Preparation method and application of oral liquid of ganoderma lucidum spore oil with improved taste

By using antioxidant and emulsifier mixture, ultrasonic treatment and low homogenization pressure in the preparation of Ganoderma lucidum spore oil oral solution, the problems of greasy, fishy smell and active substances in the prior art are solved, and a stable, uniform and good-tasting Ganoderma lucidum spore oil oral solution is prepared.

CN116210906BActive Publication Date: 2025-04-01GUANGZHOU HANFANG PHARMA CO LTD +1
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Patent Information

Application Number
CN202211722215.5
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2022-12-30
Publication Date
2025-04-01
Estimated Expiration
2042-12-30

AI Technical Summary

Technical Problem

When preparing Ganoderma lucidum spore oil oral liquid by the existing high-pressure homogenization method, it is easy to cause greasy and fishy smell and other taste problems, and the process requirements are high, resulting in an increase in the emulsion temperature and the active substances are easily destroyed.

Method used

The oil phase is formed by mixing and stirring of antioxidants, Ganoderma lucidum spore oil and emulsifier. Combined with ultrasonic treatment and low homogenization pressure, a stable final milk is prepared, followed by potting and sterilization to form a Ganoderma lucidum spore oil oral liquid that improves taste.

Benefits of technology

The oral liquid prepared by this method has stable properties and good uniformity, avoids greasy and fishy smell, increases consumer acceptance, and reduces the oxidation risk of Ganoderma lucidum spore oil.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention relates to the field of health food, and discloses a ganoderma spore oil oral liquid with improved taste and a preparation method thereof, which overcomes the taste problems of greasy feeling and fishy smell etc. existing in the conventional high-pressure preparation of ganoderma spore oil oral liquid. In view of the deficiencies of the prior art, a ganoderma spore oil oral liquid with improved taste and a preparation method thereof are provided, and the oral liquid prepared by the preparation method has stable properties, good uniformity, is not easy to demulsify, delaminate, flocculate, and has good taste, thereby improving the acceptability of consumers.
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Description

Technical Field

[0001] The invention relates to the field of health food, and in particular to a preparation method and application of a ganoderma spore oil oral liquid with improved taste. Background Art

[0002] Ganoderma spore oil is a fat-soluble oily substance extracted from extremely tiny oval reproductive cells ejected from the gills of Ganoderma during its growth and maturity period. It is rich in triterpenoids, sterols, vitamins and other biologically active substances. It also contains a large amount of unsaturated fatty acids such as oleic acid, linoleic acid, linolenic acid, etc., which can enhance the body's functional immunity. It also has the effects of regulating cardiovascular system, improving digestion, and regulating sleep.

[0003] Since Ganoderma lucidum spore oil is rich in unsaturated fatty acids, it is easily affected by air, light and temperature in the environment, making it easy to oxidize and become rancid during processing and storage, reducing the quality and value of Ganoderma lucidum spore oil. In addition, Ganoderma lucidum spore oil is a fat-soluble substance, which is an oily liquid at room temperature and has good fat solubility. It is difficult to be digested and absorbed by the human body when taken orally directly, and the oral absorption utilization rate is very low. Preparing Ganoderma lucidum spore oil into an emulsion oral liquid is a good idea to solve the above problems. Emulsion oral liquid can effectively increase the stability and bioavailability of Ganoderma lucidum spore oil.

[0004] High-pressure homogenization is one of the most commonly used methods for preparing emulsions at present, but high-pressure homogenization requires relatively high pressure, and often requires cyclic high-pressure homogenization to obtain nanoemulsions with small particle size and good stability. "A method for preparing a nanoemulsion of whole ganoderma spore oil rich in ganoderma acid" (publication number CN112043731A) discloses a method for preparing a nanoemulsion of ganoderma spore oil by repeated high-pressure homogenization, and homogenizing 8 to 12 times under the condition of a homogenization pressure of 800 to 1300 bar, and a uniform and stable nano oral emulsion of ganoderma spore oil is obtained. "A nano ganoderma spore oil and its production process and application" (publication number CN103393590A) discloses a method for preparing nano ganoderma spore oil by high-pressure homogenization, and the method needs to be homogenized 3 times under the condition of a homogenization pressure of 150 to 200 MPa, each time for 30 minutes. Although nanoemulsions with smaller particle sizes can be produced, the process requires higher homogenization pressure and time, which significantly increases the temperature of the emulsion system. The emulsion itself is a thermodynamically unstable system. Excessively high temperature leads to uneven emulsion particles and Oswald ripening, causing the distribution of emulsion particles to further widen. During long-term storage, oil and water stratification, flocculation, and rancidity are prone to occur, which in turn produces a fishy smell and a greasy feeling, seriously affecting the taste of the product. Summary of the invention

[0005] The purpose of the present invention is to overcome the taste problems of greasy and fishy smells in the conventional high-pressure preparation of oral liquid of ganoderma lucidum spore oil. In view of the deficiencies of the prior art, an oral liquid of ganoderma lucidum spore oil with improved taste and a preparation method thereof are provided. The oral liquid prepared by the preparation method has stable properties, good uniformity, is not prone to demulsification, stratification, flocculation, and has good taste, thereby improving consumer acceptance.

[0006] In order to solve the above technical problems, the present invention adopts the following technical solutions:

[0007] A method for preparing a ganoderma lucidum spore oil oral liquid with improved taste comprises the following steps:

[0008] A. Mixing antioxidant, ganoderma lucidum spore oil and emulsifier, stirring until completely dissolved and uniformly dissolved to form an oil phase;

[0009] B. Heat and keep water warm to form a water phase;

[0010] C. adding the oil phase to the water phase and stirring under high-speed shearing to prepare colostrum A;

[0011] D. adding a pH regulator to the colostrum A and performing ultrasonic treatment to prepare colostrum B;

[0012] E. homogenizing the colostrum B to obtain final milk;

[0013] F. Filling and sterilizing the final emulsion to obtain the oral liquid of Ganoderma lucidum spore oil with improved taste.

[0014] Preferably, in step C, the high-speed shearing speed is 6000-12000 rpm, the stirring time is 8-12 minutes, and the stirring temperature is 55-75°C.

[0015] Preferably, in step D, the power of ultrasonic treatment is 300-600W, and the time is 8-12 minutes.

[0016] Preferably, in step E, the homogenization pressure is 300 bar to 600 bar, and the homogenization times are 1 to 3 times.

[0017] Preferably, step A comprises: uniformly mixing the antioxidant and the ganoderma spore oil, then mixing with the emulsifier, heating and stirring until they are completely dissolved and uniform, to form the oil phase.

[0018] Antioxidants and emulsifiers can be well dissolved with the spore oil in the oil phase to form a uniform and stable oil phase.

[0019] Preferably, in step A, the temperature of heating and stirring is 35-75°C.

[0020] Preferably, in step B, the heating and insulation temperature is 55-75° C.; in step D, the pH value is adjusted to 6.5-8.0 by the pH adjuster; and in step F, the sterilization condition is that the F0 value is greater than 8.

[0021] Preferably, the Ganoderma lucidum spore oil is obtained by low-temperature carbon dioxide supercritical extraction of Ganoderma lucidum spores; the emulsifier includes one or more of lysophosphatidylcholine and polyoxyethylene xylitol monostearate; the antioxidant includes dilauryl thiodipropionate; and the pH adjuster includes hydrochloric acid or sodium hydroxide.

[0022] The selection of emulsifiers mainly considers whether it can stably prepare the emulsion without introducing odor or whether it can enhance the aroma of the entire product. For example, when egg yolk lecithin is used as an emulsifier, the oral liquid tastes more like egg, and when soybean lecithin is used as an emulsifier, the overall taste is more like soybean milk, which has a significant inhibitory effect on the unique aroma of Ganoderma lucidum spore oil. After a lot of exploration and experiments, it was unexpectedly discovered that lysophosphatidylcholine or polyoxyethylene xylitol monostearate as an emulsifier can enhance the aroma of Ganoderma lucidum spore oil.

[0023] The selection of antioxidants has a more obvious effect on the quality of oral liquids. Since the ganoderma lucidum spore oil emulsion system contains oil, water and oxygen at the same time, the final product is more likely to become rancid and have a peculiar smell when placed for a long time, compared with general oral liquids (oral liquids made of plant polysaccharides, minerals or vitamins), which affects the quality and taste of the oral liquid. The present invention selects dilauryl thiodipropionate as an antioxidant, which is a fat-soluble component compatible with the raw oil and fat, and is more conducive to the stability of the raw oil and fat.

[0024] The method for preparing the oral liquid of ganoderma spore oil with improved taste as described above comprises the following components in mass ratio: 5-25% of ganoderma spore oil, 0.5-20% of emulsifier, 0.01-0.05% of antioxidant, 0.001-0.01% of pH regulator, and the balance of water.

[0025] The main purpose of the pH adjuster is to adjust the pH value of the emulsion system. Depending on the concentration and type of the pH adjuster used and the size of the formulation, the pH can be adjusted to 6.5-8.0.

[0026] Preferably, the average particle size of the oral liquid of Ganoderma lucidum spore oil with improved taste is no more than 250 nm.

[0027] Compared with the prior art, the present invention has the following beneficial effects:

[0028] According to the preparation process of the oral liquid of ganoderma lucidum spore oil provided by the present invention, the product is more stable, and the colostrum is treated by ultrasound, which effectively reduces the homogenization pressure and the homogenization time, and the particle size of the emulsion is controlled below 250nm, so as to prevent the temperature of the emulsion from rising due to excessive pressure and too many homogenization times, and reduce the risk of oxidation of ganoderma lucidum spore oil and destruction of active substances. The oral liquid prepared by the preparation method has stable properties, good uniformity, is not easy to demulsify, stratify, flocculate, and has good taste, and improves the acceptability of consumers. BRIEF DESCRIPTION OF THE DRAWINGS

[0029] Figure 1 1 and 2 are product appearance diagrams of the embodiments of the present invention and the comparative examples, wherein: a is the product appearance of embodiment 1, b is the product appearance of embodiment 2, c is the product appearance of comparative example 1, d is the product appearance of comparative example 2, e is the product appearance of comparative example 3, f is the product appearance of comparative example 4, and g is the product appearance of comparative example 5. DETAILED DESCRIPTION

[0030] In order to make the purpose, technical solutions and advantages of the present invention more clear, the present invention will be further described in detail below in conjunction with specific embodiments.

[0031] Example 1

[0032] In the preparation of this embodiment, each 1000 mL of the preparation contains: 50 g of Ganoderma lucidum spore oil, 10 g of lysophosphatidylcholine, 1 g of polyoxyethylene xylitol anhydride monostearate, 0.1 g of dilauryl thiodipropionate, and purified water to 1000 mL. Among them, the proportion of Ganoderma lucidum spore oil as an oil phase is 5%, and the proportion of lysophosphatidylcholine and polyoxyethylene xylitol anhydride monostearate as an emulsifier is 1.1%.

[0033] (1) Mix the prescribed amount of dilauryl thiodipropionate and ganoderma lucidum spore oil, stir evenly, then add lysophosphatidylcholine and polyoxyethylene xylitol monostearate, heat to 50° C. and stir until completely dissolved, to form an oil phase;

[0034] (2) heating the remaining purified water to 60° C. to form an aqueous phase;

[0035] (3) slowly adding the oil phase of step (1) into the water phase of step (2), shearing at 8000 rpm for 9 minutes to produce colostrum; adjusting the pH to 7.5 with 0.1 mol / L sodium hydroxide solution;

[0036] (4) treating the colostrum obtained in step (3) with 500W ultrasonic waves for 10 minutes, and then homogenizing the colostrum twice at 600 bar to obtain final milk;

[0037] (5) The final milk of step (4) is sealed and sterilized by wet heat sterilization at 121° C. for 15 minutes to obtain the oral liquid.

[0038] Example 2

[0039] In the preparation of this embodiment, each 1000 mL of the preparation contains: 200 g of Ganoderma lucidum spore oil, 50 g of lysophosphatidylcholine, 5 g of polyoxyethylene xylitol anhydride monostearate, 0.2 g of dilauryl thiodipropionate, and purified water to 1000 mL. Among them, the proportion of Ganoderma lucidum spore oil as the oil phase is 20%, and the proportion of lysophosphatidylcholine and polyoxyethylene xylitol anhydride monostearate as the emulsifier is 5.5%.

[0040] (1) Mix the prescribed amount of dilauryl thiodipropionate and ganoderma lucidum spore oil, stir evenly, then add lysophosphatidylcholine and polyoxyethylene xylitol monostearate, heat to 55° C. and stir until completely dissolved, to form an oil phase;

[0041] (2) heating the remaining purified water to 65° C. to form an aqueous phase;

[0042] (3) slowly adding the oil phase of step (1) into the water phase of step (2), shearing at 8000 rpm for 9 minutes to produce colostrum; adjusting the pH to 7.5 with 0.1 mol / L sodium hydroxide solution;

[0043] (4) treating the colostrum obtained in step (3) with 500W ultrasonic waves for 10 minutes, and then homogenizing the colostrum twice at 600 bar to obtain final milk;

[0044] (5) The final milk of step (4) is sealed and sterilized by wet heat sterilization at 121° C. for 15 minutes to obtain the oral liquid.

[0045] Example 3

[0046] In the preparation of this embodiment, each 1000 mL of the preparation contains: 250 g of Ganoderma lucidum spore oil, 150 g of lysophosphatidylcholine, 15 g of polyoxyethylene xylitol anhydride monostearate, 0.25 g of dilauryl thiodipropionate, and purified water to 1000 mL. Among them, the proportion of Ganoderma lucidum spore oil as the oil phase is 25%, and the proportion of lysophosphatidylcholine and polyoxyethylene xylitol anhydride monostearate as the emulsifier is 16.5%.

[0047] (1) Mix the prescribed amount of dilauryl thiodipropionate and ganoderma lucidum spore oil, stir evenly, then add lysophosphatidylcholine and polyoxyethylene xylitol monostearate, heat to 50° C. and stir until completely dissolved, to form an oil phase;

[0048] (2) heating the remaining purified water to 65° C. to form an aqueous phase;

[0049] (3) slowly adding the oil phase of step (1) into the water phase of step (2), shearing at 8000 rpm for 9 minutes to produce colostrum; adjusting the pH to 7.5 with 0.1 mol / L sodium hydroxide solution;

[0050] (4) treating the colostrum obtained in step (3) with 500W ultrasonic waves for 10 minutes, and then homogenizing the colostrum twice at 600 bar to obtain final milk;

[0051] (5) The final milk of step (4) is sealed and sterilized by wet heat sterilization at 121° C. for 15 minutes to obtain the oral liquid.

[0052] Example 4

[0053] In the preparation of this embodiment, each 1000 mL of the preparation contains: 150 g of Ganoderma lucidum spore oil, 15 g of lysophosphatidylcholine, 2 g of polyoxyethylene xylitol anhydride monostearate, 0.15 g of dilauryl thiodipropionate, and purified water to 1000 mL. Among them, the proportion of Ganoderma lucidum spore oil as the oil phase is 15%, and the proportion of lysophosphatidylcholine and polyoxyethylene xylitol anhydride monostearate as the emulsifier is 1.7%.

[0054] (1) Mix the prescribed amount of dilauryl thiodipropionate and ganoderma lucidum spore oil, stir evenly, then add lysophosphatidylcholine and polyoxyethylene xylitol monostearate, heat to 50° C. and stir until completely dissolved, to form an oil phase;

[0055] (2) heating the remaining purified water to 60° C. to form an aqueous phase;

[0056] (3) slowly adding the oil phase of step (1) into the water phase of step (2), shearing at 8000 rpm for 9 minutes to produce colostrum; adjusting the pH to 7.5 with 0.1 mol / L sodium hydroxide solution;

[0057] (4) treating the colostrum obtained in step (3) with 500W ultrasonic waves for 10 minutes, and then homogenizing the colostrum twice at 300 bar to obtain final milk;

[0058] (5) The final milk of step (4) is sealed and sterilized by wet heat sterilization at 121° C. for 15 minutes to obtain the oral liquid.

[0059] Example 5

[0060] In the preparation of this embodiment, each 1000 mL of the preparation contains: 200 g of Ganoderma lucidum spore oil, 50 g of lysophosphatidylcholine, 5 g of polyoxyethylene xylitol anhydride monostearate, 0.2 g of dilauryl thiodipropionate, and purified water to 1000 mL. Among them, the proportion of Ganoderma lucidum spore oil as the oil phase is 20%, and the proportion of lysophosphatidylcholine and polyoxyethylene xylitol anhydride monostearate as the emulsifier is 5.5%.

[0061] (1) Mix the prescribed amount of dilauryl thiodipropionate and ganoderma lucidum spore oil, stir evenly, then add lysophosphatidylcholine and polyoxyethylene xylitol monostearate, heat to 50° C. and stir until completely dissolved, to form an oil phase;

[0062] (2) heating the remaining purified water to 60° C. to form an aqueous phase;

[0063] (3) slowly adding the oil phase of step (1) into the water phase of step (2), shearing at 8000 rpm for 9 minutes to produce colostrum; adjusting the pH to 7.5 with 0.1 mol / L sodium hydroxide solution;

[0064] (4) treating the colostrum obtained in step (3) with 400W ultrasonic waves for 10 minutes, and then homogenizing the colostrum twice at 450bar to obtain final milk;

[0065] (5) The final milk of step (4) is sealed and sterilized by wet heat sterilization at 121° C. for 15 minutes to obtain the oral liquid.

[0066] Example 6

[0067] In the preparation of this embodiment, each 1000 mL of the preparation contains: 200 g of Ganoderma lucidum spore oil, 50 g of lysophosphatidylcholine, 5 g of polyoxyethylene xylitol anhydride monostearate, 0.2 g of dilauryl thiodipropionate, and purified water to 1000 mL. Among them, the proportion of Ganoderma lucidum spore oil as the oil phase is 20%, and the proportion of lysophosphatidylcholine and polyoxyethylene xylitol anhydride monostearate as the emulsifier is 5.5%.

[0068] (1) Mix the prescribed amount of dilauryl thiodipropionate and ganoderma lucidum spore oil, stir evenly, then add lysophosphatidylcholine and polyoxyethylene xylitol monostearate, heat to 55° C. and stir until completely dissolved, to form an oil phase;

[0069] (2) heating the remaining purified water to 65° C. to form an aqueous phase;

[0070] (3) slowly adding the oil phase of step (1) into the water phase of step (2), shearing at 8000 rpm for 9 minutes to produce colostrum; adjusting the pH to 7.5 with 0.1 mol / L sodium hydroxide solution;

[0071] (4) treating the colostrum obtained in step (3) with 400W ultrasonic waves for 10 minutes, and then homogenizing the colostrum at 400 bar for 3 times to obtain final milk;

[0072] (5) The final milk of step (4) is sealed and sterilized by wet heat sterilization at 121° C. for 15 minutes to obtain the oral liquid.

[0073] Comparative Example 1

[0074] In the preparation of this embodiment, each 1000 mL of the preparation contains: 200 g of Ganoderma lucidum spore oil, 50 g of lysophosphatidylcholine, 5 g of polyoxyethylene xylitol anhydride monostearate, 0.2 g of dilauryl thiodipropionate, and purified water to 1000 mL. Among them, the proportion of Ganoderma lucidum spore oil as the oil phase is 20%, and the proportion of lysophosphatidylcholine and polyoxyethylene xylitol anhydride monostearate as the emulsifier is 5.5%.

[0075] (1) Mix the prescribed amount of dilauryl thiodipropionate and ganoderma lucidum spore oil, stir evenly, then add lysophosphatidylcholine and polyoxyethylene xylitol monostearate, heat to 50° C. and stir until completely dissolved, to form an oil phase;

[0076] (2) heating the remaining purified water to 60° C. to form an aqueous phase;

[0077] (3) slowly adding the oil phase of step (1) into the water phase of step (2), shearing at 8000 rpm for 9 minutes to produce colostrum; adjusting the pH to 7.5 with 0.1 mol / L sodium hydroxide solution;

[0078] (4) homogenizing the colostrum obtained in step (3) at 700 bar for 3 times to obtain final milk;

[0079] (5) The final milk of step (4) is sealed and sterilized by wet heat sterilization at 121° C. for 15 minutes to obtain the oral liquid.

[0080] Comparative Example 2

[0081] In the preparation of this embodiment, each 1000 mL of the preparation contains: 200 g of Ganoderma lucidum spore oil, 50 g of lysophosphatidylcholine, 5 g of polyoxyethylene xylitol anhydride monostearate, 0.2 g of dilauryl thiodipropionate, and purified water to 1000 mL. Among them, the proportion of Ganoderma lucidum spore oil as the oil phase is 20%, and the proportion of lysophosphatidylcholine and polyoxyethylene xylitol anhydride monostearate as the emulsifier is 5.5%.

[0082] (1) Mix the prescribed amount of dilauryl thiodipropionate and ganoderma lucidum spore oil, stir evenly, then add lysophosphatidylcholine and polyoxyethylene xylitol monostearate, heat to 50° C. and stir until completely dissolved, to form an oil phase;

[0083] (2) heating the remaining purified water to 60° C. to form an aqueous phase;

[0084] (3) slowly adding the oil phase of step (1) into the water phase of step (2), shearing at 8000 rpm for 9 minutes to produce colostrum; adjusting the pH to 7.5 with 0.1 mol / L sodium hydroxide solution;

[0085] (4) subjecting the product of step (3) to 600W ultrasonic treatment for 10 minutes to obtain final milk;

[0086] (5) The final milk of step (4) is sealed and sterilized by wet heat sterilization at 121° C. for 15 minutes to obtain the oral liquid.

[0087] Comparative Example 3

[0088] In the preparation of this embodiment, each 1000 mL of the preparation contains: 200 g of Ganoderma lucidum spore oil, 50 g of lysophosphatidylcholine, 5 g of polyoxyethylene xylitol anhydride monostearate, 0.2 g of dilauryl thiodipropionate, and purified water to 1000 mL. Among them, the proportion of Ganoderma lucidum spore oil as the oil phase is 20%, and the proportion of lysophosphatidylcholine and polyoxyethylene xylitol anhydride monostearate as the emulsifier is 5.5%.

[0089] (1) Mix the prescribed amount of dilauryl thiodipropionate and ganoderma lucidum spore oil, stir evenly, then add lysophosphatidylcholine and polyoxyethylene xylitol monostearate, heat to 50° C. and stir until completely dissolved, to form an oil phase;

[0090] (2) heating the remaining purified water to 60° C. to form an aqueous phase;

[0091] (3) slowly adding the oil phase of step (1) into the water phase of step (2), shearing at 8000 rpm for 9 minutes to produce colostrum; adjusting the pH to 7.5 with 0.1 mol / L sodium hydroxide solution;

[0092] (4) homogenizing the colostrum obtained in step (3) twice at 600 bar, and then subjecting it to ultrasonic treatment at 500 W for 10 minutes to obtain final milk;

[0093] (5) The final milk of step (4) is sealed and sterilized by wet heat sterilization at 121° C. for 15 minutes to obtain the oral liquid.

[0094] Effect Example 1

[0095] The average particle size, PDI, pH value, peroxide value, centrifugal stability and other indicators of the emulsions of Examples 1 to 6 and Comparative Examples 1, 2, and 3 were compared, and the results are shown in Table 1.

[0096] Table 1 Comparison of evaluation indicators of preparations

[0097]

[0098] As can be seen from Table 1, the oral liquid of ganoderma lucidum spore oil prepared by the present invention is homogenized under 300-600 bar, and the obtained liquid is uniform and stable, the particle size is below 250 nm, PDI < 0.2, and the centrifugal stability is good. As can be seen from the results of the comparative examples, comparative example 1 uses 700 bar pressure alone and homogenizes 3 times to prepare an emulsion with a particle size of less than 250 nm, but is subjected to high heat for a long time during the preparation process, resulting in an increase in the peroxide value, which affects the stability of the ganoderma lucidum spore oil in the emulsion; the emulsion particle size prepared by comparative example 2 using ultrasound 600W ultrasound alone is greater than 500 nm, and the emulsion stability is significantly worse than that of the embodiment, and the difference between comparative example 3 and the embodiment is that the preparation process is first homogenized, and then the emulsion is prepared by ultrasound, and the particle size of the obtained emulsion is increased by 53%, and the embodiment can obtain an emulsion with a smaller particle size and stable properties under the condition of reducing the number or pressure of high-pressure homogenization, which greatly reduces the oxidation of ganoderma lucidum spore oil and the risk of active substances being destroyed.

[0099] Effect Example 2

[0100] Sensory evaluation 1:

[0101] 10 people who have undergone food sensory skills training, are in good health, and have normal taste and smell are randomly selected to form an evaluation team, half of whom are male and half are female. Example 2, Comparative Examples 1, 2, and 3 are randomly numbered, and the color, smell, taste, and texture state are evaluated. The average of the evaluation scores is taken as the final result. The evaluation criteria and results are shown in Table 2. Figure 1 .

[0102] Table 2 Sensory evaluation standards

[0103]

[0104] Sensory evaluation 2:

[0105] Samples: Take the oral liquid obtained in Example 1 as a sample, take the oral liquid obtained in Example 1 as a test product, and take the oral liquid obtained in Comparative Example 3 as a reference product. Randomly number the test products and reference products, organize tasting, and evaluate the smell, taste and color of the samples.

[0106] Subjects: 10 people, who were trained in food sensory skills, in good health, and had normal taste and smell.

[0107] Scoring method: The subjects will score on a 10-point scale, with 10 points for complete consistency with the test product; 7 points for relatively similarity; 4 points for indistinguishability; and 0 points for complete difference. The judges will score within a range of 0 to 10 points based on the actual situation, and only fill in the integer score.

[0108] Data statistics: The obtained data were processed using SPSS.

[0109] Experimental results: See Table 3 below.

[0110] Table 3

[0111] Color odor taste Test product 9.1±0.83 9.2±0.75 9.4±0.49 Reference 9.0±0.78 8.6±0.91 7.6±1.30 P-value >0.01 >0.01 <0.01

[0112] Sensory evaluation - The sensory evaluation results of Example 1, Comparative Examples 1, 2, and 3 are shown in Figure 1 The overall sensory evaluation scores of the embodiment in four dimensions are significantly higher than those of the comparative example. The sensory evaluation 2 is a double-blind experiment on embodiment 1 and comparative example 3. It can be seen from Table 3 that the taste of the experimental product is better than that of the control product. After inspection, the P value is <0.01, which is a very significant difference. The preparation method of the oral liquid of ganoderma lucidum spore oil provided by this patent has a significant effect on improving the taste.

[0113] The above disclosure is only the preferred embodiment of the present invention, which cannot be used to limit the scope of the present invention. Therefore, equivalent changes made according to the claims of the present invention are still within the scope of the present invention.

Claims

1. A method for preparing a ganoderma lucidum spore oil oral liquid with improved taste, characterized in that: The steps include: A. Mixing antioxidant, ganoderma lucidum spore oil and emulsifier, stirring until completely dissolved and uniformly dissolved to form an oil phase; the emulsifier comprises one or more of lysophosphatidylcholine and polyoxyethylene xylitol monostearate; B. Heat and keep water warm to form a water phase; C. adding the oil phase to the water phase, stirring under high-speed shearing, the high-speed shearing speed is 6000-12000 rpm, the stirring time is 8-12 minutes, and the stirring temperature is 55-75° C. to prepare colostrum A; D. adding a pH regulator to the colostrum A and performing ultrasonic treatment at a power of 300-600 W for 8-12 minutes to prepare colostrum B; E. homogenizing the colostrum B to obtain final milk; the homogenization pressure is 300 bar to 600 bar, and the homogenization times are 1 to 3 times; F. Filling and sterilizing the final emulsion to obtain the oral liquid of Ganoderma lucidum spore oil with improved taste; The oral solution of ganoderma lucidum spore oil with improved taste comprises the following components in mass ratio: 5-25% of ganoderma lucidum spore oil, 0.5-20% of emulsifier, 0.01-0.05% of antioxidant, 0.001-0.01% of pH regulator, and the balance of water.

2. The method for preparing the oral liquid of Ganoderma lucidum spore oil with improved taste as claimed in claim 1, characterized in that: Step A comprises: uniformly mixing the antioxidant and the ganoderma spore oil, then mixing with the emulsifier, heating and stirring until the emulsifier is completely dissolved and uniformly dissolved to form the oil phase.

3. The method for preparing the oral liquid of Ganoderma lucidum spore oil with improved taste as claimed in claim 2, characterized in that: In step A, the temperature of heating and stirring is 35-75°C.

4. The method for preparing the oral liquid of Ganoderma lucidum spore oil with improved taste as claimed in claim 1, characterized in that: In step B, the heating and insulation temperature is 55-75° C.; in step D, the pH value is adjusted to 6.5-8.0 by the pH adjuster; and in step F, the sterilization condition is that the F0 value is greater than 8.

5. The method for preparing the oral liquid of Ganoderma lucidum spore oil with improved taste as claimed in claim 1, characterized in that: The ganoderma spore oil is obtained by low-temperature carbon dioxide supercritical extraction of ganoderma spores; the antioxidant includes dilauryl thiodipropionate; and the pH regulator includes hydrochloric acid or sodium hydroxide.

6. An oral liquid of Ganoderma lucidum spore oil with improved taste obtained by the method for preparing the oral liquid of Ganoderma lucidum spore oil with improved taste as claimed in claim 1, characterized in that: The invention comprises the following components in the following mass ratios: 5-25% of ganoderma lucidum spore oil, 0.5-20% of emulsifier, 0.01-0.05% of antioxidant, 0.001-0.01% of pH regulator, and the balance of water.

7. The oral liquid of Ganoderma lucidum spore oil with improved taste as claimed in claim 6, characterized in that: The average particle size of the oral liquid of ganoderma lucidum spore oil with improved taste is no more than 250 nm.

Citation Information

Patent Citations

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