A method for purifying graphite by cascade plasma and high-purity low-damage graphite powder

By employing a four-stage plasma treatment and pretreatment process, the problems of oxidation ablation and incomplete impurity removal in existing plasma graphite purification technologies are solved, resulting in the preparation of high-purity, low-damage graphite suitable for semiconductors and electronic devices.

CN122403440APending Publication Date: 2026-07-17MINMETALS EXPLORATION & DEVELOPMENT CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
MINMETALS EXPLORATION & DEVELOPMENT CO LTD
Filing Date
2026-06-15
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing plasma graphite purification technologies suffer from problems such as oxidation and ablation, generation of highly toxic byproducts, incomplete removal of impurities, and structural damage, making it difficult to achieve the preparation of high-purity graphite.

Method used

A four-stage plasma treatment method is adopted, which involves staged treatment under protective gas, oxidizing gas, fluorocarbon gas and reducing gas atmosphere, combined with acid washing and water washing steps, to precisely control the reaction at each stage, remove impurities on the graphite surface, between layers and in the lattice, and repair structural defects.

Benefits of technology

It has achieved the preparation of high-purity (≥99.88%) low-damage graphite, reducing the generation of highly toxic byproducts, lowering environmental pollution and safety risks, and is suitable for the semiconductor and electronic device fields.

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Abstract

本发明提供了一种梯次等离子体提纯石墨的方法和高纯低损伤石墨粉。该方法包括:对石墨原料进行第一梯次等离子体处理,得到第一中间产物;在氧化性气体的含量小于等于5vol%的第一混合气中,对第一中间产物进行第二梯次等离子体处理,得到第二中间产物;在氟碳气体的含量小于等于1.5vol%的第二混合气中,对第二中间产物进行第三梯次等离子体处理,得到第三中间产物;在还原性气体的含量大于等于1vol%的第三混合气中,对第三中间产物进行第四梯次等离子体处理,得到第四中间产物;对第四中间产物进行洗涤,得到高纯低损伤石墨粉。本发明提纯得到的高纯低损伤石墨粉的固定碳含量高且石墨结构的缺陷较少。
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