A method for determining critical adsorption pore size by combining isothermal adsorption experiment and nuclear magnetic resonance

By combining isothermal adsorption experiments with nuclear magnetic resonance technology, the problem of accurately determining the critical adsorption pore size in existing technologies has been solved, enabling precise pore size determination under real reservoir conditions and improving the efficiency of shale gas reservoir evaluation and development.

CN122409461APending Publication Date: 2026-07-17SOUTHWEST PETROLEUM UNIV

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
SOUTHWEST PETROLEUM UNIV
Filing Date
2026-05-08
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies cannot directly capture the critical pore size value of gas transitioning from a free state to an adsorbed state under real reservoir temperature and pressure conditions. Nuclear magnetic resonance technology lacks a clear theoretical basis and cannot accurately define the critical adsorption pore size of adsorbed gas, which affects the evaluation and development of shale gas reservoirs.

Method used

By combining isothermal adsorption experiments with nuclear magnetic resonance (NMR) technology, the critical relaxation time and pore throat radius were calculated by measuring the isothermal adsorption data, NMR signal area, and calibration coefficients of shale samples. The relationship between relaxation time and pore size was established, and the critical adsorption pore size was determined.

Benefits of technology

It enables precise determination of critical adsorption pore size under real reservoir conditions, improving the reliability and development efficiency of shale gas reservoir evaluation, and is applicable to the precise calculation of shale gas and coalbed methane resources.

✦ Generated by Eureka AI based on patent content.

Smart Images

  • Figure CN122409461A_ABST
    Figure CN122409461A_ABST
Patent Text Reader

Abstract

本发明属于非常规天然气勘探开发技术领域,具体涉及一种联合等温吸附实验与核磁共振的临界吸附孔径确定方法,包括以下步骤:测定目标温度条件下页岩样品的等温吸附实验数据;确定目标压力下页岩对甲烷的吸附量;对纯甲烷开展核磁共振测试,获得对应的核磁共振信号面积,并计算出纯甲烷气体体积与核磁共振信号面积的标定系数;计算出对应于吸附气核磁信号面积;基于T2谱分布数据确定临界弛豫时间;建立弛豫时间T2与孔喉半径分布曲线的转换关系式,带入临界弛豫时间求解得到的临界吸附孔径。本发明克服了吸附气临界孔径大小确定的随意性,充分考虑了气体在孔隙中的赋存状态,利用T2谱临界弛豫时间来确定临界吸附孔径大小。
Need to check novelty before this filing date? Find Prior Art