A pet shower ointment containing natural deodorizing extract and having a lasting fragrance and a preparation method thereof

Abstract

The present invention belongs to the field of pet deodorization, and specifically relates to a pet shower ointment containing a natural deodorizing extract and having a lasting fragrance, and a preparation method thereof. The raw materials of the pet shower ointment include: persimmon extract, silica, emulsifier, antioxidant, hard water ion chelating agent, thickener and solubilizing agent. The preparation method includes first mixing persimmon extract and silica to obtain solution A; mixing coconut oil, olive oil and glycerin to obtain solution B; then adding sodium polyacrylate and microcrystalline cellulose into water and dissolving; adding a hard water ion chelating agent and mixing to obtain a mixed solution; finally, adding the mixed solution to solution A and solution B, mixing, cooling, adding an antioxidant, and stirring to obtain. The persimmon extract and silica of the present invention have a good effect of promoting removal and have good application prospects.

Description

Technical Field

[0001] The invention belongs to the field of pet deodorization, and particularly relates to a pet shower ointment containing a natural deodorizing extract and having a lasting fragrance, and a preparation method thereof. Background Art

[0002] Pet odors, such as feces, urine, pet body odor, cat litter odor, etc., not only affect the quality of life of pet owners, but also greatly affect the physical health of pets and pet owners, such as affecting the respiratory system, immune system, etc. It is a problem that every pet lover wants to solve. Not only that, the odor of pets will also have a negative impact on our living environment.

[0003] To solve this problem, many people choose to use pet deodorizers. Pet deodorizers are household products specifically designed to remove pet odors. They can neutralize or mask pet body odor by releasing a special fragrance, making the air fresh and pleasant. Pet deodorizers usually contain ingredients that can deeply remove odors, such as deodorizing enzymes, fungicides, and fragrances. These ingredients can effectively eliminate the odor emitted by pets and make the indoor environment more pleasant.

[0004] Chinese invention patent application CN105724439A discloses a pet disinfection and deodorant, which includes dioctadecyl dimethyl ammonium chloride, didecyl dimethyl ammonium chloride, benzalkonium bromide, glutaraldehyde, pure plant extract, plant essential oil, and distilled water. The deodorant has a significant disinfection and deodorization effect. It can be sprayed on pet cages, urine, and feces, or sprayed in the air on parts that need disinfection and deodorization, which can play a role in disinfection and deodorization and eliminate odor. However, it contains chemical disinfection ingredients, and long-term use has great side effects.

[0005] The Chinese invention patent application CN108245449A discloses a pet deodorant, which contains linalool acetate, citronellol, phenylethyl alcohol, p-chloro-m-xylenol, lauryl methacrylate, camphor extract, polysorbate, citric acid, essence, alcohol, and deionized water. The deodorant can be directly sprayed on the pet, has a significant deodorizing effect, lasts for a long time, and has a bactericidal effect.

[0006] The prior art has done some research on pet deodorization, but the deodorization fragrance retention time needs to be further improved, and the effect on the hair and skin of animals has not been improved. Summary of the invention

[0007] In order to overcome the deficiencies of the prior art, the present invention provides a pet shower ointment containing a natural deodorizing extract and having a long-lasting fragrance, and a preparation method thereof.

[0008] The purpose of the present invention is achieved through the following technical solutions:

[0009] A pet shower ointment containing natural deodorizing extract and having a lasting fragrance. The raw materials of the pet shower ointment include: persimmon extract, silica, emulsifier, antioxidant, hard water ion chelating agent, thickener and solubilizer.

[0010] Furthermore, the emulsifier is microcrystalline wax.

[0011] Furthermore, the antioxidant is selected from tocopherol and ascorbic acid, and the solubilizer is glycerol.

[0012] Furthermore, the hard water ion chelating agent includes disodium EDTA; and the thickener is selected from one or more of sodium polyacrylate, microcrystalline cellulose, coconut oil and olive oil.

[0013] Furthermore, the thickener comprises a mixture of sodium polyacrylate, microcrystalline cellulose, coconut oil and olive oil in a mass ratio of 5-10:1-5:1-5:1-5.

[0014] Furthermore, the raw materials of the pet shower gel include, by weight: 5-15 parts of persimmon extract, 0.1-1 parts of silica, 0.1-0.5 parts of emulsifier, 0.1-10 parts of antioxidant, 0.1-0.5 parts of hard water ion chelating agent, 1-10 parts of thickener and 10-30 parts of solubilizer.

[0015] Furthermore, the raw materials of the pet shower gel also include 0.1-5 parts of preservatives, 30-50 parts of flavors, and 10-40 parts of solvents.

[0016] Another object of the present invention is to provide a method for preparing the above-mentioned pet shower gel, comprising the following steps:

[0017] (1) Mixing persimmon extract and silica, or persimmon extract, silica and essence to obtain solution A; mixing coconut oil, olive oil, glycerin and emulsifier to obtain solution B;

[0018] (2) adding sodium polyacrylate and microcrystalline cellulose into water and dissolving them; adding hard water ion chelating agent and mixing to obtain a mixed solution;

[0019] (3) Add the mixed solution to solution A and solution B, mix, cool, add antioxidant, and stir to obtain.

[0020] Furthermore, the dissolving in step (2) is performed by first stirring and dispersing, then heating to 82-88°C for complete dissolution, and maintaining the temperature for 13-18 minutes; the mixing is performed by continuing to stir at the constant temperature for 2-5 minutes, and then cooling to 62-68°C.

[0021] Preferably, the mixing in step (3) is performed by constant temperature stirring for 1-5 minutes, the cooling is performed by dropping the temperature to 40-60° C., and the stirring time is 5-15 minutes.

[0022] Beneficial effects of the present invention:

[0023] (1) After the pet uses the shower gel of the present invention for 12 hours, the fragrance on the pet's body is strong, harmonious, and lasts for a long time; after the sample is used for 48 hours, the fragrance on the pet's body is relatively strong, harmonious, and lasts for a long time; after the sample is used for 72 hours to 96 hours, the fragrance on the pet's body is slightly lighter and has no odor; this shows that the samples of Examples 1-3 have a 96-hour cleaning and deodorizing effect with a long-lasting fragrance. The study also shows that the persimmon extract and silica in the formula have a good synergistic effect in promoting deodorization and lasting fragrance.

[0024] (2) After using the showerhead perfume of the present invention for 7 days continuously, the pet's hair becomes shiny and fine, hair loss is reduced, and the skin becomes smooth and moist, having a good moisturizing effect. BRIEF DESCRIPTION OF THE DRAWINGS

[0025] Figure 1 The softening and hair removal of the pet hair in Example 1 are shown.

[0026] Figure 2 This is the softening and depilatory condition of the pet hair in Comparative Example 1.

[0027] Figure 3 This is the sebum condition on pet hair under a microscope in Example 1.

[0028] Figure 4 This is the sebum condition on pet hair under a microscope in Comparative Example 1.

[0029] Figure 5 This is the pet skin moisture condition in Example 1.

[0030] Figure 6 This is the pet skin moisturizing condition of Comparative Example 1. DETAILED DESCRIPTION

[0031] The technical solution of the present invention is further described below in conjunction with embodiments.

[0032] Example 1

[0033] The pet shower ointment of this embodiment is composed of the following components by weight, and the raw materials thereof are all conventional commercially available raw materials, and the suppliers thereof are shown in Table 1 below, but are not limited thereto.

[0034] Table 1

[0035]

[0036] The preparation method is as follows:

[0037] (1) Mixing persimmon extract, silica and essence to obtain solution A; mixing coconut oil, olive oil, glycerin, emulsifier and preservative to obtain solution B;

[0038] (2) Add sodium polyacrylate and microcrystalline cellulose to water, stir and disperse, then heat to 85°C to dissolve completely, and keep the temperature constant for 15 minutes; add hard water ion chelating agent, continue to stir at the constant temperature for 3 minutes, and then cool to 65°C to obtain a mixed solution;

[0039] (3) Add the mixed solution to solution A and solution B, continue stirring at a constant temperature for 3 minutes, then cool to 50°C, add tocopherol and ascorbic acid, and stir for 10 minutes.

[0040] Example 2

[0041] The pet shower balm of this embodiment is composed of the following components (source as in Example 1) in parts by weight, as shown in Table 2.

[0042] Table 2

[0043]

[0044] The preparation method is as follows:

[0045] (1) Mixing persimmon extract, silica and essence to obtain solution A; mixing coconut oil, olive oil, glycerin, emulsifier and preservative to obtain solution B;

[0046] (2) Add sodium polyacrylate and microcrystalline cellulose to water, stir and disperse, then heat to 82°C to dissolve completely, and keep the temperature constant for 18 minutes; add hard water ion chelating agent, continue to stir at the constant temperature for 5 minutes, and then cool to 65°C to obtain a mixed solution;

[0047] (3) Add the mixture to solution A and solution B, continue stirring at a constant temperature for 3 minutes, then cool to 40°C, add tocopherol and ascorbic acid, and stir for 10 minutes.

[0048] Example 3

[0049] The pet shower balm of this embodiment is composed of the following components (source as in Example 1) in parts by weight, as shown in Table 3.

[0050] Table 3

[0051]

[0052] The preparation method is as follows:

[0053] (1) Mixing persimmon extract, silica and essence to obtain solution A; mixing coconut oil, olive oil, glycerin, emulsifier and preservative to obtain solution B;

[0054] (2) Add sodium polyacrylate and microcrystalline cellulose to water, stir and disperse, then heat to 88°C to dissolve completely, and keep the temperature constant for 13 minutes; add hard water ion chelating agent, continue to stir at the constant temperature for 2 minutes, and then cool to 68°C to obtain a mixed solution;

[0055] (3) Add the mixture to solution A and solution B, continue stirring at a constant temperature for 3 minutes, then cool to 60°C, add tocopherol and ascorbic acid, and stir for 10 minutes.

[0056] Comparative Example 1

[0057] The pet shower ointment of this comparative example is composed of the following components (source as in Example 1) in parts by weight, as shown in Table 4.

[0058] Table 4

[0059]

[0060] The preparation method is as follows:

[0061] (1) Mix persimmon extract and essence to obtain solution A; mix coconut oil, olive oil, glycerin, emulsifier and preservative to obtain solution B;

[0062] (2) Add sodium polyacrylate and microcrystalline cellulose to water, stir and disperse, then heat to 85°C to dissolve completely, and keep the temperature constant for 15 minutes; add hard water ion chelating agent, continue to stir at the constant temperature for 3 minutes, and then cool to 65°C to obtain a mixed solution;

[0063] (3) Add the mixed solution to solution A and solution B, continue stirring at a constant temperature for 3 minutes, then cool to 50°C, add tocopherol and ascorbic acid, and stir for 10 minutes.

[0064] Comparative Example 2

[0065] The comparative pet shower ointment is composed of the following components (source as in Example 1) in parts by weight, as shown in Table 5.

[0066] Table 5

[0067]

[0068] The preparation method is as follows:

[0069] (1) Mix silica and essence to obtain solution A; mix coconut oil, olive oil, glycerin, emulsifier and preservative to obtain solution B;

[0070] (2) Add sodium polyacrylate and microcrystalline cellulose to water, stir and disperse, then heat to 85°C to dissolve completely, and keep the temperature constant for 15 minutes; add hard water ion chelating agent, continue to stir at the constant temperature for 3 minutes, and then cool to 65°C to obtain a mixed solution;

[0071] (3) Add the mixed solution to solution A and solution B, continue stirring at a constant temperature for 3 minutes, then cool to 50°C, add tocopherol and ascorbic acid, and stir for 10 minutes.

[0072] Comparative Example 3

[0073] The pet shower ointment of this comparative example is composed of the following components (source as in Example 1) in parts by weight, as shown in Table 6.

[0074] Table 6

[0075]

[0076] The preparation method is as follows:

[0077] (1) Mixing persimmon extract, silica and essence to obtain solution A; mixing coconut oil, glycerin, emulsifier and preservative to obtain solution B;

[0078] (2) Add sodium polyacrylate and microcrystalline cellulose to water, stir and disperse, then heat to 85°C to dissolve completely, and keep the temperature constant for 15 minutes; add hard water ion chelating agent, continue to stir at the constant temperature for 3 minutes, and then cool to 65°C to obtain a mixed solution;

[0079] (3) Add the mixed solution to solution A and solution B, continue stirring at a constant temperature for 3 minutes, then cool to 50°C, add tocopherol and ascorbic acid, and stir for 10 minutes.

[0080] Comparative Example 4

[0081] The composition is composed of the following components (source as in Example 1), as shown in Table 7.

[0082] Table 7

[0083]

[0084] The preparation method is as follows:

[0085] (1) Mixing persimmon extract, silica and essence to obtain solution A; mixing olive oil, glycerin, emulsifier and preservative to obtain solution B;

[0086] (2) Add sodium polyacrylate and microcrystalline cellulose to water, stir and disperse, then heat to 85°C to dissolve completely, and keep the temperature constant for 15 minutes; add hard water ion chelating agent, continue to stir at the constant temperature for 3 minutes, and then cool to 65°C to obtain a mixed solution;

[0087] (3) Add the mixed solution to solution A and solution B, continue stirring at a constant temperature for 3 minutes, then cool to 50°C, add tocopherol and ascorbic acid, and stir for 10 minutes.

[0088] Experiment 1: Experiment on the deodorizing and fragrance-retaining effects of the showerhead perfume of the present invention

[0089] This experiment applied pet shower ointment to New Zealand rabbits in different groups and observed the fragrance retention, skin and hair condition of the New Zealand rabbits over a certain period of time, so as to show whether the product has the effects of cleaning and deodorizing (long-lasting fragrance), moisturizing the skin and maintaining hair gloss.

[0090] 1.1 Experimental animals and breeding environment

[0091] Experimental animals: New Zealand rabbit, ordinary grade, New Zealand rabbit fur length: 3-4cm.

[0092] Animal certificate number: NO.430730241100192384.

[0093] Source of animals: purchased from Hunan Taiping Biotechnology Co., Ltd., the experimental animal production license number is: SCXK (Xiang) 2023-0011.

[0094] 1.2 Cleaning and deodorization (lasting fragrance) experimental steps

[0095] Experimental process: Use the shower heads of Examples 1-3 and Comparative Examples 1-4 to bathe New Zealand rabbits, shower the animals, thoroughly wash and dry their fur, observe the effect of removing dirt and odor, and making the animals clean and refreshed as a whole, and score the fragrance retention and fragrance degree of the animals at 12h, 48h, 72h, and 96h.

[0096] 1.3 Evaluation of cleaning and deodorization (lasting fragrance) results

[0097] The fragrance retention was scored by 10 researchers, and the scores were made 12-96 hours after using the product according to the fragrance retention scoring table in Table 8 below. The scoring results are shown in Table 9.

[0098] Table 8 Fragrance Retention Rating Table

[0099]

[0100] Table 9 Average score of fragrance retention

[0101]

[0102] Summary: After using the shower head of the present invention for 12 hours, the New Zealand rabbit has a strong, harmonious and lasting fragrance; after using the sample for 48 hours, the body fragrance is relatively strong, harmonious and lasting fragrance; after using the sample for 48 hours to 96 hours, the body fragrance is slightly lighter and has no odor; This shows that the samples of Examples 1-3 have a 96-hour cleaning and deodorizing effect with a long-lasting fragrance.

[0103] Experiment 2: Experiment on the effect of the shower gel of the present invention on skin and hair

[0104] Experimental process: 7 New Zealand rabbits with dry skin and rough hair were selected. 3 of them were bathed with the shower head of Example 1-3 every day. The pets were showered, their hair was thoroughly washed and blown dry. The shower head was used for 7 consecutive days. The 4 pets were subjected to the same operation with the shower heads of Comparative Examples 1, 2, 3, and 4 respectively. The hair glossiness was checked, and the hair of the animals was combed with a pet comb. The smoothness and hair removal of the pets' hair were compared. The sebum on the hair was observed under a microscope. On the 8th day, 3cm×3cm of the hair on both sides of the pet's spine was shaved off, and the moistness of the pet's skin was observed. The effects of using the shower heads of Example 1-3 and Comparative Example 1-4 are summarized in Table 10.

[0105] Table 10

[0106]

[0107] Among them, the pet hair situation of Example 1 is shown in Figure 1 The New Zealand rabbits using the shower head of the present invention have fine and shiny hair after 7 days of use, and only a few hairs fall out after combing; the hair condition of comparative example 1 is shown in Figure 2 ; The hair is shiny, and it falls off after combing, with slight hair loss;

[0108] Observe the sebum on the pet's hair under a microscope. Example 1: The hair cortex under a microscope is Figure 3 , under the microscope, there is basically no fine dandruff on the hair; under the microscope of comparative example 1, the hair cortex is Figure 4 , the hair has some fine dandruff.

[0109] Observe the moisture of the pet's skin. The results of Example 1 are shown in Figure 5 , 8 days after shaving, the skin is smooth and moist, the results of comparative example 1 are shown in Figure 6 , the skin is moist and not as smooth as in Example 1.

[0110] The above detailed description is a specific description of one feasible embodiment of the present invention. The embodiment is not intended to limit the patent scope of the present invention. Any equivalent implementation or modification that does not deviate from the present invention should be included in the scope of the technical solution of the present invention.

Claims

1. A pet shower ointment containing natural deodorant extract and having a long-lasting fragrance, characterized in that: The raw materials of the pet shower ointment include, by weight: 5-15 parts of persimmon extract, 0.1-1 parts of silica, 0.1-0.5 parts of emulsifier, 0.1-10 parts of antioxidant, 0.1-0.5 parts of hard water ion chelating agent, 1-10 parts of thickener and 10-30 parts of solubilizer; The thickener is a mixture of sodium polyacrylate, microcrystalline cellulose, coconut oil and olive oil in a mass ratio of 5-10:1-5:1-5:1-5; The emulsifier is microcrystalline wax.

2. The pet shower ointment according to claim 1, characterized in that: The antioxidants are tocopherol and ascorbic acid, and the solubilizer is glycerol.

3. The pet shower ointment according to claim 1, characterized in that: The hard water ion chelating agent includes disodium EDTA.

4. The pet shower ointment according to claim 1, characterized in that: The raw materials of the pet shower ointment further include 0.1-5 parts of preservatives, 30-50 parts of flavors and 10-40 parts of solvents by weight.

5. A method for preparing a pet shower gel containing a natural deodorizing extract and having a long-lasting fragrance according to claim 3, characterized in that: The steps include: (1) Mixing persimmon extract and silica to obtain solution A; mixing coconut oil, olive oil, a solubilizer and an emulsifier to obtain solution B; (2) adding sodium polyacrylate and microcrystalline cellulose into water and dissolving them; adding hard water ion chelating agent and mixing to obtain a mixed solution; (3) Add the mixed solution to solution A and solution B, mix, cool, add antioxidant, and stir to obtain.

6. A method for preparing a pet shower gel containing a natural deodorizing extract and having a long-lasting fragrance according to claim 4, characterized in that: The steps include: (1) Mix persimmon extract, silica and essence to obtain solution A; mix coconut oil, olive oil, solubilizer and emulsifier, and then add preservatives to obtain solution B; (2) adding sodium polyacrylate and microcrystalline cellulose into water and dissolving them; adding hard water ion chelating agent and mixing to obtain a mixed solution; (3) Add the mixed solution to solution A and solution B, mix, cool, add antioxidant, and stir to obtain.

7. The preparation method according to claim 5 or 6, characterized in that: The dissolving in step (2) is performed by first stirring and dispersing, then heating to 82-88°C for complete dissolution, and maintaining the temperature for 13-18 minutes; the mixing is performed by continuing to stir at the constant temperature for 2-5 minutes, and then cooling to 62-68°C.

8. The preparation method according to claim 5 or 6, characterized in that: The mixing in step (3) is performed by constant temperature stirring for 1-5 minutes, the cooling is performed by dropping the temperature to 40-60° C., and the stirring time is 5-15 minutes.

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