A natural gas trace adamantane analysis device and analysis method
By designing a natural gas trace adamantane analysis device, using jet condensation and filtration technology, the problems of low analysis efficiency and high equipment cost in the prior art are solved, and efficient trace adamantane analysis is achieved.
Patent Information
- Application Number
- CN202410282239.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-03-13
- Publication Date
- 2025-04-04
- Estimated Expiration
- 2044-03-13
AI Technical Summary
In the prior art, the analysis of trace amounts of natural gas requires a variety of equipment and cumbersome operating procedures, resulting in high equipment costs and low analysis efficiency.
A natural gas trace adamantane analysis device is designed, including a jet mechanism, a condenser, an analysis mechanism and a filtration mechanism. Natural gas is sprayed onto the condenser through a jet mechanism to condense. After the condensed liquid is filtered through the filter mechanism, it is sampled by a conveying pump and sent to a detection analyzer for analysis.
It realizes efficient sampling and analysis of natural gas trace adamantane, reducing equipment costs and operation complexity, and improving analysis efficiency.
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Figure CN118130749B_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of natural gas detection and analysis, and in particular to a natural gas trace adamantane analysis device and an analysis method. Background Art
[0002] Natural gas is a clean, low-carbon fossil energy source and one of the most important natural resources in human society. It will play an important role in the global energy green and low-carbon transformation. As the world transitions from coal to less polluting energy sources and tries to minimize the impact of global climate change, natural gas is a key fossil fuel. The main use of natural gas is as a fuel. It can be used to make carbon black, chemicals and liquefied petroleum gas. Propane and butane produced from natural gas are important raw materials for modern industry. Natural gas is stored in underground porous rock formations, including oilfield gas, gasfield gas, coalbed methane, mud volcano gas and biogenic gas, and a small amount is also found in coal seams. Natural gas contains many different compounds. The largest component of natural gas is methane, which accounts for more than 70% of the concentration of typical natural gas, followed by ethane, propane, butane and pentane. In addition, natural gas also contains a small amount of C6+-C14+ light hydrocarbons and non-hydrocarbon gases, such as carbon dioxide, nitrogen, hydrogen, carbon monoxide and water vapor.
[0003] Commercial natural gas reservoirs are formed by biogenic and thermogenic processes. 80% of the gas reservoirs discovered in the world are thermogenic. The main component of natural gas reservoirs is CH4, among which highly mature thermogenic natural gas often contains trace amounts of adamantane compounds. These compounds contain rich geochemical information and are of great significance for identifying the source and origin of weather and studying the migration, accumulation and preservation of natural gas. Since the content of adamantane in natural gas is very trace, its analysis is quite difficult.
[0004] At present, the existing analysis of trace diamond in natural gas requires the use of more equipment for sampling and analysis, the equipment cost is high, and the operation is cumbersome and time-consuming. Therefore, a natural gas trace diamond analysis device and analysis method are proposed to solve the above problems. Summary of the invention
[0005] 1. Technical issues to be resolved
[0006] In view of the deficiencies of the prior art, the present invention provides a natural gas trace adamantane analysis device and analysis method.
[0007] (II) Technical solution
[0008] To achieve the above-mentioned purpose, the present invention provides the following technical solutions: a natural gas trace adamantane analysis device, comprising a body, an injection mechanism, an analysis mechanism, a cover plate and a condenser, wherein the cover plate is fixedly mounted on the upper port of the body, and is used to seal the upper port of the body, and also plays a supporting role for the injection mechanism, the injection mechanism is arranged on the cover plate, and is used to inject natural gas onto the condenser in a rotating manner, the analysis mechanism is arranged on the outer wall of the body, and is used to sample and analyze the condensed natural gas liquid, wherein the injection mechanism comprises: a gas disk, which is arranged above the inside of the body, and is used to inject natural gas over a large area, an air outlet pipe, which is arranged at the bottom of the gas disk, and is used to inject the natural gas in the gas disk into the condenser, The condenser is fixedly installed inside the machine body and is located directly below the gas disk in the jet mechanism, and is used to condense the natural gas ejected from the gas disk into liquid droplets; the natural gas is introduced into the air inlet pipe through the delivery pipeline, and the natural gas is blown onto the condenser through the air outlet pipe on the gas disk, and the servo motor is started to drive the gear so that the gear ring drives the gas disk to rotate, so that the natural gas can fully contact with the condenser, thereby improving the efficiency of the natural gas condensation, and the condensed liquid is accumulated at the lower part of the machine body, and the delivery pump is started to sample the liquid through the sampling tube and transport it to the detection analyzer for detection and analysis, thereby realizing the integration of sampling and analysis, reducing the equipment cost and cumbersome steps, and improving the sampling and analysis efficiency of trace light hydrocarbon adamantane in natural gas.
[0009] Preferably, the jet mechanism further comprises an air inlet pipe and a servo motor, a sealed bearing is fixedly mounted on the lower port of the air inlet pipe, a connecting pipe is fixedly mounted on the inner wall of the inner ring of the sealed bearing, an air disc is fixedly mounted on the bottom of the connecting pipe, an air outlet pipe is arranged at the bottom of the air disc, a gear ring is fixedly mounted on the air disc, a rotating shaft is fixedly mounted on the output end of the servo motor, a gear is fixedly mounted on the lower end of the rotating shaft, and the gear is meshed with the gear ring;
[0010] Preferably, the analysis mechanism includes a detection analyzer and a placement plate, a delivery pump is fixedly installed on the placement plate, a delivery pipe is fixedly installed on the upper port of the delivery pump, the other end of the delivery pipe is connected to the detection analyzer, and a sampling tube is connected to the delivery pump.
[0011] Preferably, the air intake pipe is fixedly mounted on the cover plate, a delivery pipe is fixedly mounted on the upper end of the air intake pipe, the servo motor is fixedly mounted on the upper surface of the cover plate, a protective tube is fixedly mounted on the bottom of the cover plate, and the rotating shaft passes through the interior of the protective tube. The provision of the protective tube can protect the rotating shaft, making the rotating shaft more stable when rotating.
[0012] Preferably, a base is fixedly installed at the bottom of the body, the detection analyzer is fixedly installed on the outer wall of the body, and the placement plate is fixedly installed on the outer wall of the body. The arrangement of the placement plate can facilitate the installation and fixation of the delivery pump.
[0013] Preferably, a sampling port is provided at the right end of the body, the other end of the sampling tube is connected to the sampling port, a refrigerant inlet pipe is provided on the condenser, and a refrigerant outlet pipe is provided on the condenser. The sampling port and the sampling tube can facilitate sampling, detection and analysis of the condensed and liquefied natural gas.
[0014] Preferably, a conical bucket is fixedly installed inside the machine body, and the conical bucket is located directly below the condenser. The outer wall of the machine body is provided with a drain port, and the condensed liquid can be conveniently collected through the provision of the conical bucket.
[0015] Preferably, a filtering mechanism is provided inside the body, and the filtering mechanism includes a filter frame, a pull frame is fixedly installed on the left wall of the filter frame, a receiving block is fixedly installed inside the filter frame, a positioning column is fixedly connected to the upper surface of the receiving block, a filter plate is provided inside the filter frame, a positioning hole is provided on the filter plate, and the positioning column passes through the positioning hole. The condensed and liquefied natural gas droplets can be filtered by setting a conical bucket inside the body, and the conical bucket is located between the condenser and the filtering mechanism, so that the liquid passing through the condenser is concentrated on the conical bucket and falls onto the filter plate on the filtering mechanism, thereby facilitating the filtering of the condensed liquid.
[0016] Preferably, a side frame is fixedly installed on the right wall of the filter frame, a pull rod is provided on the side frame, a block is fixedly installed on the left end of the pull rod, a return spring is sleeved on the pull rod, and a handle is fixedly installed on the right end of the pull rod. The filter frame can be conveniently removed from the interior of the machine body by setting the pull rod. After the pull frame is disassembled from the machine body, the filter frame can be pulled out from the interior of the machine body through the pull frame. After pulling it out, the handle is pulled to the right to separate the block from the surface of the filter plate. At this time, the filter plate can be taken out from the filter frame, which is convenient for the staff to clean the impurities on the filter plate, further improving the practicability of the device.
[0017] A method for analyzing a natural gas trace adamantane analysis device, used for the natural gas trace light hydrocarbon adamantane analysis device, comprising the following steps
[0018] S1. The natural gas is introduced into the air inlet pipe through the transmission pipeline, and the natural gas is blown onto the condenser through the air outlet pipe on the gas disk. The servo motor is started to drive the gear so that the gear ring drives the gas disk to rotate, so that the natural gas can fully contact the condenser;
[0019] S2. The liquid droplets liquefied by the condenser are filtered through the filter plate on the filter mechanism to intercept and filter the impurities in the liquid droplets, and the filtered liquid droplets fall to the bottom of the body;
[0020] S3. Start the delivery pump to extract the condensed liquid inside the machine body through the sampling tube and deliver it to the detection analyzer to detect and analyze the trace light hydrocarbon adamantane content.
[0021] (III) Beneficial effects
[0022] Compared with the prior art, the present invention provides a natural gas trace adamantane analysis device and analysis method, which has the following beneficial effects:
[0023] 1. A natural gas trace diamondane analysis device and analysis method, by passing natural gas into the air inlet pipe through a delivery pipeline, the natural gas is blown onto the condenser through the air outlet pipe on the gas disk, and the servo motor is started to drive the gear so that the gear ring drives the gas disk to rotate, so that the natural gas can fully contact with the condenser, thereby improving the efficiency of natural gas condensation, and the condensed liquid is accumulated at the lower part of the body, and the delivery pump is started to sample the liquid through the sampling tube and transport it to the detection analyzer for detection and analysis, thereby realizing the integration of sampling and analysis, reducing the equipment cost and cumbersome steps, and improving the sampling and analysis efficiency of trace light hydrocarbon diamondane in natural gas.
[0024] 2. A natural gas trace diamondane analysis device and analysis method, by setting a filtering mechanism inside the body, the natural gas liquefied by the condenser droplets are filtered through the filter plate on the filtering mechanism, the impurities in the droplets are intercepted and filtered, and the filtered droplets fall to the bottom of the body, avoiding the large amount of liquid impurities after condensation in the natural gas affecting the detection and analysis data of trace light hydrocarbon diamondane in the natural gas.
[0025] 3. The natural gas trace diamond analysis device and analysis method are provided with a conical bucket inside the body, wherein the conical bucket is located between the condenser and the filter mechanism, so that the liquid passing through the condenser is concentrated on the conical bucket and falls onto the filter plate on the filter mechanism, thereby facilitating the filtering of the condensed liquid.
[0026] 4. A natural gas trace diamondane analysis device and analysis method, after the pull rack is disassembled from the body, the filter frame can be pulled out from the inside of the body through the pull rack, and after pulling out, the pull handle is pulled to the right to make the block separate from the surface of the filter plate. At this time, the filter plate can be taken out of the filter frame, which is convenient for the staff to clean the impurities on the filter plate, further improving the practicality of the device. BRIEF DESCRIPTION OF THE DRAWINGS
[0027] The accompanying drawings are used to provide a further understanding of the present invention and constitute a part of the specification. Together with the embodiments of the present invention, they are used to explain the present invention and do not constitute a limitation of the present invention. In the accompanying drawings:
[0028] Figure 1 It is a schematic diagram of the overall structure of the present invention;
[0029] Figure 2 It is a schematic diagram of the left structure of the present invention;
[0030] Figure 3 It is a schematic diagram of the internal structure of the present invention;
[0031] Figure 4 It is a schematic diagram of the structure of the jet mechanism of the present invention;
[0032] Figure 5 This is a schematic diagram of the gas disk structure of the present invention;
[0033] Figure 6 It is a schematic diagram of the structure of the analysis mechanism of the present invention;
[0034] Figure 7 It is a schematic diagram of the conical bucket structure of the present invention;
[0035] Figure 8 It is a schematic diagram of the structure of the filtering mechanism of the present invention;
[0036] Fig. 9 for Figure 8 A schematic diagram of the structure enlargement in the middle;
[0037] Fig.10 It is a schematic diagram of the filter frame structure of the present invention.
[0038] In the figure: 1, body; 2, jet mechanism; 201, air inlet pipe; 202, sealed bearing; 203, connecting pipe; 204, air disc; 205, air outlet pipe; 206, gear ring; 207, servo motor; 208, rotating shaft; 209, gear; 210, protective tube; 3, analysis mechanism; 301, detection analyzer; 302, placement plate; 303, delivery pump; 304, delivery pipe; 305, sampling Sample tube; 4. Filter mechanism; 401. Filter frame; 402. Filter plate; 403. Pull frame; 404. Side frame; 405. Pull rod; 406. Pull handle; 407. Return spring; 408. Block; 409. Receiver block; 410. Positioning column; 5. Cover plate; 6. Delivery pipeline; 7. Base; 8. Condenser; 9. Conical bucket; 10. Refrigerant inlet pipe; 11. Refrigerant outlet pipe; 12. Drain port. DETAILED DESCRIPTION
[0039] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0040] Examples of the embodiments are shown in the accompanying drawings, wherein the same or similar reference numerals throughout represent the same or similar elements or elements having the same or similar functions. The embodiments described below with reference to the accompanying drawings are exemplary and are intended to be used to explain the present invention, and should not be construed as limiting the present invention.
[0041] In the description of the present invention, it is necessary to understand that the terms "upper", "lower", "rear", "left", "right", "vertical", "bottom", "inside", "outside", etc., indicating directions or positional relationships, are based on the directions or positional relationships shown in the accompanying drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific direction, be constructed and operated in a specific direction, and therefore cannot be understood as a limitation on the present invention.
[0042] In the present invention, unless otherwise clearly specified and limited, the terms "installed", "connected", "connected", "fixed" and the like should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium, it can be the internal connection of two elements or the interaction relationship between two elements. For ordinary technicians in this field, the specific meanings of the above terms in the present invention can be understood according to specific circumstances. Example 1
[0043] like Figure 1-7As shown, the present invention provides a natural gas trace adamantane analysis device, including a body 1, an injection mechanism 2, an analysis mechanism 3, a cover plate 5 and a condenser 8. The cover plate 5 is fixedly mounted on the upper port of the body 1, and is used to seal the upper port of the body 1, and also plays a supporting role for the injection mechanism 2. The injection mechanism 2 is arranged on the cover plate 5, and is used to inject natural gas onto the condenser 8 in a rotating manner. The analysis mechanism 3 is arranged on the outer wall of the body 1, and is used to sample and analyze the condensed natural gas liquid. The injection mechanism 2 includes: a gas disk 204, which is arranged above the inside of the body 1, and is used to inject the natural gas over a large area. The gas outlet pipe 205 is arranged at the bottom of the gas disk 204, and is used to inject the natural gas in the gas disk 204 into the condenser 8. The condenser 8 is fixedly mounted inside the body 1, and is located directly below the gas disk 204 in the injection mechanism 2, and is used to condense the natural gas injected from the gas disk 204 into droplets.
[0044] Furthermore, in order to make the natural gas be uniformly and fully sprayed on the condenser 8, the purpose is achieved by setting the spray mechanism 2, which also includes an air inlet pipe 201 and a servo motor 207. The lower end of the air inlet pipe 201 is fixedly installed with a sealing bearing 202, and the inner wall of the inner ring of the sealing bearing 202 is fixedly installed with a connecting pipe 203. The bottom of the connecting pipe 203 is fixedly installed with a gas disk 204, and the bottom of the gas disk 204 is provided with an outlet pipe 205. The gas disk 204 is fixedly installed with a gear ring 206. The servo motor 207 is provided with a gear ring 206. A rotating shaft 208 is fixedly mounted on the output end of the motor 207, and a gear 209 is fixedly mounted on the lower end of the rotating shaft 208, and the gear 209 is meshed with the gear ring 206; by passing natural gas into the air inlet pipe 201 through the delivery pipeline 6, the natural gas is blown onto the condenser 8 through the air outlet pipe 205 on the air disk 204, and the servo motor 207 is started to drive the gear 209 so that the gear ring 206 drives the air disk 204 to rotate, so that the natural gas can fully contact the condenser 8, thereby improving the efficiency of natural gas condensation.
[0045] Furthermore, in order to detect and analyze the trace light hydrocarbon adamantane in the liquid natural gas formed after condensation, the liquid natural gas is detected and analyzed by the analysis mechanism 3, which includes a detection analyzer 301 and a placement plate 302. A delivery pump 303 is fixedly installed on the placement plate 302, and a delivery pipe 304 is fixedly installed on the upper port of the delivery pump 303. The other end of the delivery pipe 304 is connected to the detection analyzer 301, and a sampling pipe 305 is connected to the delivery pump 303; the delivery pump 303 is started to sample the liquid natural gas through the sampling pipe 305 and transport the sample to the detection analyzer 301 for detection and analysis, thereby realizing the integration of sampling and analysis, reducing the equipment cost and cumbersome steps, and improving the sampling and analysis efficiency of the trace light hydrocarbon adamantane in the natural gas.
[0046] Furthermore, in order to introduce natural gas into the jet mechanism 2, the delivery pipeline 6 is connected to the air intake pipe 201 to achieve the purpose of natural gas delivery. The air intake pipe 201 is fixedly installed on the cover plate 5, the delivery pipeline 6 is fixedly installed on the upper end of the air intake pipe 201, the servo motor 207 is fixedly installed on the upper surface of the cover plate 5, and the bottom of the cover plate 5 is fixedly installed with a protective tube 210. The rotating shaft 208 passes through the interior of the protective tube 210. The setting of the protective tube 210 can protect the rotating shaft 208, making the rotating shaft 208 more stable when rotating. The delivery pipeline 6 can deliver natural gas to the air intake pipe 201 of the jet mechanism 2, and the air intake pipe 201 is connected to the connecting pipe 203, so that the natural gas can enter the gas disk 204.
[0047] like Figure 1 , 6 As shown, in order to protect the bottom of the body 1 and fix the delivery pump 303, a base 7 is fixedly installed at the bottom of the body 1, the detection analyzer 301 is fixedly installed on the outer wall of the body 1, and the placement plate 302 is fixedly installed on the outer wall of the body 1. The placement of the placement plate 302 can facilitate the installation and fixation of the delivery pump 303, and the setting of the base 7 can prevent the bottom of the body 1 from directly contacting the ground, thereby achieving the protection of the bottom of the body 1.
[0048] like Figure 3 , 6 As shown, in order to facilitate the analysis mechanism 3 to sample, detect and analyze the liquid natural gas, a sampling port is opened at the right end of the body 1, and the other end of the sampling tube 305 is connected to the sampling port. A refrigerant inlet pipe 10 is provided on the condenser 8, and a refrigerant outlet pipe 11 is provided on the condenser 8. The setting of the sampling port and the sampling tube 305 can facilitate sampling, detection and analysis of the condensed and liquefied natural gas.
[0049] like Figure 3 , 7 As shown, in order to concentrate the liquefied natural gas droplets condensed from the condenser 8 onto the filtering mechanism 4, a conical bucket 9 is fixedly installed inside the body 1. The conical bucket 9 is located directly below the condenser 8. The outer wall of the body 1 is provided with a drain port 12. The setting of the conical bucket 9 can conveniently concentrate the condensed liquid so that it falls onto the filtering mechanism 4. Example 2
[0050] like Figure 8-10As shown, in order to prevent the large amount of liquid impurities after condensation in natural gas from affecting the detection and analysis data of trace light hydrocarbon adamantane in natural gas, a filtering mechanism 4 is arranged inside the body 1, and the filtering mechanism 4 includes a filtering frame 401, and a pull frame 403 is fixedly installed on the left wall of the filtering frame 401, and a receiving block 409 is fixedly installed inside the filtering frame 401, and a positioning column 410 is fixedly connected to the upper surface of the receiving block 409. A filter plate 402 is arranged inside the filtering frame 401, and a positioning hole is opened on the filter plate 402. The positioning column 410 runs through the interior of the positioning hole. The setting of the filtering mechanism 4 can filter the condensed and liquefied natural gas droplets. By arranging a filtering mechanism 4 inside the body 1, the liquid droplets of the natural gas liquefied by the condenser 8 are filtered through the filter plate 402 on the filtering mechanism 4, and the impurities in the liquid droplets are intercepted and filtered. The filtered liquid droplets fall on the inner bottom of the body 1, so as to avoid the influence of a large amount of liquid impurities in the natural gas after condensation on the detection and analysis data of trace light hydrocarbon adamantane in the natural gas. By arranging a conical bucket 9 inside the body 1, the conical bucket 9 is located between the condenser 8 and the filtering mechanism 4, so that the liquid passing through the condenser 8 is concentrated on the conical bucket 9 and falls onto the filter plate 402 on the filtering mechanism 4, thereby facilitating the filtering of the condensed liquid.
[0051] like Fig. 9 , 10 As shown, in order to facilitate the removal of the filter plate 402 on the filter mechanism 4 for cleaning impurities, a side frame 404 is fixedly installed on the right wall of the filter frame 401, a pull rod 405 is arranged on the side frame 404, a block 408 is fixedly installed on the left end of the pull rod 405, a return spring 407 is sleeved on the pull rod 405, and a handle 406 is fixedly installed on the right end of the pull rod 405. Through the arrangement of the pull rod 405, the filter frame 401 can be conveniently taken out from the inside of the machine body 1. After the pull frame 403 is removed from the machine body 1, the filter frame 401 can be pulled out from the inside of the machine body 1 through the pull frame 403. After being pulled out, the handle 406 is pulled to the right to separate the block 408 from the surface of the filter plate 402. At this time, the filter plate 402 can be taken out from the filter frame 401, which is convenient for the staff to clean the impurities on the filter plate 402, further improving the practicality of the device. Example 3
[0052] like Figure 1-10 As shown, based on Example 1, the present invention provides an analysis method for a natural gas trace adamantane analysis device, comprising the following steps:
[0053] S1. The natural gas is introduced into the air inlet pipe 201 through the delivery pipeline 6, and the natural gas is blown onto the condenser 8 through the air outlet pipe 205 on the air disk 204. The servo motor 207 is started to drive the gear 209 so that the gear ring 206 drives the air disk 204 to rotate, so that the natural gas can fully contact the condenser 8;
[0054] S2, the liquid droplets liquefied by the condenser 8 are filtered through the filter plate 402 on the filter mechanism 4, and the impurities in the liquid droplets are intercepted and filtered, and the filtered liquid droplets fall to the inner bottom of the body 1;
[0055] S3, start the delivery pump 303 to extract the condensed liquid inside the body 1 through the sampling tube 305, and deliver it to the detection analyzer 301 to detect and analyze the trace light hydrocarbon adamantane.
[0056] The working principle of the natural gas trace adamantane analysis device and analysis method is described in detail below.
[0057] like Figure 1-10 As shown, when in use, natural gas is introduced into the air inlet pipe 201 through the delivery pipeline 6, and the natural gas is blown onto the condenser 8 through the air outlet pipe 205 on the gas disc 204. The servo motor 207 is started to drive the gear 209 so that the gear ring 206 drives the gas disc 204 to rotate, so that the natural gas can fully contact with the condenser 8, thereby improving the efficiency of natural gas condensation. By arranging a filtering mechanism 4 inside the body 1, the liquid droplets of the natural gas after liquefaction through the condenser 8 are filtered through the filter plate 402 on the filtering mechanism 4, and the impurities in the liquid droplets are intercepted and filtered. The filtered liquid droplets fall on the bottom of the body 1, thereby preventing the liquid impurities in the natural gas from being condensed. In order to improve the detection and analysis data of trace light hydrocarbon adamantane in natural gas, a conical bucket 9 is arranged inside the body 1, and the conical bucket 9 is located between the condenser 8 and the filter mechanism 4, so that the liquid passing through the condenser 8 is concentrated on the conical bucket 9 and falls onto the filter plate 402 on the filter mechanism 4, thereby facilitating the filtering of the condensed liquid. The condensed and filtered liquid is accumulated at the lower part of the body 1, and the delivery pump 303 is started to sample the liquid through the sampling tube 305 and deliver it to the detection analyzer 301 for detection and analysis, thereby realizing the integration of sampling and analysis, reducing the equipment cost and cumbersome steps, and improving the sampling and analysis efficiency of trace light hydrocarbon adamantane in natural gas.
[0058] The above shows and describes the basic principles, main features and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited by the above embodiments. The above embodiments and descriptions are only preferred examples of the present invention and are not intended to limit the present invention. Without departing from the spirit and scope of the present invention, the present invention may have various changes and improvements, which fall within the scope of the present invention. The scope of protection of the present invention is defined by the attached claims and their equivalents.
Claims
1. A natural gas trace adamantane analysis device, characterized in that: It comprises a body (1), an air injection mechanism (2), an analysis mechanism (3), a cover plate (5) and a condenser (8); The cover plate (5) is fixedly mounted on the upper port of the machine body (1) and is used to seal the upper port of the machine body (1), while also supporting the jet mechanism (2); The jet mechanism (2) is arranged on the cover plate (5) and is used to jet natural gas onto the condenser (8) in a rotating manner; The analysis mechanism (3) is arranged on the outer wall of the body (1) and is used to sample and analyze the condensed natural gas liquid; The jet mechanism (2) includes: An air disc (204) is arranged above the interior of the machine body (1) and is used to spray the air heat over a large area; An air outlet pipe (205) is disposed at the bottom of the gas tray (204) and is used to spray the natural gas in the gas tray (204) into the condenser (8); The condenser (8) is fixedly mounted inside the machine body (1) and is located directly below the gas disk (204) in the jet mechanism (2), and is used to condense the natural gas ejected from the gas disk (204) into liquid droplets.
2. A natural gas trace adamantane analysis device according to claim 1, characterized in that: The jet mechanism (2) further comprises an air intake pipe (201) and a servo motor (207); a sealing bearing (202) is fixedly mounted on the lower end of the air intake pipe (201); a connecting pipe (203) is fixedly mounted on the inner wall of the inner ring of the sealing bearing (202); an air disk (204) is fixedly mounted on the bottom of the connecting pipe (203); an air outlet pipe (205) is arranged at the bottom of the air disk (204); a gear ring (206) is fixedly mounted on the air disk (204); a rotating shaft (208) is fixedly mounted on the output end of the servo motor (207); a gear (209) is fixedly mounted on the lower end of the rotating shaft (208); and the gear (209) meshes with the gear ring (206).
3. A natural gas trace adamantane analysis device according to claim 1, characterized in that: The analysis mechanism (3) comprises a detection analyzer (301) and a placement plate (302), a delivery pump (303) being fixedly mounted on the placement plate (302), a delivery pipe (304) being fixedly mounted on an upper end of the delivery pump (303), the other end of the delivery pipe (304) being docked with the detection analyzer (301), and a sampling pipe (305) being connected to the delivery pump (303).
4. A natural gas trace adamantane analysis device according to claim 2, characterized in that: The air intake pipe (201) is fixedly mounted on the cover plate (5); a delivery pipe (6) is fixedly mounted on the upper end of the air intake pipe (201); the servo motor (207) is fixedly mounted on the upper surface of the cover plate (5); a protective tube (210) is fixedly mounted on the bottom of the cover plate (5); and the rotating shaft (208) passes through the interior of the protective tube (210).
5. A natural gas trace adamantane analysis device according to claim 3, characterized in that: A base (7) is fixedly mounted on the bottom of the machine body (1), the detection analyzer (301) is fixedly mounted on the outer wall of the machine body (1), and the placement plate (302) is fixedly mounted on the outer wall of the machine body (1).
6. A natural gas trace adamantane analysis device according to claim 3, characterized in that: A sampling port is provided at the right end of the machine body (1), and the other end of the sampling tube (305) is connected to the sampling port. A refrigerant inlet pipe (10) is provided on the condenser (8), and a refrigerant outlet pipe (11) is provided on the condenser (8).
7. The natural gas trace adamantane analysis device according to claim 1, characterized in that: A conical bucket (9) is fixedly installed inside the machine body (1), and the conical bucket (9) is located directly below the condenser (8). A liquid drain port (12) is provided on the outer wall of the machine body (1).
8. The natural gas trace adamantane analysis device according to claim 1, characterized in that: A filter mechanism (4) is arranged inside the machine body (1), and the filter mechanism (4) comprises a filter frame (401), a pull frame (403) is fixedly installed on the left wall of the filter frame (401), a receiving block (409) is fixedly installed inside the filter frame (401), a positioning column (410) is fixedly connected to the upper surface of the receiving block (409), a filter plate (402) is arranged inside the filter frame (401), a positioning hole is opened on the filter plate (402), and the positioning column (410) passes through the inside of the positioning hole.
9. A natural gas trace adamantane analysis device according to claim 8, characterized in that: A side frame (404) is fixedly mounted on the right wall of the filter frame (401), a pull rod (405) is provided on the side frame (404), a clamping block (408) is fixedly mounted on the left end of the pull rod (405), a return spring (407) is sleeved on the pull rod (405), and a handle (406) is fixedly mounted on the right end of the pull rod (405).
10. An analysis method for a natural gas trace adamantane analysis device, used for using the natural gas trace light hydrocarbon adamantane analysis device according to any one of claims 1 to 9, characterized in that: The following steps are involved: S1. The natural gas is introduced into the air inlet pipe (201) through the delivery pipeline (6), and the natural gas is blown onto the condenser (8) through the air outlet pipe (205) on the air disk (204). The servo motor (207) is started to drive the gear (209) so that the gear ring (206) drives the air disk (204) to rotate, so that the natural gas can fully contact the condenser (8); S2, the liquid droplets liquefied by the condenser (8) are filtered through the filter plate (402) on the filter mechanism (4), impurities in the liquid droplets are intercepted and filtered, and the filtered liquid droplets fall to the bottom of the body (1); S3, starting the delivery pump (303) to extract the condensed liquid inside the body (1) through the sampling tube (305), and delivering it to the detection analyzer (301), and performing content detection and analysis on the trace light hydrocarbon adamantane.
Citation Information
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