4-fluoroisoquinoline sulfate impurity removal equipment

Abstract

The utility model relates to the technical field of 4-fluoroisoquinoline sulfate impurity removal, in particular to 4-fluoroisoquinoline sulfate impurity removal equipment which is characterized in that a solvent and 4-fluoroisoquinoline sulfate are poured into a storage mechanism and are circularly conveyed through a mixing mechanism; meanwhile, the storage mechanism is heated through the temperature adjusting mechanism, so that the solvent and the 4-fluoroisoquinoline sulfate in the storage mechanism are rapidly mixed and heated, after impurity removal is completed, the stored solvent and the 4-fluoroisoquinoline sulfate are rapidly cooled through the temperature adjusting mechanism, and then the cooled solvent and the cooled 4-fluoroisoquinoline sulfate are discharged through the storage mechanism; the practicability of the equipment is improved; comprising a storage mechanism; the device further comprises a mixing mechanism and a temperature adjusting mechanism, the storage mechanism is installed in the temperature adjusting mechanism, and the mixing mechanism is installed on the storage mechanism. The storage mechanism is used for storing a solvent, the mixing mechanism is used for circularly conveying the solvent, and the temperature adjusting mechanism is used for adjusting the temperature of the solvent.

Description

Technical Field

[0001] The utility model relates to the technical field of 4-fluoroisoquinoline sulfate impurity removal, in particular to 4-fluoroisoquinoline sulfate impurity removal equipment. Background Art

[0002] 4-Fluoroisoquinoline sulfate needs to be treated for impurities during the preparation process. The traditional method is to use a certain amount of mixed solvent, put the crystals into the solvent, and heat the solvent through a groove-wound low-temperature heating kettle disclosed in the utility model patent with application number 201520380257.4 and a stirring and concentrating heating kettle disclosed in the utility model patent with application number 202320814843.X to make the solvent boil, and then cool the solvent, discharge the cooled solvent, and filter it to obtain 4-fluoroisoquinoline sulfate with higher purity.

[0003] However, it was found during use that the existing heating kettle has a relatively simple structure, poor heating and cooling uniformity, and is inconvenient to clean the inside of the equipment, resulting in poor practicality. Therefore, a 4-fluoroisoquinoline sulfate impurity removal device is urgently needed to improve the above problems. Utility Model Content

[0004] In order to solve the above technical problems, the utility model provides a 4-fluoroisoquinoline sulfate impurity removal device, which pours a solvent and 4-fluoroisoquinoline sulfate into a storage mechanism, circulates and transports the solvent and 4-fluoroisoquinoline sulfate through a mixing mechanism, and heats the storage mechanism through a temperature regulating mechanism, so that the solvent and 4-fluoroisoquinoline sulfate in the storage mechanism are quickly mixed and heated, and after the impurity removal is completed, the storage is quickly cooled by the temperature regulating mechanism, and then the cooled solvent and 4-fluoroisoquinoline sulfate are discharged through the storage mechanism, thereby improving the practicality of the device.

[0005] The utility model discloses a 4-fluoroisoquinoline sulfate impurity removal device, comprising a storage mechanism, a mixing mechanism and a temperature regulating mechanism, wherein the storage mechanism is installed in the temperature regulating mechanism, and the mixing mechanism is installed on the storage mechanism; the storage mechanism stores the solvent, the mixing mechanism circulates and transports the solvent, and the temperature regulating mechanism regulates the temperature of the solvent;

[0006] The solvent and 4-fluoroisoquinoline sulfate are poured into a storage mechanism, and the solvent and 4-fluoroisoquinoline sulfate are circulated and transported through a mixing mechanism. At the same time, the storage mechanism is heated through a temperature regulating mechanism, so that the solvent and 4-fluoroisoquinoline sulfate in the storage mechanism are quickly mixed and heated. After the impurity removal is completed, the storage is quickly cooled down through the temperature regulating mechanism, and then the cooled solvent and 4-fluoroisoquinoline sulfate are discharged through the storage mechanism, thereby improving the practicability of the equipment.

[0007] Preferably, the storage mechanism includes a debris removal box and a stirring mechanism, the debris removal box is installed inside the temperature regulating mechanism, and a feed valve is provided at the top of the debris removal box, a discharge valve is provided at the bottom of the rear end of the debris removal box, and the stirring mechanism is installed on the debris removal box; the solvent and 4-fluoroisoquinoline sulfate are poured into the debris removal box, and the solvent and 4-fluoroisoquinoline sulfate are stirred and mixed by the mixing mechanism and the stirring mechanism, thereby improving the practicability of the equipment.

[0008] Preferably, the stirring mechanism includes a stirring shaft, multiple groups of first nozzles, a driving motor, a gear and a gear ring, the stirring shaft is rotatably installed on the top of the impurity removal box, the bottom end of the stirring shaft extends to the interior of the impurity removal box, and a drainage channel is provided inside the stirring shaft, the multiple groups of first nozzles are installed on the stirring shaft, the driving motor is installed on the top of the impurity removal box, the gear is installed on the output shaft of the driving motor, the gear ring is installed on the top of the stirring shaft, and the gear is meshed with the gear ring; turn on the driving motor, and drive the stirring shaft to rotate through the meshing transmission of the gear and the gear ring to stir the solvent and 4-fluoroisoquinoline sulfate in the impurity removal box, after the solvent and 4-fluoroisoquinoline sulfate in the impurity removal box are discharged, the top of the stirring shaft is connected to the water source through a rotary joint, and then water is sprayed into the interior of the impurity removal box through the multiple groups of first nozzles to clean the interior of the impurity removal box, thereby improving the practicability of the equipment.

[0009] Preferably, the mixing mechanism includes a circulation pump, an annular tube, multiple groups of circulation tubes and multiple groups of second nozzles, the circulation pump is installed at the bottom end of the impurity removal box, the water suction port of the circulation pump is communicated with the interior of the impurity removal box, and an electric control valve is provided on the water suction port of the circulation pump, the annular tube is installed on the discharge port of the circulation pump, one end of the multiple groups of circulation tubes are all installed on the annular tube, the other ends of the multiple groups of circulation tubes are all extended to the interior of the impurity removal box, and the multiple groups of second nozzles are respectively installed on the other ends of the multiple groups of circulation tubes; turn on the circulation pump, discharge the solvent and 4-fluoroisoquinoline sulfate in the impurity removal box into the annular tube, and then spray the solvent and 4-fluoroisoquinoline sulfate back into the impurity removal box through the multiple groups of second nozzles, so that the solvent and 4-fluoroisoquinoline sulfate are quickly mixed, thereby improving the practicability of the equipment.

[0010] Preferably, the temperature regulating mechanism comprises a temperature regulating box, a base, an inlet valve and an outlet valve, the temperature regulating box is installed on the base, the impurity removal box is installed inside the temperature regulating box, the inlet valve is installed at the top of the right end of the temperature regulating box, and the outlet valve is installed at the bottom of the left end of the temperature regulating box; the inlet valve is opened to discharge steam into the temperature regulating box, so that the steam heats the impurity removal box and multiple groups of circulation pipes, and then the steam is discharged through the outlet valve to quickly heat the solvent. After purifying 4-fluoroisoquinoline sulfate, clean water is discharged into the temperature regulating box through the inlet valve, and then the clean water is discharged through the outlet valve to quickly cool the solvent, thereby improving the practicality of the equipment.

[0011] Preferably, it also includes a plurality of groups of temperature conduction plates, which are respectively installed on the plurality of groups of circulation pipes; the temperature is conducted by the plurality of groups of temperature conduction plates, so that the solvent is quickly heated or cooled, thereby improving the practicability of the equipment.

[0012] Preferably, a pressure relief valve is provided at the top of the impurity removal box; excess air in the impurity removal box is discharged through the pressure relief valve, thereby improving the practicability of the equipment.

[0013] Compared with the prior art, the utility model has the following beneficial effects: the solvent and 4-fluoroisoquinoline sulfate are poured into the storage mechanism, the solvent and 4-fluoroisoquinoline sulfate are circulated and transported through the mixing mechanism, and the storage mechanism is heated through the temperature regulating mechanism at the same time, so that the solvent and 4-fluoroisoquinoline sulfate in the storage mechanism are quickly mixed and heated, and after the impurity removal is completed, the storage is quickly cooled down through the temperature regulating mechanism, and then the cooled solvent and 4-fluoroisoquinoline sulfate are discharged through the storage mechanism, thereby improving the practicality of the equipment. BRIEF DESCRIPTION OF THE DRAWINGS

[0014] Figure 1 It is a first axonometric structural schematic diagram of the utility model;

[0015] Figure 2 It is a second axonometric structural schematic diagram of the utility model;

[0016] Figure 3 It is a front view structural schematic diagram of the utility model;

[0017] Figure 4 It is a front view cross-sectional structural schematic diagram of the utility model;

[0018] Figure 5 This utility model Figure 4 Schematic diagram of the enlarged structure of part A in FIG.

[0019] Markings in the attached drawings: 1. impurity removal box; 2. stirring shaft; 3. first nozzle; 4. driving motor; 5. gear; 6. gear ring; 7. circulation pump; 8. annular pipe; 9. circulation pipe; 10. second nozzle; 11. electric control valve; 12. temperature control box; 13. base; 14. inlet valve; 15. outlet valve; 16. temperature conduction plate; 17. pressure relief valve. DETAILED DESCRIPTION

[0020] In order to facilitate the understanding of the utility model, the utility model will be described more comprehensively below with reference to the relevant drawings. The utility model can be implemented in many different forms and is not limited to the embodiments described herein. On the contrary, the purpose of providing these embodiments is to make the disclosure of the utility model more thorough and comprehensive.

[0021] Example 1

[0022] including storage institutions;

[0023] It also includes a mixing mechanism and a temperature regulating mechanism, the storage mechanism is installed in the temperature regulating mechanism, and the mixing mechanism is installed on the storage mechanism;

[0024] The storage mechanism stores the solvent, the mixing mechanism circulates and transports the solvent, and the temperature regulating mechanism regulates the temperature of the solvent;

[0025] The storage mechanism includes a debris removal box 1 and a stirring mechanism. The debris removal box 1 is installed inside the temperature adjustment mechanism, and a feed valve is provided at the top of the debris removal box 1, and a discharge valve is provided at the bottom of the rear end of the debris removal box 1. The stirring mechanism is installed on the debris removal box 1;

[0026] The stirring mechanism includes a stirring shaft 2, multiple groups of first nozzles 3, a driving motor 4, a gear 5 and a gear ring 6. The stirring shaft 2 is rotatably mounted on the top of the impurity removal box 1, the bottom end of the stirring shaft 2 extends to the inside of the impurity removal box 1, and a drainage channel is provided inside the stirring shaft 2. The multiple groups of first nozzles 3 are all mounted on the stirring shaft 2, the driving motor 4 is mounted on the top of the impurity removal box 1, the gear 5 is mounted on the output shaft of the driving motor 4, the gear ring 6 is mounted on the top of the stirring shaft 2, and the gear 5 is meshed and connected with the gear ring 6;

[0027] The solvent and 4-fluoroisoquinoline sulfate are poured into the impurity removal box 1, and the driving motor 4 is turned on. The gear 5 is meshed with the gear ring 6 to drive the stirring shaft 2 to rotate to stir the solvent and 4-fluoroisoquinoline sulfate in the impurity removal box 1, and the solvent and 4-fluoroisoquinoline sulfate are circulated and transported through the mixing mechanism. At the same time, the storage mechanism is heated by the temperature regulating mechanism to make the solvent and 4-fluoroisoquinoline sulfate in the storage mechanism quickly mix and heat up. After the impurity removal is completed, the storage is quickly cooled by the temperature regulating mechanism, and then the cooled solvent and 4-fluoroisoquinoline sulfate are discharged through the storage mechanism. The top of the stirring shaft 2 is connected to the water source through a rotary joint, and then water is sprayed into the interior of the impurity removal box 1 through multiple groups of first nozzles 3 to clean the interior of the impurity removal box 1, thereby improving the practicability of the equipment.

[0028] Example 2

[0029] like Figures 1 to 5 As shown, including a storage mechanism;

[0030] It also includes a mixing mechanism and a temperature regulating mechanism, the storage mechanism is installed in the temperature regulating mechanism, and the mixing mechanism is installed on the storage mechanism;

[0031] The storage mechanism stores the solvent, the mixing mechanism circulates and transports the solvent, and the temperature regulating mechanism regulates the temperature of the solvent;

[0032] The storage mechanism includes a debris removal box 1 and a stirring mechanism. The debris removal box 1 is installed inside the temperature adjustment mechanism, and a feed valve is provided at the top of the debris removal box 1, and a discharge valve is provided at the bottom of the rear end of the debris removal box 1. The stirring mechanism is installed on the debris removal box 1;

[0033] The stirring mechanism includes a stirring shaft 2, multiple groups of first nozzles 3, a driving motor 4, a gear 5 and a gear ring 6. The stirring shaft 2 is rotatably mounted on the top of the impurity removal box 1, the bottom end of the stirring shaft 2 extends to the inside of the impurity removal box 1, and a drainage channel is provided inside the stirring shaft 2. The multiple groups of first nozzles 3 are all mounted on the stirring shaft 2, the driving motor 4 is mounted on the top of the impurity removal box 1, the gear 5 is mounted on the output shaft of the driving motor 4, the gear ring 6 is mounted on the top of the stirring shaft 2, and the gear 5 is meshed and connected with the gear ring 6;

[0034] The mixing mechanism includes a circulation pump 7, an annular pipe 8, multiple groups of circulation pipes 9 and multiple groups of second nozzles 10. The circulation pump 7 is installed at the bottom end of the impurity removal box 1. The water suction port of the circulation pump 7 is communicated with the interior of the impurity removal box 1, and an electric control valve 11 is provided on the water suction port of the circulation pump 7. The annular pipe 8 is installed on the drainage port of the circulation pump 7. One ends of the multiple groups of circulation pipes 9 are all installed on the annular pipe 8. The other ends of the multiple groups of circulation pipes 9 extend to the interior of the impurity removal box 1. The multiple groups of second nozzles 10 are respectively installed on the other ends of the multiple groups of circulation pipes 9.

[0035] The temperature regulating mechanism includes a temperature regulating box 12, a base 13, an inlet valve 14 and an outlet valve 15. The temperature regulating box 12 is installed on the base 13, the impurity removal box 1 is installed inside the temperature regulating box 12, the inlet valve 14 is installed on the top of the right end of the temperature regulating box 12, and the outlet valve 15 is installed on the bottom of the left end of the temperature regulating box 12;

[0036] It also includes a plurality of groups of heat transfer plates 16, which are respectively installed on the plurality of groups of circulation pipes 9;

[0037] A pressure relief valve 17 is provided at the top of the impurity removal box 1;

[0038] The solvent and 4-fluoroisoquinoline sulfate are poured into the impurity removal box 1, the driving motor 4 is turned on, and the gear 5 is meshed with the gear ring 6 to drive the stirring shaft 2 to rotate to stir the solvent and 4-fluoroisoquinoline sulfate in the impurity removal box 1, and the circulating pump 7 is turned on to discharge the solvent and 4-fluoroisoquinoline sulfate in the impurity removal box 1 into the annular pipe 8, and then the solvent and 4-fluoroisoquinoline sulfate are sprayed back into the impurity removal box 1 through multiple groups of second nozzles 10, so that the solvent and 4-fluoroisoquinoline sulfate are quickly mixed, and at the same time, the inlet valve 14 is opened to discharge the steam into the temperature regulating box 12, and the temperature is conducted through multiple groups of temperature conduction plates 16, so that the steam can heat the impurity removal box. 1 and multiple groups of circulation pipes 9 are heated, and then the steam is discharged through the discharge valve 15 to quickly heat the solvent, and the excess air in the impurity removal box 1 is discharged through the pressure relief valve 17. After purifying 4-fluoroisoquinoline sulfate, clean water is discharged into the temperature adjustment box 12 through the inlet valve 14, and then the clean water is discharged through the discharge valve 15 to quickly cool the solvent. Then, the cooled solvent and 4-fluoroisoquinoline sulfate are discharged through the storage mechanism, the top of the stirring shaft 2 is connected to the water source through a rotary joint, and then water is sprayed into the interior of the impurity removal box 1 through multiple groups of first nozzles 3 to clean the interior of the impurity removal box 1, thereby improving the practicality of the equipment.

[0039] The driving motor 4, circulating pump 7 and electric control valve 11 of the 4-fluoroisoquinoline sulfate impurity removal device of the utility model are purchased on the market, and technicians in the industry only need to install and operate them according to the accompanying instruction manual, without the need for creative labor by technicians in the field.

[0040] The above is only a preferred embodiment of the present invention. It should be pointed out that for ordinary technicians in this technical field, several improvements and modifications can be made without departing from the technical principle of the present invention. These improvements and modifications should also be regarded as the protection scope of the present invention.

Claims

1. A 4-fluoroisoquinoline sulfate impurity removal device, comprising a storage mechanism; characterized in that: It also includes a mixing mechanism and a temperature regulating mechanism, the storage mechanism is installed in the temperature regulating mechanism, and the mixing mechanism is installed on the storage mechanism; The storage mechanism stores the solvent, the mixing mechanism circulates and transports the solvent, and the temperature regulating mechanism regulates the temperature of the solvent; The storage mechanism comprises a de-powder box (1) and a stirring mechanism, the de-powder box (1) is installed inside the temperature regulating mechanism, a feed valve is arranged at the top of the de-powder box (1), a discharge valve is arranged at the bottom of the rear end of the de-powder box (1), and the stirring mechanism is installed on the de-powder box (1); The stirring mechanism comprises a stirring shaft (2), a plurality of first nozzles (3), a driving motor (4), a gear (5) and a gear ring (6); the stirring shaft (2) is rotatably mounted on the top of the impurity removal box (1); the bottom end of the stirring shaft (2) extends into the interior of the impurity removal box (1); a drainage channel is provided inside the stirring shaft (2); the plurality of first nozzles (3) are mounted on the stirring shaft (2); the driving motor (4) is mounted on the top of the impurity removal box (1); the gear (5) is mounted on the output shaft of the driving motor (4); the gear ring (6) is mounted on the top of the stirring shaft (2); and the gear (5) is meshedly connected with the gear ring (6); The mixing mechanism comprises a circulation pump (7), an annular tube (8), a plurality of circulation tubes (9) and a plurality of second nozzles (10); the circulation pump (7) is mounted at the bottom end of the impurity removal box (1); a water suction port of the circulation pump (7) is communicated with the interior of the impurity removal box (1); an electric control valve (11) is provided on the water suction port of the circulation pump (7); the annular tube (8) is mounted on the drainage port of the circulation pump (7); one end of the plurality of circulation tubes (9) are mounted on the annular tube (8); the other end of the plurality of circulation tubes (9) are extended to the interior of the impurity removal box (1); and the plurality of second nozzles (10) are respectively mounted on the other end of the plurality of circulation tubes (9).

2. A 4-fluoroisoquinoline sulfate impurity removal device as claimed in claim 1, characterized in that: The temperature regulating mechanism comprises a temperature regulating box (12), a base (13), an inlet valve (14) and an outlet valve (15); the temperature regulating box (12) is mounted on the base (13); the impurity removal box (1) is mounted inside the temperature regulating box (12); the inlet valve (14) is mounted on the top of the right end of the temperature regulating box (12); and the outlet valve (15) is mounted on the bottom of the left end of the temperature regulating box (12).

3. A 4-fluoroisoquinoline sulfate impurity removal device as claimed in claim 1, characterized in that: It also includes a plurality of groups of temperature conducting plates (16), which are respectively installed on the plurality of groups of circulation pipes (9).

4. A 4-fluoroisoquinoline sulfate impurity removal device as claimed in claim 1, characterized in that: A pressure relief valve (17) is provided at the top of the impurity removal box (1).

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