Ziziphus jujube fruit-containing ancient formula bath essence capable of effectively improving sleep and promoting sleep and preparation method of ancient formula bath essence

Abstract

The invention provides ancient formula bath essence containing wild jujube fruits and capable of effectively improving and promoting sleep and a preparation method of the ancient formula bath essence. The raw materials for preparing the ancient formula bath essence containing the wild jujube fruits and capable of effectively improving and promoting sleep comprise a bath lotion component and a wild jujube fruit compound component, according to the ancient formula bath essence containing wild jujube fruits and capable of effectively improving sleep and promoting sleep, wild jujube fruit active ingredients are extracted from wild jujube fruit compound ingredients through supercritical CO2, the effect of calming nerves is achieved, mental stress is helped to be relieved, deep sleep is promoted, the wild jujube fruit extract is compounded with plant extracts of lavender, ligusticum wallichii and the like, a synergistic interaction formula is formed, and the effect of improving sleep and promoting sleep is achieved. The product enhances sedation, relieves anxiety and promotes sleep, the preparation process is efficient and stable, and the product has wide market prospects.

Description

Technical Field

[0001] The present invention relates to the field of body wash, and particularly to an ancient formula body wash essence containing wild jujube fruit that can effectively improve sleep and promote sleep, and a preparation method thereof. Background Art

[0002] With the rapid development of modern society, people are facing increasing work pressure, accelerating life rhythms, and overuse of various electronic products. Sleep problems have become a common health challenge globally. According to statistics from the World Health Organization, approximately one-third of the global population suffers from sleep disorders to varying degrees. In China, this proportion is also concerning, with the incidence of insomnia among adults as high as 38.2%. Sleep problems not only seriously affect people's daily lives, work efficiency, and learning abilities, but long-term sleep deprivation can also trigger a series of physical and mental health problems, such as decreased immunity, increased risk of cardiovascular diseases, and mental disorders such as anxiety and depression. According to relevant research, the risk of hypertension in long-term insomnia patients is nearly twice as high as that in the normal population, and the probability of suffering from depression is several times that of ordinary people.

[0003] In the process of seeking safer and more effective methods to improve sleep, natural plants have gradually attracted people's attention due to their low side effects and high safety. The active ingredients contained in many plants have the effects of sedation, calming the nerves, and regulating the nervous system function, providing a new way to improve sleep.

[0004] Wild jujube fruit has a long medicinal history in China. Modern medical research shows that wild jujube fruit is rich in various active ingredients such as flavonoids, saponins, and alkaloids. These ingredients can regulate the function of the nervous system, inhibit the excitement of the central nervous system, and thus play a sedative and hypnotic role. Among them, jujuboside can reduce the content of excitatory neurotransmitters in the brain, and flavonoids can regulate the neuroendocrine system and promote the secretion of sleep-related hormones. Lavender is famous for its unique aroma. Its volatile oil contains components such as linalool and linalyl acetate, which have significant sedative, soothing, and anti-anxiety effects. Chuanxiong is a commonly used traditional Chinese medicine, and its main active ingredient, tetramethylpyrazine, has the effect of dilating cerebral blood vessels and improving cerebral blood circulation. Angelica contains various active ingredients such as ferulic acid and volatile oil, which have the effects of enriching blood and promoting blood circulation, regulating immunity, etc. In terms of improving sleep, Angelica can regulate the body's endocrine system and relieve insomnia symptoms caused by endocrine disorders. Ginseng is rich in various bioactive substances such as ginsenosides, which have the effects of anti-fatigue and regulating the function of the nervous system. Traditional methods for extracting plant active ingredients, such as solvent extraction and water extraction, have many disadvantages, such as low extraction efficiency, high impurity content, and organic solvent residues. These problems not only affect the quality and safety of the extracts but also limit their application in the fields of medicine, health products, etc. Supercritical CO2 extraction technology, as a new extraction technology, has unique advantages. In the supercritical state, CO2 has the characteristics of both gas and liquid, with low viscosity and high diffusion coefficient, and can quickly penetrate into the interior of plant cells and selectively dissolve the target active ingredients. Compared with traditional extraction methods, supercritical CO2 extraction technology has high extraction efficiency, good product quality, and high safety. Bathing, as an important part of people's daily life, not only has the function of cleaning the body but also can affect the physiological and psychological states of the human body through skin absorption and olfactory stimulation. Adding plant extracts with sleep-improving effects to bath products to develop bath essence with sleep-promoting functions provides consumers with a new and convenient way to improve sleep. Such products can meet people's pursuit of a healthy and comfortable life.

[0005] At present, although there are already some bath products with sleep-promoting functions on the market, most of the product formulas are simple, lacking scientific synergistic design, and there are deficiencies in extraction technology and product quality. Therefore, it is of great practical significance and market value to develop a bath essence containing wild jujube fruit that can effectively improve sleep and promote sleep, which is formulated by compounding a variety of plant extracts with synergistic effects using advanced extraction technology.

[0006] Aiming at the problems existing in the prior art, this application aims to solve the problems such as the simple formula of bath products on the market, poor effect in helping relieve mental stress and promoting deep sleep, and unstable product process. Summary of the Invention

[0007] Object of the Invention: The object of the present invention is to provide an ancient formula bath essence containing wild jujube fruit that can effectively improve sleep and promote sleep, and a preparation method thereof, so as to solve the problems such as simple formula of bath products, poor effect in helping relieve mental stress and promoting deep sleep, and unstable product process.

[0008] Technical Solution of the Present Invention:

[0009] The present invention provides an ancient formula bath essence containing wild jujube fruit that can effectively improve sleep and promote sleep. The raw materials for preparing the ancient formula bath essence containing wild jujube fruit that can effectively improve sleep and promote sleep include bath lotion components and wild jujube fruit compound components.

[0010] Furthermore, the addition amount of the wild jujube fruit compound component is 4-10% of the total weight of the bath lotion components.

[0011] Furthermore, the raw materials of the bath lotion components, by weight, include: 30-40 parts of surfactant, 10-15 parts of humectant, 1-2 parts of stabilizer, 0.3-0.8 of antioxidant, and 40-55 parts of water.

[0012] Furthermore, the raw materials of the wild jujube fruit compound component, by weight, include: 3-8 parts of wild jujube fruit extract, 1-3 parts of lavender extract, 0.5-2 parts of chuanxiong extract, 0.5-1.5 parts of angelica extract, 0.5-2 parts of ginseng extract, 0.5-2 parts of ganoderma lucidum extract, 0.1-0.5 parts of chamomile essential oil, and 1-2 parts of lactic acid bacteria.

[0013] Furthermore, the preparation method of the wild jujube fruit extract includes the following steps:

[0014] S1: Wash, dry, and crush the wild jujube fruit, then put the wild jujube fruit powder into the extraction kettle of the supercritical extraction equipment and seal the extraction kettle;

[0015] S2: Add an appropriate amount of ethanol to the extraction kettle in step S1, then introduce carbon dioxide gas, adjust the extraction temperature to 30-60 °C, the pressure to 10-50 MPa, and the extraction time to 1-5 hours;

[0016] S3: After the extraction in step S2 is completed, make the supercritical CO2 fluid become gaseous by reducing the pressure, and extract to obtain the wild jujube fruit extract.

[0017] Furthermore, the surfactant is one or a mixture of more of sodium lauryl polyether sulfate, cocamidopropyl betaine, and lauryl glucoside.

[0018] Furthermore, the humectant is one or more of butanediol, hydrolyzed corn starch, and panthenol.

[0019] Further, the stabilizer is one or a mixture of more than one of citric acid, disodium ethylenediaminetetraacetate, and sodium sulfate.

[0020] Further, the antioxidant is one or a mixture of more than one of phenoxyethanol and tocopheryl acetate.

[0021] The present invention also provides a preparation method of an ancient formula bath essence containing wild jujube fruit that effectively improves sleep and promotes sleep, comprising the following steps:

[0022] Step 1: Accurately weigh the bath lotion ingredients and the wild jujube fruit compound ingredients according to parts by weight;

[0023] Step 2: Add the bath lotion ingredients weighed in Step 1 into a container with a stirring device. After mixing evenly, a bath lotion base solution is formed;

[0024] Step 3: Slowly add the weighed wild jujube fruit compound ingredients into the bath lotion base solution prepared in Step 2, and mix evenly to obtain an ancient formula bath essence containing wild jujube fruit that effectively improves sleep and promotes sleep.

[0025] Beneficial effects:

[0026] The present invention provides an ancient formula bath essence containing wild jujube fruit that effectively improves sleep and promotes sleep. The ancient formula bath essence containing wild jujube fruit of the present invention uses supercritical CO2 to extract the active ingredients of wild jujube fruit, which plays a role in calming the nerves, helps relieve mental stress, promotes deep sleep, and is compounded with plant extracts such as lavender and chuanxiong to form a synergistic formula, enabling the product to enhance sedation, relieve anxiety, and promote sleep. The preparation process is efficient and stable, and has a broad market prospect. Specific embodiments

[0027] The following will illustrate the present invention in combination with specific implementation schemes. It should be noted that the following examples are examples of the present invention, only used to illustrate the present invention, and not used to limit the present invention. Other combinations and various improvements within the concept of the present invention can be made without departing from the main idea or scope of the present invention.

[0028] Unless otherwise specified, other chemical reagents used in the present invention are all ordinary commercially available analytical pure.

[0029] Lactic acid bacteria were purchased from Shandong Zhongke Jiayi Co., Ltd.; hydrolyzed corn starch was purchased from Xi'an Huaxing Biotechnology Co., Ltd.; sodium lauryl polyether sulfate was purchased from Shandong Jinyuanyuan New Materials Co., Ltd.

[0030] Preparation of wild jujube fruit extract:

[0031] S1: Wash, dry, and crush 10 kg of wild jujube fruit, then put the wild jujube fruit powder into the extraction kettle of the supercritical extraction equipment and seal the extraction kettle;

[0032] S2: Add an appropriate amount of ethanol to the extraction kettle in step S1, then introduce carbon dioxide gas, adjust the extraction temperature to 54 °C, the pressure to 25 MPa, and the extraction time to 2 hours.

[0033] S3: After the extraction in step S2 is completed, make the supercritical CO2 fluid become gaseous by reducing the pressure, and extract to obtain the wild jujube fruit extract.

[0034] Example 1

[0035] Preparation of the ancient formula bath essence containing wild jujube fruit that effectively improves sleep and promotes sleep:

[0036] Step 1: Accurately weigh the shower gel ingredients (20 parts of sodium lauryl polyether sulfate, 10 parts of cocamidopropyl betaine, 8 parts of butanediol, 1 part of hydrolyzed corn starch, 1 part of panthenol, 1 part of citric acid, 0.5 part of disodium ethylenediaminetetraacetate, 0.5 part of phenoxyethanol, 45 parts of water) according to weight parts, and accurately weigh the wild jujube fruit compound ingredients (3 parts of wild jujube fruit extract, 3 parts of lavender extract, 0.5 part of chuanxiong extract, 1.5 parts of angelica extract, 0.5 part of ginseng extract, 2 parts of ganoderma lucidum extract, 0.1 part of chamomile essential oil, 3 parts of lactic acid bacteria) according to the same weight parts.

[0037] Step 2: Add the water weighed in step 1 to a container with a stirring device, start stirring, slowly add the weighed sodium lauryl polyether sulfate and cocamidopropyl betaine, stir evenly to fully dissolve the surfactant in the water, and sequentially add butanediol, hydrolyzed corn starch, panthenol, citric acid, disodium ethylenediaminetetraacetate, and phenoxyethanol, and continue stirring to ensure that all components are fully mixed evenly to form the shower gel base solution.

[0038] Step 3: Mix all components of the wild jujube fruit compound ingredients weighed in step 1 evenly, then slowly add 4% of the total weight of the shower gel ingredients of the wild jujube fruit compound ingredients to the shower gel base solution prepared in step 2, and continue stirring to fully mix the wild jujube fruit compound ingredients with the shower gel base solution evenly to obtain the ancient formula bath essence containing wild jujube fruit that effectively improves sleep and promotes sleep.

[0039] Example 2

[0040] The differences from the ancient formula bath essence containing wild jujube fruit prepared in Example 1, which effectively improves sleep and promotes sleep, are as follows: In Step 1, "Weigh the bath lotion ingredients (20 parts of sodium lauryl polyether sulfate, 10 parts of cocamidopropyl betaine, 8 parts of butanediol, 1 part of hydrolyzed corn starch, 1 part of panthenol, 1 part of citric acid, 0.5 part of disodium ethylenediaminetetraacetate, 0.5 part of phenoxyethanol, 45 parts of water)" is replaced with "Weigh the bath lotion ingredients (10 parts of sodium lauryl polyether sulfate, 15 parts of cocamidopropyl betaine, 5 parts of lauryl glucoside, 10 parts of butanediol, 2 parts of hydrolyzed corn starch, 2 parts of panthenol, 1 part of citric acid, 0.5 part of disodium ethylenediaminetetraacetate, 0.2 part of phenoxyethanol, 41 parts of water)"; "The wild jujube fruit compound ingredients (3 parts of wild jujube fruit extract, 1 part of lavender extract, 0.5 part of chuanxiong extract, 0.5 part of angelica extract, 0.5 part of ginseng extract, 2 parts of ganoderma lucidum extract, 0.1 part of chamomile essential oil, 3 parts of lactic acid bacteria)" is replaced with "The wild jujube fruit compound ingredients (2 parts of wild jujube fruit extract, 2 parts of lavender extract, 0.5 part of chuanxiong extract, 0.5 part of angelica extract, 1 part of ginseng extract, 1 part of ganoderma lucidum extract, 0.3 part of chamomile essential oil, 3.2 parts of lactic acid bacteria)".

[0041] Example 3

[0042] The differences from the ancient formula bath essence containing wild jujube fruit prepared in Example 1, which effectively improves sleep and promotes sleep, are as follows: In Step 3, "Weigh 4% of the total weight of the bath lotion ingredients of the wild jujube fruit compound ingredients and slowly add them to the bath lotion base prepared in Step 2" is replaced with "Weigh 10% of the total weight of the bath lotion ingredients of the wild jujube fruit compound ingredients and slowly add them to the bath lotion base prepared in Step 2".

[0043] Example 4

[0044] The differences from the ancient formula bath essence containing wild jujube fruit prepared in Example 1, which effectively improves sleep and promotes sleep, are as follows: In Step 3, "Weigh 4% of the total weight of the bath lotion ingredients of the wild jujube fruit compound ingredients and slowly add them to the bath lotion base prepared in Step 2" is replaced with "Weigh 3% of the total weight of the bath lotion ingredients of the wild jujube fruit compound ingredients and slowly add them to the bath lotion base prepared in Step 2".

[0045] Example 5:

[0046] The differences from the ancient formula bath essence containing wild jujube fruit prepared in Example 1, which effectively improves sleep and promotes sleep, are as follows: In Step 3, "Weigh 4% of the total weight of the bath lotion ingredients of the wild jujube fruit compound ingredients and slowly add them to the bath lotion base prepared in Step 2" is replaced with "Weigh 12% of the total weight of the bath lotion ingredients of the wild jujube fruit compound ingredients and slowly add them to the bath lotion base prepared in Step 2".

[0047] Example 6:

[0048] The difference from the ancient formula bath essence containing wild jujube fruit prepared in Example 1, which effectively improves sleep and promotes sleep, lies in that in Step 1, the "compound wild jujube fruit ingredient (3 parts of wild jujube fruit extract, 1 part of lavender extract, 0.5 part of chuanxiong extract, 0.5 part of angelica extract, 0.5 part of ginseng extract, 2 parts of ganoderma lucidum extract, 0.1 part of chamomile essential oil, 3 parts of lactic acid bacteria)" is replaced with "compound wild jujube fruit ingredient (1 part of wild jujube fruit extract, 1 part of lavender extract, 1 part of chuanxiong extract, 0.5 part of angelica extract, 0.5 part of ginseng extract, 3 parts of ganoderma lucidum extract, 0.2 part of chamomile essential oil, 4.3 parts of lactic acid bacteria)".

[0049] Example 7:

[0050] The difference from the ancient formula bath essence containing wild jujube fruit prepared in Example 1, which effectively improves sleep and promotes sleep, lies in that in Step 1, the "compound wild jujube fruit ingredient (3 parts of wild jujube fruit extract, 1 part of lavender extract, 0.5 part of chuanxiong extract, 0.5 part of angelica extract, 0.5 part of ginseng extract, 2 parts of ganoderma lucidum extract, 0.1 part of chamomile essential oil, 3 parts of lactic acid bacteria)" is replaced with "compound wild jujube fruit ingredient (6 parts of wild jujube fruit extract, 0.5 part of lavender extract, 0.5 part of chuanxiong extract, 0.3 part of angelica extract, 0.3 part of ginseng extract, 1 part of ganoderma lucidum extract, 0.1 part of chamomile essential oil, 1.3 parts of lactic acid bacteria)".

[0051] The ancient formula bath essence containing wild jujube fruit prepared in Examples 1 - 7 was subjected to the following tests:

[0052] 1. Recruit 70 volunteers with sleep problems, with 10 people in a group. Subjectively evaluate the sleep quality of the volunteers through the Pittsburgh Sleep Quality Index (PSQI) professional scale. Use the bath essence of Examples 1 - 7 respectively. After a 4 - week experiment, subjectively evaluate the sleep quality of the volunteers through the Pittsburgh Sleep Quality Index (PSQI) professional scale again. The following scores and evaluations are the average scores of 10 people; the PSQI score range is 0 - 21 points. The higher the score, the worse the sleep quality. Generally, it is considered that a PSQI score ≤ 5 points indicates very good sleep quality; 6 - 10 points indicates acceptable sleep quality; 11 - 15 points indicates average sleep quality; 16 - 21 points indicates very poor sleep quality.

[0053] 2. Sleep deprivation model experiment: Use 70 white rats at 36 weeks old, evenly divide them into 7 groups, and then intervene by giving different bath essence of Examples 1 - 7. Record the sleep parameters of the animals, such as total sleep time and sleep latency, through polysomnography (PSG) to observe the improvement effect of the product on sleep.

[0054] Table 1: Pittsburgh Sleep Quality Test Results Table

[0055] Serial number PSQI score before intervention PSQI score after intervention Score change value (after intervention - before intervention) Example 1 16 4 -12 Example 2 16 5 -11 Example 3 19 7 -10 Example 4 17 9 -8 Example 5 16 9 -7 Example 6 18 12 -6 Example 7 18 11 -7

[0056] Table 2: Experimental Results Table of Sleep Deprivation Model

[0057]

[0058] In Experiment 1, the Pittsburgh Sleep Quality Test scores decreased after using the bath essence, indicating that it can relieve anxiety and promote sleep. In Experiment 2, the ingredients in the bath essence have a sedative and nerve-soothing effect, which can prolong the total sleep time of white rats; the time required for white rats to enter the sleep state from the waking state is shortened, which means that the bath essence can help white rats fall asleep faster and reduce the difficulty of falling asleep. This is because the effective active ingredients, trace elements and other active ingredients in wild jujube fruits play a role in sedating nerves, helping to relieve mental stress, promoting deep sleep, and working together with extracts such as lavender and chamomile to relieve anxiety, enabling white rats to calm down faster and enter the sleep state.

[0059] Therefore, the ancient formula bath essence containing wild jujube fruits prepared by the present invention has a sedative effect on nerves, helps to relieve mental stress, promotes deep sleep, and is compounded with plant extracts such as lavender and chuanxiong to form a synergistic formula, enhancing the sedative, anxiety-relieving and sleep-promoting effects of the product. Specifically, it can be seen from the comparison between Example 4 and Example 1 that if the addition amount of the wild jujube fruit compound component is too much, the effects of the ancient formula bath essence containing wild jujube fruits on sedating nerves, relieving mental stress, promoting deep sleep and promoting sleep will become worse and fail to achieve the expected effects; it can be seen from the comparison between Example 5 and Example 1 that if the addition amount of the wild jujube fruit compound component is too much, the effects of the ancient formula bath essence containing wild jujube fruits on sedating nerves, relieving mental stress, promoting deep sleep and promoting sleep will become worse and fail to achieve the expected effects; it can be seen from the comparison between Examples 6-7 and Example 1 that if the weight ratio between the wild jujube fruit extract and lavender extract, chuanxiong extract, angelica extract, ginseng extract, ganoderma extract, chamomile essential oil and lactic acid bacteria in the wild jujube fruit compound component is unreasonable, the effects of the ancient formula bath essence containing wild jujube fruits on sedating nerves, relieving mental stress, promoting deep sleep and promoting sleep will become worse and fail to achieve the expected effects.

[0060] The present invention can also have many other embodiments. Without departing from the spirit and essence of the present invention, those skilled in the art can make various corresponding changes and deformations according to the present invention, but these corresponding changes and deformations should all fall within the protection scope of the appended claims of the present invention.

Claims

1. An ancient formula bath essence containing wild jujube fruit, which can effectively improve sleep and promote sleep, is characterized in that, The raw materials for preparing the ancient formula bath essence containing wild jujube fruit, which can effectively improve sleep and promote sleep, include bath lotion ingredients and wild jujube fruit compound ingredients.

2. The ancient formula bath essence containing wild jujube fruit and effectively improving sleep and promoting sleep according to claim 1, wherein The addition amount of the wild jujube fruit compound ingredients is 4-10% of the total weight of the bath lotion ingredients.

3. The ancient formula bath essence containing wild jujube fruit that effectively improves sleep and promotes sleep according to claim 1, wherein, The raw materials of the bath lotion ingredients, by weight, include: 30-40 parts of surfactant, 10-15 parts of moisturizer, 1-2 parts of stabilizer, 0.3-0.8 parts of antioxidant, and 40-55 parts of water.

4. The ancient formula bath essence containing wild jujube fruit for effectively improving sleep and promoting sleep according to claim 1, characterized in that, The raw materials of the wild jujube fruit compound ingredients, by weight, include: 3-8 parts of wild jujube fruit extract, 1-3 parts of lavender extract, 0.5-2 parts of chuanxiong extract, 0.5-1.5 parts of angelica extract, 0.5-2 parts of ginseng extract, 0.5-2 parts of ganoderma lucidum extract, 0.1-0.5 parts of chamomile essential oil, and 1-2 parts of lactic acid bacteria.

5. The ancient formula bath essence containing wild jujube fruit and effectively improving sleep and promoting sleep according to claim 4, characterized in that, The preparation method of the wild jujube fruit extract includes the following steps: S1: Wash, dry, and crush the wild jujube fruit, then put the wild jujube fruit powder into the extraction kettle of the supercritical extraction equipment and seal the extraction kettle. S2: Add an appropriate amount of ethanol to the extraction kettle in step S1, then introduce carbon dioxide gas, adjust the extraction temperature to 30-60°C, the pressure to 10-50 MPa, and the extraction time to 1-5 hours. S3: After the extraction in step S2, make the supercritical CO2 fluid become gaseous by decompression, and extract to obtain the wild jujube fruit extract.

6. The ancient formula bath essence containing wild jujube fruit that can effectively improve sleep and promote sleep according to claim 3, characterized in that, The surfactant is one or a mixture of sodium lauryl polyether sulfate, cocamidopropyl betaine, and lauryl glucoside.

7. The ancient formula bath essence containing wild jujube fruit that effectively improves sleep and promotes sleep according to claim 3, characterized in that, The moisturizer is one or more of butanediol, hydrolyzed corn starch, and panthenol.

8. The ancient formula bath essence containing wild jujube fruit and effectively improving sleep and promoting sleep according to claim 3, characterized in that The stabilizer is one or a mixture of citric acid, disodium ethylenediaminetetraacetate, and sodium sulfate.

9. The ancient formula bath essence containing wild jujube fruit and effectively improving sleep and promoting sleep according to claim 3, characterized in that, The antioxidant is one or a mixture of phenoxyethanol and tocopheryl acetate.

10. The preparation method of the ancient formula bath essence containing wild jujube fruit that can effectively improve sleep and promote sleep according to any one of claims 1-9, characterized in that, It includes the following steps: Step 1: Accurately weigh the bath lotion ingredients and the wild jujube fruit compound ingredients according to the weight parts. Step 2: Add the bath lotion ingredients weighed in step 1 into a container with a stirring device, mix well to form a bath lotion base solution. Step 3: Slowly add the weighed wild jujube fruit compound ingredients into the bath lotion base solution prepared in step 2, mix evenly to obtain the ancient formula bath essence containing wild jujube fruit, which can effectively improve sleep and promote sleep.

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