material placement assembly 8 is connected to the rotating rod 7. The driving device 5 drives the rotating rod 7 to rotate.
[0039] Depend on Figure 4 As shown, in this embodiment, the rotating rod 7 includes a rod body 701. The top of the rod body 701 extends to the outer side of the upper part of the tank body 1 and is connected to a driven gear 702. A limiting rod 704 is coaxially connected to the lower part of the rod body 701. The limiting rod 704 drives the material placement assembly 8 to rotate, and the output end of the driving device 5 drives the driven gear 702 to rotate.
[0040] For the convenience of arranging the position of the drive device 5, the output shaft of the drive device 5 is connected to a drive gear 6, which meshes with the driven gear 702 or is connected via a transmission belt.
[0041] The horizontal cross-sectional shape of the limiting rod 704 is polygonal. Figure 5 As shown, the material placement assembly 8 includes a sleeve 801, which is sleeved on the limiting rod 704. The inner cavity shape of the sleeve 801 is the same as the horizontal cross-sectional shape of the limiting rod 704. Several material cylinders 803 are connected to the circumferential surface of the sleeve 801 through a connecting plate 802.
[0042] The material cylinder 803 has an open top and several through holes on its surface. In this embodiment, the granular solid material to be extracted is placed in a water-permeable bag, and then the bag is inserted into the material cylinder 803 through the open top. After the extraction is completed, the bag is removed from the material cylinder 803.
[0043] For ease of material handling, the material handling ports are arc-shaped, with at least two spaced-apart material handling ports located directly above the material cylinder 803 on the top surface of the tank body 1. Materials can be sequentially handled by rotating the material placement assembly 8.
[0044] To allow the material to immerse in the liquid and achieve immersion extraction, the material cylinder 803 is positioned as close as possible to the lower part of the tank 1 during the extraction operation. However, this position makes it inconvenient to load or unload the material. When loading or unloading, the material cylinder 803 should be closer to the loading / unloading port for easier operation. This necessitates that the material cylinder 803 can move vertically. To achieve this vertical movement, in this embodiment, a slide rod 703 is coaxially arranged above the driven gear 702.
[0045] The sleeve 801 is provided with several vertically arranged pull rods 805. The upper end of the pull rod 805 passes through the driven gear 702. The top of the pull rod 805 is fixed with a sliding sleeve 806, which is sleeved on the sliding rod 703.
[0046] A lifting drive assembly is fixed to the top of the tank body 1, which controls the up-and-down movement of the sliding sleeve 806. Further, the lifting drive assembly includes a vertically arranged electric linear module 10. The sliding part of the electric linear module 10 is fixed with a semi-circular retaining sleeve 9 via a connecting rod 901. The semi-circular retaining sleeve 9 is rotatably connected to the sliding sleeve 806. Specifically, the upper and lower ends of the sliding sleeve 806 are provided with limiting rings with larger outer diameters, and the semi-circular retaining sleeve 9 is engaged between the two limiting rings.
[0047] Thus, during the extraction process, the drive device 5 drives the material placement assembly 8 to rotate via the rotating rod 7, with the rotation speed controlled at 40-100 r / min. This agitates the liquid during extraction, ensuring that the content of effective components extracted from different areas of the liquid is uniform, thereby improving extraction efficiency. To enhance the turbulence effect, a baffle plate 804 protrudes from the outer circumferential surface of the material cylinder 803.
[0048] After the extraction operation is completed, the drain pipe 3 is opened and the liquid flows out. However, when the liquid level inside the tank 1 is lower than that inside the material cylinder 803, the power of the drive device 5 is increased and the rotation speed of the material placement assembly 8 is increased to more than 1000 r / min. The material inside the material cylinder 803 is spun dry by centrifugal force to achieve solid-liquid separation.
[0049] In order to support the rotating rod 7, in this embodiment, the bottom of the rotating rod 7 is inserted into the support shaft 11, and the support shaft 11 is rotatably connected to the bottom of the tank body 1.
[0050] The tank body 1 has a bearing hole at its bottom, and a support shaft 11 is connected to the bearing hole through a bearing. Several drain holes 101 are arranged in a circular array around the bearing hole. The tank body 1 has a liquid collection tank 2 at its bottom, which is located directly below the drain holes 101. The drain pipe 3 is connected to the liquid collection tank 2.
[0051] Depend on Figure 7As shown, the top surface of the support shaft 11 is recessed with an insertion hole 1101, the bottom of the limiting rod 704 is inserted into the insertion hole 1101, and a limiting plate 1102 is provided on the circumferential surface of the support shaft 11, which is placed above the bearing hole.
[0052] An electric heating device is installed inside the tank 1 to achieve high-temperature extraction.
[0053] The embodiments of this application have been described in detail above with reference to the accompanying drawings. However, this application is not limited to the above embodiments. Within the scope of knowledge possessed by those skilled in the art, various changes can be made without departing from the spirit of this application.
Claims
1. An extraction and separation device for fine chemical production, comprising a tank (1), characterized in that: The tank (1) is provided with a material loading and unloading port and a driving device (5) at the top. The tank body (1) is coaxially provided with a rotating rod (7), and a material placement assembly (8) is connected to the rotating rod (7). The driving device (5) drives the rotating rod (7) to rotate. The bottom of the tank (1) is connected to a drain pipe (3).
2. The extraction and separation device for fine chemical production according to claim 1, characterized in that: The rotating rod (7) includes a rod body (701), the top of the rod body (701) extends to the outer side of the upper part of the tank body (1) and is connected to a driven gear (702), and a limit rod (704) is coaxially connected to the lower part of the rod body (701). The limit rod (704) drives the material placement assembly (8) to rotate. The output end of the drive device (5) drives the driven gear (702) to rotate.
3. The extraction and separation device for fine chemical production according to claim 2, characterized in that: The output shaft of the drive device (5) is connected to a drive gear (6), which meshes with the driven gear (702) or is connected via a transmission belt.
4. An extraction and separation device for fine chemical production according to claim 2 or 3, characterized in that: The horizontal cross-sectional shape of the limiting rod (704) is polygonal; The material placement assembly (8) includes a sleeve (801), which is sleeved on a limiting rod (704). The inner cavity shape of the sleeve (801) is the same as the horizontal cross-sectional shape of the limiting rod (704). Several material cylinders (803) are connected to the circumferential surface of the sleeve (801) through a connecting plate (802). The material cylinder (803) is open at the top and has several through holes on its surface.
5. The extraction and separation device for fine chemical production according to claim 4, characterized in that: The material cylinder (803) has a baffle plate (804) protruding from the outer side of its circumference.
6. The extraction and separation device for fine chemical production according to claim 4, characterized in that: A slide rod (703) is coaxially arranged above the driven gear (702); The sleeve (801) is provided with several vertically arranged pull rods (805), the upper end of the pull rods (805) passes through the driven gear (702), and a sliding sleeve (806) is fixed on the top of the pull rods (805), which is sleeved on the sliding rod (703). The top of the tank (1) is fixed with a lifting drive assembly, which controls the sliding sleeve (806) to move up and down.
7. The extraction and separation device for fine chemical production according to claim 6, characterized in that: The lifting drive assembly includes a vertically arranged electric linear module (10). The sliding part of the electric linear module (10) is fixed with a semi-circular sleeve (9) through a connecting rod (901). The semi-circular sleeve (9) is rotatably connected to the sliding sleeve (806).
8. An extraction and separation apparatus for fine chemical production according to any one of claims 1-3 or 5-7, characterized in that: The bottom of the rotating rod (7) is inserted into the support shaft (11), and the support shaft (11) is rotatably connected to the bottom of the tank (1).
9. The extraction and separation device for fine chemical production according to claim 8, characterized in that: The bottom of the tank (1) is provided with a bearing hole, and a support shaft (11) is connected inside the bearing hole through a bearing. Several drain holes (101) are arranged in a ring array around the bearing hole. The tank body (1) has a liquid collection tank (2) at the bottom. The liquid collection tank (2) is located directly below the drain hole (101). The drain pipe (3) is connected to the liquid collection tank (2).
10. An extraction and separation apparatus for fine chemical production according to any one of claims 1-3, 5-7, or 9, characterized in that: The top of the tank (1) is covered with a removable cover plate (4).