A formula and manufacturing method for an old black ointment

Abstract

This invention discloses a formula and manufacturing method for an old black plaster. The old black plaster formula mainly consists of the following components in parts by weight: Clematis chinensis 1, Gentiana macrophylla 1, Clematis armandii 1, Curcuma longa 2, Alpinia officinarum 1, Eupolyphaga sinensis 0.5, Angelica dahurica 0.6, Cinnamomum cassia 1, natural copper 1, Lycopodium clavatum 0.8, Spatholobus suberectus 1, Boswellia carterii 1, Commiphora myrrha 1, Beeswax 1, Rosa rugosa 1, Gastrodia elata 1, Gardenia jasminoides 1, Drynaria fortunei 2, Angelica pubescens 1.5, Taxillus chinensis 1, Achyranthes bidentata 1.1, and Piper kadsura 0.8. This invention also provides a manufacturing method for the old black plaster, including steps such as crushing and mixing, vacuum frying, refining oil until it forms beads when dripped, adding cinnabar to form a plaster, removing heat toxicity, and spreading. This invention's formula targets the pathogenesis of qi stagnation and blood stasis caused by wind-cold-dampness obstructing the meridians, resulting in pain due to obstruction. It has comprehensive effects of dispelling wind, dispersing cold, removing dampness, promoting blood circulation, resolving stasis, unblocking meridians, strengthening tendons, and relieving pain, with significant therapeutic effects.

Description

Technical Field

[0001] This invention relates to a formula and manufacturing method for an old black plaster, belonging to the technical field of external preparations of traditional Chinese medicine. Background Technology

[0002] Old Black Plaster is a traditional Chinese medicine external application black plaster. Its formula primarily uses herbs that dispel wind and dampness, promote blood circulation, reduce swelling, and relieve pain, combined with a base of plant-based sesame oil. For example, a classic traditional Old Black Plaster formula includes: 30g Angelica sinensis, 30g Ligusticum chuanxiong, 30g Carthamus tinctorius, 30g Clematis chinensis, 30g Angelica pubescens, 30g Clematis armandii, 30g Achyranthes bidentata, 20g Zaocys dhumnades, 20g Eupolyphaga sinensis, 20g Notopterygium incisum, 20g Saposhnikovia divaricata, 20g Angelica dahurica, 20g Zingiber officinale, and 150g Litharge. The ingredients are fried in oil to extract the active ingredients. Then, the plaster is melted back in the pan over low heat, removed from the heat, and the fine ingredients are added, including 15g Frankincense, 15g Myrrh, 15g Dragon's Blood, 8g Borneol, and 8g Camphor. The mixture is stirred well, spread on paper while still hot, and allowed to cool.

[0003] The efficacy of the aforementioned classic traditional black ointment formula is limited and unsatisfactory. How to improve its efficacy is a technical problem that urgently needs to be solved by those skilled in the art. Summary of the Invention

[0004] To overcome the above-mentioned shortcomings, the purpose of this invention is to provide a formula for an old black ointment that has better therapeutic effects.

[0005] To achieve the above objectives, the technical solution adopted by the present invention is: a formula for an old black ointment, which mainly consists of the following components in parts by weight: Clematis chinensis 1 part by weight, Gentiana macrophylla 1 part by weight, Clematis armandii 1 part by weight, Curcuma longa 2 parts by weight, Alpinia officinarum 1 part by weight, Eupolyphaga sinensis 0.5 parts by weight, Angelica dahurica 0.6 parts by weight, Cinnamomum cassia 1 part by weight, natural copper 1 part by weight, Lycopodium clavatum 0.8 parts by weight, Spatholobus suberectus 1 part by weight, Boswellia carterii 1 part by weight, Commiphora myrrha 1 part by weight, Beeswax 1 part by weight, Prickly pear 1 part by weight, Gastrodia elata 1 part by weight, Gardenia jasminoides 1 part by weight, Drynaria fortunei 2 parts by weight, Angelica pubescens 1.5 parts by weight, Taxillus chinensis 1 part by weight, Achyranthes bidentata 1.1 parts by weight, and Piper kadsura 0.8 parts by weight.

[0006] This invention also provides a method for manufacturing old black paste, comprising the following steps: (a) Crush and mix 1 part by weight of Clematis chinensis, 1 part by weight of Gentiana macrophylla, 1 part by weight of Clematis armandii, 2 parts by weight of Curcuma longa, 1 part by weight of Alpinia galanga, 0.5 parts by weight of Eupolyphaga sinensis, 0.6 parts by weight of Angelica dahurica, 1 part by weight of Cinnamomum cassia, 1 part by weight of natural copper, 0.8 parts by weight of Lycopodium clavatum, 1 part by weight of Spatholobus suberectus, 1 part by weight of Boswellia carterii, 1 part by weight of Commiphora myrrha, 1 part by weight of beeswax, 1 part by weight of Prickly pear, 1 part by weight of Gastrodia elata, 1 part by weight of Gardenia jasminoides, 2 parts by weight of Drynaria fortunei, 1.5 parts by weight of Angelica pubescens, 1 part by weight of Taxillus chinensis, 1.1 parts by weight of Achyranthes bidentata, and 0.8 parts by weight of Piper kadsura to obtain a mixed medicinal powder with a particle size of 150-180 μm. (ii) Add the mixed powder to 30 parts by weight of vegetable oil and fry the mixture under vacuum. (iii) Heat the vegetable oil over a high flame to 225-255°C and refine it for 30-60 minutes until it reaches the state where "drops form beads"; (iv) Reduce the oil temperature to 200℃±5℃, and sprinkle in the dried lead oxide and clove oil in batches, stirring until the paste is brownish-black, viscous and stringy; the lead oxide is 5 to 15 parts by weight and the clove oil is 6 to 9 parts by weight. (v) Pour the hot paste into cold water containing EDTA and licorice powder, knead repeatedly until the paste is black and shiny and odorless; (vi) Spread the paste onto the composite cloth, with a thickness of 0.2 to 0.5 cm, and let it cool.

[0007] A further feature of the present invention is that the composite fabric includes an anti-adhesive layer, a pressure-sensitive adhesive layer, and a backing layer, and the paste is applied onto the pressure-sensitive adhesive layer.

[0008] Compared with existing technologies, the beneficial effects of this invention are: this formula targets the pathogenesis of wind-cold-dampness obstructing the meridians, leading to qi stagnation and blood stasis, and pain due to obstruction. The formula includes a group for dispelling wind and dampness, dispersing cold and relieving pain; a group for promoting blood circulation, removing blood stasis, reducing swelling and relieving pain; a group for clearing the meridians and dispersing nodules, and powerfully relieving pain; and a group for auxiliary repair and shaping. It has the effects of dispelling wind, dispersing cold, removing dampness, promoting blood circulation, removing blood stasis, clearing the meridians, strengthening muscles and tendons, and relieving pain. Specifically: First, the group that dispels wind and dampness, disperses cold and relieves pain. Clematis chinensis, Gentiana macrophylla, Clematis armandii, and Clematis armandii: powerfully dispel wind and dampness, and promote joint mobility, making them the main force in relieving rheumatic pain.

[0009] Galangal, cinnamon, and angelica: Focus on warming the meridians and dispelling cold. Cold is the main cause of cold pain and cramps; this group of herbs provides heat to dispel deep-seated cold pathogens.

[0010] Gastrodia elata: dispels external wind, unblocks meridians, and also treats numbness of limbs.

[0011] Second, the blood-activating, stasis-removing, swelling-reducing, and pain-relieving group. Frankincense and myrrh: a classic medicinal pair that invigorates blood circulation, promotes qi flow, reduces swelling, and promotes tissue regeneration, forming the core of pain relief.

[0012] Turmeric and chicken blood vine: promote blood circulation, relieve pain and menstrual pain. Turmeric has a strong effect in breaking up blood stasis, while chicken blood vine can also nourish blood.

[0013] Earthworm and natural copper: break up blood stasis and promote bone healing. This is a "heavy weapon" for old injuries, stagnant blood, heavy blood stasis, and even fractures, with strong force and penetrating power.

[0014] Third, the auxiliary repair and shaping group Prickly pear: Rich in vitamin C and vitamin E, it helps with anti-oxidation and promotes local tissue repair.

[0015] Beeswax: As a base (excipient), it adjusts the consistency of the ointment, making it easy to apply, and also has a gentle astringent and protective effect.

[0016] The above description is merely an overview of the technical solution of the present invention. In order to better understand the technical means of the present invention and to implement it in accordance with the contents of the specification, the preferred embodiments of the present invention are described in detail below with reference to the accompanying drawings. Attached Figure Description

[0017] Figure 1 This is a schematic diagram of a preferred embodiment of the method for manufacturing black paste according to the present invention. Detailed Implementation

[0018] The preferred embodiments of the present invention will now be described in detail with reference to the accompanying drawings, so that the advantages and features of the present invention can be more easily understood by those skilled in the art, thereby providing a clearer and more explicit definition of the scope of protection of the present invention.

[0019] It should be noted that the "parts by weight" mentioned in this invention are approximate values. Those skilled in the art will understand that, under the premise of achieving the purpose of this invention, each component can vary independently within ±10% of the given value without affecting the realization of the technical effect of this invention.

[0020] Example 1: This embodiment presents a formula for an old black ointment, which mainly consists of the following components in parts by weight: Clematis chinensis 1 part by weight, Gentiana macrophylla 1 part by weight, Clematis armandii 1 part by weight, Curcuma longa 2 parts by weight, Alpinia officinarum 1 part by weight, Eupolyphaga sinensis 0.5 parts by weight, Angelica dahurica 0.6 parts by weight, Cinnamomum cassia 1 part by weight, natural copper 1 part by weight, Lycopodium clavatum 0.8 parts by weight, Spatholobus suberectus 1 part by weight, Boswellia carterii 1 part by weight, Commiphora myrrha 1 part by weight, Beeswax 1 part by weight, Prickly pear 1 part by weight, Gastrodia elata 1 part by weight, Gardenia jasminoides 1 part by weight, Drynaria fortunei 2 parts by weight, Angelica pubescens 1.5 parts by weight, Taxillus chinensis 1 part by weight, Achyranthes bidentata 1.1 parts by weight, and Piper kadsura 0.8 parts by weight; the particle size of each component is 150-180μm.

[0021] In this embodiment, the functions of each component are as follows: 1. Clematis chinensis: dispelling wind and dampness, dredging meridians, stopping arthralgia. It is good at walking around, treating numbness of limbs and migratory pain.

[0022] 2. Gentiana macrophylla: dispelling wind and dampness, clearing damp-heat, stopping arthralgia. It is of neutral nature and can reconcile the cold and heat of various herbs.

[0023] 3. Speranskia tuberculata: expelling wind and removing dampness, promoting blood circulation to relieve pain. Its medicinal power can penetrate into muscles and bones.

[0024] 4. Lycopodium clavatum: expelling wind and removing dampness, relaxing muscles and activating collaterals. It is specifically used to treat the inability to flex and extend joints and cramped tendons.

[0025] 5. Gastrodia elata: expelling wind and dredging collaterals. It is good at relieving numbness of limbs and paralysis of hands and feet.

[0026] 6. Curcuma longa: promoting blood circulation to remove blood stasis, promoting qi movement, dredging meridians and stopping pain. It is for pain caused by qi stagnation and blood stasis.

[0027] 7. Eupolyphaga seu Steleophaga: promoting blood circulation to remove blood stasis, mending tendons and setting bones. It is for severe blood stasis, old injuries and fractures.

[0028] 8. Pyritum: dissipating stasis to relieve pain, mending bones and treating injuries. It promotes bone healing.

[0029] 9. Spatholobus suberectus: promoting blood circulation and nourishing blood, relaxing muscles and activating collaterals. It can promote blood circulation and nourish blood at the same time.

[0030] 10. Olibanum: promoting blood circulation and qi movement, detumescing and promoting granulation.

[0031] 11. Myrrha: dissipating stasis to relieve pain, detumescing and promoting granulation.

[0032] 12. Alpinia officinarum: warming the middle-jiao to dispel cold and relieve pain. It has a strong effect of warming the middle-jiao and dispelling cold.

[0033] 13. Cinnamomum cassia: warming the meridians and promoting blood circulation, dispelling cold and relieving pain. It provides deep heat and leads fire back to its origin.

[0034] 14. Angelica dahurica: dispersing wind and removing dampness, opening the nasal passages and relieving pain. It can disperse cold and dry dampness, and can also expel pus.

[0035] 15. Beeswax: excipient. It regulates the softness and hardness of the paste, facilitates application, and has a mild astringent effect.

[0036] 16. Rosa roxburghii: auxiliary component. It is rich in vitamins and helps with antioxidant and promoting local tissue repair.

[0037] 17. Gardenia jasminoides: clearing away heat and promoting diuresis, cooling blood and detoxifying.

[0038] 18. Drynaria fortunei: tonifying the kidney and strengthening bones, mending injuries and relieving pain.

[0039] 19. Angelica pubescens: expelling wind and removing dampness, dredging collaterals and relieving pain. It is especially good at treating rheumatic arthralgia of the lower body.

[0040] 20. Mistletoe: dispels wind and dampness, nourishes the liver and kidneys, and strengthens muscles and bones.

[0041] 21. Achyranthes bidentata: Nourishes the liver and kidneys, strengthens tendons and bones, removes blood stasis and promotes menstruation, and guides blood downward.

[0042] 22. Sea Breeze Vine: Dispels wind and dampness, unblocks meridians, and relieves pain.

[0043] Example 2: This invention also provides a method for manufacturing old black paste, comprising the following steps: (a) Crush and mix 1 part by weight of Clematis chinensis, 1 part by weight of Gentiana macrophylla, 1 part by weight of Clematis armandii, 2 parts by weight of Curcuma longa, 1 part by weight of Alpinia galanga, 0.5 parts by weight of Eupolyphaga sinensis, 0.6 parts by weight of Angelica dahurica, 1 part by weight of Cinnamomum cassia, 1 part by weight of natural copper, 0.8 parts by weight of Lycopodium clavatum, 1 part by weight of Spatholobus suberectus, 1 part by weight of Boswellia carterii, 1 part by weight of Commiphora myrrha, 1 part by weight of beeswax, 1 part by weight of Prickly pear, 1 part by weight of Gastrodia elata, 1 part by weight of Gardenia jasminoides, 2 parts by weight of Drynaria fortunei, 1.5 parts by weight of Angelica pubescens, 1 part by weight of Taxillus chinensis, 1.1 parts by weight of Achyranthes bidentata, and 0.8 parts by weight of Piper kadsura to obtain a mixed medicinal powder with a particle size of 150-180 μm. (ii) Add the mixed powder to 30 parts by weight of vegetable oil and fry the mixture under vacuum. (iii) Heat the vegetable oil over a high flame to 225-255°C and refine it for 30-60 minutes until it reaches the state where "drops form beads"; (iv) Reduce the oil temperature to 200℃±5℃, and sprinkle in the dried lead oxide and clove oil in batches, stirring until the paste is brownish-black, viscous and stringy; the lead oxide is 5 to 15 parts by weight and the clove oil is 6 to 9 parts by weight. (v) Pour the hot paste into cold water containing EDTA and licorice powder, knead repeatedly until the paste is black and shiny and odorless; (vi) Spread the paste onto the composite cloth, with a thickness of 0.2 to 0.5 cm, and let it cool.

[0044] A further embodiment of the present invention is that the composite fabric comprises an anti-adhesive layer, a pressure-sensitive adhesive layer, and a backing layer, wherein the paste is applied onto the pressure-sensitive adhesive layer. The anti-adhesive layer protects the paste; it is removed before use. The pressure-sensitive adhesive layer carries the paste and controls the release of the drug. The backing layer provides support and determines flexibility and breathability.

[0045] EDTA binds with heavy metal ions in the ointment to form chelates, reducing the risk of heavy metal ions. Licorice powder can more quickly neutralize the heat toxins in the ointment, after which the ointment gradually becomes dark and shiny, and has no pungent odor. It is gentle and non-irritating when applied to the skin. There are no discomfort symptoms such as erythema, papules, or itching.

[0046] The main component of the plaster is plant oil, which reacts with litharge to form a dense, oily paste. During application, the high-temperature plaster penetrates the gaps in the pressure-sensitive adhesive layer, which is made of fabric fibers. Upon cooling, this forms a continuous, waterproof, and airtight oily film that tightly covers the surface and interior of the fabric. This oily film acts as an excellent hydrophobic barrier, effectively preventing the penetration of external liquid water and also preventing the free evaporation of sweat and moisture from the skin. It protects the plaster from being diluted or washed away by water. In treating certain types of arthralgia requiring "closed sweating," it can act as a kind of "occlusive" seal, promoting drug penetration. Newly applied plasters have almost no air or moisture permeability due to the dense seal of the plaster. It is a completely closed system. After a period of time, such as 24-72 hours, the plaster will slowly soften and melt under body temperature. Its structure will become looser, and some of the oily components may be absorbed or oxidized by the skin. At this time, the tiny channels between the fabric fibers may reopen. More importantly, the cream itself may develop tiny cracks due to changes in moisture and temperature, forming a breathable structure. This increases the overall breathability and moisture permeability of the old black cream, which is beneficial to skin health.

[0047] Example 3 (Comparative Example): Example 3 is basically the same as Example 1, except that Clematis chinensis, Gentiana macrophylla, Clematis armandii, Lycopodium clavatum, Alpinia officinarum, Cinnamomum cassia, Angelica dahurica, and Gastrodia elata are omitted.

[0048] Example 4 (Comparative Example): Example 4 is basically the same as Example 1, except that frankincense, myrrh, turmeric, chicken blood vine, earthworm, and natural copper are omitted.

[0049] Example 5 (Comparative Example): Example 5 is basically the same as Example 1, except that the prickly pear and beeswax are omitted.

[0050] Example 6 (Comparative Example): Example 6 is basically the same as Example 2, except that EDTA and licorice powder are omitted.

[0051] Example 7 (Comparative Example): Example 7 is basically the same as Example 2, except that clove oil is omitted.

[0052] Examples 1, 3 to 5 all use the manufacturing method described in Example 2.

[0053] The effects of each embodiment are shown in the table below: The above embodiments are only for illustrating the technical concept and features of the present invention. Their purpose is to enable those skilled in the art to understand the content of the present invention and implement it. They should not be used to limit the scope of protection of the present invention. All equivalent changes or modifications made in accordance with the spirit and essence of the present invention should be covered within the scope of protection of the present invention.

Claims

1. An old-fashioned salve formulation, characterized in that, The old black ointment formula mainly consists of the following components by weight: 1 part of Wulingteng, 1 part of Qinjiao, 1 part of Tougucao, 2 parts of Rhizoma Curcumae, 1 part of Gao Liang Jiang, 0.5 part of Tu Yuan, 0.6 part of Bai Zhi, 1 part of Rou Gui, 1 part of Zhi Ru, 0.8 part of Shenjincao, 1 part of Jixueteng, 1 part of Ru Xiang, 1 part of Mo Yao, 1 part of Feng Feng Teng, 1 part of Zhizi, 2 parts of Gusuibu, 1.5 parts of Du Huo, 1 part of Sangjisheng, 1.1 parts of Huai Niuxi, and 0.8 parts of Sea Wind.

2. A method of manufacturing an old black paste, characterized by, The method comprises the following steps: (1) Wulingteng 1 part, Qinjiao 1 part, Tougucao 1 part, Rhizoma Curcumae 2 parts, Gao Liang Jiang 1 part, Tu Yuan 0.5 part, Bai Zhi 0.6 part, Rou Gui 1 part, Zhi Ru 1 part, Shenjincao 0.8 part, Jixueteng 1 part, Ru Xiang 1 part, Mo Yao 1 part, Feng Feng Teng 1 part, Zhizi 1 part, Gusuibu 2 parts, Du Huo 1.5 parts, Sangjisheng 1 part, Huai Niuxi 1.1 parts, and Sea Wind 0.8 parts are crushed and mixed to obtain mixed medicine powder with a particle size of 150-180 μm; (2) The mixed medicine powder is added into 30 parts of vegetable oil, and the oil is fried in a vacuum state; (3) The vegetable oil is heated to 225-255 °C with a strong fire, and the oil is refined for 30-60 minutes until it reaches the state of "water droplets forming beads"; (4) The oil temperature is reduced to 200 °C ± 5 °C, and the dry lead and clove oil are added into the oil in batches, and stirred until the ointment is brown-black and viscous and stringy; wherein the lead is 5-15 parts by weight, and the clove oil is 6-9 parts by weight; (5) The ointment is poured into cold water while it is hot, and the cold water contains EDTA and licorice powder, and the ointment is kneaded repeatedly until it is black and shiny and has no odor; (6) The ointment is spread on a composite cloth, and the thickness of the ointment is 0.2-0.5 cm, and the ointment is cooled.

3. The method of claim 2, wherein The composite cloth comprises an anti-sticking layer, a pressure-sensitive adhesive layer, and a backing layer, and the ointment is spread on the pressure-sensitive adhesive layer.

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