Automatic control continuous production device of diazo compound
By introducing an automatically controlled stirring mechanism and gear meshing connection in the diazon compound production device, the problem of uneven stirring of materials is solved, and the yield and quality of diazon salts are improved.
Patent Information
- Application Number
- CN202421695202.8
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-07-17
- Publication Date
- 2025-09-05
- Estimated Expiration
- 2034-07-17
AI Technical Summary
The materials in the existing diazotization reactor are unevenly stirred, resulting in uneven temperature, affecting the quality and yield of diazonium salt.
The automatic control continuous production device is adopted, including the meshing connection between the stirring mechanism and the gear, to ensure uniform stirring and turning of the materials, and the motor assembly is used to drive the stirring shaft and the reactor body to rotate in reverse, improving mixing uniformity.
The uniform stirring and temperature uniformity of the materials in the reactor are achieved, and the yield and quality of the diazonium substance are improved.
Smart Images
Figure CN223299998U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of diazo compounds, in particular to an automatic control continuous production device for diazo compounds. Background Art
[0002] The saccharin industry is a traditional process with a long history of development in the fine chemical industry. At present, the phthalic anhydride method is mainly used to prepare saccharin in China. This method has a simple process and high yield, but the automatic control technology is relatively backward, especially the diazotization reaction. The reaction conditions are harsh and the yield is low. Improving the level of automation in this field has always been the unremitting goal pursued by people in the industry. Diazotized compounds are generally prepared by intermittent diazotization reactions.
[0003] Currently, there are many devices for diazotization reactions, among which the reactor is one of them. However, it is difficult to ensure uniform stirring in all parts of the reactor. Local material ratios deviate from the reaction conditions, and the temperature in the reactor is uneven. These phenomena will lead to the decomposition of diazonium salts and various side reactions, resulting in poor quality and low yield of diazonium salts. Utility Model Content
[0004] (1) Technical problems solved
[0005] In response to the shortcomings of the existing technology, the utility model provides an automatically controlled continuous production device for diazo compounds, which has the function of enabling the materials inside the reactor to undergo a uniform stirring reaction, thereby making the temperature in the reactor more uniform, thereby avoiding the low yield and poor quality of the produced diazo substances.
[0006] (2) Technical solution
[0007] To achieve the above-mentioned purpose, the present invention provides the following technical solution: an automatic controlled continuous production device for diazo compounds, comprising two fixed blocks, the two fixed blocks being arranged front and back, and the lower sides of the two fixed blocks being fixedly connected to support legs;
[0008] The reactor body is rotatably connected between the two fixed blocks, and there is no blocking cover on the front side of the reactor body;
[0009] A blocking cover is fixedly connected to the rear side of the reactor body, and an open groove is provided on the outer surface of the reactor body;
[0010] The opening groove is communicated with the interior of the reactor body, a switch door is provided on the opening groove, and a rotating shaft is rotatably connected between the switch door and the opening groove;
[0011] The switch door and the opening slot are rotatably connected by a rotating shaft. The switch door and the rotating shaft can be snapped together. A handle is fixedly connected to the upper side of the switch door. A stirring mechanism is provided inside the fixed block on the front side and the reactor body. The stirring mechanism can evenly stir the material inside the reactor body.
[0012] The stirring mechanism includes a motor assembly, a stirring shaft, three stirring blades, a rotating ring groove, a first gear and a second gear.
[0013] Preferably, the motor assembly is fixedly connected to the front side of the fixed block, the output end of the motor assembly is fixedly connected to the transmission shaft, and the rear end of the transmission shaft rotates and passes through the front fixed block.
[0014] Preferably, the rear end of the transmission shaft rotates and extends into the interior of the reactor body, the stirring shaft is fixedly connected to the rear end of the transmission shaft, and a rotating ring groove is formed on the rear wall of the reactor body. Preferably, the rear end of the stirring shaft is slidably connected to the rear wall of the rotating ring groove, and the three stirring blades are fixedly connected to the outer surface of the stirring shaft.
[0015] Preferably, the three stirring blades are arranged in a ring array on the outer surface of the stirring shaft, the three stirring blades are all arranged inside the reactor body, and the first gear is fixedly sleeved on the outer surface of the stirring shaft.
[0016] Preferably, the first gear is arranged on the rear side of the stirring blade, the second gear is fixedly connected to the rear wall of the reactor body, and the second gear is meshed with the first gear.
[0017] (3) Beneficial effects
[0018] Compared with the prior art, the present invention provides an automatic control continuous production device for diazo compounds, which has the following beneficial effects:
[0019] (1) The automatic control continuous production device of the diazo compound starts the motor assembly, which transmits power from the output end. After the transmission, the material can be turned over while being stirred by the stirring blade, so that the material can be stirred evenly. After the reaction is completed, it only needs to turn the switch door to the lower side, and then it can be discharged from the open slot.
[0020] (2) In the automatic control continuous production device for diazo compounds, since the first gear is meshed with the second gear, the rotation direction of the stirring shaft and the reaction kettle body are opposite, which further improves the efficiency of uniform mixing of materials. BRIEF DESCRIPTION OF THE DRAWINGS
[0021] Figure 1 This is a schematic structural diagram of the automatic control continuous production device for diazo compounds of the utility model;
[0022] Figure 2 This is a schematic diagram of the cross-sectional connection structure of the reactor body of the utility model;
[0023] Figure 3 for Figure 2 A magnified schematic diagram of .
[0024] In the figure: 1. Fixed block; 2. Support leg; 3. Reactor body; 4. Opening slot; 5. Switch door; 6. Rotating shaft; 7. Handle; 8. Motor assembly; 9. Transmission shaft; 10. Stirring shaft; 11. Stirring blade; 12. Rotating ring groove; 13. First gear; 14. Second gear. DETAILED DESCRIPTION
[0025] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the embodiments described are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative efforts are within the scope of protection of the present invention.
[0026] See also Figures 1 to 3 The utility model provides a new technical solution: an automatic control continuous production device for diazo compounds, comprising two fixed blocks 1, the two fixed blocks 1 are arranged in a front-to-back manner, the lower sides of the two fixed blocks 1 are fixedly connected to support legs 2, a reactor body 3 is rotatably connected between the two fixed blocks 1, the front side of the reactor body 3 has no blocking cover, the rear side of the reactor body 3 is fixedly connected to a blocking cover, the outer surface of the reactor body 3 is provided with an opening groove 4, the opening groove 4 is communicated with the interior of the reactor body 3, a switch door 5 is provided on the opening groove 4, the switch door 5 and the opening A rotating shaft 6 is rotatably connected between the grooves 4, and the switch door 5 and the open groove 4 are rotatably connected through the rotating shaft 6. The switch door 5 and the rotating shaft 6 can be snapped together. The switch door 5 is an existing structure, so no further explanation is given. A handle 7 is fixedly connected to the upper side of the switch door 5. A stirring mechanism is provided inside the front fixing block 1 and the reactor body 3. The stirring mechanism can evenly stir the material inside the reactor body 3. The stirring mechanism includes a motor assembly 8, a stirring shaft 10, three stirring blades 11, a rotating ring groove 12, a first gear 13 and a second gear 14.
[0027] Furthermore, the motor assembly 8 is fixedly connected to the front side of the fixed block 1, and the output end of the motor assembly 8 is fixedly connected to the transmission shaft 9. The rear end of the transmission shaft 9 rotates and passes through the front fixed block 1. The rear end of the transmission shaft 9 rotates and extends into the interior of the reactor body 3. The stirring shaft 10 is fixedly connected to the rear end of the transmission shaft 9. The rotating annular groove 12 is opened on the rear wall of the reactor body 3. The rear end of the stirring shaft 10 is slidingly connected to the rear wall of the rotating annular groove 12. The three stirring blades 11 are all fixedly connected to the outer surface of the stirring shaft 10. The three stirring blades 11 are arranged in a ring array on the outer surface of the stirring shaft 10. The three stirring blades 11 are all arranged in the interior of the reactor body 3. The first gear 13 is fixedly sleeved on the outer surface of the stirring shaft 10. The first gear 13 is arranged on the rear side of the stirring blade 11. The second gear 14 is fixedly connected to the rear wall of the reactor body 3, and the second gear 14 is meshed with the first gear 13.
[0028] Furthermore, when the reaction is carried out, the switch door 5 is opened after the card is released, and then various materials are poured into the interior of the reactor body 3, and then the switch door 5 is closed and carded, and then the motor assembly 8 is started. The motor assembly 8 starts to transmit power from the output end, driving the transmission shaft 9 to start rotating, and the transmission shaft 9 drives the stirring shaft 10 to rotate, and the stirring shaft 10 drives the stirring blade 11 to start rotating. When the stirring blade 11 rotates, it will stir the material inside the reactor body 3. At the same time, the stirring shaft 10 will drive the first gear 13 to rotate synchronously, and the first gear 13 drives the meshing second gear 14 to rotate synchronously, and the second gear 14 drives the fixedly connected reactor body 3 to rotate. At this time, the stirring shaft 10 The rear end is slidably connected to the inside of the rotating ring groove 12. When the reactor body 3 rotates, the material inside it will be driven to turn over, so that the material is turned over while being stirred by the stirring blades 11, and the material can be stirred evenly. Moreover, because the first gear 13 is meshed with the second gear 14, the rotation direction of the stirring shaft 10 is opposite to that of the reactor body 3, which further improves the efficiency of uniform mixing. After the reaction is completed, it is only necessary to rotate the switch door 5 to the lower side, and then it can be discharged from the open groove 4. In this way, the material inside the reactor body 3 can be stirred and reacted evenly, so that the temperature in the reactor body 3 will be more uniform, avoiding the low yield and poor quality of the produced diazo substance.
[0029] Working principle: When the reaction is carried out, first release the clamping and open the switch door 5, then pour various materials into the interior of the reactor body 3, then close the switch door 5 and clamp it, and then start the motor assembly 8. The motor assembly 8 starts to transmit power from the output end, driving the transmission shaft 9 to start rotating, the transmission shaft 9 drives the stirring shaft 10 to rotate, and the stirring shaft 10 drives the stirring blade 11 to start rotating. When the stirring blade 11 rotates, it will stir the materials inside the reactor body 3, and at the same time, the stirring shaft 10 will drive the first gear 13 to rotate synchronously, and the first gear 13 will drive the meshing second gear 14 to rotate synchronously. The first gear 13 and the second gear 14 are meshed and connected to each other, so the rotation direction of the stirring shaft 10 is opposite to that of the reactor body 3, which further improves the mixing efficiency. After the reaction is completed, it is only necessary to rotate the switch door 5 to the bottom side to discharge it from the opening slot 4.
[0030] Although the embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and variations may be made to these embodiments without departing from the principles and spirit of the present invention, and the scope of the present invention is defined by the appended claims and their equivalents.
Claims
1. An automatic controlled continuous production device for a diazo compound, comprising two fixed blocks (1), the two fixed blocks (1) being arranged front and back, and the lower sides of the two fixed blocks (1) being fixedly connected to support legs (2); The reactor body (3) is rotatably connected between the two fixed blocks (1), and the front side of the reactor body (3) has no blocking cover; A blocking cover is fixedly connected to the rear side of the reactor body (3), and an opening groove (4) is provided on the outer surface of the reactor body (3); The opening groove (4) is in communication with the interior of the reactor body (3); a switch door (5) is provided on the opening groove (4); and a rotating shaft (6) is rotatably connected between the switch door (5) and the opening groove (4); The switch door (5) and the opening slot (4) are rotatably connected via a rotating shaft (6). The switch door (5) and the rotating shaft (6) can be snapped together. A handle (7) is fixedly connected to the upper side of the switch door (5). The present invention is characterized in that: A stirring mechanism is provided inside the fixed block (1) and the reactor body (3) on the front side, and the stirring mechanism can evenly stir the materials inside the reactor body (3); The stirring mechanism comprises a motor assembly (8), a stirring shaft (10), three stirring blades (11), a rotating ring groove (12), a first gear (13) and a second gear (14).
2. The automatic control continuous production device for diazo compounds according to claim 1, characterized in that: The motor assembly (8) is fixedly connected to the front side of the fixed block (1); the output end of the motor assembly (8) is fixedly connected to a transmission shaft (9); the rear end of the transmission shaft (9) rotates and passes through the front side fixed block (1).
3. The automatic control continuous production device of a diazo compound according to claim 2, characterized in that: The rear end of the transmission shaft (9) rotates and extends into the interior of the reactor body (3), the stirring shaft (10) is fixedly connected to the rear end of the transmission shaft (9), and the rotating ring groove (12) is opened on the rear wall of the reactor body (3).
4. The automatic control continuous production device of a diazo compound according to claim 3, characterized in that: The rear end of the stirring shaft (10) is slidably connected to the rear wall of the rotating ring groove (12), and the three stirring blades (11) are fixedly connected to the outer surface of the stirring shaft (10).
5. The automatic control continuous production device of a diazo compound according to claim 4, characterized in that: The three stirring blades (11) are arranged in a ring array on the outer surface of the stirring shaft (10). The three stirring blades (11) are all arranged inside the reactor body (3). The first gear (13) is fixedly sleeved on the outer surface of the stirring shaft (10).
6. The automatic control continuous production device for diazo compounds according to claim 5, characterized in that: The first gear (13) is arranged on the rear side of the stirring blade (11), and the second gear (14) is fixedly connected to the rear wall of the reactor body (3), and the second gear (14) is meshed with the first gear (13).