Resource utilization system and method for acetic acid-containing wastewater in acrylic acid production

By designing a resource utilization system that includes a concentration separation module for acetic acid wastewater, n-butyl acetate preparation module and sodium polyacrylate preparation module, the problem of acetic acid wastewater treatment in acrylic production is solved, efficient concentration and resource utilization is achieved, and high-purity n-butyl acetate and sodium polyacrylate are produced, reducing energy consumption and production costs.

CN119680484APending Publication Date: 2025-03-25PINGHU PETROCHEM +1
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Patent Information

Application Number
CN202411788497.8
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-12-06
Publication Date
2025-03-25

AI Technical Summary

Technical Problem

The acetic acid-containing wastewater produced in acrylic acid production cannot be directly entered into the biochemical treatment, resulting in high energy consumption and production costs of incineration treatment, and at the same time, the effective components cannot be fully utilized.

Method used

A resource utilization system was designed, including acetic acid wastewater concentration separation module, n-butyl acetate preparation module and sodium polyacrylate preparation module. Acetic acid and acrylic acid in wastewater were extracted and utilized through technical means such as liquid phase film concentration, multi-stage tandem reactor and distillation tower.

Benefits of technology

It has achieved efficient concentration and resource utilization of acetic acid wastewater, and produced high-purity n-butyl acetate and sodium polyacrylate, reducing energy consumption and production costs, while reducing environmental pollution.

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Abstract

The invention discloses a resource utilization system and method for acetic acid-containing wastewater in acrylic acid production, which are used for resource utilization of a large amount of acetic acid-containing wastewater generated in industrial production of acrylic acid through cooperation of multiple working sections. Acetic acid and acrylic acid contained in the wastewater are separated and synthesized to obtain 99.5 wt% butyl acetate and 50 wt% sodium polyacrylate aqueous solution products. The method has the advantages of low equipment investment cost, flexible production, continuous process, long reaction retention time, wide available concentration range of acetic acid and acrylic acid raw materials, high conversion per pass of n-butyl alcohol, environmental friendliness and the like.
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