Method for preparing cleansing and moisturizing facial mask using vermiculite and camel hump as raw materials

Abstract

The embodiment of the present invention discloses a method for preparing a clean and moisturizing facial mask using vermiculite and camel hump as raw materials. The present invention uses abandoned camel hump as raw material, first extracts high-quality camel oil, by modified nano vermiculite flakes, nano vermiculite flakes, camel oil, aloe or cucumber or vegetable extract, honey, collagen, glycerol, sodium hydroxymethyl cellulose, emulsifier, camel glycerol and sodium stearate, capric triglyceride, parahydroxyacetophenone, cetearyl alcohol, sodium hyaluronate, allantoin, potassium lauryl phosphate, 1,2-hexanediol, tetrahydromethylpyrimidine carboxylic acid, water etc. are regulated and synthesized, and mud film or facial mask are obtained. The moisturizing facial mask of the present invention has lasting moisturizing performance, good affinity and moisturizing performance, high degree of skin fit (based on nano-layered vermiculite), heat-resistant, cold-resistant and good stability, gentle and non-irritating, with excellent moisturizing effect, with good application prospects.

Description

Technical Field

[0001] The invention relates to the field of personal care products, and in particular to a method for preparing a cleansing and moisturizing facial mask by taking vermiculite and camel hump as raw materials. Background Art

[0002] Facial mask is a personal care product commonly used by people in daily life. It covers the stratum corneum of the skin, provides moisture to the stratum corneum, and makes the stratum corneum fully hydrated, thereby improving the appearance and elasticity of the skin. During the drying process of the mask as the moisture evaporates, the mask causes the skin to shrink moderately, and the sealing effect causes the skin temperature to temporarily rise, promoting blood circulation. During the peeling or washing process of partial peeling or wash-off masks, dead skin on the face and dirt on the skin surface can be removed, and it has a certain cleansing effect.

[0003] However, the inventors have noticed that the essences used in existing commonly used facial masks are mostly chemically added ingredients, and after long-term use, the effect gradually deteriorates and may even damage the skin. A few facial mask products with purely natural sources have unsatisfactory effects.

[0004] The hump refers to the peak-like part of the camel's back, which stores a lot of fat. The hump fat is used to maintain the normal movement of the camel. Research has found that the hump fat has the effect of treating stubborn arthritis, malignant sores, swollen muscles, etc. It also contains rich natural nutrients, highly unsaturated fatty acids and rich vitamin E. The diameter of the hump fat globules is small, the permeability is strong, and it is easily absorbed by the skin. It is rich in immune active substances that can promote the body's self-healing ability and metabolism, promote the regeneration of new cells, relieve pain, and have antibacterial and anti-inflammatory effects. At present, the hump fat is directly discarded and not fully utilized.

[0005] Therefore, it is urgent to develop a natural, safe and non-toxic facial mask using camel hump as raw material. Summary of the invention

[0006] Therefore, the present invention provides a method for preparing a cleansing and moisturizing facial mask by taking vermiculite and camel hump as raw materials.

[0007] In order to achieve the above object, the present invention provides the following technical solutions:

[0008] A method for preparing a cleansing and moisturizing facial mask using vermiculite and camel hump as raw materials, comprising the following steps:

[0009] Step 1: Using camel hump as the starting material to obtain raw hump fat;

[0010] Step 2: washing the camel hump fat with ethanol to remove odor, and then heating to volatilize the ethanol to remove remaining odor and moisture, thereby obtaining camel hump fat;

[0011] Step 3: Put the camel hump fat in an ultrasonic oil bath, add a small amount of lavender oil as a base oil, then add protease and stir evenly, and extract camel oil and oil residue at low temperature;

[0012] Step 4: heating the pretreated camel oil with sodium hydroxide or ammonia water under alkaline conditions to obtain camel glycerin and sodium stearate;

[0013] Step 5: taking expanded vermiculite and shearing and crushing it, removing impurities by flotation, adding camel glycerin and sodium stearate modifiers, and shearing and crushing it to prepare a modified nano vermiculite flake solution;

[0014] Step 6: Take the modified nano vermiculite flake solution, nano vermiculite flakes, camel glycerin and sodium stearate as raw materials, add aloe vera or cucumber or vegetable extract, honey, collagen, capric triglyceride, p-hydroxyacetophenone, cetearyl alcohol, sodium hyaluronate, allantoin, potassium lauryl phosphate, 1,2-hexanediol, tetrahydromethylpyrimidine carboxylic acid, sodium hydroxymethyl cellulose, emulsifier, and water as raw materials to prepare a cleansing and moisturizing mud mask or facial mask;

[0015] Step 7: Take the oil residue as raw material, mix with clean water or organic reactants, and ferment in a sealed manner to prepare high-grade fertilizers, sterilizers, decontamination products, etc.

[0016] In some preferred embodiments, in step 2, the heating temperature is 45°C to 160°C.

[0017] In some preferred embodiments, in step 3, the heating oil of the ultrasonic oil bath is camel oil prepared from camel hump, and the ultrasonic frequency is 1 MHz to 300 MHz;

[0018] The amount of bottom oil added can cover the entire bottom of the oil bath pot, so as to achieve the purpose of uniform mixing and heat transfer; the stirring temperature is 45-260°C, and the time is 0.2-15 hours; the low-temperature extraction temperature is 40-180°C, and the time is 0.1-20 hours;

[0019] The protease is papain, neutral protease or alkaline protease, and its usage is 3-6% of the camel hump fat mass.

[0020] In some preferred embodiments, in step six, the emulsifier is OP-10, castor oil or camel oil.

[0021] In some preferred embodiments, in step six, water and sodium hydroxymethyl cellulose are homogenized and completely dissolved, glycerin, emulsifier, capric triglyceride, parahydroxyacetophenone, cetearyl alcohol, sodium hyaluronate, allantoin, potassium lauryl phosphate, 1,2-hexanediol, and tetrahydromethylpyrimidine carboxylic acid are added, and the mixture is stirred and heated to 70-85° C., kept warm for 30-60 minutes, and stirred to completely dissolve to obtain phase A; honey is heated to 70-85° C., then added to phase A, and microwaved and homogenized. The frequency of the wave homogenization is 300 to 1000 MHz, and phase B is obtained by stirring; naturally cooling to 38 to 42° C., adding camel oil, aloe vera or cucumber or vegetable extract, collagen, modified nano vermiculite flake solution and nano vermiculite flakes, stirring and homogenizing to obtain a mud mask; or adding a solvent, reducing the modified nano vermiculite flakes and the nano vermiculite flake solution to make an essence, squeezing the mask cloth into thin sheets, and then immersing the sheet in the essence, loosening the mask cloth to allow the mask cloth to absorb the essence, and obtaining the moisturizing mask.

[0022] In some preferred embodiments, the preparation method of the facial mask cloth is:

[0023] The cotton is made into a non-woven cotton layer through a needle punching process;

[0024] Fiber cloths are respectively pasted on the upper and lower surfaces of the non-woven cotton layer to obtain a facial mask cloth.

[0025] Compared with the prior art, the present invention has at least the following beneficial effects:

[0026] (1) The present invention uses abandoned camel hump as raw material, first extracts high-quality camel oil, and then modifies and synthesizes the modified nano vermiculite flakes, nano vermiculite flakes, camel oil, aloe vera or cucumber or vegetable extract, honey, collagen, glycerol, sodium hydroxymethyl cellulose, emulsifier, camel glycerol and sodium stearate, capric triglyceride, p-hydroxyacetophenone, cetearyl alcohol, sodium hyaluronate, allantoin, potassium lauryl phosphate, 1,2-hexanediol, tetrahydromethylpyrimidine carboxylic acid, water, etc. to obtain a mud film or a facial mask. The moisturizing facial mask of the present invention has long-lasting moisturizing performance, good wetting performance, high skin adhesion (based on nano-layered vermiculite), good heat resistance, cold resistance and stability, mild and non-irritating, excellent moisturizing effect, and good application prospects.

[0027] (2) The method for preparing a moisturizing facial mask provided by the present invention has simple and easy steps and is suitable for large-scale industrial production.

[0028] (3) The camel oil extraction of the present invention adopts an enzyme method, which maintains the efficacy of the natural ingredients of camel throughout the process and enhances the efficacy of the moisturizing mask. BRIEF DESCRIPTION OF THE DRAWINGS

[0029] In order to more clearly illustrate the implementation methods of the present invention or the technical solutions in the prior art, the following briefly introduces the drawings required for the implementation methods or the description of the prior art. Obviously, the drawings in the following description are only exemplary, and for ordinary technicians in this field, other implementation drawings can be derived from the provided drawings without creative work.

[0030] Figure 1 A schematic diagram of a process for preparing a cleansing and moisturizing facial mask using vermiculite and camel hump as raw materials provided in an embodiment of the present invention. DETAILED DESCRIPTION

[0031] The following is a description of the implementation of the present invention by specific embodiments. People familiar with the art can easily understand other advantages and effects of the present invention from the contents disclosed in this specification. Obviously, the described embodiments are part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0032] Example 1

[0033] (1) Using camel hump as the starting material to obtain raw hump fat;

[0034] (2) washing the camel hump fat with ethanol to remove odor, and then heating at 50° C. to volatilize the ethanol to remove remaining odor and moisture, thereby obtaining camel hump fat;

[0035] (3) Place camel hump fat in an ultrasonic oil bath with an ultrasonic frequency of 6 MHz, add a small amount of lavender oil as a base oil, and then add 5% papain, stir at 37°C for 2 hours, and then extract at 60°C until the water is fully evaporated, filter to remove solid particles and other debris, and obtain clear camel oil and oil residue. The camel oil is cooled for use. The oil residue is mixed with clean water or organic reactants and fermented in a sealed manner to prepare high-grade fertilizers, sterilizers, decontamination products, etc.;

[0036] (4) heating the pretreated camel oil and sodium hydroxide under alkaline conditions to obtain camel glycerin and sodium stearate;

[0037] (5) taking expanded vermiculite and shearing and crushing it, removing impurities by flotation, adding glycerol and sodium stearate as modifiers, and shearing and crushing it to prepare a modified nano vermiculite flake colloidal solution;

[0038] (6) 85 g of sodium hydroxymethylcellulose was homogenized and completely dissolved in water, and 4 g of glycerol, 2 g of emulsifier, 2 g of capric triglyceride, 2 g of p-hydroxyacetophenone, 2 g of cetearyl alcohol, 1 g of sodium hyaluronate, 2 g of allantoin, 1 g of potassium lauryl phosphate, 4 g of 1,2-hexanediol, and 2 g of tetrahydromethylpyrimidine carboxylic acid were added, and the mixture was stirred and heated to keep warm for 50 min. After stirring and completely dissolving, phase A was obtained; honey was heated to 85° C., and then added to the phase A, and microwave homogenization was performed. The frequency of microwave homogenization was 950 MHz, stirring to obtain phase B; naturally cooling to 40°C, adding camel oil, aloe vera or cucumber or vegetable extract, collagen, modified nano vermiculite flake solution and nano vermiculite flakes, stirring and homogenizing, when the vermiculite nano flake content reaches more than 65%, obtaining a mud film; or adding a solvent, reducing the content of modified nano vermiculite flakes and nano vermiculite flake solution, making an essence, squeezing the mask cloth into thin sheets, and then immersing the sheet in the essence, loosening the mask cloth, allowing the mask cloth to absorb the essence, and obtaining the moisturizing mask.

[0039] Example 2

[0040] (1) Using camel hump as the starting material to obtain raw hump fat;

[0041] (2) washing the camel hump fat with ethanol to remove odor, and then heating at 45° C. to volatilize the ethanol to remove remaining odor and moisture, thereby obtaining camel hump fat;

[0042] (3) placing camel hump fat in an ultrasonic oil bath with an ultrasonic frequency of 6 MHz, adding a small amount of lavender oil as a base oil, and then adding 5% papain, stirring at 37° C. for 2 hours, and then extracting at 60° C. until the water is fully dried and volatilized, filtering to remove solid particles and other debris such as residues, and obtaining clear camel oil and oil residue, cooling the camel oil for use, and mixing the oil residue with clean water or organic reactants for sealed fermentation, etc., to prepare high-grade fertilizers, sterilizers, decontamination products, etc.;

[0043] (4) heating the pretreated camel oil and ammonia water under alkaline conditions to obtain camel glycerin and sodium stearate;

[0044] (5) taking expanded vermiculite and shearing and crushing it, removing impurities by flotation, adding glycerol and sodium stearate as modifiers, and shearing and crushing it to prepare a modified nano vermiculite flake colloidal solution;

[0045] (6) 90 g of sodium hydroxymethylcellulose was homogenized and completely dissolved, and 4 g of glycerol, 2 g of emulsifier, 2 g of capric triglyceride, 2 g of p-hydroxyacetophenone, 2 g of cetearyl alcohol, 1 g of sodium hyaluronate, 2 g of allantoin, 1 g of potassium lauryl phosphate, 4 g of 1,2-hexanediol, and 2 g of tetrahydromethylpyrimidine carboxylic acid were added, and the mixture was stirred and heated to keep warm for 60 min. After stirring and completely dissolving, phase A was obtained; honey was heated to 85° C., and then added to phase A, and microwave homogenization was performed. The frequency of microwave homogenization was 900 MHz, stirring to obtain phase B; naturally cooling to 40°C, adding camel oil, aloe vera or cucumber or vegetable extract, collagen, modified nano vermiculite flake solution and nano vermiculite flakes, stirring and homogenizing, when the vermiculite nano flake content reaches more than 70%, obtaining a mud film; or adding a solvent, reducing the content of modified nano vermiculite flakes and nano vermiculite flake solution, making an essence, squeezing the mask cloth into thin sheets, and then immersing the sheet in the essence, loosening the mask cloth, allowing the mask cloth to absorb the essence, and obtaining the moisturizing mask.

[0046] Example 3

[0047] (1) Using camel hump as the starting material to obtain raw hump fat;

[0048] (2) washing the camel hump fat with ethanol to remove odor, and then heating at 50° C. to volatilize the ethanol to remove remaining odor and moisture, thereby obtaining camel hump fat;

[0049] (3) placing camel hump fat in an ultrasonic oil bath with an ultrasonic frequency of 6 MHz, adding a small amount of lavender oil as a base oil, and then adding 5% papain, stirring at 37° C. for 2 hours, and then extracting at 60° C. until the water is fully dried and volatilized, filtering to remove solid particles and other debris such as residues, and obtaining clear camel oil and oil residue, cooling the camel oil for use, and mixing the oil residue with clean water or organic reactants for sealed fermentation, etc., to prepare high-grade fertilizers, sterilizers, decontamination products, etc.;

[0050] (4) heating the pretreated camel oil and ammonia water under alkaline conditions to obtain camel glycerin and sodium stearate;

[0051] (5) taking expanded vermiculite and shearing and crushing it, removing impurities by flotation, adding glycerol and sodium stearate as modifiers, and shearing and crushing it to prepare a modified nano vermiculite flake colloidal solution;

[0052] (6) 95 g of sodium hydroxymethylcellulose was homogenized and completely dissolved in water, and 4 g of glycerol, 2 g of emulsifier, 2 g of capric triglyceride, 2 g of p-hydroxyacetophenone, 2 g of cetearyl alcohol, 1 g of sodium hyaluronate, 2 g of allantoin, 1 g of potassium lauryl phosphate, 4 g of 1,2-hexanediol, and 2 g of tetrahydromethylpyrimidine carboxylic acid were added, and the mixture was heated to 75° C. and kept warm for 55 min. After the mixture was completely dissolved by stirring, phase A was obtained. Honey was heated to 75° C. and then added to phase A. The microwave homogenization was performed. The frequency of the microwave homogenization was 2.5 The rate is 800 MHz, and phase B is obtained by stirring; naturally cooling to 40°C, adding camel oil, aloe vera or cucumber or vegetable extract, collagen, modified nano vermiculite flake solution and nano vermiculite flakes, stirring and homogenizing, and when the vermiculite nano flake content reaches more than 75%, a mud film is obtained; or a solvent is added to reduce the content of modified nano vermiculite flakes and nano vermiculite flake solution to prepare an essence, squeezing the mask cloth into thin sheets, and then immersing the sheet into the essence, loosening the mask cloth to allow the mask cloth to absorb the essence, and obtaining the moisturizing mask.

[0053] Test Example 1

[0054] The stability of the essences of Examples 1-3 was tested

[0055] 1. Heat resistance test

[0056] The essence was placed in a 10 mL glass bottle at 25°C, 35°C, and 45°C for 24 hours. Then, without direct sunlight, its color and texture were observed to see if there was any significant difference from before placement, and whether there was any floating oil or stratification.

[0057] 2. Cold resistance test

[0058] The mask essence was placed in a 10 mL glass bottle and placed at -5°C, 0°C, and 5°C for 24 hours. The color and texture were observed to see if there were any differences compared to before the placement, while avoiding direct sunlight.

[0059] 3. Centrifugal stability test

[0060] Place the mask essence in a centrifuge tube and centrifuge at 2000r / min, 3000r / min, and 4000r / min for 15min respectively. Observe the color and texture of the essence without direct sunlight to see if there is any difference from before placement.

[0061] The results are shown in Table 1.

[0062] Table 1

[0063]

[0064] The results show that the essence provided by the embodiment of the present invention has excellent stability.

[0065] Test Example 2

[0066] A questionnaire survey was conducted on the use effects of the moisturizing facial masks of Examples 1 to 3. The scoring criteria are shown in Table 2.

[0067] Table 2

[0068]

[0069] The questionnaire survey results are shown in Table 3.

[0070] Table 3

[0071] sample odor Irritant Usage Total score Example 1 8.5 8.2 8.7 25.4 Example 2 8.7 8.9 9.2 26.8 Example 3 8.6 8.7 8.3 25.6

[0072] The results show that the odor, irritation and use feeling of the moisturizing facial mask of the present invention meet the requirements of consumers.

[0073] Although the present invention has been described in detail above by general description and specific embodiments, it is obvious to those skilled in the art that some modifications or improvements can be made to the present invention. Therefore, these modifications or improvements made without departing from the spirit of the present invention all belong to the scope of protection claimed by the present invention.

Claims

1. A method for preparing a cleansing and moisturizing facial mask using vermiculite and camel hump as raw materials, characterized in that: The steps include: Step 1: Using camel hump as the starting material to obtain raw hump fat; Step 2: washing the original camel hump fat with ethanol to remove odor, and then heating to volatilize the ethanol to remove remaining odor and moisture, thereby obtaining camel hump fat; Step 3: placing the camel hump fat in an ultrasonic oil bath, adding a small amount of lavender oil as a base oil, then adding protease to stir evenly, and extracting at low temperature to obtain camel oil and oil residue; Step 4: heating the pretreated camel oil with sodium hydroxide or ammonia water under alkaline conditions to obtain camel glycerin and sodium stearate; Step 5: taking expanded vermiculite and shearing and crushing it, removing impurities by flotation, adding camel glycerin and sodium stearate modifiers, and shearing and crushing it to prepare a modified nano vermiculite flake solution; Step 6: Homogenize and completely dissolve water and sodium hydroxymethyl cellulose, add glycerin, emulsifier, capric triglyceride, p-hydroxyacetophenone, cetearyl alcohol, sodium hyaluronate, allantoin, potassium lauryl phosphate, 1,2-hexanediol, tetrahydromethylpyrimidine carboxylic acid, stir and heat to 70-85°C, keep warm for 30-60 minutes, and stir to completely dissolve to obtain phase A; heat honey to 70-85°C, then add it to phase A, and perform microwave homogenization. The frequency is 300-1000 MHz, and phase B is obtained by stirring; naturally cooling to 38-42°C, adding camel oil, vegetable extract, collagen, modified nano vermiculite flake solution and nano vermiculite flakes, stirring and homogenizing to obtain a mud film; or, adding a solvent, reducing the modified nano vermiculite flake solution and nano vermiculite flakes to make an essence, squeezing the mask cloth into thin sheets, and then immersing the sheet into the essence, loosening the mask cloth, allowing the mask cloth to absorb the essence, and obtaining the moisturizing mask.

2. The method for preparing a cleansing and moisturizing facial mask using vermiculite and camel hump as raw materials according to claim 1, characterized in that: In step 2, the heating temperature is 45°C to 160°C.

3. The method for preparing a cleansing and moisturizing facial mask using vermiculite and camel hump as raw materials according to claim 1, characterized in that: In step 3, the heating oil of the ultrasonic oil bath is camel oil prepared from camel hump, and the ultrasonic frequency is 1 MHz to 300 MHz; The amount of base oil added can cover the entire bottom of the oil bath pot, so as to achieve the purpose of mixing and even heat transfer; the stirring temperature is 45-260°C, and the time is 0.2-15 hours; the low-temperature extraction temperature is 40-180°C, and the time is 0.1-20 hours; The protease is papain, neutral protease or alkaline protease, and its usage is 3-6% of the camel hump fat mass.

4. The method for preparing a cleansing and moisturizing facial mask using vermiculite and camel hump as raw materials according to claim 1, characterized in that: In step six, the emulsifier is OP-10, castor oil or camel oil.

5. The method for preparing a cleansing and moisturizing facial mask using vermiculite and camel hump as raw materials according to claim 1, characterized in that: The preparation method of the facial mask cloth: The cotton is made into a non-woven cotton layer through a needle punching process; Fiber cloths are respectively pasted on the upper and lower surfaces of the non-woven cotton layer to obtain a facial mask cloth.

6. The method for preparing a cleansing and moisturizing facial mask using vermiculite and camel hump as raw materials according to claim 1, characterized in that: The mud mask contains more than 50% of nano vermiculite flakes, and the essence contains less than 40% of nano vermiculite flakes.

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