A liquid nuclear magnetic resonance spectrometer variable temperature protection system and method

By using a large nitrogen storage tank and a control valve to switch the flow of the gas stream, a stable supply of high-temperature and low-temperature nitrogen is provided for the nuclear magnetic resonance spectrometer, which solves the problem of the simple and outdated gas supply protection system in the existing technology and realizes automated control and improved safety.

CN115684237BActive Publication Date: 2026-06-12SOUTH CHINA BOTANICAL GARDEN CHINESE ACADEMY OF SCI

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
SOUTH CHINA BOTANICAL GARDEN CHINESE ACADEMY OF SCI
Filing Date
2022-09-21
Publication Date
2026-06-12

AI Technical Summary

Technical Problem

Existing nuclear magnetic resonance spectrometers have simple and outdated gas supply protection systems in high-temperature and low-temperature experiments, with low automation, low nitrogen utilization efficiency, and potential safety hazards. Manual control of the switching valve opening and closing also poses risks.

Method used

A large nitrogen storage tank is used as the gas supply source. The automatic control is achieved by switching the flow pipeline through the regulating valve group, which provides a stable nitrogen supply for high temperature and low temperature experiments. Humidity detection and dryer are installed in the gas pipeline to ensure gas quality.

🎯Benefits of technology

It achieves a stable supply of nitrogen for extended periods, improves automation, reduces operational risks, and enhances the reliability and practicality of the gas supply system.

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Abstract

The application discloses a kind of liquid nuclear magnetic resonance spectrometer variable temperature protection system and method, the variable temperature protection system includes nitrogen storage tank, regulating valve group, high-temperature liquid nuclear magnetic resonance spectrometer, low-temperature liquid nuclear magnetic resonance spectrometer, the output of the nitrogen storage tank is connected with the one end of main conveying pipe, the other end of the main conveying pipe is connected with regulating valve group, first shunt pipe is connected with the regulating valve group, the first shunt pipe is connected with the input of four-way connector, the first output of the four-way connector is connected with the one end of temperature control gas pipe, the other end of the temperature control gas pipe is connected with high-temperature liquid nuclear magnetic resonance spectrometer, can carry out individual high-temperature nuclear magnetic test or low-temperature nuclear magnetic test, can also carry out high-low temperature nuclear magnetic test simultaneously, and automation control is realized, the cost of whole regulating valve group is low, easy to assemble, practicality is stronger, and reliability is high.
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