Preparation process of dendrobium huoshanense concentrated solution suitable for facial mask
Through the process of cleaning, cutting, crushing, cooking, low-temperature treatment, adding ethanol, ultrafiltration and mixing effective substances of the mask, the problem of low concentration of active ingredients in the Huoshan Dendrobium concentrate was solved, and the effect of using the mask and the cleanliness of the concentrate was significantly improved.
Patent Information
- Application Number
- CN202510033564.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-01-09
- Publication Date
- 2025-05-02
AI Technical Summary
The concentration of active ingredients in Huoshan Dendrobium concentrate is not high, resulting in poor facial mask use.
Through cleaning, cutting, crushing, cooking, low-temperature treatment, adding ethanol, ultrafiltration treatment and mixing effective substances of the mask, the effective ingredient concentration of Huoshan Dendrobium concentrate is improved.
The effective ingredient concentration of Huoshan Dendrobium concentrate was significantly improved, the effect of using the mask was enhanced, and the cleanliness of the concentrate was improved through ultrafiltration.
Abstract
Description
Technical Field
[0001] The invention relates to the field of Huoshan dendrobium concentrated liquid technology, and in particular to a preparation process of Huoshan dendrobium concentrated liquid suitable for facial masks. Background Art
[0002] Huoshan Dendrobium Concentrate is a healthy drink made from Huoshan Dendrobium through physical extraction technology. Huoshan Dendrobium has the effects of harmonizing yin and yang, improving immunity, strengthening the spleen and stomach, and delaying aging. These effects also have a positive impact on skin health.
[0003] Huoshan Dendrobium concentrate can be used as a facial mask to condition the skin and improve skin quality. When preparing the Huoshan Dendrobium concentrate, the dry Huoshan Dendrobium stems are steamed and the boiled extract is treated at low temperature to facilitate concentration. However, some substances in the Huoshan Dendrobium concentrate do not release their effective ingredients during this production process, resulting in a low concentration of the effective ingredients in the concentrate and a poor effect as a facial mask. Summary of the invention
[0004] 1. Technical issues to be resolved
[0005] In view of the deficiencies in the prior art, the present invention provides a preparation process of a Huoshan Dendrobium concentrate suitable for a facial mask, which solves the problem that the concentration of active ingredients in the Huoshan Dendrobium concentrate is not high and the facial mask effect is not good.
[0006] (II) Technical solution
[0007] To achieve the above objectives, the present invention is implemented by the following technical scheme: A preparation process of Huoshan Dendrobium concentrate suitable for facial mask, comprising the following steps:
[0008] S1. Cleaning materials: cleaning and drying the dried stems of Dendrobium huoshanense;
[0009] S2, cutting and crushing: cutting the dry stems of Dendrobium huoshanense in S1, crushing them by a crusher, and filtering them;
[0010] S3, material cooking: placing the material in S2 in water for cooking;
[0011] S4, low temperature treatment: filtering the extract in S3 and performing low temperature condensation treatment;
[0012] S5, adding ethanol: adding the ethanol solution into S4, stirring and filtering;
[0013] S6, ultrafiltration treatment: filtering the S5 using an ultrafiltration membrane;
[0014] S7, preparation: adding effective substances for the facial mask to S6.
[0015] Preferably, the effective substances in the facial mask in S7 include vitamin C, collagen, sodium hyaluronate and xanthan gum, and the proportions of the Huoshan dendrobium concentrate, vitamin C, collagen, sodium hyaluronate and xanthan gum are: Huoshan dendrobium concentrate is 60-80 parts, vitamin C is 5-10 parts, collagen is 15-20 parts, sodium hyaluronate is 5-10 parts, and xanthan gum is 20-30 parts.
[0016] Preferably, the pulverizer in S2 uses a vacuum low-temperature liquid continuous dryer for pulverization.
[0017] Preferably, the S3 cooking time is 3-5 hours.
[0018] Preferably, the S5 is added and stirred for 10-20 minutes, and then allowed to stand for 0.5-1 hour, and filtered by centrifugal filtration.
[0019] Preferably, the temperature of the S4 low temperature treatment is 50°C.
[0020] Preferably, the S7 is prepared and added with effective substances for the facial mask, and the effective substances for the facial mask include vitamin C, collagen, sodium hyaluronate and xanthan gum, which are mixed with water and stirred, indicating that the mixture is D. The mixture D is mixed with the Huoshan Dendrobium concentrate and stirred, and filtered, and the filtering method is multiple centrifugal filtration.
[0021] (III) Beneficial effects
[0022] The present invention provides a preparation process of Huoshan Dendrobium officinale concentrated solution suitable for facial mask, which has the following beneficial effects:
[0023] By arranging to cut, crush and add ethanol to the material, the amount of effective substances released from the dry Huoshan Dendrobium stems is increased, the use effect of the Huoshan Dendrobium concentrated liquid mask is increased, and the concentrated liquid is filtered through an ultrafiltration membrane to facilitate filtering of impurities in the concentrated liquid and increase the cleanliness of the concentrated liquid. DETAILED DESCRIPTION
[0024] The technical solutions in the embodiments of the present invention are described clearly and completely below. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of them. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0025] Embodiment 1:
[0026] A preparation process of a Huoshan Dendrobium concentrate suitable for a facial mask comprises the following steps:
[0027] S1. Cleaning materials: Cleaning and drying the dried stems of Dendrobium huoshanense. Drying is convenient for later cutting and crushing. The dried stems of Dendrobium huoshanense are tilted to clean the stains in the stems.
[0028] S2, cutting and crushing: cutting the dry stems of Dendrobium huoshanense in S1, crushing them by a crusher, filtering, crushing and cutting, so that the effective ingredients in the dry stems of Dendrobium huoshanense are released, and filtering the crushed powder material to filter out impurities.
[0029] S3, material cooking: the material in S2 is placed in water for cooking, the crusher in S2 uses a vacuum low-temperature liquid continuous dryer for crushing, and the cooking time in S3 is 3 hours.
[0030] S4, low temperature treatment: the extract in S3 is filtered and subjected to low temperature condensation treatment. The temperature of S4 low temperature treatment is 50°C. Low temperature treatment helps to retain the heat-sensitive components in Huoshan Dendrobium.
[0031] S5, adding ethanol: adding ethanol solution to S4, stirring and filtering, adding S5 and stirring for 10 minutes, and standing for 0.5 hours, filtering by centrifugal filtration, adding ethanol to precipitate effective ingredients such as polysaccharides, while other impurities are dissolved in ethanol, standing and filtering to filter out the precipitate, thereby increasing the concentration of effective ingredients in the Huoshan Dendrobium concentrate.
[0032] S6, ultrafiltration treatment: Use ultrafiltration membrane to filter S5 to remove impurities.
[0033] S7. Preparation: Add effective substances for facial mask into S6. The effective substances for facial mask in S7 include vitamin C, collagen, sodium hyaluronate and xanthan gum. The proportions of Huoshan dendrobium concentrate, vitamin C, collagen, sodium hyaluronate and xanthan gum are as follows: Huoshan dendrobium concentrate is 60 parts, vitamin C is 5 parts, collagen is 15 parts, sodium hyaluronate is 5 parts and xanthan gum is 20 parts. S7 is prepared and added with effective substances for facial mask. The effective substances for facial mask include vitamin C, collagen, sodium hyaluronate and xanthan gum which are mixed with water and stirred, indicating that the mixture is D. The mixture D is mixed with Huoshan dendrobium concentrate and stirred, and filtered, and the filtration method is multiple centrifugal filtration.
[0034] Embodiment 2:
[0035] A preparation process of a Huoshan Dendrobium concentrate suitable for a facial mask comprises the following steps:
[0036] S1. Cleaning materials: Cleaning and drying the dried stems of Dendrobium huoshanense. Drying is convenient for later cutting and crushing. The dried stems of Dendrobium huoshanense are tilted to clean the stains in the stems.
[0037] S2, cutting and crushing: cutting the dry stems of Dendrobium huoshanense in S1, crushing them by a crusher, filtering, crushing and cutting, so that the effective ingredients in the dry stems of Dendrobium huoshanense are released, and filtering the crushed powder material to filter out impurities.
[0038] S3, material cooking: the material in S2 is placed in water for cooking, the crusher in S2 uses a vacuum low-temperature liquid continuous dryer for crushing, and the cooking time in S3 is 4 hours.
[0039] S4, low temperature treatment: the extract in S3 is filtered and subjected to low temperature condensation treatment. The temperature of S4 low temperature treatment is 50°C. Low temperature treatment helps to retain the heat-sensitive components in Huoshan Dendrobium.
[0040] S5, adding ethanol: adding ethanol solution to S4, stirring and filtering, S5 adding stirring time is 15min, and standing for 0.8 hours, filtering method is centrifugal filtration, adding ethanol, so that the effective ingredients such as polysaccharides are precipitated, and other impurities are dissolved in ethanol, standing and filtering to filter the precipitate, thereby increasing the concentration of the effective ingredients of the Huoshan Dendrobium concentrate.
[0041] S6, ultrafiltration treatment: Use ultrafiltration membrane to filter S5 to remove impurities.
[0042] S7, preparation: adding effective substances for facial mask to S6, the effective substances for facial mask in S7 include vitamin C, collagen, sodium hyaluronate and xanthan gum, the proportions of Huoshan dendrobium concentrate, vitamin C, collagen, sodium hyaluronate and xanthan gum are: 70 parts of Huoshan dendrobium concentrate, 8 parts of vitamin C, 18 parts of collagen, 8 parts of sodium hyaluronate and 25 parts of xanthan gum, S7 is prepared and added with effective substances for facial mask, the effective substances for facial mask include vitamin C, collagen, sodium hyaluronate and xanthan gum mixed with water, stirred, denoted as mixture D, mixture D is mixed with Huoshan dendrobium concentrate and stirred, and filtered, and the filtration method is multiple centrifugal filtration.
[0043] Embodiment three:
[0044] A preparation process of a Huoshan Dendrobium concentrate suitable for a facial mask comprises the following steps:
[0045] S1. Cleaning materials: Cleaning and drying the dried stems of Dendrobium huoshanense. Drying is convenient for later cutting and crushing. The dried stems of Dendrobium huoshanense are tilted to clean the stains in the stems.
[0046] S2, cutting and crushing: cutting the dry stems of Dendrobium huoshanense in S1, crushing them by a crusher, filtering, crushing and cutting, so that the effective ingredients in the dry stems of Dendrobium huoshanense are released, and filtering the crushed powder material to filter out impurities.
[0047] S3, material cooking: the material in S2 is placed in water for cooking, the crusher in S2 uses a vacuum low-temperature liquid continuous dryer for crushing, and the cooking time in S3 is 4.5 hours.
[0048] S4, low temperature treatment: the extract in S3 is filtered and subjected to low temperature condensation treatment. The temperature of S4 low temperature treatment is 50°C. Low temperature treatment helps to retain the heat-sensitive components in Huoshan Dendrobium.
[0049] S5, adding ethanol: adding ethanol solution to S4, stirring and filtering, adding S5 and stirring for 18 minutes, and standing for 0.9 hours, filtering by centrifugal filtration, adding ethanol to precipitate effective ingredients such as polysaccharides, while other impurities are dissolved in ethanol, standing and filtering to filter out the precipitate, thereby increasing the concentration of effective ingredients in the Huoshan Dendrobium concentrate.
[0050] S6, ultrafiltration treatment: Use ultrafiltration membrane to filter S5 to remove impurities.
[0051] S7, preparation: adding effective substances for facial mask to S6, the effective substances for facial mask in S7 include vitamin C, collagen, sodium hyaluronate and xanthan gum, the proportions of Huoshan dendrobium concentrate, vitamin C, collagen, sodium hyaluronate and xanthan gum are: Huoshan dendrobium concentrate is 75 parts, vitamin C is 7 parts, collagen is 17 parts, sodium hyaluronate is 7 parts, xanthan gum is 27 parts, S7 is prepared and added with effective substances for facial mask, the effective substances for facial mask include vitamin C, collagen, sodium hyaluronate and xanthan gum mixed with water, stirred, denoted as mixture D, mixture D is mixed with Huoshan dendrobium concentrate and stirred, and filtered, and the filtration method is multiple centrifugal filtration.
[0052] Implementation 4:
[0053] A preparation process of a Huoshan Dendrobium concentrate suitable for a facial mask comprises the following steps:
[0054] S1. Cleaning materials: Cleaning and drying the dried stems of Dendrobium huoshanense. Drying is convenient for later cutting and crushing. The dried stems of Dendrobium huoshanense are tilted to clean the stains in the stems.
[0055] S2, cutting and crushing: cutting the dry stems of Dendrobium huoshanense in S1, crushing them by a crusher, filtering, crushing and cutting, so that the effective ingredients in the dry stems of Dendrobium huoshanense are released, and filtering the crushed powder material to filter out impurities.
[0056] S3, material cooking: the material in S2 is placed in water for cooking, the crusher in S2 uses a vacuum low-temperature liquid continuous dryer for crushing, and the cooking time in S3 is 4.6 hours.
[0057] S4, low temperature treatment: the extract in S3 is filtered and subjected to low temperature condensation treatment. The temperature of S4 low temperature treatment is 50°C. Low temperature treatment helps to retain the heat-sensitive components in Huoshan Dendrobium.
[0058] S5, adding ethanol: adding ethanol solution to S4, stirring and filtering, S5 adding stirring time is 19 minutes, and standing for 0.9 hours, filtering method is centrifugal filtration, adding ethanol, so that the effective ingredients such as polysaccharides are precipitated, and other impurities are dissolved in ethanol, standing and filtering to filter out the precipitate, thereby increasing the concentration of the effective ingredients of the Huoshan Dendrobium concentrate.
[0059] S6, ultrafiltration treatment: Use ultrafiltration membrane to filter S5 to remove impurities.
[0060] S7, preparation: adding effective substances for facial mask to S6, the effective substances for facial mask in S7 include vitamin C, collagen, sodium hyaluronate and xanthan gum, the proportions of Huoshan dendrobium concentrate, vitamin C, collagen, sodium hyaluronate and xanthan gum are: Huoshan dendrobium concentrate is 78 parts, vitamin C is 8 parts, collagen is 18 parts, sodium hyaluronate is 8 parts, xanthan gum is 28 parts, S7 is prepared and added with effective substances for facial mask, the effective substances for facial mask include vitamin C, collagen, sodium hyaluronate and xanthan gum mixed with water, stirred, denoted as mixture D, mixture D is mixed with Huoshan dendrobium concentrate and stirred, and filtered, and the filtration method is multiple centrifugal filtration.
[0061] Embodiment five:
[0062] A preparation process of a Huoshan Dendrobium concentrate suitable for a facial mask comprises the following steps:
[0063] S1. Cleaning materials: Cleaning and drying the dried stems of Dendrobium huoshanense. Drying is convenient for later cutting and crushing. The dried stems of Dendrobium huoshanense are tilted to clean the stains in the stems.
[0064] S2, cutting and crushing: cutting the dry stems of Dendrobium huoshanense in S1, crushing them by a crusher, filtering, crushing and cutting, so that the effective ingredients in the dry stems of Dendrobium huoshanense are released, and filtering the crushed powder material to filter out impurities.
[0065] S3, material cooking: the material in S2 is placed in water for cooking, the crusher in S2 uses a vacuum low-temperature liquid continuous dryer for crushing, and the cooking time in S3 is 4.9 hours.
[0066] S4, low temperature treatment: the extract in S3 is filtered and subjected to low temperature condensation treatment. The temperature of S4 low temperature treatment is 50°C. Low temperature treatment helps to retain the heat-sensitive components in Huoshan Dendrobium.
[0067] S5, adding ethanol: adding ethanol solution to S4, stirring and filtering, S5 adding stirring time is 19 minutes, and standing for 0.9 hours, filtering method is centrifugal filtration, adding ethanol, so that the effective ingredients such as polysaccharides are precipitated, and other impurities are dissolved in ethanol, standing and filtering to filter out the precipitate, thereby increasing the concentration of the effective ingredients of the Huoshan Dendrobium concentrate.
[0068] S6, ultrafiltration treatment: Use ultrafiltration membrane to filter S5 to remove impurities.
[0069] S7, preparation: adding effective substances for facial mask to S6, the effective substances for facial mask in S7 include vitamin C, collagen, sodium hyaluronate and xanthan gum, the proportions of Huoshan dendrobium concentrate, vitamin C, collagen, sodium hyaluronate and xanthan gum are: Huoshan dendrobium concentrate is 79 parts, vitamin C is 9 parts, collagen is 19 parts, sodium hyaluronate is 9 parts, xanthan gum is 29 parts, S7 is prepared and added with effective substances for facial mask, the effective substances for facial mask include vitamin C, collagen, sodium hyaluronate and xanthan gum mixed with water, stirred, denoted as mixture D, mixture D is mixed with Huoshan dendrobium concentrate and stirred, and filtered, and the filtration method is multiple centrifugal filtration.
[0070] Embodiment six:
[0071] A preparation process of a Huoshan Dendrobium concentrate suitable for a facial mask comprises the following steps:
[0072] S1. Cleaning materials: Cleaning and drying the dried stems of Dendrobium huoshanense. Drying is convenient for later cutting and crushing. The dried stems of Dendrobium huoshanense are tilted to clean the stains in the stems.
[0073] S2, cutting and crushing: cutting the dry stems of Dendrobium huoshanense in S1, crushing them by a crusher, filtering, crushing and cutting, so that the effective ingredients in the dry stems of Dendrobium huoshanense are released, and filtering the crushed powder material to filter out impurities.
[0074] S3, material cooking: the material in S2 is placed in water for cooking, the crusher in S2 uses a vacuum low-temperature liquid continuous dryer for crushing, and the cooking time in S3 is 5 hours.
[0075] S4, low temperature treatment: the extract in S3 is filtered and subjected to low temperature condensation treatment. The temperature of S4 low temperature treatment is 50°C. Low temperature treatment helps to retain the heat-sensitive components in Huoshan Dendrobium.
[0076] S5, adding ethanol: adding ethanol solution to S4, stirring and filtering, adding S5 and stirring for 20 minutes, and letting it stand for 1 hour, filtering by centrifugal filtration, adding ethanol to precipitate effective ingredients such as polysaccharides, while other impurities are dissolved in ethanol, letting it stand and filtering to filter out the precipitate, thereby increasing the concentration of effective ingredients in the Huoshan Dendrobium concentrate.
[0077] S6, ultrafiltration treatment: Use ultrafiltration membrane to filter S5 to remove impurities.
[0078] S7. Preparation: Add effective substances for facial mask into S6. The effective substances for facial mask in S7 include vitamin C, collagen, sodium hyaluronate and xanthan gum. The proportions of Huoshan dendrobium concentrate, vitamin C, collagen, sodium hyaluronate and xanthan gum are as follows: Huoshan dendrobium concentrate is 80 parts, vitamin C is 10 parts, collagen is 20 parts, sodium hyaluronate is 10 parts and xanthan gum is 30 parts. S7 is prepared and added with effective substances for facial mask. The effective substances for facial mask include vitamin C, collagen, sodium hyaluronate and xanthan gum which are mixed with water and stirred, indicating that the mixture is D. The mixture D is mixed with Huoshan dendrobium concentrate and stirred, and filtered, and the filtration method is multiple centrifugal filtration.
[0079] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.
Claims
1. A preparation process of a Huoshan Dendrobium concentrate suitable for a facial mask, characterized in that: The following steps are involved: S1. Cleaning materials: cleaning and drying the dried stems of Dendrobium huoshanense; S2, cutting and crushing: cutting the dry stems of Dendrobium huoshanense in S1, crushing them by a crusher, and filtering them; S3, material cooking: placing the material in S2 in water for cooking; S4, low temperature treatment: filtering the extract in S3 and performing low temperature condensation treatment; S5, adding ethanol: adding the ethanol solution into S4, stirring and filtering; S6, ultrafiltration treatment: filtering the S5 using an ultrafiltration membrane; S7, preparation: adding effective substances for the facial mask to S6.
2. The process for preparing a concentrated solution of Dendrobium huoshanense suitable for a facial mask according to claim 1, characterized in that: The effective substances in the S7 facial mask include vitamin C, collagen, sodium hyaluronate and xanthan gum. The proportions of the Huoshan dendrobium concentrate, vitamin C, collagen, sodium hyaluronate and xanthan gum are as follows: Huoshan dendrobium concentrate is 60-80 parts, vitamin C is 5-10 parts, collagen is 15-20 parts, sodium hyaluronate is 5-10 parts, and xanthan gum is 20-30 parts.
3. The process for preparing a concentrated solution of Dendrobium huoshanense suitable for a facial mask according to claim 1, characterized in that: The pulverizer in S2 uses a vacuum low-temperature liquid continuous dryer for pulverization.
4. The process for preparing a concentrated solution of Dendrobium huoshanense suitable for a facial mask according to claim 1, characterized in that: The S3 cooking time is 3-5 hours.
5. The process for preparing a concentrated solution of Dendrobium huoshanense suitable for a facial mask according to claim 1, characterized in that: The S5 is added and stirred for 10-20 minutes, and then allowed to stand for 0.5-1 hour, and filtered by centrifugal filtration.
6. The process for preparing a concentrated solution of Dendrobium huoshanense suitable for a facial mask according to claim 1, characterized in that: The temperature of the S4 low temperature treatment is 50°C.
7. The process for preparing a concentrated solution of Dendrobium huoshanense suitable for a facial mask according to claim 1, characterized in that: The S7 prepares and adds effective substances for the mask, and the effective substances for the mask include vitamin C, collagen, sodium hyaluronate and xanthan gum, which are mixed with water and stirred, indicating that the mixture is D. The mixture D is mixed with Huoshan Dendrobium concentrate and stirred, and filtered, and the filtering method is multiple centrifugal filtration.