Vitamin K3 oxidation waste liquid recovery device based on glucose reduction

By introducing multiple detection devices and stirring devices into the vitamin K3 oxidation waste liquid recovery device, precise pH control and uniform mixing of the glucose reduction process are achieved, solving the problems of inaccurate monitoring and uneven mixing in the existing technology, improving reaction efficiency and product purity, and reducing the risk of environmental pollution.

CN120681814APending Publication Date: 2025-09-23YUNNAN LULIANG PEACE TECH CO LTD
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Patent Information

Application Number
CN202510938282.8
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-07-08
Publication Date
2025-09-23

AI Technical Summary

Technical Problem

The existing technology for treating glucose-reduced vitamin K3 oxidation waste liquid has problems such as inaccurate pH monitoring, uneven liquid mixing, and difficulty in adjusting the liquid dosage, resulting in low reaction efficiency, poor product purity, and the risk of environmental pollution.

Method used

A vitamin K3 oxidation waste liquid recovery device based on glucose reduction was designed. Multiple detection devices and comparison devices were used to monitor the pH value in real time. Combined with a stirring device and a proportional control valve, the dosage of reagents and waste liquid was precisely controlled to ensure reaction stability and uniformity.

Benefits of technology

The reaction stability and product purity are improved, the generation of by-products is avoided, the recovery efficiency is improved, the production cost is reduced and the risk of environmental pollution is reduced.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention discloses a vitamin K3 oxidation waste liquid recovery device based on glucose reduction, and relates to the technical field of waste liquid recovery, the recovery device comprises a tank body, a stirring device, a detection device, a comparison device, a medicament adding pipe, a glucose adding pipe and a waste liquid adding pipe, the tank body is connected with the stirring device, the tank body is connected with the detection device, and the tank body is connected with the comparison device. The tank body is connected with the comparison device, the comparison device is connected with the stirring device, the tank body is communicated with the agent feeding pipe, the tank body is communicated with the glucose feeding pipe, the tank body is communicated with the waste liquid feeding pipe, the comparison device is connected with the agent feeding pipe, the stirring device is arranged in the tank body, the detection devices and the comparison devices are arranged on the tank body, and a discharging pipe is arranged on the tank body. And the detection device is connected with the medicament adding pipe and the comparison device.
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Description

Technical Field

[0001] The present invention relates to the technical field of waste liquid recovery devices, in particular to a vitamin K3 oxidation waste liquid recovery device based on glucose reduction. Background Art

[0002] In the production process of vitamin K3, the treatment of oxidative waste liquid has always been a difficult problem to be solved in the industry.

[0003] When treating vitamin K3 oxidation wastewater from glucose reduction, traditional wastewater recovery devices often suffer from inaccurate pH monitoring and delayed control. This leads to side reactions during the reduction process, reducing recovery efficiency and product purity. Furthermore, uneven mixing of liquids within the device results in incomplete reactions, impacting the final recovery. Furthermore, the amount of liquid added is difficult to flexibly adjust based on actual reaction requirements, making over- or under-reaction more likely. This not only wastes resources but also poses a risk of environmental pollution. Therefore, a new vitamin K3 oxidation wastewater recovery device is urgently needed to improve the efficiency and quality of wastewater recovery and treatment. Summary of the Invention

[0004] The object of the present invention is to provide a vitamin K3 oxidation waste liquid recovery device based on glucose reduction to solve the problems raised in the prior art.

[0005] To achieve the above object, the present invention provides the following technical solutions: A vitamin K oxidation waste liquid recovery device based on glucose reduction, the recovery device includes a tank body, a stirring device, a detection device, a comparison device, a drug dosing pipe, a glucose dosing pipe and a waste liquid dosing pipe, the tank body is connected to the stirring device, the tank body is connected to the detection device, the tank body is connected to the comparison device, the comparison device is connected to the stirring device, the tank body is connected to the drug dosing pipe, the tank body is connected to the glucose dosing pipe, the tank body is connected to the waste liquid dosing pipe, the comparison device is connected to the drug dosing pipe, the stirring device is placed in the tank body, there are several detection devices, there are several comparison devices, a discharge pipe is provided on the tank body, the detection device is connected to the drug dosing pipe, and the detection device is connected to the comparison device.

[0006] The tank body is used as the main installation base for the installation and positioning of other components. Waste liquid is added to the tank body through the waste liquid addition pipe, glucose solution is added to the tank body through the glucose addition pipe, the pH value of the waste liquid in the tank body is detected by the detection device, and then the reagent addition pipe is controlled to add reagents according to the detection results to control the pH value. When the detection device detects that the pH value rises outside the controllable range, the detection device transmits a signal to the waste liquid addition pipe to lower the pH value by adding acidic waste liquid. When the detection device detects that the pH value drops outside the controllable range, the detection device transmits a signal to the reagent addition control pipe to add alkaline reagent to the reagent addition pipe to increase the pH value. Then the solution after reduction is completed is discharged through the discharge pipe.

[0007] Furthermore, a first mounting groove and a first mounting cavity are provided in the tank body. There are several first mounting grooves and several first mounting cavities. Detection devices are provided in several first mounting grooves, and comparison devices are provided in several first mounting cavities. The comparison device is connected to the first mounting cavity, and the detection device is fastened to the first mounting groove.

[0008] The plurality of first installation grooves are provided to provide installation positions for the plurality of detection devices, and the plurality of first installation cavities are provided to provide installation positions for the plurality of comparison devices, so that the detection devices can directly detect the pH value of the solution at various positions in the tank body, thereby improving the detection strength of the pH value of the solution.

[0009] Furthermore, the detection device includes a reference electrode, a glass electrode, a circuit amplifier, a signal processing device and a detection shell. The detection shell is fastened to the first mounting groove, the reference electrode is connected to the detection shell, the glass electrode is connected to the detection shell, a second mounting cavity is provided in the detection shell, the circuit amplifier is placed in the second mounting cavity, the signal processing device is placed in the second mounting cavity, the signal processing device is connected to the second mounting cavity, the glass electrode is connected to the circuit amplifier wire, the reference electrode is connected to the circuit amplifier wire, the circuit amplifier is electrically connected to the signal processing device, the signal processing device is connected to the drug dosing tube, and the signal processing device is connected to the comparison device.

[0010] The detection shell serves as the main installation basis for the installation of other components. The concentration of hydrogen ions in the solution in the tank is detected by the reference electrode and the glass electrode. The higher the concentration of hydrogen ions in the solution, the greater the current on the reference electrode and the glass electrode. The current signal detected by the reference electrode and the glass electrode is amplified by the circuit amplifier and then transmitted to the signal processing device. The signal is processed by the signal processing device to control the addition of the reagent dosing pipe and the waste liquid dosing pipe.

[0011] Furthermore, the signal processing device includes a first electromagnet, a first power-on switch, a sliding rheostat and a support frame, the first electromagnet and the second mounting cavity are fastened together, the first power-on switch and the first electromagnet are fastened together, the first electromagnet and the support frame are fastened together, the support frame and the second mounting cavity are fastened together, the sliding rheostat and the second mounting cavity are fastened together, the first power-on switch is provided with a first connecting groove and a second connecting groove, the support frame is provided with a third connecting groove, and the circuit amplifier and the first electromagnet are electrically connected.

[0012] The circuit amplifier provides current to the first electromagnet so that the first electromagnet can excite a magnetic field. At the same time, the first electromagnet serves as the main connection basis for connecting other components. The first power switch controls the presence or absence of current on the sliding rheostat. The supporting frame is provided so that the sliding rheostat can slide on the supporting frame. The first connecting groove, the second connecting groove and the third connecting groove provide an installation basis for other components.

[0013] Furthermore, the signal processing device also includes a detection magnet, a return spring, a blocking block, a connecting column and a first connecting switch. The detection magnet and the sliding rheostat are tightly connected, the detection magnet is placed in the third connecting slot, the detection magnet and the third connecting slot are slidingly connected, the detection magnet and the first connecting switch are tightly connected, the first connecting switch is placed in the first connecting slot, the first connecting switch and the first connecting slot are slidingly connected, the connecting column and the second connecting slot are slidingly connected, the connecting column is placed in the second connecting slot, the return spring and the sliding rheostat are tightly connected, the return spring is tightly connected to the blocking block at one end away from the sliding rheostat, the blocking block and the slider of the sliding rheostat are tightly connected, there are two sliding rheostats, detection magnets, return springs, blocking blocks, connecting columns and first connecting switches each and they are symmetrically distributed about the first power-on switch, the two sliding rheostats output ends are respectively connected to the drug addition pipe and the waste liquid addition pipe, and the two sliding rheostats output ends are connected to the comparison device.

[0014] One of the two return springs is in a compressed state, and the other is normally extended and retracted. The detection magnet connected to the return spring in the compressed state and the magnetic field excited by the first electromagnet repel each other, and the output end of the sliding rheostat on one side of the return spring in the compressed state is electrically connected to the waste liquid addition tube. The detection magnet connected to the return spring in the normal extended state and the magnetic field excited by the first electromagnet attract each other, and the output end of the sliding rheostat on one side of the return spring in the normal extended state is electrically connected to the drug addition tube. The current transmitted from the reference electrode and the glass electrode is amplified by the circuit amplifier, and then the amplified current controls the magnetic field excited by the first electromagnet. When the hydrogen ion concentration in the solution is low, the current flowing from the circuit amplifier to the first electromagnet decreases, and the intensity of the magnetic field excited by the first electromagnet decreases, so that the detection magnet that repels the magnetic field of the first electromagnet is affected by the elastic potential energy released by the return spring. The return spring releases elastic potential energy to drive the first connection switch to move so that the first connection switch and the first power-on switch are connected, so that the first power-on switch energizes the waste liquid feeding pipe, so that the waste liquid feeding pipe can add acidic waste liquid into the tank body, thereby lowering the pH value and increasing the hydrogen ion concentration, so that the oxidized waste liquid does not produce other products during the reduction process, thereby improving the stability of the reaction. When the hydrogen ion concentration in the solution is high, the current flowing from the circuit amplifier to the first electromagnet increases, so that the force on the detection magnet is enhanced, so that the detection magnet subjected to repulsion moves away from the first power-on switch, and the detection magnet subjected to attraction approaches the first power-on switch until the first power-on switch and the first connection switch are connected, thereby controlling the connected reagent feeding pipe to add alkaline reagent into the tank body, thereby raising the pH value and improving the stability of the solution in the tank body.

[0015] Furthermore, the comparison device includes a second electromagnet, a second power-on switch, a second connecting switch and a mounting shell. The mounting shell is placed in the first mounting cavity. The mounting shell and the first mounting cavity are tightly connected. The second electromagnet, the second power-on switch and the second connecting switch are placed in the first mounting cavity. The second electromagnet and the first mounting cavity are tightly connected. There are two second electromagnets. A second power-on switch is provided on the second electromagnet. The second power-on switch and the second electromagnet are tightly connected. The second connecting switch is placed between the two second electromagnets. The second connecting switch is slidably connected to the first mounting cavity. The two second electromagnets are electrically connected to different output ends of the sliding rheostat respectively. The second power-on switch is electrically connected to the stirring device.

[0016] By sliding the rheostat at different positions, the output current of the two second electromagnets is different, so that the magnetic fields excited by the second electromagnets are different. The two second electromagnets excite magnetic fields of different intensities, so that the second connection switch moves to the side with a stronger magnetic field. At the same time, a spring is provided in the first installation cavity, and the spring is used to reset the second connection switch. When the second connection switch moves to the side of the second power-on switch on the side with a stronger magnetic field and is connected to the second power-on switch, the second power-on switch transmits an electrical signal to the stirring device, thereby controlling the stirring device to stir the side with a stronger electrical signal, and diffuse the area with a higher hydrogen ion concentration to the surrounding area.

[0017] Furthermore, the stirring device includes a stirring motor, a support column and a turbine agitator. The stirring motor is tightly connected to the tank body, the output end of the stirring motor is tightly connected to the support column, a slide groove is provided on the support column, the turbine agitator is connected to the slide groove, a linear motor is provided on the turbine agitator, a V-groove is provided on the blades of the turbine agitator, and the linear motor is electrically connected to the second power switch.

[0018] The linear motor is used to drive the turbine agitator to move on the slide. When the solution in the tank needs to be stirred, the stirring motor outputs a torque to rotate the support column, and the rotation of the support column drives the turbine agitator to rotate, so that the turbine agitator stirs the liquid in the tank so that the liquid is evenly mixed and fully reacted. At the same time, the V-shaped groove on the turbine agitator allows the blades to send the liquid to both sides of the groove during rotation, thereby increasing the mixing effect of the liquid. When the turbine agitator is needed to work, the second power switch outputs an electrical signal to the linear motor to move the turbine agitator to a position with higher hydrogen ion concentration for stirring, thereby sending hydrogen ions to a position with lower concentration, further balancing the pH value in the tank.

[0019] Furthermore, the drug adding pipe, the glucose adding pipe and the waste liquid adding pipe are all provided with proportional regulating valves.

[0020] By setting up a proportional regulating valve, the opening of the drug addition pipe, glucose addition pipe and waste liquid addition pipe can be adjusted according to the size of the electrical signal, thereby controlling the liquid addition amount and preventing overreaction.

[0021] Compared with the prior art, the present invention has the following beneficial effects: 1. By installing multiple detection devices and comparison devices in the tank, the pH value of the solution at different locations can be fully monitored in real time. The detection device uses a reference electrode and a glass electrode to detect the hydrogen ion concentration in the solution. The circuit amplifier and signal processing device convert it into a control signal, accurately controlling the addition of acid and alkali substances to the reagent and waste liquid feeding pipes, effectively avoiding the generation of by-products during the reduction of oxidized waste liquid, and greatly improving reaction stability and product purity.

[0022] 2. The turbine agitator blades in the stirring device are equipped with V-grooves. Driven by the stirring motor, they not only evenly mix the liquid in the tank, ensuring the reaction proceeds fully, but also utilize the V-groove structure to deliver the liquid to both sides of the groove, enhancing the mixing effect. Simultaneously, the comparison device controls the turbine agitator to move to locations with high hydrogen ion concentrations based on electrical signals from different areas, providing targeted stirring and diffusion, further balancing the pH value in the tank and improving reaction efficiency. 3. The drug dosing pipe, glucose dosing pipe and waste liquid dosing pipe are all equipped with proportional control valves, which can intelligently adjust the valve opening according to the size of the electrical signal feedback from the detection device, accurately control the liquid dosage, avoid over-reaction or under-reaction, realize the rational use of resources, reduce production costs, reduce the risk of environmental pollution, and make the entire waste liquid recovery process more intelligent and refined. BRIEF DESCRIPTION OF THE DRAWINGS

[0023] Figure 1 It is a schematic diagram of the overall structure of the present invention; Figure 2 It is a schematic diagram of the tank structure of the present invention; Figure 3 Schematic diagram of the stirring device structure of the present invention; Figure 4 It is a schematic structural diagram of the turbine agitator of the present invention; Figure 5 Schematic diagram of the structure of the detection device of the present invention; Figure 6 for Figure 5 A magnified view of the local area A; Figure 7 This is a schematic diagram of the support structure of the present invention; Figure 8 Schematic diagram of the comparative device structure of the present invention.

[0024] In the figure: 1. tank body; 11. first mounting groove; 12. first mounting cavity; 2. stirring device; 21. stirring motor; 22. supporting column; 23. turbine stirrer; 3. detection device; 31. reference electrode; 32. glass electrode; 33. circuit amplifier; 34. signal processing device; 341. first electromagnet; 342. first power switch; 3421. first connecting groove; 3422. second connecting groove; 343. sliding rheostat; 344. supporting frame; 3441. third connecting groove; 345. detection magnet; 346. return spring; 347. blocking block; 348. connecting column; 349. first connecting switch; 35. detection shell; 351. second mounting cavity; 4. comparison device; 41. second electromagnet; 42. second power switch; 43. second connecting switch; 44. mounting shell; 5. drug dosing tube; 6. glucose dosing tube; 7. waste liquid dosing tube. DETAILED DESCRIPTION

[0025] The following will clearly and completely describe the technical solutions in the embodiments of the present invention in conjunction with the accompanying drawings. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative efforts are within the scope of protection of the present invention.

[0026] Example: Figures 1-8 As shown, the present invention provides a technical solution of a vitamin K3 oxidation waste liquid recovery device based on glucose reduction. The recovery device includes a tank body 1, a stirring device 2, a detection device 3, a comparison device 4, a drug dosing pipe 5, a glucose dosing pipe 6 and a waste liquid dosing pipe 7. The tank body 1 is connected to the stirring device 2, the tank body 1 is connected to the detection device 3, the tank body 1 is connected to the comparison device 4, the comparison device 4 is connected to the stirring device 2, the tank body 1 is connected to the drug dosing pipe 5, the tank body 1 is connected to the glucose dosing pipe 6, the tank body 1 is connected to the waste liquid dosing pipe 7, the comparison device 4 is connected to the drug dosing pipe 5, the stirring device 2 is placed in the tank body 1, there are several detection devices 3, there are several comparison devices 4, a discharge pipe is provided on the tank body 1, the detection device 3 is connected to the drug dosing pipe 5, and the detection device 3 is connected to the comparison device 4.

[0027] The tank body 1 serves as the main installation base for the installation and positioning of other components. Waste liquid is added to the tank body 1 through the waste liquid addition pipe 7, and glucose solution is added to the tank body 1 through the glucose addition pipe 6. The pH value of the waste liquid in the tank body 1 is detected by the detection device 3, and then the reagent addition pipe 5 is controlled to add reagents according to the detection results to control the pH value. When the detection device 3 detects that the pH value rises outside the controllable range, the detection device 3 transmits a signal to the waste liquid addition pipe 7 to lower the pH value by adding acidic waste liquid. When the detection device 3 detects that the pH value drops outside the controllable range, the detection device 3 transmits a signal to the reagent addition pipe 5 to control the reagent addition pipe 5 to add alkaline reagent, thereby increasing the pH value. Then, the solution after reduction is completed is discharged through the discharge pipe.

[0028] like Figure 1-Figure 4 As shown, a first mounting groove 11 and a first mounting cavity 12 are provided in the tank body 1. There are several first mounting grooves 11 and several first mounting cavities 12. Detection devices 3 are provided in several first mounting grooves 11, and comparison devices 4 are provided in several first mounting cavities 12. The comparison device 4 is connected to the first mounting cavity 12, and the detection device 3 is firmly connected to the first mounting groove 11.

[0029] The plurality of first mounting grooves 11 are provided to provide mounting positions for the plurality of detection devices 3, and the plurality of first mounting cavities 12 are provided to provide mounting positions for the plurality of comparison devices 4, so that the detection device 3 can directly detect the pH value of the solution at various positions in the tank body 1, thereby improving the detection strength of the pH value of the solution.

[0030] like Figure 2 、 Figure 3 、 Figure 5 and Figure 6 As shown, the detection device 3 includes a reference electrode 31, a glass electrode 32, a circuit amplifier 33, a signal processing device 34 and a detection shell 35. The detection shell 35 is fastened to the first mounting groove 11, the reference electrode 31 is connected to the detection shell 35, the glass electrode 32 is connected to the detection shell 35, a second mounting cavity 351 is provided in the detection shell 35, the circuit amplifier 33 is placed in the second mounting cavity 351, the signal processing device 34 is placed in the second mounting cavity 351, the signal processing device 34 is connected to the second mounting cavity 351, the glass electrode 32 is connected to the circuit amplifier 33 by wire, the reference electrode 31 is connected to the circuit amplifier 33 by wire, the circuit amplifier 33 is electrically connected to the signal processing device 34, the signal processing device 34 is connected to the drug dosing tube 5, and the signal processing device 34 is connected to the comparison device 4.

[0031] The detection shell 35 serves as the main installation base for the installation of other components. The concentration of hydrogen ions in the solution in the tank body 1 is detected by the reference electrode 31 and the glass electrode 32. The higher the hydrogen ion concentration in the solution, the greater the current on the reference electrode 31 and the glass electrode 32. The current signal detected by the reference electrode 31 and the glass electrode 32 is amplified by the circuit amplifier 33 and then transmitted to the signal processing device 34. The signal processing device 34 processes the electrical signal, thereby controlling the addition of the reagent dosing tube 5 and the waste liquid dosing tube 7.

[0032] like Figure 5-Figure 7 As shown, the signal processing device 34 includes a first electromagnet 341, a first power-on switch 342, a sliding rheostat 343 and a support frame 344, the first electromagnet 341 and the second mounting cavity 351 are fastened together, the first power-on switch 342 and the first electromagnet 341 are fastened together, the first electromagnet 341 and the support frame 344 are fastened together, the support frame 344 and the second mounting cavity 351 are fastened together, the sliding rheostat 343 and the second mounting cavity 351 are fastened together, the first power-on switch 342 is provided with a first connecting groove 3421 and a second connecting groove 3422, the support frame 344 is provided with a third connecting groove 3441, and the circuit amplifier 33 and the first electromagnet 341 are electrically connected.

[0033] The circuit amplifier 33 provides current to the first electromagnet 341 so that the first electromagnet 341 can excite a magnetic field. At the same time, the first electromagnet 341 serves as the main connection basis for connecting other components. The first power-on switch 342 controls the presence or absence of current on the sliding rheostat 343. The support frame 344 is provided so that the sliding rheostat 343 can slide on the support frame 344. The first connecting groove 3421, the second connecting groove 3422 and the third connecting groove 3441 provide an installation basis for other components.

[0034] like Figure 6-Figure 7 As shown, the signal processing device 34 further includes a detection magnet 345, a return spring 346, a blocking block 347, a connecting post 348 and a first connecting switch 349. The detection magnet 345 is fastened to the sliding rheostat 343, the detection magnet 345 is placed in the third connecting groove 3441, the detection magnet 345 and the third connecting groove 3441 are slidingly connected, the detection magnet 345 and the first connecting switch 349 are fastened to each other, the first connecting switch 349 is placed in the first connecting groove 3421, the first connecting switch 349 and the first connecting groove 3421 are slidingly connected, the connecting post 348 is slidingly connected to the second connecting groove 3422, and the connecting post 348 is fastened to the sliding rheostat 343. 48 is placed in the second connecting groove 3422, the reset spring 346 and the sliding rheostat 343 are tightly connected, the reset spring 346 is tightly connected to the blocking block 347 at one end away from the sliding rheostat 343, the blocking block 347 is tightly connected to the slider of the sliding rheostat 343, there are two sliding rheostats 343, detection magnets 345, reset springs 346, blocking blocks 347, connecting columns 348 and first connecting switches 349 and they are symmetrically distributed about the first power-on switch 342, the output ends of the two sliding rheostats 343 are respectively connected to the drug dosing pipe 5 and the waste liquid dosing pipe 7, and the output ends of the two sliding rheostats 343 are connected to the comparison device 4.

[0035] One of the two return springs 346 is in a compressed state, and the other is normally extended. The detection magnet 345 connected to the return spring 346 in the compressed state and the magnetic field excited by the first electromagnet 341 repel each other, and the output end of the sliding rheostat 343 on one side of the return spring 346 in the compressed state is electrically connected to the waste liquid feeding tube 7. The detection magnet 345 connected to the return spring 346 in the normally extended state and the magnetic field excited by the first electromagnet 341 attract each other, and the output end of the sliding rheostat 343 on one side of the return spring 346 in the normally extended state is electrically connected to the reagent feeding tube 5. The current transmitted from the reference electrode 31 and the glass electrode 32 is amplified by the circuit amplifier 33, and then the amplified current controls the magnetic field excited by the first electromagnet 341. When the hydrogen ion concentration in the solution is low, the current flowing from the circuit amplifier 33 to the first electromagnet 341 decreases, and the intensity of the magnetic field excited by the first electromagnet 341 decreases, so that the detection magnet 345 that repels the magnetic field of the first electromagnet 341 is affected by the return spring 346. The elastic potential energy is released, and the elastic potential energy released by the return spring 346 drives the first connection switch 349 to move, so that the first connection switch 349 is connected to the first power switch 342, so that the first power switch 342 energizes the waste liquid addition pipe 7, so that the waste liquid addition pipe 7 can add acidic waste liquid into the tank body 1, thereby lowering the pH value and increasing the hydrogen ion concentration, so that no other products are produced during the reduction process of the oxidized waste liquid, thereby improving the stability of the reaction. When the hydrogen ion concentration in the solution is high, the current flowing from the circuit amplifier 33 to the first electromagnet 341 increases, thereby increasing the force on the detection magnet 345, causing the detection magnet 345 subjected to repulsion to move away from the first power switch 342, and causing the detection magnet 345 subjected to attraction to move closer to the first power switch 342 until the first power switch 342 is connected to the first connection switch 349, thereby controlling the connected reagent addition pipe 5 to add alkaline reagent to the tank body 1, thereby raising the pH value and stabilizing the solution in the tank body 1.

[0036] like Figure 8 As shown, the comparison device 4 includes a second electromagnet 41, a second power-on switch 42, a second connection switch 43 and a mounting shell 44. The mounting shell 44 is placed in the first mounting cavity 12, and the mounting shell 44 and the first mounting cavity 12 are fastened together. The second electromagnet 41, the second power-on switch 42 and the second connection switch 43 are placed in the first mounting cavity 12, and the second electromagnet 41 and the first mounting cavity 12 are fastened together. There are two second electromagnets 41, and the second power-on switch 42 is provided on the second electromagnet 41. The second power-on switch 42 and the second electromagnet 41 are fastened together. The second connection switch 43 is placed between the two second electromagnets 41, and the second connection switch 43 is slidably connected to the first mounting cavity 12. The two second electromagnets 41 are electrically connected to different output ends of the sliding rheostat 343 respectively, and the second power-on switch 42 is electrically connected to the stirring device 2.

[0037] By sliding the rheostat 343 at different positions, the output current of the two second electromagnets 41 is different, so that the magnetic fields excited by the second electromagnets 41 are different. By exciting magnetic fields of different intensities by the two second electromagnets 41, the second connection switch 43 is moved to the side of the stronger magnetic field. At the same time, a spring is provided in the first installation cavity 12, and the spring is used to reset the second connection switch 43. When the second connection switch 43 moves to the side of the second power-on switch 42 on the side of the stronger magnetic field and is connected to the second power-on switch 42, the second power-on switch 42 transmits an electrical signal to the stirring device 2, thereby controlling the stirring device 2 to stir the side with the stronger electrical signal, and diffuse the area with higher hydrogen ion concentration to the surrounding area.

[0038] like Figure 1-Figure 4 As shown, the stirring device 2 includes a stirring motor 21, a support column 22 and a turbine agitator 23. The stirring motor 21 is firmly connected to the tank body 1, the output end of the stirring motor 21 is firmly connected to the support column 22, a slide groove is provided on the support column 22, the turbine agitator 23 is connected to the slide groove, a linear motor is provided on the turbine agitator 23, a V-groove is provided on the blades of the turbine agitator 23, and the linear motor is electrically connected to the second power switch 42.

[0039] The linear motor is used to drive the turbine agitator 23 to move on the slide. When the solution in the tank body 1 needs to be stirred, the stirring motor 21 outputs a torque to rotate the support column 22. The rotation of the support column 22 drives the turbine agitator 23 to rotate, so that the turbine agitator 23 stirs the liquid in the tank body 1 so that the liquid is evenly mixed and fully reacted. At the same time, the V-shaped groove on the turbine agitator 23 enables the blades to send the liquid to both sides of the groove during rotation, thereby increasing the mixing effect of the liquid. When the turbine agitator 23 is needed to work, the second power-on switch 42 outputs an electrical signal to the linear motor so that the turbine agitator 23 moves to a position with a higher hydrogen ion concentration for stirring, thereby sending the hydrogen ions to a position with a lower concentration, further balancing the pH value in the tank body 1.

[0040] like Figure 1-Figure 2 As shown, the drug adding pipe 5, the glucose adding pipe 6 and the waste liquid adding pipe 7 are all provided with proportional regulating valves.

[0041] By setting up the proportional regulating valve, the opening of the drug adding pipe 5, the glucose adding pipe 6 and the waste liquid adding pipe 7 can be adjusted according to the size of the electrical signal, thereby controlling the liquid addition amount and preventing excessive reaction.

[0042] The working principle of the present invention is as follows: the tank body 1 is used as the main installation base for the installation and positioning of other components. Waste liquid is added to the tank body 1 through the waste liquid addition pipe 7, and glucose solution is added to the tank body 1 through the glucose addition pipe 6. The pH value of the waste liquid in the tank body 1 is detected by the detection device 3, and then the agent addition pipe 5 is controlled to add agents according to the detection result to control the pH value. When the detection device 3 detects that the pH value rises outside the controllable range, the detection device 3 transmits a signal to the waste liquid addition pipe 7, and lowers the pH value by adding acidic waste liquid. When the hydrogen ion concentration in the solution is low, the current flowing from the circuit amplifier 33 to the first electromagnet 341 is reduced, and the magnetic field strength excited by the first electromagnet 341 is reduced, so that the detection magnet 345 that repels the magnetic field of the first electromagnet 341 is affected by the return spring 346 to release elastic potential energy. The elastic potential energy released by the return spring 346 drives the first connection switch 349 to move so that the first connection switch 349 is connected to the first power-on switch 342, thereby making the first The power switch 342 energizes the waste liquid addition pipe 7, so that the waste liquid addition pipe 7 can add acidic waste liquid into the tank body 1, thereby lowering the pH value and increasing the hydrogen ion concentration, so that no other products are produced during the reduction process of the oxidized waste liquid. When it is necessary to stir the solution in the tank body 1, the stirring motor 21 outputs a torque to rotate the support column 22, and the rotation of the support column 22 drives the turbine agitator 23 to rotate, so that the turbine agitator 23 stirs the liquid in the tank body 1 so that the liquid is evenly mixed and reacts fully. At the same time, the V-shaped groove on the turbine agitator 23 causes the blades to send the liquid to both sides of the groove during rotation, thereby increasing the mixing effect of the liquid. When the turbine agitator 23 is needed to work, the second power switch 42 outputs an electrical signal to the linear motor so that the turbine agitator 23 moves to a position with a higher hydrogen ion concentration for stirring, thereby sending hydrogen ions to a position with a lower concentration, further balancing the pH value in the tank body 1, and then the solution after reduction is completed is discharged through the discharge pipe.

[0043] It will be apparent to those skilled in the art that the present invention is not limited to the details of the exemplary embodiments described above and that the invention can be embodied in other specific forms without departing from the spirit or essential characteristics of the invention. Therefore, the embodiments should be considered in all respects as illustrative and non-restrictive, and the scope of the invention is defined by the appended claims, not the foregoing description, and all variations within the meaning and range of equivalents of the claims are intended to be included therein. Any reference sign in a claim should not be construed as limiting the claim to which it relates.

Claims

1. A vitamin K3 oxidation waste liquid recovery device based on glucose reduction, characterized by: The recovery device comprises a tank body (1), a stirring device (2), a detection device (3), a comparison device (4), a drug dosing pipe (5), a glucose dosing pipe (6) and a waste liquid dosing pipe (7), wherein the tank body (1) is connected to the stirring device (2), the tank body (1) is connected to the detection device (3), the tank body (1) is connected to the comparison device (4), the comparison device (4) is connected to the stirring device (2), the tank body (1) is connected to the drug dosing pipe (5), and the waste liquid dosing pipe (7) is connected to the detection device (3). The tank body (1) is connected to the glucose dosing pipe (6), the tank body (1) is connected to the waste liquid dosing pipe (7), the comparison device (4) is connected to the drug dosing pipe (5), the stirring device (2) is placed in the tank body (1), there are a plurality of detection devices (3), there are a plurality of comparison devices (4), a discharge pipe is provided on the tank body (1), the detection device (3) is connected to the drug dosing pipe (5), and the detection device (3) is connected to the comparison device (4).

2. The vitamin K3 oxidation waste liquid recovery device based on glucose reduction according to claim 1, characterized in that: The tank body (1) is provided with a first mounting groove (11) and a first mounting cavity (12). There are a plurality of first mounting grooves (11) and a plurality of first mounting cavities (12). A plurality of the first mounting grooves (11) are provided with detection devices (3), and a plurality of the first mounting cavities (12) are provided with comparison devices (4). The comparison devices (4) are connected to the first mounting cavity (12), and the detection devices (3) are fastened to the first mounting grooves (11).

3. The vitamin K3 oxidation waste liquid recovery device based on glucose reduction according to claim 2, characterized in that: The detection device (3) comprises a reference electrode (31), a glass electrode (32), a circuit amplifier (33), a signal processing device (34) and a detection housing (35); the detection housing (35) is fastened to the first mounting groove (11); the reference electrode (31) is connected to the detection housing (35); the glass electrode (32) is connected to the detection housing (35); a second mounting cavity (351) is provided in the detection housing (35); and the circuit amplifier (33) is placed in the second mounting cavity (351). The signal processing device (34) is placed in the second installation cavity (351), the signal processing device (34) is connected to the second installation cavity (351), the glass electrode (32) is connected to the circuit amplifier (33) by wire, the reference electrode (31) is connected to the circuit amplifier (33) by wire, the circuit amplifier (33) is electrically connected to the signal processing device (34), the signal processing device (34) is connected to the drug dosing tube (5), and the signal processing device (34) is connected to the comparison device (4).

4. The vitamin K3 oxidation waste liquid recovery device based on glucose reduction according to claim 3, characterized in that: The signal processing device (34) comprises a first electromagnet (341), a first power switch (342), a sliding rheostat (343) and a support frame (344); the first electromagnet (341) and the second mounting cavity (351) are fastened together; the first power switch (342) and the first electromagnet (341) are fastened together; the first electromagnet (341) and the support frame (344) are fastened together; the support frame (344) and the second mounting cavity (351) are fastened together; the sliding rheostat (343) and the second mounting cavity (351) are fastened together; the first power switch (342) is provided with a first connecting slot (3421) and a second connecting slot (3422); the support frame (344) is provided with a third connecting slot (3441); and the circuit amplifier (33) and the first electromagnet (341) are electrically connected.

5. The vitamin K3 oxidation waste liquid recovery device based on glucose reduction according to claim 4, characterized in that: The signal processing device (34) further includes a detection magnet (345), a return spring (346), a blocking block (347), a connecting column (348) and a first connecting switch (349), wherein the detection magnet (345) and the sliding rheostat (343) are fastened together, the detection magnet (345) is placed in the third connecting slot (3441), the detection magnet (345) and the third connecting slot (3441) are slidingly connected, the detection magnet (345) and the first connecting switch (349) are fastened together, the first connecting switch (349) is placed in the first connecting slot (3421), the first connecting switch (349) and the first connecting slot (3421) are slidingly connected, the connecting column (348) and the second connecting slot (3422) are slidingly connected, and the The connecting column (348) is placed in the second connecting groove (3422), the return spring (346) and the sliding rheostat (343) are fastened together, the end of the return spring (346) away from the sliding rheostat (343) is fastened together with the blocking block (347), the blocking block (347) and the sliding piece of the sliding rheostat (343) are fastened together, the sliding rheostat (343), the detection magnet (345), the return spring (346), the blocking block (347), the connecting column (348) and the first connecting switch (349) are each two and are symmetrically distributed about the first power-on switch (342), the two output ends of the sliding rheostat (343) are electrically connected to the drug dosing tube (5), and the two output ends of the sliding rheostat (343) are connected to the comparison device (4).

6. The vitamin K3 oxidation waste liquid recovery device based on glucose reduction according to claim 5, characterized in that: The comparison device (4) comprises a second electromagnet (41), a second power switch (42), a second connection switch (43) and a mounting shell (44), wherein the mounting shell (44) is placed in the first mounting cavity (12), the mounting shell (44) and the first mounting cavity (12) are fastened together, the second electromagnet (41), the second power switch (42) and the second connection switch (43) are placed in the first mounting cavity (12), the second electromagnet (41) and the first mounting cavity (12) are fastened together, there are two second electromagnets (41), a second power switch (42) is provided on the second electromagnet (41), the second power switch (42) and the second electromagnet (41) are fastened together, the second connection switch (43) is placed between the two second electromagnets (41), the second connection switch (43) and the first mounting cavity (12) are slidably connected, the two second electromagnets (41) are electrically connected to different output ends of the sliding rheostat (343), and the second power switch (42) is electrically connected to the stirring device (2).

7. The vitamin K3 oxidation waste liquid recovery device based on glucose reduction according to claim 6, characterized in that: The stirring device (2) comprises a stirring motor (21), a support column (22) and a turbine stirrer (23), wherein the stirring motor (21) is tightly connected to the tank body (1), the output end of the stirring motor (21) is tightly connected to the support column (22), a slide groove is provided on the support column (22), the turbine stirrer (23) is connected to the slide groove, the turbine stirrer (23) is provided with a linear motor, the blades on the turbine stirrer (23) are provided with a V-shaped groove, and the linear motor is electrically connected to the second power switch (42).

8. The vitamin K3 oxidation waste liquid recovery device based on glucose reduction according to claim 1, characterized in that: The drug dosing pipe (5), the glucose dosing pipe (6) and the waste liquid dosing pipe (7) are all provided with proportional regulating valves.

Citation Information

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