Functional anti-aging microcapsule composition for cosmetics and preparation method of functional anti-aging microcapsule composition
By preparing a microcapsule composition containing water, sodium alginate, retinol, compound plant extracts, triglyceride (ethylhexanoate), and stabilizers, the dispersion and stability problems of microencapsulation technology in cosmetics were solved, achieving both stability and anti-aging effects in cosmetics.
Patent Information
- Application Number
- CN202511276755.9
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-09-08
- Publication Date
- 2025-10-31
AI Technical Summary
Existing microencapsulation technologies in cosmetics suffer from problems such as poor dispersion of solid microcapsules and instability of liquid microcapsule compositions, resulting in uneven and unstable dispersion in cosmetic matrices.
A microcapsule composition was prepared using water, sodium alginate, retinol, compound plant extracts, triglyceride (ethylhexanoate), and stabilizers. The stability and anti-aging effect of the composition were enhanced by combining sodium alginate, sodium octenyl succinate starch, and sodium di(lauryl ether-7) citrate.
This approach achieves stability and anti-aging function of cosmetic microcapsules, enhances the stability and anti-inflammatory effect of the composition, and improves the transdermal absorption rate of active ingredients and skin moisturizing effect.
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Figure CN120859855A_ABST
Abstract
Description
Technical Field
[0001] This invention relates to the field of cosmetics, and more particularly to a cosmetic functional anti-aging microcapsule composition and its preparation method. Background Technology
[0002] Microencapsulation technology significantly enhances the functionality and stability of cosmetics by encapsulating active ingredients in a capsule structure. Its core functions include: (1) Protecting sensitive ingredients: Many functional ingredients in cosmetics (such as vitamin C, retinol, and plant essential oils) are easily degraded by light, heat, oxygen, or pH changes; microencapsulation forms a barrier through physical isolation, extending the shelf life of the ingredients. (2) Precisely controlling release: Microcapsules can be designed for sustained release or stimulus-responsive release. The sustained release mechanism is controlled by the porosity of the polymer wall material, allowing the active ingredients to act continuously on the skin surface; the stimulus-responsive mechanism can achieve targeted release. (3) Improving sensory characteristics: Some active ingredients (such as plant extracts and sunscreens) may have unpleasant odors or textures. Microencapsulation can mask odors and optimize the skin feel. (4) Enhancing bioavailability: Microencapsulation can promote transdermal absorption through nanoscale structures; for example, the transdermal absorption rate of vitamin E encapsulated in liposomes is significantly improved.
[0003] Solid microcapsule products face challenges in compatibility with their application environment, exhibiting difficulties in dispersion or uneven dispersion within cosmetic matrices. Liquid microcapsule compositions, due to the presence of solvents and other components, are easier to disperse in cosmetic matrices and more convenient to use; however, these compositions suffer from instability. Therefore, providing a stable and highly effective liquid microcapsule composition is a key technical problem that needs to be solved. Summary of the Invention
[0004] To address the aforementioned technical problems, this invention provides a cosmetic functional anti-aging microcapsule composition and its preparation method.
[0005] This invention provides a cosmetic-grade anti-aging microcapsule composition, comprising water, sodium alginate, retinol, compound plant extracts, triglycerides (ethylhexanoate), and a stabilizer. The microencapsulated composition effectively stabilizes the retinol and compound plant extracts within the contents, imparting excellent anti-aging and anti-inflammatory functions. Simultaneously, it is rich in triglycerides (ethylhexanoate), effectively moisturizing the skin.
[0006] Preferably, the composition of the composition by weight percentage is: 2-4% sodium alginate, 0.5-3% retinol, 1.5-6% compound plant extract, 10-20% triglyceride (ethylhexanoate), 4-10% stabilizer and balance water.
[0007] Preferably, the stabilizers include sodium octenyl succinate starch and sodium di(laurene-7) citrate. This invention uses sodium alginate, sodium octenyl succinate starch, and sodium di(laurene-7) citrate to prepare microencapsulated compositions, imparting excellent stability to the compositions.
[0008] Preferably, sodium octenyl succinate starch and sodium di(lauryl ether-7) citrate are combined in a weight ratio of 1:2-3.5. Using the above combination can further improve the stability of the composition.
[0009] Preferably, the preparation method of the compound plant extract includes: using Pteris mutilida and pine bark as raw materials, adding water, heating and stirring, cooling, adding cellulase for enzymatic hydrolysis, adding papain for enzymatic hydrolysis, then concentrating and adding an extractant composed of organic and inorganic phases for extraction, separating the extracted organic phase, and then concentrating and freeze-drying to obtain the final product. The above extraction method can effectively extract the active ingredients and enhance the efficacy of the extract.
[0010] Preferably, the preparation method of the compound plant extract includes: crushing the aerial parts of Pteris vittata and the bark of Pinus hainanensis, mixing them to obtain a mixture, adding water, heating and stirring, cooling to obtain a material, adding 50-300 u / g of cellulase to hydrolyze and inactivate the enzyme, adding 50-300 u / g of papain to hydrolyze and inactivate the enzyme, filtering, taking the filtrate and concentrating to obtain a concentrate, mixing the concentrate with an extractant, stirring and extracting, allowing it to stand and separate into layers, taking the organic phase, concentrating, and freeze-drying to obtain the compound plant extract.
[0011] Preferably, the weight ratio of the organic phase to the inorganic phase in the extractant is 1:0.2-0.35. The organic phase consists of chloroform and diethyl ether; using chloroform and diethyl ether in the organic phase can significantly improve the anti-inflammatory and other properties of the extract. The inorganic phase is a 0.01-2% sodium chloride solution.
[0012] Preferably, the weight ratio of chloroform to ether is 1:0.6-1. Choosing this ratio can further enhance the anti-inflammatory effect of the extract.
[0013] Preferably, the ratio of pteris vittata and sea pine bark is 1:0.5-1.5 by weight.
[0014] Preferably, the amount of water added is 3-50 times the weight of the mixture.
[0015] Preferably, the heating and stirring are carried out at 40-60℃ for 0.5-3 hours.
[0016] Preferably, cellulase is added for enzymatic hydrolysis for 0.5-3 hours at a hydrolysis temperature of 30-50℃.
[0017] Preferably, papain is added and hydrolyzed for 0.5-3 hours at a hydrolysis temperature of 30-50℃.
[0018] Preferably, the filtrate is concentrated to 8-15% of its weight to obtain a concentrate.
[0019] Preferably, the concentrate and the extractant are mixed at a weight ratio of 1:4-20.
[0020] Preferably, extraction is performed at 25-50℃ with stirring for 2-6 hours.
[0021] Preferably, the preparation method of the compound plant extract includes: pulverizing *Pteris vittata* (aerial part) and *Pinus koraiensis* bark; mixing *Pteris vittata* and *Pinus koraiensis* bark at a weight ratio of 1:0.5-1.5 to obtain a mixture; adding 3-50 times the weight of water of the mixture; heating and stirring at 40-60℃ for 0.5-3 hours; cooling to obtain the material; adding 50-300 u / g of cellulase to enzymatically hydrolyze the material for 0.5-3 hours to inactivate the enzyme; adding 50-300 u / g of papain to enzymatically hydrolyze the material for 0.5-3 hours to inactivate the enzyme; filtering; concentrating the filtrate to 8-15% of the filtrate weight to obtain a concentrate; mixing the concentrate with an extractant at a weight ratio of 1:4-20; stirring and extracting at 25-50℃ for 2-6 hours; allowing to stand and separate into layers; taking the organic phase; concentrating; and freeze-drying to obtain the compound plant extract. The weight ratio of the organic phase to the inorganic phase in the extractant is 1:0.2-0.35. The organic phase consists of chloroform and diethyl ether; using a combination of chloroform and diethyl ether in the extraction organic phase significantly enhances the anti-inflammatory and other properties of the extract. The inorganic phase is a 0.01-2% sodium chloride solution. The weight ratio of chloroform to diethyl ether is 1:0.6-1.
[0022] Preferably, the composition further includes 0.05-0.4% preservative.
[0023] The present invention also provides a method for preparing the composition, comprising the following steps:
[0024] (1) Heat water, add sodium alginate and stabilizer, stir to obtain aqueous phase;
[0025] (2) Heat the triglyceride (ethylhexanoate), add retinol and compound plant extract, stir, and obtain the oil phase;
[0026] (3) Pour the oil phase into the aqueous phase, keep warm and shear emulsify to obtain the composition.
[0027] Preferably, in step (1), the water is heated to 35-50°C. In step (2), the triglyceride (ethylhexanoate) is heated to 30-40°C. In step (3), the temperature for heat preservation and shear emulsification is 30-40°C.
[0028] Preferably, when the composition contains other water-soluble excipients, such as preservatives, they can be used to prepare an aqueous phase before preparing the microencapsulated composition.
[0029] The present invention also provides the use of the composition in the production of skin care products, wherein the composition is used in the skin care products at an amount of 0.001-10 wt%.
[0030] This invention also provides a skincare product, comprising, by weight percentage: 10-40% glycerin, 2-5% butylene glycol, 0.5-1% calcium alginate, 0.3-1% xanthan gum, 0.05-0.2% gellan gum, 0.5-1% 1,2-hexanediol, 0.001-0.3% p-hydroxyacetophenone, 0.1-1% trehalose, 0.3-0.8% agar, 0.1-0.5% chondrus crispus extract, 0.1-0.5% hydroxyethyl cellulose, and EDTA. - Disodium 0.01-0.05%, Sodium hyaluronate 0.01-0.05%, Centella asiatica extract 0.003-0.005%, Cynanchum atratum extract 0.003-0.005%, Olive leaf extract 0.002-0.004%, Scutellaria baicalensis extract 0.002-0.004%, Soluble collagen 0.003-0.01%, Synthetic fluorophlogopite 0-1%, Pigment 0-0.1%, the composition 0.001-5%, and the balance being water.
[0031] The beneficial effects of this invention are as follows:
[0032] This invention uses water, sodium alginate, retinol, compound plant extracts, triglyceride (ethylhexanoate), and stabilizers to prepare a composition. The composition prepared from the above-mentioned active ingredients, such as moisturizing, anti-aging, and anti-inflammatory ingredients, has excellent anti-aging and anti-inflammatory functions, can effectively moisturize the skin, and has strong stability, effectively resisting the adverse effects of temperature environment.
[0033] The extract obtained by heating and stirring with water, enzymatic hydrolysis with cellulase and papain, extraction with an extractant and post-treatment can effectively inhibit the expression of inflammatory factors and has a good anti-inflammatory effect.
[0034] This invention uses both Pteris mutilida and pine bark as raw materials, which is more effective than using only one. The active ingredients of the two complement each other, enhancing their anti-inflammatory properties. The combination of chloroform and ether in the extraction solvent has a significant impact on the anti-inflammatory effect of the extract. Extracts obtained by using either one alone have poor anti-inflammatory properties, and when using both as the organic phase for extraction, the extract with a ratio of 1:0.6-1 shows better anti-inflammatory properties.
[0035] The composition prepared by this invention using water, sodium alginate, retinol, compound plant extracts, triglyceride (ethylhexanoate) and stabilizers has a high ZETA potential value, good system stability, and strong resistance to environmental challenges.
[0036] This invention selects sodium octenyl succinate starch and sodium di(lauryl ether-7) citrate as stabilizers, which can significantly improve the stability of the composition. The combination of sodium octenyl succinate starch and sodium di(lauryl ether-7) citrate in this invention has a complexing effect, significantly improving the stability of the composition, and the stability is even better when the ratio of the two is 1:2-3.5. Attached Figure Description
[0037] Figure 1 : Expression level of TNF-α in each test group.
[0038] Figure 2 : Expression level of IL-1α in each test group.
[0039] Figure 3 ZETA potential of compositions 1-7. Detailed Implementation
[0040] The present invention will be further illustrated by the following specific embodiments, but the technology of the present invention is not limited to the following specific embodiments.
[0041] I. Preparation and Testing of Plant Extracts
[0042] Example 1: The preparation steps are as follows: (1) The above-ground parts of Pteris multifida and the bark of pine trees are crushed. The Pteris multifida and the pine bark are mixed at a weight ratio of 1:0.5 to obtain a mixture. Add 10 times the weight of water to the mixture and heat and stir at 50°C and 100 rpm for 1 hour. Cool to room temperature to obtain the material; (2) Add 150 u / g of cellulase to the material and stir at 40°C and 100 rpm for 1.5 hours to inactivate the enzyme. Add 150 u / g of papain to the material and stir at 40°C and 100 rpm for 1.5 hours to inactivate the enzyme. Add 150 u / g of papain to the material and stir at 40°C and 100 rpm for 1 hour to inactivate the enzyme. (2) Stir at pm for 2 hours to inactivate the enzyme, filter, and concentrate the filtrate at 60℃ under reduced pressure to 10% of the filtrate weight to obtain the concentrate; (3) Mix the concentrate with the extractant (the extractant is composed of organic phase and inorganic phase in a weight ratio of 1:0.2, the organic phase is composed of chloroform and diethyl ether in a weight ratio of 1:0.6, and the inorganic phase is 0.35% sodium chloride solution) at a weight ratio of 1:10, stir and extract at 40℃ and 60rpm for 4 hours, let stand at room temperature for 2 hours to separate the layers, take the organic phase, concentrate under reduced pressure until no organic phase can be detected, freeze dry at -42℃ and 20Pa for 8 hours to obtain the compound plant extract.
[0043] Example 2: The preparation steps are as follows: (1) The above-ground parts of Pteris multifida and the bark of pine trees are crushed. The Pteris multifida and the pine bark are mixed at a weight ratio of 1:1.5 to obtain a mixture. Add 10 times the weight of water to the mixture and heat and stir at 50°C and 100 rpm for 1.2 hours. Cool to room temperature to obtain the material; (2) Add 120 u / g of cellulase to the material and stir at 40°C and 100 rpm for 2 hours to inactivate the enzyme. Add 140 u / g of papain to the material and stir at 40°C and 100 rpm for 2 hours to inactivate the enzyme. Stirring for 1.8 hours for enzymatic hydrolysis, inactivating enzymes, filtering, and concentrating the filtrate under reduced pressure at 60°C to 11% of the filtrate weight to obtain a concentrate; (3) Mix the concentrate with an extractant (the extractant is composed of an organic phase and an inorganic phase in a weight ratio of 1:0.35, the organic phase is composed of chloroform and diethyl ether in a weight ratio of 1:1, and the inorganic phase is 0.37% sodium chloride solution) at a weight ratio of 1:15, stir and extract at 42°C and 60 rpm for 3.5 hours, let stand at room temperature for 2.5 hours to separate the layers, take the organic phase, concentrate under reduced pressure until no organic phase is detected, freeze dry at -42°C and 20 Pa for 8 hours to obtain the compound plant extract.
[0044] Example 3: The only difference from Example 1 is that the fern is not used. Step (1) is as follows: the bark of the coastal pine is crushed to obtain a powder, 10 times the weight of water is added to the powder and heated and stirred at 50°C and 100 rpm for 1 hour, and then cooled to room temperature to obtain the material. Everything else is the same as in Example 1.
[0045] Example 4: The only difference from Example 1 is that the bark of the coastal pine is not used. Step (1) is as follows: the above-ground parts of the fern are crushed to obtain a powder, 10 times the weight of water is added to the powder and heated and stirred at 50°C and 100 rpm for 1 hour, and then cooled to room temperature to obtain the material. Everything else is the same as in Example 1.
[0046] Example 5: The only difference from Example 1 is that chloroform is not used as the extractant. Step (3) is as follows: The concentrate and the extractant (composed of an organic phase and an inorganic phase in a weight ratio of 1:0.2, the organic phase being diethyl ether and the inorganic phase being a 0.35% sodium chloride solution) are mixed at a weight ratio of 1:10, stirred and extracted at 40°C and 60 rpm for 4 hours, and allowed to stand at room temperature for 2 hours to separate the layers. The organic phase is taken, concentrated under reduced pressure until no organic phase is detected, and freeze-dried at -42°C and 20 Pa for 8 hours to obtain the composite plant extract. Everything else is the same as in Example 1.
[0047] Example 6: The only difference from Example 1 is that the extractant does not use diethyl ether. Step (3) is as follows: The concentrate and the extractant (the extractant consists of an organic phase and an inorganic phase in a weight ratio of 1:0.2, the organic phase being chloroform and the inorganic phase being 0.35% sodium chloride solution) are mixed at a weight ratio of 1:10, stirred and extracted at 40°C and 60 rpm for 4 hours, and allowed to stand at room temperature for 2 hours to separate the layers. The organic phase is taken, concentrated under reduced pressure until no organic phase is detected, and freeze-dried at -42°C and 20 Pa for 8 hours to obtain the composite plant extract. Everything else is the same as in Example 1.
[0048] Example 7: The only difference from Example 1 is the composition of the extractant. Step (3) is as follows: The concentrate and the extractant (composed of an organic phase and an inorganic phase in a weight ratio of 1:0.2, the organic phase being chloroform and diethyl ether in a weight ratio of 1:0.2, and the inorganic phase being a 0.35% sodium chloride solution) are mixed at a weight ratio of 1:10, stirred and extracted at 40°C and 60 rpm for 4 hours, allowed to stand at room temperature for 2 hours to separate the layers, the organic phase is taken, concentrated under reduced pressure until no organic phase is detected, and freeze-dried at -42°C and 20 Pa for 8 hours to obtain the composite plant extract. Everything else is the same as in Example 1.
[0049] Example 8: The only difference from Example 1 is the composition of the extractant. Step (3) is as follows: The concentrate and the extractant (the extractant is composed of an organic phase and an inorganic phase in a weight ratio of 1:0.2, the organic phase is composed of chloroform and diethyl ether in a weight ratio of 1:3, and the inorganic phase is a 0.35% sodium chloride solution) are mixed at a weight ratio of 1:10, stirred and extracted at 40°C and 60 rpm for 4 hours, and allowed to stand at room temperature for 2 hours to separate the layers. The organic phase is taken, concentrated under reduced pressure until no organic phase is detected, and freeze-dried at -42°C and 20 Pa for 8 hours to obtain the composite plant extract. Everything else is the same as in Example 1.
[0050] Example 9: The only difference from Example 1 is the composition of the extractant. Step (3) is as follows: The concentrate and the extractant (the extractant is composed of an organic phase and an inorganic phase in a weight ratio of 1:0.2, the organic phase is composed of chloroform and diethyl ether in a weight ratio of 1:7, and the inorganic phase is a 0.35% sodium chloride solution) are mixed at a weight ratio of 1:10, stirred and extracted at 40°C and 60 rpm for 4 hours, and allowed to stand at room temperature for 2 hours to separate the layers. The organic phase is taken, concentrated under reduced pressure until no organic phase is detected, and freeze-dried at -42°C and 20 Pa for 8 hours to obtain the composite plant extract. Everything else is the same as in Example 1.
[0051] The extracts obtained in Examples 1-9 above were tested. The anti-inflammatory properties of the extracts were characterized by inhibiting the expression of inflammatory factors TNF-α and IL-1α using a lipopolysaccharide (LPS)-induced RAW264.7 macrophage inflammation model.
[0052] RAW264.7 cells were cultured at 7.5 × 10⁻⁶. 5Each sample was seeded in a 12-well plate with 2 mL of culture medium per well and incubated at 37°C and 5% CO2 for 24 h. The supernatant was removed, and the following dosages were applied to the controlled groups: Model group: 5 μg / mL lipopolysaccharide + culture medium to 2 mL; Blank group: culture medium to 2 mL; Positive control group: 5 μg / mL lipopolysaccharide + 200 μg / mL dexamethasone + culture medium to 2 mL; Extract group (Examples 1-9): 5 μg / mL lipopolysaccharide + 0.1 wt% extract from Examples 1-9 + culture medium to 2 mL. Each group was repeated in triplicate. The plates were then incubated at 37°C and 5% CO2 for another 24 h. The supernatant was collected, and the expression levels of TNF-α and IL-1α were measured according to the kit instructions. Results are shown in Tables 1-2 and 1-3. Figure 1-2 .
[0053] Table 1: Expression levels of TNF-α and IL-1α
[0054]
[0055]
[0056] Table 2: Inhibition rate of each group compared to the model group
[0057]
[0058]
[0059] Combined with Table 1-2 and Figure 1-2 The results show that the extract obtained by the present invention through water heating and stirring, enzymatic hydrolysis with cellulase and papain, extraction with an extractant, and post-treatment can effectively inhibit the expression of inflammatory factors and has a good anti-inflammatory effect. A comparison of Examples 1-2 and 3-4 shows that using both Pteris mutilida and pine bark as raw materials is more effective than using only one, as their active ingredients complement each other and enhance the anti-inflammatory properties. A comparison of Examples 1-2 and 5-9 shows that the combination of chloroform and ether in the extractant of the present invention has a significant impact on the anti-inflammatory effect of the extract. Extracts obtained by using either one alone have poor anti-inflammatory properties, and when using both as the organic phase for extraction, the extract has better anti-inflammatory properties when the ratio of chloroform to ether is 1:0.6-1.
[0060] II. Preparation and Testing of the Composition
[0061] The composition of the raw materials of the composition is shown in Table 3; wherein, λ is the weight ratio of sodium octenyl succinate starch and sodium di(lauryl ether-7) citrate, compositions 1 and 3-7 use the compound plant extract of Example 1, and composition 2 uses the compound plant extract of Example 2.
[0062] Table 3: Composition of the composition
[0063]
[0064]
[0065] The preparation method of the above composition is as follows:
[0066] (1) Heat water to 45°C, add sodium alginate, stabilizer (sodium octenyl succinate starch, sodium di(lauryl ether-7) citrate) and phenoxyethanol, stir at 120 rpm for 20 minutes to obtain the aqueous phase;
[0067] (2) Heat the triglyceride (ethylhexanoate) to 37°C, add retinol and compound plant extract, stir at 120 rpm for 15 minutes to obtain the oil phase;
[0068] (3) Slowly pour the oil phase into the aqueous phase, keep it at 35°C and shear emulsify at 800 rpm for 20 minutes, stop shear emulsification, and let it cool naturally to room temperature to obtain the composition.
[0069] The stability of the above composition was tested to measure the ZETA potential and its rate of change. The ZETA potential characterizes the stability of the composition, while the rate of change characterizes its ability to withstand environmental challenges. The specific test method was as follows: the above composition was mixed with deionized water at a weight ratio of 1:100, stirred at 800 rpm for 30 minutes at 35°C, and then allowed to cool naturally to room temperature. The ZETA potential ζ1 was measured. The sample was then stored in a sealed container at 35°C for 3 days, and the ZETA potential ζ2 was measured again. Each group was tested in triplicate. The rate of change of ζ was then calculated as δ = |(ζ2-ζ1) / ζ1|. A larger absolute value of ζ indicates a more stable system, while a smaller value of δ indicates a stronger ability to withstand environmental challenges. Specific results are shown in Table 4 and... Figure 3 .
[0070] Table 4: Zeta potentials ζ and δ
[0071] Group ζ1 / mV ζ2 / mV δ Composition 1 -37.15 -33.47 9.91% Composition 2 -35.73 -31.85 10.86% Composition 3 -30.62 -25.99 15.12% Composition 4 -29.04 -24.16 16.80% Composition 5 -33.25 -29.01 12.75% Composition 6 -32.78 -28.32 13.61% Composition 7 -20.13 -15.08 25.09%
[0072] According to Table 4 and Figure 3 Tests show that the composition prepared by the present invention using water, sodium alginate, retinol, compound plant extracts, triglyceride (ethylhexanoate) and stabilizer has a high ZETA potential value, good system stability, and strong resistance to environmental challenges.
[0073] A comparison of compositions 1 and 7 shows that the selection of sodium octenyl succinate starch and sodium di(lauryl ether-7) citrate as stabilizers in this invention significantly improves the stability of the compositions. Furthermore, a comparison of compositions 1, 3-6 shows that the combination of sodium octenyl succinate starch and sodium di(lauryl ether-7) citrate is more effective than either alone, exhibiting a complexing effect and significantly improving the stability of the compositions, with even better stability observed at a ratio of 1:2-3.5.
[0074] It should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention, and not to limit them; any deductions or substitutions made by those skilled in the art without departing from the concept of the present invention are within the protection scope of the present invention.
Claims
1. A cosmetic functional anti-aging microcapsule composition, characterized in that, The raw material composition is: water, sodium alginate, retinol, compound plant extracts, triglyceride (ethylhexanoate) and stabilizer; Stabilizers include sodium octenyl succinate starch and sodium di(lauryl ether-7) citrate.
2. The cosmetic functional anti-aging microcapsule composition according to claim 1, characterized in that, The raw material composition by weight percentage is: 2-4% sodium alginate, 0.5-3% retinol, 1.5-6% compound plant extracts, 10-20% triglyceride (ethylhexanoate), 4-10% stabilizer and balance water.
3. The cosmetic functional anti-aging microcapsule composition according to claim 1, characterized in that, Sodium octenyl succinate starch and sodium di(lauryl alcohol polyether-7) citrate are combined in a weight ratio of 1:2-3.
5.
4. The cosmetic functional anti-aging microcapsule composition according to claim 1, characterized in that, The preparation method of the compound plant extract includes: using fern and sea pine bark as raw materials, adding water, heating and stirring, cooling and adding cellulase for enzymatic hydrolysis, adding papain for enzymatic hydrolysis, then concentrating and adding an extractant composed of organic and inorganic phases for extraction, separating the extracted organic phase, and then concentrating and freeze-drying to obtain the final product.
5. The cosmetic functional anti-aging microcapsule composition according to claim 4, characterized in that, The organic phase consists of chloroform and diethyl ether, and the aqueous phase is a 0.01-2% sodium chloride solution.
6. The cosmetic functional anti-aging microcapsule composition according to claim 5, characterized in that, The weight ratio of chloroform to diethyl ether is 1:0.6-1.
7. A method for preparing the composition according to any one of claims 1-6, characterized in that, Includes the following steps: (1) Heat water, add sodium alginate and stabilizer, stir to obtain aqueous phase; (2) Heat the triglyceride (ethylhexanoate), add retinol and compound plant extract, stir, and obtain the oil phase; (3) Pour the oil phase into the aqueous phase, keep warm and shear emulsify to obtain the composition.
8. The preparation method according to claim 7, characterized in that, In step (1), the water is heated to 35-50℃; in step (2), the triglyceride (ethylhexanoate) is heated to 30-40℃; in step (3), the temperature for heat preservation and shear emulsification is 30-40℃.
9. An application of the composition according to any one of claims 1-8 in the production of skin care products, characterized in that, The composition is used in skin care products at an amount of 0.001-10 wt%.
10. A skincare product, characterized in that, The product comprises the composition according to any one of claims 1-8; the skin care product having the following composition by weight percentage: 10-40% glycerin, 2-5% butylene glycol, 0.5-1% calcium alginate, 0.3-1% xanthan gum, 0.05-0.2% gellan gum, 0.5-1% 1,2-hexanediol, 0.001-0.3% p-hydroxyacetophenone, 0.1-1% trehalose, 0.3-0.8% agar, 0.1-0.5% chondrus crispus extract, 0.1-0.5% hydroxyethyl cellulose, and EDT. 0.01-0.05% disodium A, 0.01-0.05% sodium hyaluronate, 0.003-0.005% centella asiatica extract, 0.003-0.005% cynanchum atratum extract, 0.002-0.004% olive leaf extract, 0.002-0.004% scutellaria baicalensis extract, 0.003-0.01% soluble collagen, 0-1% synthetic fluorophlogopite, 0-0.1% pigment, 0.001-5% of the composition according to any one of claims 1-8, and the balance being water.