Self-cleaning type 2-ethyl anthraquinone reaction kettle
The design of a self-cleaning 2-ethylanthraquinone reactor solves the problems of single introduction method, low mixing uniformity and incomplete cleaning of traditional reactors. It realizes flexible introduction of raw materials, uniform mixing and automatic cleaning, and improves production efficiency and product quality.
Patent Information
- Application Number
- CN202422625771.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-10-30
- Publication Date
- 2025-09-23
- Estimated Expiration
- 2034-10-30
AI Technical Summary
In the production process of 2-ethylanthraquinone, traditional reactors have problems such as a single introduction method, low mixing uniformity and efficiency, and incomplete cleaning, which affect product quality and production efficiency.
A self-cleaning 2-ethylanthraquinone reactor was designed. It adopted multiple inlet pipes, stirring motors, stirring shafts and stirring rods, combined with a heating distribution ring and an inclined nozzle to achieve flexible introduction of raw materials, uniform mixing and self-cleaning functions.
It improves the mixing uniformity and mixing efficiency of raw materials, reduces the risk of raw material leakage, shortens the reaction time, realizes automatic cleaning, and improves production efficiency and product quality.
Smart Images

Figure CN223366914U_ABST
Abstract
Description
Technical Field
[0001] The utility model belongs to the technical field related to reactors, and particularly relates to a self-cleaning 2-ethylanthraquinone reactor. Background Art
[0002] Reactors play a crucial role in the production of 2-ethylanthraquinone. However, conventional reactors present several challenges. First, they lack a single method for introducing raw materials, preventing the number of inlet tubes used from being flexibly adjusted based on the type of raw materials being processed, and failing to effectively prevent leakage from unused inlet tubes.
[0003] Secondly, when it comes to mixing raw materials, traditional reactors often only stir in a single direction, resulting in low mixing uniformity and efficiency, which affects product quality and production efficiency. Furthermore, the raw materials are often not effectively preheated before entering the reactor, which means it takes a long time for the raw materials to reach the reaction temperature inside the reactor, reducing reaction efficiency.
[0004] Furthermore, traditional reactors require manual cleaning after use, which is not only time-consuming and labor-intensive, but can also result in incomplete cleaning, impacting subsequent production. To address these issues, improve 2-ethylanthraquinone production efficiency and product quality, and enable automated reactor cleaning, a new self-cleaning 2-ethylanthraquinone reactor is urgently needed. Utility Model Content
[0005] The purpose of the utility model is to provide a self-cleaning 2-ethylanthraquinone reactor to solve the problems of the traditional reactors proposed in the above background technology, such as the relatively simple introduction method, low mixing uniformity and mixing efficiency.
[0006] To achieve the above-mentioned purpose, the present invention provides the following technical solutions: a self-cleaning 2-ethylanthraquinone reactor, comprising a reactor body, a plurality of inlet pipes extending outward from the inner upper side of the cylindrical outer wall of the reactor body, and the plurality of inlet pipes are perpendicular to the central axis of the reactor body and are arranged in a centrally symmetrical manner, a stirring motor is provided at the center of the upper end of the reactor body, a stirring shaft is rotatably connected at the center of the lower end of the stirring motor, a plurality of stirring rods are fixedly connected to the cylindrical outer wall of the stirring shaft, an outlet pipe is connected to the outer side of the lower end of the reactor body, and a plurality of support legs are fixedly connected to the outer side of the lower end of the reactor body.
[0007] Preferably, a diverter baffle ring is fixedly connected to the lower side of the cylindrical inner wall of the kettle body, and the diverter baffle ring is located under the multiple stirring rods. The outer side of the upper end of the diverter baffle ring is connected to multiple diverter ducts with openings facing upward.
[0008] Preferably, the diversion duct is fixedly connected to the inner wall of the kettle body, a plurality of centrifugal blades are rotatably connected between the diversion baffle ring and the inner wall of the lower end of the kettle body, and the plurality of centrifugal blades are fixedly connected to the lower side of the outer wall of the stirring shaft cylinder.
[0009] Preferably, the inlet pipe is located on the cylindrical outer wall inside the kettle body and is connected to a plurality of inclined nozzles, and the plurality of inclined nozzles are arranged at a forty-five degree angle in the vertical downward direction. A heating distribution ring is arranged between the plurality of the inlet pipes, and the heating distribution ring is located outside the stirring shaft and inside the kettle body.
[0010] Preferably, the front and rear sides of the center of the upper end of the heating distribution ring are connected with electrical connectors, and the upper ends of the two electrical connectors respectively penetrate upward into the front and rear sides of the center of the upper end of the kettle body, and a plurality of heating support rods are connected to the cylindrical outer wall of the heating distribution ring.
[0011] Preferably, the plurality of heating support rods are perpendicular to the central axis of the kettle body and are centrally symmetrically arranged. The plurality of heating support rods respectively penetrate the interior of the plurality of inlet pipes and leave gaps between the heating support rods and the cylindrical inner walls of the inlet pipes.
[0012] Preferably, a blocking ring is provided inside the end of the inlet pipe away from the kettle body, a limiting ring is provided at the end of the blocking ring away from the kettle body, and a blocking spring is provided between the blocking ring and the limiting ring.
[0013] Preferably, the limiting ring is fixedly connected to the outer side of one end close to the kettle body with a plurality of connecting slide rods, and the plurality of connecting slide rods pass through the inside of the sealing ring and are slidably connected to the sealing ring, and the plurality of connecting slide rods are fixedly connected to the end away from the limiting ring with a blocking block, and the blocking block is located at the end of the sealing ring close to the kettle body, and a gap is left between the inner wall of the inlet pipe.
[0014] Compared with the prior art, the present invention provides a self-cleaning 2-ethylanthraquinone reactor with the following beneficial effects:
[0015] 1. Overall structural innovation: The reactor includes the reactor body, stirring motor, stirring shaft, stirring rod, inlet pipe, outlet pipe and support legs. These parts work together to achieve the production of 2-ethylanthraquinone and self-cleaning function.
[0016] 2. Innovative inlet pipe structure: A sealing ring, limit ring, sealing spring, connecting slide bar, and sealing block are installed inside the end of the inlet pipe away from the kettle body. When connecting the raw material pipeline to the inlet pipe, the number of inlet pipes connected is selected according to the type and quantity of raw materials. The raw materials will push the sealing block to form a guide gap for the raw materials to enter. Unused inlet pipes can be automatically blocked to prevent raw material leakage.
[0017] 3. Innovation in Stirring and Mixing: The stirring motor drives the stirring shaft and stirring rod to stir the mixed materials horizontally in the kettle. The kettle is equipped with a diversion baffle ring, diversion duct and centrifugal rotor. The stirring motor drives the centrifugal rotor to rotate, generating centrifugal force in the mixed materials, stirring them vertically inside the kettle, improving the mixing uniformity and mixing efficiency.
[0018] 4. Heating innovation: A heating distribution ring is set between multiple inlet tubes. The electrical connector on the heating distribution ring is connected to an external power supply. Multiple heating rods on the cylindrical outer wall of the heating distribution ring penetrate the interior of the inlet tube. The raw materials in the inlet tube can be heated to the reaction temperature by the heating rods, thereby improving the reaction efficiency.
[0019] 5. Innovation in raw material injection: The inlet pipe is located on the outer wall of the cylinder inside the kettle body and is connected to multiple inclined nozzles set at a 45-degree angle. When the raw materials are sprayed into the kettle body through the inclined nozzles, they can form spins. Multiple raw materials are injected at intervals to improve the mixing uniformity and mixing efficiency of the raw materials.
[0020] 6. Self-cleaning innovation: After the raw material reaction is completed, the cleaning liquid can be introduced through the inlet pipe, and the stirring motor is turned on for self-cleaning. The cleaning liquid will fully clean the inside of the reactor under the action of various components of the reactor, and finally the cleaning liquid will be discharged through the outlet pipe. BRIEF DESCRIPTION OF THE DRAWINGS
[0021] Figure 1 This is a schematic diagram of the three-dimensional structure of the 2-ethylanthraquinone reactor of the present invention.
[0022] Figure 2 It is a schematic diagram of the three-dimensional cross-sectional structure of the 2-ethylanthraquinone reactor of the present utility model.
[0023] Figure 3 This is a schematic diagram of the diverter baffle ring connection structure of the utility model.
[0024] Figure 4 This is a schematic diagram of the centrifugal blade connection structure of the present utility model.
[0025] Figure 5 This is a schematic diagram of the heating distribution ring connection structure of the present utility model.
[0026] Figure 6 For the utility model Figure 5 Enlarged schematic diagram of point A in the middle.
[0027] In the figure: 1. Kettle body; 2. Inlet pipe; 3. Stirring motor; 4. Stirring shaft; 5. Stirring rod; 6. Outlet pipe; 7. Support leg; 8. Diverter ring; 9. Diverter guide tube; 10. Centrifugal impeller; 11. Oblique nozzle; 12. Heating distribution ring; 13. Electrical connection head; 14. Heating support rod; 15. Sealing ring; 16. Limiting ring; 17. Sealing spring; 18. Connecting slide rod; 19. Sealing block. DETAILED DESCRIPTION
[0028] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the embodiments described are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative efforts are within the scope of protection of the present invention.
[0029] The utility model provides Figures 1-6 The self-cleaning 2-ethylanthraquinone reactor shown in the figure comprises a reactor body 1, a plurality of inlet pipes 2 are penetrated outward from the inner side of the cylindrical outer wall of the reactor body 1, and the plurality of inlet pipes 2 are perpendicular to the central axis of the reactor body 1 and are arranged symmetrically with respect to the center. A stirring motor 3 is provided at the center of the upper end of the reactor body 1, a stirring shaft 4 is rotatably connected to the center of the lower end of the stirring motor 3, a plurality of stirring rods 5 are fixedly connected to the cylindrical outer wall of the stirring shaft 4, an outlet pipe 6 is connected to the outer side of the lower end of the reactor body 1, and a plurality of support legs 7 are fixedly connected to the outer side of the lower end of the reactor body 1 for supporting the bottom of the reactor body 1. During the production process of 2-ethylanthraquinone, a stirring motor 3 is provided at the center of the upper end of the reactor body 1, a stirring shaft 4 is rotatably connected to the lower end of the stirring motor 3, a plurality of stirring rods 5 are fixedly connected to the cylindrical outer wall of the stirring shaft 4, a plurality of stirring rods 5 are fixedly connected to the outer side of the lower end of the reactor body 1, and a plurality of support legs 7 are fixedly connected to the outer side of the lower end of the reactor body 1 for supporting the bottom of the reactor body 1. Multiple inlet pipes 2 introduce the production raw materials into the kettle body 1 for mixing, and the stirring motor 3 is turned on. The stirring motor 3 drives the multiple stirring rods 5 to rotate inside the kettle body 1 through the stirring shaft 4, and the multiple stirring rods 5 stir the mixed raw materials, so that the mixed raw materials are stirred horizontally inside the kettle body 1. After the raw material reaction is completed, the crude stock solution of 2-ethylanthraquinone is discharged through the outlet pipe 6 for the next purification step, and then the cleaning liquid is introduced into the kettle body 1 through the multiple inlet pipes 2, and the stirring motor 3 is turned on to allow the reactor to self-clean, and the cleaning liquid can be introduced into the kettle body 1 through the outlet pipe 6.
[0030] Preferably, a sealing ring 15 is provided inside the end of the inlet pipe 2 away from the kettle body 1, and a limiting ring 16 is provided at the end of the sealing ring 15 away from the kettle body 1. A sealing spring 17 is provided between the sealing ring 15 and the limiting ring 16, and a plurality of connecting slides 18 are fixedly connected to the outside of the limiting ring 16 near the end of the kettle body 1, and a plurality of connecting slides 18 pass through the sealing ring 15 and are slidably connected to the sealing ring 15. A plurality of connecting slides 18 are fixedly connected to a sealing block 19 at one end away from the limiting ring 16, and the sealing block 19 is located at the end of the sealing ring 15 near the kettle body 1, and a gap is left between the inner wall of the inlet pipe 2. In the process of introducing raw materials into the inlet pipe 2, the raw material pipeline is connected to the inlet pipe 2 through a thread, and the number of connecting inlet pipes 2 can be selected according to the type of raw materials. The introduction of raw materials into the inlet pipe 2 will have a certain The sealing block 19 forms an extrusion pressure and pushes the sealing block 19 toward the side close to the kettle body 1, so that a guide gap is formed between the sealing block 19 and the sealing ring 15, thereby connecting the raw material pipeline with the interior of the inlet pipe 2, and the raw material is introduced into the sealing ring 15 through the interior of the limit ring 16 and between multiple connecting slides 18, and is introduced into the interior of the inlet pipe 2 through the guide gap between the sealing ring 15 and the sealing block 19, thereby introducing the raw material into the inlet pipe 2, and the interior of the unused inlet pipe 2 away from the kettle body 1 can be blocked by the sealing block 19, the sealing block 19 is connected to the limit ring 16 through multiple connecting slides 18, and slides toward the side away from the kettle body 1 through the limit ring 16 and the sealing spring 17, so that the sealing block 19 fits with the sealing ring 15, thereby sealing the interior of the end of the inlet pipe 2 away from the kettle body 1.
[0031] Preferably, the inlet pipe 2 is located on the cylindrical outer wall inside the kettle body 1 and is connected to a plurality of inclined nozzles 11, and the plurality of inclined nozzles 11 are arranged at a forty-five degree angle in the vertical downward direction. A heating distribution ring 12 is provided between the plurality of inlet pipes 2, and the heating distribution ring 12 is located outside the stirring shaft 4 and inside the kettle body 1. The front and rear sides of the center of the upper end of the heating distribution ring 12 are connected to electric heads 13, and the upper ends of the two electric heads 13 respectively penetrate upwardly through the front and rear sides of the center of the upper end of the kettle body 1. A plurality of heating support rods 14 are connected to the cylindrical outer wall of the heating distribution ring 12, and the plurality of heating support rods 14 are perpendicular to the central axis of the kettle body 1 and are centrally The kettle body 1 is symmetrically arranged with a plurality of heating support rods 14 respectively passing through the interior of the plurality of inlet pipes 2, and a gap is left between the heating support rods 14 and the cylindrical inner wall of the inlet pipe 2. In the process of spraying the raw materials into the interior of the kettle body 1, the raw materials transported to the interior of the inlet pipe 2 can be sprayed into the interior of the kettle body 1 through the plurality of inclined nozzles 11. Since the inclined nozzles 11 are all set at a forty-five degree angle in the vertical downward direction, and the plurality of inlet pipes 2 are perpendicular to the central axis of the kettle body 1 and are symmetrically arranged with a center, the raw materials sprayed into the interior of the kettle body 1 can form a spin under the spraying of the inclined nozzles 11, and the injection of multiple raw materials at intervals can not only improve the mixing uniformity of the raw materials, but also improve the mixing efficiency of the raw materials.
[0032] Preferably, when the raw materials are introduced into the inlet pipe 2, they can be heated by the heating support rod 14 inside the inlet pipe 2, so that the raw materials are heated to the reaction temperature before being sprayed into the kettle body 1, so that the raw materials can react quickly after being sprayed into the kettle body 1, thereby improving the reaction efficiency and further improving the production efficiency.
[0033] Preferably, a diverter baffle 8 is fixedly connected to the lower side of the cylindrical inner wall of the kettle body 1, and the diverter baffle 8 is located at the lower side of the multiple stirring rods 5. The outer side of the upper end of the diverter baffle 8 is connected to multiple diverter ducts 9 with openings upward. The diverter ducts 9 are fixedly connected to the inner wall of the kettle body 1. A plurality of centrifugal blades 10 are rotatably connected between the diverter baffle 8 and the inner wall of the lower end of the kettle body 1, and the plurality of centrifugal blades 10 are fixedly connected to the lower side of the cylindrical outer wall of the stirring shaft 4. In the process of stirring the mixed raw materials, the stirring motor 3 can drive the plurality of centrifugal blades 10 through the stirring shaft 4. The diverter baffle ring 8 rotates with the inner wall of the lower end of the kettle body 1, so that the mixed raw materials between the diverter baffle ring 8 and the inner wall of the lower end of the kettle body 1 can generate centrifugal force through the rotation of multiple centrifugal blades 10, and are thrown into the interior of multiple diverter ducts 9 through centrifugal force, and then discharged through the opening at the upper end of the diverter duct 9. At the same time, the mixed raw materials at the upper end of the diverter baffle ring 8 are sucked into the space between the diverter baffle ring 8 and the inner wall of the lower end of the kettle body 1 from the opening at the center of the diverter baffle ring 8, so that the mixed raw materials are stirred vertically inside the kettle body 1, thereby improving the mixing uniformity and mixing efficiency of the raw materials.
[0034] Finally, it should be noted that the above is only a preferred embodiment of the present invention and is not intended to limit the present invention. Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art can still modify the technical solutions described in the aforementioned embodiments or make equivalent replacements for some of the technical features therein. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present invention should be included in the scope of protection of the present invention.
Claims
1. A self-cleaning 2-ethylanthraquinone reactor, characterized in that: The invention comprises a kettle body (1), wherein a plurality of inlet pipes (2) are penetrated outward from the inner side of the cylindrical outer wall of the kettle body (1), and the plurality of inlet pipes (2) are perpendicular to the central axis of the kettle body (1) and are centrally symmetrically arranged. A stirring motor (3) is arranged at the center of the upper end of the kettle body (1), and a stirring shaft (4) is rotatably connected to the center of the lower end of the stirring motor (3). A plurality of stirring rods (5) are fixedly connected to the cylindrical outer wall of the stirring shaft (4). An outlet pipe (6) is connected to the outer side of the lower end of the kettle body (1), and a plurality of supporting legs (7) are fixedly connected to the outer side of the lower end of the kettle body (1).
2. A self-cleaning 2-ethylanthraquinone reactor according to claim 1, characterized in that: A diversion baffle ring (8) is fixedly connected to the lower side of the cylindrical inner wall of the kettle body (1), and the diversion baffle ring (8) is located on the lower side of the multiple stirring rods (5). The outer side of the upper end of the diversion baffle ring (8) is connected to multiple diversion conduits (9) with openings upward.
3. A self-cleaning 2-ethylanthraquinone reactor according to claim 2, characterized in that: The diversion conduit (9) is fixedly connected to the inner wall of the kettle body (1), and a plurality of centrifugal blades (10) are rotatably connected between the diversion baffle ring (8) and the inner wall of the lower end of the kettle body (1), and the plurality of centrifugal blades (10) are fixedly connected to the lower side of the cylindrical outer wall of the stirring shaft (4).
4. The self-cleaning 2-ethylanthraquinone reactor according to claim 1, characterized in that: The inlet pipe (2) is located on the outer wall of the cylinder inside the kettle body (1) and is connected to a plurality of inclined nozzles (11), and the plurality of inclined nozzles (11) are arranged at a 45-degree angle in the vertical downward direction. A heating distribution ring (12) is arranged between the plurality of inlet pipes (2), and the heating distribution ring (12) is located outside the stirring shaft (4) and inside the kettle body (1).
5. The self-cleaning 2-ethylanthraquinone reactor according to claim 4, characterized in that: The front and rear sides of the center of the upper end of the heating distribution ring (12) are both connected to electrical connectors (13), and the upper ends of the two electrical connectors (13) respectively penetrate upwards into the front and rear sides of the center of the upper end of the kettle body (1), and a plurality of heating support rods (14) are connected to the cylindrical outer wall of the heating distribution ring (12).
6. The self-cleaning 2-ethylanthraquinone reactor according to claim 5, characterized in that: The plurality of heating support rods (14) are perpendicular to the central axis of the kettle body (1) and are centrally symmetrically arranged. The plurality of heating support rods (14) respectively penetrate the interior of the plurality of inlet pipes (2) and leave gaps between the heating support rods (14) and the cylindrical inner walls of the inlet pipes (2).
7. The self-cleaning 2-ethylanthraquinone reactor according to claim 6, characterized in that: A blocking ring (15) is provided inside the end of the inlet pipe (2) away from the kettle body (1), a limiting ring (16) is provided at the end of the blocking ring (15) away from the kettle body (1), and a blocking spring (17) is provided between the blocking ring (15) and the limiting ring (16).
8. The self-cleaning 2-ethylanthraquinone reactor according to claim 7, characterized in that: The outer side of the limit ring (16) close to the kettle body (1) is fixedly connected with a plurality of connecting slides (18), and the plurality of connecting slides (18) pass through the inside of the blocking ring (15) and are slidably connected to the blocking ring (15). The ends of the plurality of connecting slides (18) away from the limit ring (16) are fixedly connected with a blocking block (19), and the blocking block (19) is located at the end of the blocking ring (15) close to the kettle body (1) and has a gap between it and the inner wall of the inlet pipe (2).