Phthalocyanine compound synthesizer

By designing the stirring and deodorizing components of the phthalocyanine compound synthesis device, the problem of low synthesis efficiency of phthalocyanine pigments was solved, and small-batch experiments of compounds and cost reduction were achieved, while odor treatment was convenient.

CN223381598UActive Publication Date: 2025-09-26ZIBO FUYAN CHEM IND GROUP
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Patent Information

Application Number
CN202422532812.2
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-10-21
Publication Date
2025-09-26
Estimated Expiration
2034-10-21

AI Technical Summary

Technical Problem

The existing phthalocyanine pigment synthesis discharging and mixing system is not convenient for conducting synthesis and decomposition experiments on the compound first, resulting in low phthalocyanine pigment synthesis efficiency and high cost.

Method used

A phthalocyanine compound synthesis device was designed, including a base, an electric furnace, a synthesis container, a stirring assembly, and a deodorization assembly. By stirring with a stirring rod and absorbing ammonia odor with an exhaust fan, compound decomposition experiments and odor treatment can be carried out to improve synthesis efficiency.

Benefits of technology

It is convenient for small batch compound experiments, reduces costs, improves the synthesis efficiency of phthalocyanine pigment compounds, avoids odor affecting operations, and has an easy-to-use structure.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model relates to the technical field of phthalocyanine compounds, in particular to a phthalocyanine compound synthesizing device which comprises a base, an electric furnace, a synthesizing container, a stirring component and a deodorizing component, the electric furnace is mounted on the base; the synthesis container is mounted on the electric furnace; the stirring assembly comprises a stirring rod arranged in the synthesis container, the stirring rod is rotationally connected to the exterior of the upper end of the supporting frame and rotationally connected with a driving device b, and the stirring end stirs the phthalocyanine pigment compound in the synthesis container; the odor removal assembly comprises an air inlet end mounting cover arranged on the synthesis container and a pipe body arranged on the mounting cover, the pipe body is provided with an exhaust fan, an air outlet end of the exhaust fan is provided with a connecting pipe, the connecting pipe is provided with a box body, and ammonia odor generated by synthesis of phthalocyanine pigment compounds is absorbed by turning on the exhaust fan and the mounting cover; and finally, the ammoniacal odor is stored in the box body for treatment by using the pipe body and the connecting pipe. According to the utility model, the synthesis efficiency of phthalocyanine pigment compounds is improved, and the use of the phthalocyanine compound synthesis device is improved.
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Description

Technical Field

[0001] The utility model relates to the technical field of phthalocyanine compounds, in particular to a phthalocyanine compound synthesis device. Background Art

[0002] Phthalocyanine compounds can be produced by two methods: solid-phase and solvent-based methods. Phthalocyanine is also widely used in pigments, with phthalocyanine blue and phthalocyanine green being the primary two types. Phthalocyanine blue, with its excellent heat and weather fastness and vibrant color, is widely used in inks, coatings, plastics, rubber, leather, and stationery. In recent years, it has also played a special role in catalysis, semiconductors, electronic photography, and light energy conversion.

[0003] Chinese patent announcement number CN218530702U discloses a phthalocyanine pigment synthesis and discharging mixing system, including a synthesis device, a solvent storage tank, and a discharging mixer. The utility model adds a material premixer before the phthalocyanine pigment slurry and the solvent enter the discharging mixer. The shape of the material premixer is one of a truncated cone, a trapezoidal cone, and a cone with a central axis parallel to the horizontal direction, and the positions of the pigment slurry inlet and the solvent inlet are optimized to ensure that the pigment mixed slurry and the solvent are mixed evenly, ensuring that other components in the slurry except the phthalocyanine pigment molecules are fully dissolved in the solvent, so that the phthalocyanine pigment particles can be fully precipitated, and it can ensure to the greatest extent that all phthalocyanine pigment slurries are in contact with fresh solvent, minimize or avoid the influence of the pigment particles precipitated first on the pigment particles precipitated later, and prevent the occurrence of particle agglomeration.

[0004] Before phthalocyanine pigments are synthesized and then synthesized in large quantities for production, a small portion of the phthalocyanine pigment synthesis compound is first taken for experimentation. This operation is used to achieve the highest synthesis efficiency and minimize costs. However, the existing phthalocyanine pigment synthesis and discharging mixing system is not convenient for conducting synthesis and decomposition experiments on the compound first, resulting in reduced synthesis efficiency and increased synthesis costs. Utility Model Content

[0005] In view of the problems existing in the background technology, a phthalocyanine compound synthesis device is proposed.

[0006] The utility model provides a phthalocyanine compound synthesis device, comprising:

[0007] base;

[0008] Electric furnace, mounted on a base;

[0009] Synthesis container, installed on the electric furnace;

[0010] A stirring assembly includes a stirring rod disposed inside the synthesis container, the stirring rod being rotatably connected to the outside of the upper end of the support frame and rotatably connected to the driving device b, and the stirring end stirring the phthalocyanine pigment compound in the synthesis container;

[0011] And a deodorizing component, including an air inlet end mounting cover arranged on a synthesis container and a pipe body provided on the mounting cover, an exhaust fan provided on the pipe body, a connecting pipe provided on the air outlet end of the exhaust fan, and a box body provided on the connecting pipe. By turning on the exhaust fan, the mounting cover absorbs the ammonia odor generated by the synthesis of the phthalocyanine pigment compound, and finally the pipe body and the connecting pipe are used to store the ammonia odor in the box for treatment.

[0012] Preferably, an opening is provided at the upper end of the synthesis container, and a cover is provided at the opening, and the phthalocyanine pigment compound is added into the synthesis container for synthesis by opening the cover.

[0013] Preferably, the stirring assembly further comprises a lifting device a, a driving device a, a support frame, and a driving device b;

[0014] The lower end of the lifting device a is installed on the base, and the telescopic end of the lifting device a is provided with a driving device a; the driving end of the driving device a is provided with a support frame, and one end of the support frame is provided with a driving device b;

[0015] The support frame is adjusted in height by the lifting device a, and the angle is adjusted by the driving device a and the stirring rod is taken out of the synthesis container.

[0016] Preferably, the deodorizing assembly further comprises a base and a lifting device b;

[0017] The base is installed under the exhaust fan and is used to support the exhaust fan; the lifting base is installed on the telescopic end of the lifting device b and is used to adjust the position of the exhaust fan;

[0018] The base is provided with a connecting piece and a clamping piece.

[0019] Preferably, the connecting member includes a connecting plate at one end of the mounting base, the connecting plate is hollow and provided with a telescopic plate;

[0020] The connecting plate and the telescopic plate are connected using bolts and clamps.

[0021] Preferably, the clamping member includes two sets of mounting blocks and a clamping sleeve.

[0022] The two sets of mounting blocks are connected by bolts and support the mounting cover from above;

[0023] The two sets of mounting blocks and the connecting plate are connected by bolts, and the size of the clamping sleeve is adjusted by the bolts so that the sleeve can be installed on the periphery of the synthesis container, and the bolts can detach the connecting piece and the clamping piece.

[0024] Compared with the prior art, the present invention has the following beneficial technical effects:

[0025] The utility model adds the phthalocyanine pigment compound into the synthesis container according to the required number of particles. By adding the phthalocyanine pigment compound into the synthesis container, it is convenient to take a small portion of the phthalocyanine pigment synthesis compound for experimentation, thereby conveniently reducing the phthalocyanine pigment synthesis cost to a minimum and conveniently improving the synthesis efficiency of the phthalocyanine pigment compound.

[0026] The utility model opens the exhaust fan, which is connected to the installation cover through a pipe body. When the phthalocyanine pigment compound is heated and dissolved, the phthalocyanine pigment compound will generate an ammonia smell during the dissolution process. The installation cover absorbs the ammonia smell, effectively preventing the smell from affecting the operation of the phthalocyanine pigment compound.

[0027] The utility model uses a lifting device a and a driving device b, and the driving device b is connected to a stirring rod, so that the stirring rod is convenient for dissolving and stirring the phthalocyanine pigment compound, facilitates automatic stirring, and improves the efficiency of synthesizing the phthalocyanine pigment compound. At the same time, by adjusting the position, the structures of the phthalocyanine compound synthesis device are convenient for coordinated use. BRIEF DESCRIPTION OF THE DRAWINGS

[0028] Figure 1 It is a schematic diagram of the overall structure of the utility model;

[0029] Figure 2 This is a schematic diagram of the structure of the stirring assembly in the present utility model;

[0030] Figure 3 This is a schematic diagram of the installation cover structure in the utility model;

[0031] Figure 4 This is a schematic diagram of the base structure in the utility model.

[0032] Figure numerals: 1. base; 2. electric furnace; 3. synthesis container; 301. cover; 4. stirring assembly; 401. lifting device a; 402. driving device a; 403. support frame; 404. driving device b; 405. stirring rod; 5. mounting cover; 501. pipe body; 502. exhaust fan; 503. connecting pipe; 504. box body; 505. base; 506. lifting device b; 507. connecting plate; 508. telescopic plate; 509. mounting block; 510. clamping sleeve. DETAILED DESCRIPTION

[0033] The following describes the specific embodiments of the present disclosure in detail with reference to the accompanying drawings. It should be understood that the specific embodiments described herein are only used to illustrate and explain the present disclosure and are not intended to limit the present disclosure.

[0034] Example 1

[0035] like Figure 1-Figure 4As shown, the present invention provides a phthalocyanine compound synthesis device, comprising: a base 1, an electric furnace 2, a synthesis container 3, a stirring component 4 and a deodorizing component;

[0036] The electric furnace 2 is installed on the base 1; the synthesis container 3 is installed on the electric furnace 2; the stirring component 4 includes a stirring rod 405 arranged inside the synthesis container 3, the stirring rod 405 is rotatably connected to the outside of the upper end of the support frame 403 and is rotatably connected to the driving device b404, and the stirring end stirs the phthalocyanine pigment compound in the synthesis container 3; and the deodorization component includes an air inlet end mounting cover 5 arranged on the synthesis container 3 and the mounting cover 5 is provided with a tube body 501, the tube body 501 is provided with an exhaust fan 502, the exhaust fan 502 is provided with a connecting pipe 503 at the air outlet end, and the connecting pipe 503 is provided with a box body 504. By turning on the exhaust fan 502, the mounting cover 5 absorbs the ammonia smell generated by the synthesis of the phthalocyanine pigment compound, and finally uses the tube body 501 and the connecting pipe 503 to store the ammonia smell in the box body 504 for treatment. By movably connecting the synthesis container 3 to the electric furnace 2 and starting the electric furnace 2, the synthesis container 3 is heated to dissolve the phthalocyanine pigment compound in the synthesis container 3, and the compound raw materials used for the phthalocyanine pigment are added thereto according to the requirements and proportions, so as to conduct a small-scale experiment first and then carry out batch synthesis. At the same time, the stirring rod 405 is driven and connected by the driving device b404, and then the driving device b404 and the driving device b are selected from but not limited to rotating motors, and the driving device b404 and the lifting device a401 are selected from but not limited to cylinders. The driving device b404 is started to rotate the stirring rod 405, and the stirring rod 405 rotates to stir and dissolve the phthalocyanine pigment compound. At the same time, an exhaust fan 502 is provided, and the exhaust fan 502 is connected to the installation cover 5 through the pipe body 501. During the synthesis of the phthalocyanine pigment compound, the exhaust fan 502 is used to absorb and process the ammonia smell generated, so as to improve the working and use of the phthalocyanine compound synthesis device.

[0037] Further explanation: The deodorization assembly also includes a base 505 and a lifting mechanism b506. The base 505 is installed below the exhaust fan 502 and serves to support it. The lifting mechanism b506 is mounted on the telescopic end of the lifting mechanism b506 to adjust the position of the exhaust fan 502. The base 505 is equipped with connectors and clamps. The base 505 supports the exhaust fan 502 through the lifting mechanism b506. The exhaust fan 502's outlet is connected to the housing 504, absorbing the ammonia odor into the housing 504. Furthermore, a treatment pipe interface is provided on the housing 504 to facilitate the subsequent treatment of the absorbed ammonia.

[0038] Further explaining, the connector includes a hollow connecting plate 507 at one end of the mounting base 505 and is provided with a telescopic plate 508. The connecting plate 507 and the telescopic plate 508 are connected using bolts and clamps. The connecting plate 507 and the telescopic plate 508 cooperate, forming an "L" shape. The connecting plate 507 is larger than the telescopic plate 508, allowing the telescopic plate 508 to move into the connecting plate 507, facilitating installation and support with the clamps.

[0039] Further explanation: The clamping member includes two sets of mounting blocks 509 and a clamping sleeve 510. The two sets of mounting blocks 509 are mounted on the connecting plate 507, and the clamping sleeve 510 is mounted on the two sets of mounting blocks 509. The two sets of mounting blocks 509 are connected by bolts and support the mounting cover 5 from above. The two sets of mounting blocks 509 and the connecting plate 507 are bolted together, and the clamping sleeve 510 is adjusted in size by the bolts so that it can be installed outside the synthesis container 3. The bolts can be detachably connected to the clamping member. Bolts are used to penetrate the connecting plate 507, the expansion plate 508, and the inner side of the mounting blocks 509 to connect them. The bolts are installed to facilitate the removal of the clamping member. At the same time, bolts are passed through the mounting blocks 509 to connect the mounting blocks 509 with the clamping sleeve 510 to the outside of the synthesis container 3. When the clamping sleeve 510 is removed or clamped, the bolts penetrate the mounting blocks 509 to control the connection range of the mounting blocks 509 and adjust the distance between the clamping sleeve 510.

[0040] Example 2

[0041] like Figure 1 and Figure 2 As shown, the present invention proposes a phthalocyanine compound synthesis device. Based on the above embodiment, this embodiment also records in detail the specific components and the coordination method.

[0042] To further illustrate, the synthesis container 3 has an open top with a lid 301. The lid 301 is opened to allow the phthalocyanine pigment compound to be added to the synthesis container 3 for synthesis. When the phthalocyanine pigment compound dissolves and decomposes within the synthesis container 3, the lid 301 is sealed and connected to the synthesis container 3, allowing the phthalocyanine pigment compound to be synthesized and used.

[0043] Further explanation, the stirring assembly 4 also includes a lifting device a401, a driving device a402, a support frame 403, and a driving device b404; the lower end of the lifting device a401 is installed on the base 1, and the telescopic end of the lifting device a401 is provided with a driving device a402; the driving end of the driving device a402 is provided with a support frame 403, and one end of the support frame 403 is provided with a driving device b404; the support frame 403 is adjusted in height by the lifting device a401, and the angle is adjusted by rotating the driving device a402 and the stirring rod 405 is taken out of the synthesis container 3. When the phthalocyanine pigment compound is added into the synthesis container 3, the stirring rod 405 is in a stopped state and is installed at one end of the outer side of the synthesis container 3, and then the electric furnace 2 is started to heat the synthesis container 3 so that the phthalocyanine pigment compound is heated and dissolved. After dissolving for a certain period of time, the lifting device a401 is started, and the lifting device a401 drives the driving device a402 and the support frame 403, as well as the driving device b404 and the stirring rod 405 to adjust the height, and then the lifting device a401 is closed and stopped working, and the driving device a402 is opened to drive the support frame 403 and the driving device b404, and the stirring rod 405 to rotate onto the synthesis container 3, and then the lifting device a401 is started again to move the stirring rod 405 into the synthesis container 3, and the driving device b404 is started to drive the stirring rod 405 to rotate, and the stirring rod 405 stirs the phthalocyanine pigment compound, and then after stirring.

[0044] The working principle of the present invention is as follows: during the processing and synthesis of phthalocyanine pigment compounds, the height of the base 505 is adjusted by starting the lifting device b506. The base 505 carries the exhaust fan 502. The exhaust fan 502 is connected to the pipe body 501 and the mounting cover 5. The mounting cover 5 is movably connected to the mounting block 509 to achieve the height adjustment of the mounting cover 5 according to the height of the synthesis container 3. After the mounting cover 5 is adjusted to one side of the synthesis container 3, the exhaust fan 502 is started. The exhaust fan 502 absorbs the ammonia smell into the pipe body 501 through the mounting cover 5, and then the exhaust fan 502 is connected to the connecting pipe 503 so that the ammonia smell is transported to the connecting pipe 503 through the air outlet of the exhaust fan 502. The connecting pipe 503 is connected to the box body 504 to absorb the ammonia smell into the box body 504. Then the staff can deal with the ammonia smell in the box body 504.

[0045] The embodiments of the present invention are described in detail above with reference to the accompanying drawings, but the present invention is not limited thereto. Various changes can be made within the knowledge scope of those skilled in the art without departing from the purpose of the present invention.

Claims

1. A phthalocyanine compound synthesis device, characterized in that: include: Base (1); An electric furnace (2) is mounted on the base (1); A synthesis container (3) is installed on the electric furnace (2); A stirring assembly (4) includes a stirring rod (405) disposed inside the synthesis container (3), the stirring rod (405) being rotatably connected to the outside of the upper end of the support frame (403) and rotatably connected to the driving device b (404), and the stirring end stirring the phthalocyanine pigment compound in the synthesis container (3); The invention also provides a deodorizing component, comprising an air inlet end mounting cover (5) arranged on a synthesis container (3), a pipe body (501) provided on the mounting cover (5), an exhaust fan (502) provided on the pipe body (501), a connecting pipe (503) provided on the air outlet end of the exhaust fan (502), and a box body (504) provided on the connecting pipe (503). By turning on the exhaust fan (502), the mounting cover (5) absorbs the ammonia odor generated by the synthesis of the phthalocyanine pigment compound, and finally the ammonia odor is stored in the box body (504) for treatment using the pipe body (501) and the connecting pipe (503).

2. A phthalocyanine compound synthesis device according to claim 1, characterized in that: The upper end of the synthesis container (3) is provided with an opening, and the opening is provided with a cover (301). The phthalocyanine pigment compound is added into the synthesis container (3) for synthesis by opening the cover (301).

3. The phthalocyanine compound synthesis device according to claim 1, characterized in that: The stirring assembly (4) further comprises a lifting device a (401), a driving device a (402), a support frame (403), and a driving device b (404); The lower end of the lifting device a (401) is mounted on the base (1), and the telescopic end of the lifting device a (401) is provided with a driving device a (402); the driving end of the driving device a (402) is provided with a support frame (403), and one end of the support frame (403) is provided with a driving device b (404); The support frame (403) is adjusted in height by the lifting device a (401), and the angle is adjusted by the driving device a (402) and the stirring rod (405) is taken out from the synthesis container (3).

4. A phthalocyanine compound synthesis device according to claim 1, characterized in that: The deodorizing assembly further includes a base (505) and a lifting device b (506); The base (505) is installed below the exhaust fan (502) and is used to support the exhaust fan (502); the base (505) is set on the telescopic end of the lifting device b (506) and is used to adjust the position of the exhaust fan (502); The base (505) is provided with a connecting piece and a clamping piece.

5. A phthalocyanine compound synthesis device according to claim 4, characterized in that: The connecting member includes a connecting plate (507) at one end of the mounting base (505), the connecting plate (507) is hollow and is provided with a telescopic plate (508); The connecting plate (507) and the telescopic plate (508) are connected using bolts and clamps.

6. The phthalocyanine compound synthesis device according to claim 5, characterized in that: The clamping member includes two sets of mounting blocks (509) and a clamping sleeve (510). Two groups of mounting blocks (509) are mounted on the connecting plate (507), and the clamping sleeve (510) is mounted on the two groups of mounting blocks (509); and the two groups of mounting blocks (509) are connected by bolts and support the mounting cover (5) from above; The two sets of mounting blocks (509) and the connecting plate (507) are connected by bolts, and the size of the clamping sleeve (510) is adjusted by the bolts so that it can be installed on the periphery of the synthesis container (3). The bolts can detach the connecting piece and the clamping piece.

Citation Information

Patent Citations

  • Phthalocyanine pigment synthesis discharging mixing system

    CN218530702U