Quicksand type potassium perchlorate production device

Abstract

The utility model discloses a quicksand type potassium perchlorate production device which comprises a centrifugal machine, a centrifugal head tank, a material mixing device, a material screening device and a soaking tank, the material mixing device comprises a charging barrel, a stirring mechanism, a sealing cover plate mechanism and a discharging port, the stirring mechanism is connected with the charging barrel, the sealing cover plate mechanism is installed on a feeding port of the charging barrel in a sealing mode, and the material screening device is installed on the discharging port of the charging barrel. The discharge port is formed in the bottom of the charging barrel; the stirring mechanism is used for mixing a plurality of materials in the charging barrel; the material screening device comprises a material screening groove, a discharging bin, a filter screen and a vibration motor, the material screening groove is formed in the bottom of the material barrel, the discharging port is communicated with the material screening groove, the discharging bin is installed at an opening in the lower portion of the material screening groove, the filter screen is installed in the material screening groove, the discharging port is higher than the filter screen, and the vibration motor is installed on the material screening groove; the potassium perchlorate production device aims at solving the problem that in the prior art, when a potassium perchlorate production device is used for producing potassium perchlorate, potassium perchlorate is caked.

Description

Technical Field

[0001] The utility model relates to the technical field of producing potassium perchlorate, in particular to a quicksand type potassium perchlorate production device. Background Art

[0002] Quicksand potassium perchlorate is an improved potassium perchlorate product with optimized particle size and flowability to meet the stringent requirements of modern industrial and military applications. Traditional potassium perchlorate production often faces problems with particle aggregation and poor flowability, which not only affects processing efficiency but also increases safety risks during use. To address these issues, the production technology for quicksand potassium perchlorate utilizes high-precision particle control and special surface treatment methods, resulting in more uniform particle size and a smoother surface, significantly improving the product's flowability and stability. This improvement makes quicksand potassium perchlorate safer and more reliable for use in rocket propellants, pyrotechnics, and explosives, while also reducing production and storage costs.

[0003] The utility model patent with application number CN202222777382.1 and publication number CN218210629U (hereinafter referred to as "Prior Art 1") discloses a crystalline potassium perchlorate production system, which relates to the field of potassium perchlorate production equipment. The utility model comprises a hot air mixing section, a cyclone separation section, a vibrating screen separation section, and a packaging section. The hot air discharge end of the hot air mixing section is connected to the cyclone separation section, and the top air discharge end of the cyclone separation section is connected to a bag dust collector. The bottom discharge end of the cyclone separation section is connected to the vibrating screen separation section, the lower discharge end of the vibrating screen separation section is connected to the packaging section, the upper discharge end of the vibrating screen separation section is connected to the feed end of a mill, and the discharge end of the mill is connected to the packaging section.

[0004] The specification of prior art 1 discloses a kind of crystalline potassium perchlorate production system, during use, allow semi-finished product potassium perchlorate material to enter hot air mixing section, after being subjected to hot air drying, material both enters cyclonic separation section along with hot air, thereby on the one hand, the material that allows to enter cyclonic separation section is blown in by hot air, thereby increases the contact time of material and hot air, improves drying efficiency. However, in actual application, potassium perchlorate cannot be prevented from caking when being stored by drying and heating, and potassium perchlorate all has the characteristic of easy caking during storage. Potassium perchlorate caking is due to the combined effect of particle self-factors and external factors, makes dissolving and recrystallization occur on particle surface, thereby forms crystal bridge on the mutual contact point between crystal grains, makes crystal grains stick together, loses fluidity, and gradually forms hard block. Potassium perchlorate caking has seriously affected its sale and use. Utility Model Content

[0005] The utility model provides a quicksand type potassium perchlorate production device, which aims to solve the problem of potassium perchlorate agglomeration in the potassium perchlorate production device in the prior art during the production of potassium perchlorate.

[0006] In order to solve the above technical problems, the technical solution adopted by the present invention is:

[0007] A quicksand-type potassium perchlorate production device includes a centrifuge, a centrifugal high-level tank, a mixing device, a screening device, and a soaking tank. The mixing device includes a barrel, a stirring mechanism, a sealing cover mechanism, and a discharge port. The stirring mechanism is connected to the barrel, the sealing cover mechanism is sealed on the barrel inlet, and the discharge port is opened at the bottom of the barrel. The stirring mechanism is used to mix multiple materials inside the barrel.

[0008] The screening device includes: a screening trough, a lower hopper, a filter screen and a vibration motor. The screening trough is installed at the bottom of the barrel, the discharge port is connected to the screening trough, and the discharge port is used to open or close; the lower hopper is installed at the lower opening of the screening trough, the filter screen is installed inside the screening trough, the height of the discharge port is higher than the filter screen, and the vibration motor is installed on the screening trough;

[0009] The inlet end of the soaking tank is connected to the outlet end of the lower hopper, the outlet end of the soaking tank is connected to the centrifugal high-level tank, the centrifugal high-level tank is used to store the material in the soaking tank, and the outlet end of the centrifugal high-level tank is connected to the centrifuge, which is used to separate the soaked material into dry and wet parts.

[0010] Furthermore, the stirring mechanism includes a motor, a rotating shaft and a stirring blade. The fixed end of the motor is installed on the barrel, the movable end is fixedly connected to the rotating shaft, the rotating shaft is rotatably installed on the barrel, the output shaft of the motor is connected to the rotating shaft and is used to drive the rotating shaft to rotate, and the stirring blade is fixedly installed on the rotating shaft.

[0011] Furthermore, the motor is connected to the rotating shaft through a reducer.

[0012] Furthermore, the sealing cover mechanism includes a cover body and cylinders arranged on both sides of the cover body, the cover body is hinged on the barrel, the cylinder body of the cylinder is hinged to the barrel, and the rod body of the cylinder is hinged to the cover body.

[0013] Furthermore, a hinge portion is provided on the cover body, and the rod portion is hinged to the cover body via the hinge portion.

[0014] Furthermore, a stepped groove is provided at the opening position of the barrel, and a sealing gasket is provided below the cover body. When the cover body is closed, the sealing gasket contacts the stepped groove to form a seal.

[0015] Furthermore, a workbench is provided below the barrel, and the screening trough and the motor are both installed on the workbench.

[0016] Furthermore, the discharge port is connected to the feed port on the side wall of the screening trough through a discharge channel. The discharge channel is inclined and a gate is provided on the discharge port.

[0017] Furthermore, a plurality of brackets are provided on the screening trough, and each of the brackets is provided with a vibration motor.

[0018] Compared with the prior art, the present invention has the following beneficial effects:

[0019] The utility model mainly comprises a centrifuge, a centrifugal high-level tank, a mixing device, a screening device and a soaking tank; in actual use, a worker first adds 65% of the volume of soft water into the soaking tank, and then adds SDS, TX10 and KF865 in a ratio of 1:1:1, and heats the soaking tank to dissolve the blocky potassium perchlorate in the soaking tank to form potassium perchlorate wet crystals; then the potassium perchlorate wet crystals are poured into the barrel, and a nano-scale hydrophobic powder anti-caking agent is added into the barrel, and then a stirring mechanism is driven to fully stir and mix the potassium perchlorate wet crystals and the nano-scale hydrophobic powder anti-caking agent in the barrel, and the stirred potassium perchlorate wet crystals are discharged through the discharge port. The wet potassium perchlorate crystals are fed into the screening tank and the vibration motor is started at the same time. After the vibration of the vibration motor, the wet potassium perchlorate crystals are screened through a filter screen and finally discharged from the lower hopper and passed into the soaking tank. The wet potassium perchlorate crystals in the soaking tank are then stirred again for 10-15 minutes. After the stirring is completed, the stirred wet potassium perchlorate crystals in the soaking tank are passed into the centrifugal high-level tank for temporary storage. After a certain amount of wet potassium perchlorate crystals are stored, the wet potassium perchlorate crystals in the centrifugal high-level tank are passed into the centrifuge for centrifugation. The liquid formed after the centrifugation is returned to the soaking tank, and the solids are collected. Finally, the collected solids are dried to form quicksand-like potassium perchlorate. The advantage of this arrangement is that the hydrophilic groups are adsorbed on the surface of the potassium perchlorate particles, and the hydrophobic groups are oriented toward the gas phase, making the particle surface hydrophobic, hindering the entry of atmospheric moisture, and inhibiting the deliquescence of the granular product. The adsorbed surfactant can also reduce the capillary adsorption force of the particles to the solution, improve the crystallization habits of the solid particles, greatly reduce the interfacial energy of the particle crystals, and inhibit nucleation, thereby having a good anti-caking effect on the potassium perchlorate particles. BRIEF DESCRIPTION OF THE DRAWINGS

[0020] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the following is a brief introduction to the drawings required for use in the embodiments. It should be understood that the following drawings only show certain embodiments of the present invention and therefore should not be regarded as limiting the scope. For ordinary technicians in this field, other relevant drawings can be obtained based on these drawings without creative work.

[0021] Figure 1 It is a structural diagram of the present utility model.

[0022] Figure 2 For this utility model Figure 1 A partial enlarged view of .

[0023] Figure 3 It is a schematic diagram of the connection relationship between the screening trough and the filter screen in the utility model.

[0024] Figure 4 For this utility model Figure 3 A partial enlarged view of .

[0025] In the figure, 101-barrel, 102-stirring mechanism, 103-sealing cover mechanism, 104-discharge port, 105-screen trough, 106-discharge bin, 107-filter, 108-vibration motor, 109-motor, 110-rotating shaft, 111-stirring blade, 112-reducer, 113-cover body, 114-cylinder, 115-hinge part, 116-step trough, 117-workbench, 118-discharge channel, 119-bracket. DETAILED DESCRIPTION

[0026] The present invention is further described below in conjunction with embodiments. The embodiments described are only a portion of the embodiments of the present invention and are not intended to be all embodiments. Based on the embodiments of the present invention, other embodiments obtained by persons of ordinary skill in the art without creative work are all within the scope of protection of the present invention.

[0027] See also Figure 1-Figure 4 As shown, this embodiment discloses a production device, specifically a quicksand-type potassium perchlorate production device, which is used to stir and filter quicksand-type potassium perchlorate; wherein the device includes a centrifuge, a centrifugal high-level tank, a mixing device, a screening device, and an immersion tank; the mixing device includes: a barrel 101, a stirring mechanism 102, a sealing cover mechanism 103, and a discharge port 104; the stirring mechanism 102 is connected to the barrel 101, the sealing cover mechanism 103 is sealed and installed on the inlet of the barrel 101, and the discharge port 104 is opened at the bottom of the barrel 101; the stirring mechanism 102 is used to mix multiple materials inside the barrel 101;

[0028] The screening device includes: a screening trough 105, a lower bin 106, a filter 107 and a vibration motor 108. The screening trough 105 is installed at the bottom of the barrel 101, and the discharge port 104 is connected to the screening trough 105. The discharge port 104 is used to open or close; the lower bin 106 is installed at the lower opening of the screening trough 105, the filter 107 is installed inside the screening trough 105, the height of the discharge port 104 is higher than the filter 107, and the vibration motor 108 is installed on the screening trough 105;

[0029] The inlet end of the soaking tank is connected to the outlet end of the lower hopper 106, and the outlet end of the soaking tank is connected to the centrifugal high-level tank, which is used to store the material in the soaking tank. The outlet end of the centrifugal high-level tank is connected to a centrifuge, which is used to separate the soaked material into dry and wet parts.

[0030] The utility model mainly comprises a centrifuge, a centrifugal high-level tank, a mixing device, a screening device and a soaking tank; in actual use, the staff first adds 65% of the volume of soft water into the soaking tank, and then adds SDS, TX10 and KF865 in a ratio of 1:1:1, and heats the soaking tank to dissolve the blocky potassium perchlorate inside the soaking tank to form potassium perchlorate wet crystals; then the potassium perchlorate wet crystals are poured into the barrel 101, and a nano-scale hydrophobic powder anti-caking agent is added into the barrel 101, and then the stirring mechanism 102 is driven to fully stir and mix the potassium perchlorate wet crystals and the nano-scale hydrophobic powder anti-caking agent inside the barrel 101, and the stirred potassium perchlorate wet crystals pass through the discharge port 104. The potassium perchlorate wet crystals enter the screening trough 105, and the vibration motor 108 is started at the same time. After the vibration of the vibration motor 108, the potassium perchlorate wet crystals are screened through the filter screen 107, and finally discharged from the lower hopper 106 and passed into the soaking tank; then the potassium perchlorate wet crystals in the soaking tank are stirred again for 10-15 minutes. After the stirring is completed, the stirred potassium perchlorate wet crystals in the soaking tank are passed into the centrifugal high-level tank for temporary storage. After a certain amount of potassium perchlorate wet crystals are stored, the potassium perchlorate wet crystals in the centrifugal high-level tank are passed into the centrifuge for centrifugation. The liquid formed after centrifugation is returned to the soaking tank, and the solids are collected. Finally, the collected solids are dried to form quicksand potassium perchlorate. The stirring mechanism can fully stir the potassium perchlorate wet crystals and the nano-hydrophobic powder anti-caking agent to make the potassium perchlorate wet crystals less likely to agglomerate. The screening trough 105 can also filter the lumpy potassium perchlorate wet crystals. During the vibration of the vibration motor 108, some large lumps of potassium perchlorate wet crystals can be disintegrated into small lumps and powdered potassium perchlorate wet crystals, thereby further improving the anti-caking effect.

[0031] It should be noted that SDS, TX10 and KF865 are all dispersants in the prior art.

[0032] In some embodiments, the stirring mechanism 102 includes a motor 109, a rotating shaft 110 and a stirring blade 111. The fixed end of the motor 109 is installed on the barrel 101, and the movable end is fixedly connected to the rotating shaft 110. The rotating shaft 110 is rotatably installed on the barrel 101. The output shaft of the motor 109 is connected to the rotating shaft 110 and is used to drive the rotating shaft 110 to rotate. The stirring blade 111 is fixedly installed on the rotating shaft 110.

[0033] During actual use, when it is necessary to stir the potassium perchlorate wet crystals, it is necessary to control the motor 109 to rotate. After the motor 109 rotates, it drives the rotating shaft 110 to rotate. After the rotating shaft 110 rotates, it drives the stirring blade 111 to rotate. After the stirring blade 111 rotates, it drives the potassium perchlorate wet crystals and the nano-scale hydrophobic powder anti-caking agent to be fully stirred and mixed, so that the potassium perchlorate wet crystals are affected by the anti-caking agent to avoid agglomeration.

[0034] In some embodiments, the motor 109 is connected to the rotating shaft 110 via a reducer 112 .

[0035] In actual use, the speed reducer 112 can effectively control the rotation speed of the shaft 110 , and there is no need to configure the model of the motor 109 to match the rotation speed of the shaft 110 , which is more convenient to use.

[0036] In some embodiments, the sealing cover mechanism 103 includes a cover body 113 and a cylinder 114 arranged on both sides of the cover body 113. The cover body 113 is hinged on the barrel 101, the cylinder body of the cylinder 114 is hinged to the barrel 101, and the rod body of the cylinder 114 is hinged to the cover body 113.

[0037] During actual use, when it is necessary to open the cover body 113, the staff controls the extension of the cylinder 114. At this time, the rod body of the cylinder 114 slides out from the cylinder body of the cylinder 114, and then the rod body of the cylinder 114 extends to support the cover body 113, so that the cover body 113 rotates around the barrel 101, thereby opening the barrel 101; conversely, when it is necessary to close the cover body 113, it is necessary to control the originally extended cylinder 114 to retract. After the cylinder 114 retracts, it pulls the cover body 113 to close, thereby completing the closing of the barrel 101.

[0038] In some embodiments, a hinge portion 115 is provided on the cover body 113 , and the rod portion is hinged to the cover body 113 via the hinge portion 115 .

[0039] In actual use, the hinge portion 115 can make the rotation between the cover body 113 and the barrel 101 smoother.

[0040] In some embodiments, a stepped groove 116 is provided at the opening of the barrel 101 , and a sealing gasket is provided below the cover body 113 . When the cover body 113 is closed, the sealing gasket contacts the stepped groove 116 to form a seal.

[0041] During actual use, when the cover body 113 is closed, the sealing gasket under the cover body 113 is placed in the stepped groove 116, and the cylinder 114 pulls the cover body 113 so that the sealing gasket fits tightly against the upper end surface of the stepped groove 116, thereby completing the sealing of the cover body 113, which is beneficial to prevent potassium perchlorate from leaking.

[0042] In some embodiments, a workbench 117 is provided below the barrel 101 , and the screening trough 105 and the motor 109 are both installed on the workbench 117 .

[0043] In actual use, the purpose of providing the workbench 117 is to install the screening trough 105 and the motor 109 .

[0044] In some embodiments, the discharge port 104 is connected to the feed port on the side wall of the screening trough 105 through a discharge channel 118 . The discharge channel 118 is inclined, and a gate is provided on the discharge port 104 .

[0045] During actual use, it is necessary to first slightly open the gate so that the material inside the barrel 101 falls into the discharge channel 118 due to gravity. Since the discharge channel 118 is inclined, the material will enter the screening trough 105 along the inclined discharge channel 118.

[0046] In some embodiments, a plurality of brackets 119 are provided on the screening trough 105 , and each of the brackets 119 is provided with a vibration motor 108 .

[0047] In actual use, the function of the vibration motor 108 is to make the screening trough 105 vibrate, thereby screening the potassium perchlorate wet crystals, and the larger potassium perchlorate wet crystals are re-entered into the soaking tank for dissolution.

[0048] In the description of the present invention, it should be understood that the terms "coaxial", "bottom", "one end", "top", "middle", "the other end", "upper", "one side", "top", "inside", "front", "center", "two ends", etc., indicating the orientation or position relationship, are based on the orientation or position relationship shown in the accompanying drawings, and are only for the convenience of describing the present invention and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the present invention.

[0049] In addition, the terms "first", "second", "third" and "fourth" are used for descriptive purposes only and cannot be understood as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Therefore, the features defined as "first", "second", "third" and "fourth" may explicitly or implicitly include at least one such feature.

[0050] In the present invention, unless otherwise clearly stipulated and limited, the terms such as "installation", "setting", "connection", "fixation" and "screw-on" should be understood in a broad sense. For example, it can be a fixed connection, a detachable connection, or an integrated connection; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium, it can be the internal connection of two elements or the interaction relationship between two elements. Unless otherwise clearly defined, ordinary technicians in this field can understand the specific meanings of the above terms in the present invention according to the specific circumstances.

[0051] Although the embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and variations may be made to these embodiments without departing from the principles and spirit of the present invention, and the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A quicksand type potassium perchlorate production device, comprising a centrifuge, a centrifugal high-level tank and a soaking tank, characterized in that: Also includes: A mixing device comprises: a barrel (101), a stirring mechanism (102), a sealing cover mechanism (103) and a discharge port (104), wherein the stirring mechanism (102) is connected to the barrel (101), the sealing cover mechanism (103) is sealed and installed on the feed port of the barrel (101), and the discharge port (104) is opened at the bottom of the barrel (101); and the stirring mechanism (102) is used to mix a plurality of materials inside the barrel (101); and The screening device comprises: a screening trough (105), a lower material bin (106), a filter screen (107) and a vibration motor (108); the screening trough (105) is installed at the bottom of the barrel (101); the discharge port (104) is communicated with the screening trough (105); the discharge port (104) is used to open or close; the lower material bin (106) is installed at the lower opening of the screening trough (105); the filter screen (107) is installed inside the screening trough (105); the height of the discharge port (104) is higher than the filter screen (107); and the vibration motor (108) is installed on the screening trough (105); The inlet end of the soaking tank is connected to the outlet end of the lower hopper (106), the outlet end of the soaking tank is connected to the centrifugal high-level tank, the centrifugal high-level tank is used to store the material in the soaking tank, and the outlet end of the centrifugal high-level tank is connected to a centrifuge, which is used to separate the soaked material into dry and wet parts.

2. A quicksand type potassium perchlorate production device according to claim 1, characterized in that: The stirring mechanism (102) comprises a motor (109), a rotating shaft (110) and a stirring blade (111). The fixed end of the motor (109) is mounted on the barrel (101), and the movable end is fixedly connected to the rotating shaft (110). The rotating shaft (110) is rotatably mounted on the barrel (101). The output shaft of the motor (109) is connected to the rotating shaft (110) and is used to drive the rotating shaft (110) to rotate. The stirring blade (111) is fixedly mounted on the rotating shaft (110).

3. A quicksand type potassium perchlorate production device according to claim 2, characterized in that: The motor (109) is connected to the rotating shaft (110) via a speed reducer (112).

4. A quicksand type potassium perchlorate production device according to claim 1, characterized in that: The sealing cover plate mechanism (103) comprises a cover plate body (113) and cylinders (114) arranged on both sides of the cover plate body (113); the cover plate body (113) is hinged on the barrel (101); the cylinder body of the cylinder (114) is hinged to the barrel (101); and the rod body of the cylinder (114) is hinged to the cover plate body (113).

5. A quicksand type potassium perchlorate production device according to claim 4, characterized in that: A hinge portion (115) is provided on the cover plate body (113), and the rod portion is hinged to the cover plate body (113) via the hinge portion (115).

6. A quicksand type potassium perchlorate production device according to claim 4, characterized in that: A stepped groove (116) is provided at the opening of the barrel (101), and a sealing gasket is provided below the cover body (113). When the cover body (113) is closed, the sealing gasket contacts the stepped groove (116) to form a seal.

7. A quicksand type potassium perchlorate production device according to claim 2, characterized in that: A workbench (117) is provided below the barrel (101), and the screening trough (105) and the motor (109) are both installed on the workbench (117).

8. A quicksand type potassium perchlorate production device according to claim 1, characterized in that: The discharge port (104) is connected to the feed port on the side wall of the screening trough (105) through a discharge channel (118). The discharge channel (118) is inclined, and a gate is provided on the discharge port (104).

9. A quicksand type potassium perchlorate production device according to claim 1, characterized in that: A plurality of brackets (119) are provided on the screening trough (105), and each of the brackets (119) is provided with a vibration motor (108).

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