A method for preparing high-purity quartz by flux-assisted calcination-water quenching and high-purity quartz prepared by the method

By using flux-assisted calcination-water quenching, the problems of impurity solidification and low purification efficiency in the preparation of high-purity quartz were solved, and high-purity quartz with SiO2 content greater than 99.99% was achieved.

CN122403459APending Publication Date: 2026-07-17
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Filing Date
2026-04-28
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In the preparation of high-purity quartz using existing technology, the calcination-water quenching treatment before grinding is prone to side reactions at high temperatures, which can cause impurities to solidify or enter the crystal lattice. Furthermore, the small particle size of quartz makes it difficult to generate sufficient internal stress to burst inclusions, resulting in low purification efficiency.

Method used

The flux-assisted calcination-water quenching method is adopted. By adding fluxes such as sodium/potassium salts to lower the phase transformation temperature of quartz, combined with water quenching and rapid cooling, the rapid volume change of quartz is promoted to generate microcracks, exposing internal impurities and improving acid leaching efficiency.

Benefits of technology

It effectively opens the internal inclusions of quartz, improves the purification efficiency of high-purity quartz, avoids the solidification of impurities, enhances the subsequent acid leaching effect, and obtains high-purity quartz with a SiO2 content greater than 99.99%.

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Abstract

本发明提供了一种助熔剂辅助煅烧‑水淬制备的高纯石英及制备方法,该方法步骤包括对石英原矿进行破碎、清洗,得到第一石英颗粒;对第一石英颗粒进行细磨、过筛,得到第二石英颗粒;对第二石英颗粒进行磁选、浮选,得到第三石英颗粒;对第三石英颗粒进行助熔剂辅助煅烧、水淬急冷处理,得到第四石英颗粒,对第四石英颗粒进行酸洗、水洗,得到高纯石英。本发明提供的制备高纯石英的方法能够有效在石英内部制造大量微裂纹,以提高打开矿物包裹体的效率;高纯石英SiO2含量大于99.99%。
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