Quantitative-feeding catalyst preparation equipment

The quantitative addition catalyst configuration equipment solves the problems of inaccurate catalyst configuration and manual transfer in the preparation of traditional alkyl zinc reagents, achieves accurate addition and mixing uniformity of the catalyst, and improves preparation efficiency and product quality.

CN223337268UActive Publication Date: 2025-09-16上海豪胜化工科技有限公司
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Patent Information

Application Number
CN202422811146.6
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-11-19
Publication Date
2025-09-16
Estimated Expiration
2034-11-19

AI Technical Summary

Technical Problem

In the traditional preparation process of alkyl zinc reagents, the selection and configuration of catalysts rely on the experimenter's experience and lack precise control, resulting in low efficiency and unstable product quality. In addition, the existing configuration equipment requires manual transfer of raw materials after weighing, which affects the feeding efficiency.

Method used

A quantitative catalyst preparation equipment was designed. It used an electronic scale combined with a screw feeder to achieve automatic quantitative addition. It was equipped with a blower to dry the discharge pipe, a stirring motor and stirring blades for mixing, and a built-in electric heater and a delivery pump in the barrel to control the amount of liquid added.

Benefits of technology

It achieves precise quantitative addition of catalysts, reduces manual operations, improves feeding efficiency and consistency of product quality, and ensures mixing uniformity and ease of configuration.

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Abstract

The utility model relates to the technical field of pharmaceutical configuration equipment, in particular to catalyst configuration equipment capable of quantitatively adding materials, which comprises a configuration barrel, a feeding barrel fixedly mounted at the top of the configuration barrel, a supporting plate fixedly mounted on a barrel body at the top of the configuration barrel, an electronic scale fixedly mounted on the supporting plate, and a supporting beam fixedly mounted on a weighing platform of the electronic scale. A spiral feeding machine is fixedly installed at the top of the supporting beam, a discharging pipe is fixedly installed at the discharging end of the spiral feeding machine and matched with the feeding cylinder in an inserted connection mode, a vertical pipe is fixedly installed at the top end of the discharging pipe, a fan is fixedly installed on the inner wall of the vertical pipe, and a flushing pipe is fixedly installed on a cylinder body at the top of the configuration cylinder; a conveying pump is arranged on one side of the configuration cylinder, a suction pipe is fixedly installed at the liquid inlet end of the conveying pump, a liquid medicine pipe is fixedly installed at the liquid outlet end of the conveying pump, and a flow meter is fixedly installed on the liquid medicine pipe. The device is convenient to carry out quantitative material adding and mixing preparation operation, and is convenient to use.
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Description

Technical Field

[0001] The utility model relates to the technical field of pharmaceutical preparation equipment, in particular to a catalyst preparation equipment for quantitative addition. Background Art

[0002] Alkyl zinc reagents are an important class of organic synthesis reagents with a wide range of applications, including medicinal chemistry, materials science, and organic chemistry. In the pharmaceutical field, alkyl zinc reagents are widely used in the synthesis and modification of drugs due to their unique reactivity and selectivity. However, in the preparation and application of alkyl zinc reagents, the selection and configuration of catalysts are one of the key factors restricting their performance.

[0003] In the traditional preparation process of alkyl zinc reagents, the selection and configuration of catalysts often rely on the experimenter's experience and intuition, lacking precise control and quantitative analysis. This traditional preparation method is not only inefficient, but also difficult to ensure the consistency and stability of product quality.

[0004] Currently, to achieve quantitative feeding, most catalyst dispensing equipment is equipped with an electronic scale to weigh the raw materials. However, after the electronic scale is used to complete the weighing operation, these dispensing equipment still requires manual removal of the weighed raw materials and then manually adding them to the corresponding dispensing device. This operation is relatively cumbersome, affects the efficiency of feeding, and brings inconvenience to the user. In view of this, we have proposed a catalyst dispensing equipment with quantitative feeding. Utility Model Content

[0005] The purpose of the present invention is to provide a catalyst configuration device with quantitative addition to solve the defects mentioned in the above background technology.

[0006] To achieve the above purpose, the present invention provides the following technical solutions:

[0007] A catalyst configuration device for quantitative addition includes a configuration cylinder, a feed cylinder is fixedly installed on the top of the configuration cylinder, a second unloading valve is fixedly installed on the feed cylinder, a support plate is fixedly installed on the top cylinder body of the configuration cylinder, an electronic scale is fixedly installed on the support plate, a support beam is fixedly installed on the scale platform of the electronic scale, a screw feeder is fixedly installed on the top of the support beam, a discharge pipe is fixedly installed on the discharge end of the screw feeder, the discharge pipe is located in the feed cylinder and is plugged into the feed cylinder, a vertical pipe arranged vertically is fixedly installed on the top of the discharge pipe, a fan is fixedly installed on the inner wall of the vertical pipe, a feed pipe is fixedly installed on the feed end of the screw feeder, and a feed hopper is fixedly installed on the top of the feed pipe.

[0008] Preferably, the distance between the discharge pipe and the inner wall of the feed barrel is greater than 1 mm, and the fan is arranged toward one side of the discharge pipe.

[0009] Preferably, an electric heater is fixedly mounted on the cylinder body of the configuration cylinder, and a conical cylinder is fixedly mounted on the bottom of the configuration cylinder.

[0010] Preferably, a discharge pipe is fixedly installed at the bottom end of the conical cylinder, and a first discharge valve is fixedly installed on the discharge pipe.

[0011] Preferably, a flushing tube is fixedly mounted on the top cylinder of the configuration cylinder, and the inner diameter of the flushing tube is greater than 3 cm.

[0012] Preferably, a delivery pump is provided on one side of the configuration cylinder, a suction tube is fixedly mounted on the liquid inlet end of the delivery pump, a medicine liquid tube is fixedly mounted on the liquid outlet end of the delivery pump, and a flow meter is fixedly mounted on the medicine liquid tube.

[0013] Preferably, a stirring motor is fixedly mounted at the center of the top surface of the configuration cylinder, a vertical stirring shaft is fixedly mounted at the end of the output shaft of the stirring motor, and a first stirring blade is fixedly mounted on the stirring shaft.

[0014] Preferably, a material passing gap is provided on the first stirring blade, and a second stirring blade is fixedly mounted on the stirring shaft, and the second stirring blade is located on one side of the material passing gap.

[0015] Compared with the prior art, the beneficial effects of the present invention are:

[0016] 1. The utility model can perform weighing operations through the electronic scale provided. After weighing, a spiral feeder is used to directly transport the weighed quantitative raw materials into the configuration cylinder to complete the quantitative addition operation. In addition, the vertical pipe and fan provided can dry the discharge pipe part to avoid moisture and sticking of the material in the discharge pipe part, which affects the accuracy of raw material addition, thereby achieving the effect of facilitating the quantitative addition of raw materials.

[0017] 2. The utility model can control the amount of added liquid through the provision of a delivery pump and a flow meter. In addition, the provision of a stirring motor, a stirring shaft, a first stirring blade and a second stirring blade can achieve the effect of stirring the raw materials, which is convenient to use. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] Figure 1 It is a schematic diagram of the overall structure of the utility model;

[0019] Figure 2 This is a schematic diagram of the explosion structure of the utility model;

[0020] Figure 3 This is one of the partial structural diagrams of the utility model;

[0021] Figure 4 This is the second schematic diagram of the partial structure of the utility model;

[0022] The meaning of each number in the figure is:

[0023] 1. Configuration cylinder; 10. Electric heater; 11. Conical cylinder; 12. Discharge pipe; 13. First discharge valve; 14. Flushing pipe; 15. Support plate; 16. Delivery pump; 161. Suction pipe; 17. Liquid medicine pipe; 171. Flow meter; 18. Feed cylinder; 181. Second discharge valve;

[0024] 2. Stirring motor; 20. Stirring shaft; 21. First stirring blade; 211. Material gap; 22. Second stirring blade;

[0025] 3. Electronic scale; 30. Support beam; 31. Screw feeder; 32. Discharge pipe; 33. Vertical pipe; 34. Fan; 35. Feed pipe; 36. Feed hopper. DETAILED DESCRIPTION

[0026] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the embodiments described are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative efforts are within the scope of protection of the present invention.

[0027] See also Figure 1-Figure 4 The utility model provides a technical solution: a catalyst configuration device for quantitative addition, comprising a configuration cylinder 1, a feed cylinder 18 is fixedly mounted on the top of the configuration cylinder 1, a second discharge valve 181 is fixedly mounted on the feed cylinder 18, a support plate 15 is fixedly mounted on the top cylinder body of the configuration cylinder 1, an electronic scale 3 is fixedly mounted on the support plate 15, a support beam 30 is fixedly mounted on the weighing platform of the electronic scale 3, a screw feeder 31 is fixedly mounted on the top of the support beam 30, a discharge end of the screw feeder 31 is fixedly mounted with a discharge pipe 32, the discharge pipe 32 is located in the feed cylinder 18 and is plugged into and matched with the feed cylinder 18, the distance between the discharge pipe 32 and the inner wall of the feed cylinder 18 is greater than 1 mm, so that the discharge pipe 32 and the feed cylinder 18 will not affect the weighing accuracy due to friction;

[0028] Specifically, a vertical tube 33 arranged vertically is fixedly installed on the top of the discharge pipe 32, a fan 34 is fixedly installed on the inner wall of the vertical tube 33, a feed pipe 35 is fixedly installed on the feed end of the spiral feeder 31, and a feed hopper 36 is fixedly installed on the top of the feed pipe 35. The fan 34 is arranged toward one side of the discharge pipe 32 to achieve a drying operation on the discharge pipe 32 by using the fan 34 to avoid moist and sticky materials in the discharge pipe 32, which affects the accuracy of material addition.

[0029] In this embodiment, an electric heater 10 is fixedly installed on the cylinder body of the configuration cylinder 1, and the electric heater 10 is used for heating operation; a conical cylinder 11 is fixedly installed on the bottom of the configuration cylinder 1, and a discharge pipe 12 is fixedly installed on the bottom end of the conical cylinder 11, and a first discharge valve 13 is fixedly installed on the discharge pipe 12, which is convenient for opening the first discharge valve 13 to perform discharge operation.

[0030] Specifically, a flushing pipe 14 is fixedly installed on the top cylinder of the configuration cylinder 1. The inner diameter of the flushing pipe 14 is greater than 3 cm. The flushing pipe 14 is used to connect to an external flushing pipe for flushing operations.

[0031] Furthermore, a delivery pump 16 is provided on one side of the configuration barrel 1, a suction tube 161 is fixedly installed on the liquid inlet end of the delivery pump 16, a medicine liquid tube 17 is fixedly installed on the liquid outlet end of the delivery pump 16, and a flow meter 171 is fixedly installed on the medicine liquid tube 17 to realize the addition operation of liquid medicine.

[0032] In addition, a stirring motor 2 is fixedly installed at the center position of the top surface of the configuration barrel 1, and a vertically arranged stirring shaft 20 is fixedly installed at the end of the output shaft of the stirring motor 2. A first stirring blade 21 is fixedly installed on the stirring shaft 20, and a material passing gap 211 is provided on the first stirring blade 21. A second stirring blade 22 is fixedly installed on the stirring shaft 20, and the second stirring blade 22 is located on one side of the material passing gap 211, so as to realize the stirring operation of the prepared raw materials and promote more complete mixing of the raw materials.

[0033] Finally, it should be noted that the components involved in the present invention, such as the screw feeder 31, electric heater 10, electronic scale 3, conveying pump 16 and flow meter 171, are all universal standard parts or components known to those skilled in the art. Their structures and principles are known to those skilled in the art through technical manuals or through conventional experimental methods. In the idle space of this device, all the above-mentioned electrical components, which refer to power elements, electrical components, and adapted controllers and power supplies, are connected through wires. The specific connection means should refer to the working principle of the present invention. The electrical connection between each electrical component is completed in a sequential working order, and the detailed connection means are all well-known technologies in the art.

[0034] When the catalyst configuration device with quantitative addition of the present invention is in use, the raw materials are put into the feed hopper 36, and the corresponding weight of the raw materials is weighed by the electronic scale 3. After the weighing is completed, the second discharge valve 181 is opened, and the screw feeder 31 is started at the same time. The screw feeder 31 is used to transport the raw materials to the configuration cylinder 1 for addition operation. In addition, the suction tube 161 is connected to the external liquid medicine delivery pipeline, and the delivery pump 16 is started to transport the liquid medicine. The amount of added liquid medicine is controlled according to the flow meter 171. After all the raw materials are added, the stirring motor 2 is started and made to work. When the stirring motor 2 works, the output shaft thereon rotates to drive the stirring shaft 20, the first stirring blade 21 and the second stirring blade 22 to rotate, so as to realize stirring and mixing operation. After the mixing is completed, the first discharge valve 13 is opened for unloading operation.

[0035] The above shows and describes the basic principles, main features, and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited to the above embodiments. The above embodiments and descriptions are merely preferred examples of the present invention and are not intended to limit the present invention. Various changes and improvements may be made to the present invention without departing from the spirit and scope of the present invention, and such changes and improvements fall within the scope of the present invention. The scope of protection claimed in the present invention is defined by the appended claims and their equivalents.

Claims

1. A catalyst preparation device for quantitative addition, comprising a preparation cylinder (1), characterized in that: A feeding cylinder (18) is fixedly mounted on the top of the configuration cylinder (1), a second discharge valve (181) is fixedly mounted on the feeding cylinder (18), a support plate (15) is fixedly mounted on the top cylinder of the configuration cylinder (1), an electronic scale (3) is fixedly mounted on the support plate (15), a support beam (30) is fixedly mounted on the scale platform of the electronic scale (3), a screw feeder (31) is fixedly mounted on the top of the support beam (30), and the outlet of the screw feeder (31) is fixedly mounted on the top cylinder of the configuration cylinder (1). A discharge pipe (32) is fixedly installed at the material end, and the discharge pipe (32) is located in the feed barrel (18) and is plugged into the feed barrel (18). A vertical pipe (33) arranged vertically is fixedly installed at the top end of the discharge pipe (32), and a fan (34) is fixedly installed on the inner wall of the vertical pipe (33). A feed pipe (35) is fixedly installed at the feed end of the screw feeder (31), and a feed hopper (36) is fixedly installed at the top end of the feed pipe (35).

2. The quantitative addition catalyst preparation device according to claim 1, characterized in that: The distance between the discharge pipe (32) and the inner wall of the feed barrel (18) is greater than 1 mm, and the fan (34) is arranged toward one side of the discharge pipe (32).

3. The quantitative addition catalyst preparation device according to claim 1, characterized in that: An electric heater (10) is fixedly mounted on the body of the configuration cylinder (1), and a conical cylinder (11) is fixedly mounted on the bottom of the configuration cylinder (1).

4. The quantitative addition catalyst preparation device according to claim 3, characterized in that: A discharge pipe (12) is fixedly mounted on the bottom end of the conical cylinder (11), and a first discharge valve (13) is fixedly mounted on the discharge pipe (12).

5. The quantitative addition catalyst preparation device according to claim 1, characterized in that: A flushing tube (14) is fixedly mounted on the top cylinder of the configuration cylinder (1), and the inner diameter of the flushing tube (14) is greater than 3 cm.

6. The quantitative addition catalyst preparation device according to claim 1, characterized in that: A delivery pump (16) is provided on one side of the configuration cylinder (1), a suction pipe (161) is fixedly mounted on the liquid inlet end of the delivery pump (16), a liquid medicine pipe (17) is fixedly mounted on the liquid outlet end of the delivery pump (16), and a flow meter (171) is fixedly mounted on the liquid medicine pipe (17).

7. The quantitative addition catalyst preparation device according to claim 1, characterized in that: A stirring motor (2) is fixedly mounted at the center of the top surface of the configuration cylinder (1), a stirring shaft (20) arranged vertically is fixedly mounted at the end of the output shaft of the stirring motor (2), and a first stirring blade (21) is fixedly mounted on the stirring shaft (20).

8. The quantitative addition catalyst preparation device according to claim 7, characterized in that: A material passing gap (211) is provided on the first stirring blade (21), and a second stirring blade (22) is fixedly mounted on the stirring shaft (20), wherein the second stirring blade (22) is located on one side of the material passing gap (211).