Adiantium leaf polyphenol and extraction method thereof

This multi-step method, involving fermentation, extraction with ethanol and sodium tripolyphosphate aqueous solution, membrane separation, and purification with D201 macroporous anion exchange resin, solves the problems of low extraction efficiency and insufficient purity of polyphenols from Cyclocarya paliurus leaves, achieving efficient and environmentally friendly polyphenol extraction suitable for industrial production.

CN122398885APending Publication Date: 2026-07-17HUBEI SIHUI BIOTECHNOLOGY CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
HUBEI SIHUI BIOTECHNOLOGY CO LTD
Filing Date
2026-05-19
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing polyphenol extraction technologies from Cyclocarya paliurus leaves suffer from problems such as unsatisfactory extraction efficiency, long extraction time, large solvent consumption or residual risks, high energy consumption, expensive equipment, easy damage to the structure of active ingredients, and difficulty in achieving both high yield and high purity.

Method used

A multi-step method was adopted, which involved fermentation to disrupt the cell wall, extraction with ethanol and sodium tripolyphosphate aqueous solution, membrane separation, and purification with D201 macroporous anion exchange resin. The method combined fermentation and drying under specific conditions, utilized sodium tripolyphosphate to improve the water solubility and antioxidant properties of polyphenols, removed impurities through membrane separation, used D201 macroporous anion exchange resin for adsorption and separation, and finally achieved efficient purification by ethanol elution.

Benefits of technology

It achieves efficient, rapid, and environmentally friendly polyphenol extraction, reduces energy and solvent consumption, improves the purity and yield of polyphenols, avoids structural damage, and is suitable for large-scale industrial production and long-term storage.

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Abstract

本发明涉及植物提取技术领域,具体涉及一种青钱柳叶多酚的提取方法,包括如下步骤:S1.将发酵后的青钱柳叶与溶剂按1:(8~15)的质量比进行加热提取,将提取液过滤得滤液;所述溶剂为含有质量比为10:(1~2)的乙醇和三聚磷酸钠的水溶液;所述三聚磷酸钠在所述溶剂中的质量浓度为1%~2%;和 / 或,所述乙醇在所述溶剂中的质量浓度为8%~12%;S2.将所述滤液依次经过至少两次膜分离浓缩,得浓缩液;所述两次膜分离的截留分子量差至少为500Da;S3.将所述的浓缩液过树脂柱分离,随后洗脱,收集洗脱液并从中分离青钱柳叶多酚。上述方法能克服现有技术的不足,提供一种高效、快速、环保的青钱柳叶多酚提取方法。
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