Vanadium electrolyte concentration detection equipment

Abstract

The utility model discloses vanadium electrolyte concentration detection equipment, which belongs to the technical field of electrolyte detection equipment and comprises a titrator, a support column is riveted on one side of the titrator, symmetrical connecting grooves are arranged on the inner wall of the support column, tooth columns are slidably connected inside the connecting grooves, and the tooth columns are connected with the titrator. The tooth column is of a square column body structure with a plurality of tooth grooves evenly formed in one side, a motor is installed on the side, provided with the tooth grooves, of the tooth column, a rotating rod is fixedly connected to the output end of the motor, the other end of the rotating rod is rotationally connected with the inner wall of the supporting column, a gear is fixedly connected to a rod body of the rotating rod, and the gear is fixedly connected to the rod body of the rotating rod. By means of the structure, the effect that the height of a burette on a current titrator can be adjusted is achieved, and therefore the vanadium electrolyte concentration detection precision is greatly improved.

Description

Technical Field

[0001] This utility model belongs to the technical field of electrolyte detection equipment, specifically relating to a vanadium electrolyte concentration detection device. Background Technology

[0002] Vanadium electrolyte concentration detection equipment is mainly used to accurately measure the concentration of vanadium ions in different valence states in vanadium redox flow batteries to ensure battery performance and stability. This type of equipment typically employs redox titration or more advanced spectroscopic analysis techniques, such as ultraviolet-visible spectroscopy and atomic absorption spectroscopy. Among these, a titrator is a commonly used tool. It accurately determines the total vanadium concentration or the concentration of vanadium ions in specific valence states in the vanadium electrolyte by precisely controlling the amount of titrant added and combining it with magnetic stirring to achieve homogeneous mixing of the solution. These devices are crucial for the research, development, and maintenance of high-efficiency vanadium redox flow batteries.

[0003] Existing burettes are usually fixed in traditional manual or semi-automatic titration devices and cannot be adjusted, which leads to a decrease in the detection accuracy of the titrator and an increase in the difficulty of cleaning. This phenomenon has become a problem that urgently needs to be solved by those in the field. Utility Model Content

[0004] The purpose of this invention is to provide a vanadium electrolyte concentration detection device to address the problems mentioned in the background art.

[0005] To solve the above-mentioned technical problems, this utility model provides the following technical solution: a vanadium electrolyte concentration detection device, including a titrator, a support column riveted to one side of the titrator, a symmetrical connecting groove on the inner wall of the support column, a toothed column slidably connected inside the connecting groove, the toothed column being a square column structure with a plurality of teeth evenly opened on one side, a motor installed on the side of the toothed column with teeth, and the motor being fixedly connected to the inner wall of the support column;

[0006] A rotating rod is fixedly connected to the output end of the motor. The other end of the rotating rod is rotatably connected to the inner wall of the support column. A gear is fixedly connected to the rod body, and the gear meshes with the tooth groove on the gear column.

[0007] The present invention further describes that the support column has a hollow structure, a groove is provided on one outer wall of the support column, a support rod is provided in the groove, and the outer end of the support rod has a hollow frame structure.

[0008] The present invention further explains that the end of the support rod is fixedly connected to the side of the tooth column opposite to the tooth groove side.

[0009] This utility model further illustrates that a lead screw is rotatably connected to the inner walls of the two sides of the hollow frame of the support rod. The lead screw has a structure with opposite thread directions at both ends. The other end of the lead screw passes through the inner wall of the other side of the hollow frame of the support rod and is fixedly connected to a knob. A positioning rod is fixedly connected to one side of the lead screw. Two opposing clamps are movably connected to the body of the positioning rod. The lead screw and the clamps are movably connected by threads.

[0010] This utility model further illustrates that a burette is provided between the two clamping plates.

[0011] The present invention further describes that a display screen is installed on one side of the titrator, and a placement groove is formed on the upper surface of the titrator.

[0012] The present invention further illustrates that a stirring table is installed on the side of the titrator away from the placement slot, and a positioning slot is formed on the upper surface of the stirring table.

[0013] This utility model further illustrates that the motor is connected to the display screen via signal.

[0014] Compared with the prior art, the beneficial effects achieved by this utility model are: This utility model,

[0015] (1) By setting up a connecting groove, toothed column, motor, rotating rod and gear to realize the up and down displacement of the burette, it can be more easily positioned to a suitable position for adding titrant, reducing manual intervention;

[0016] (2) The burette can be detached and installed by setting a screw, knob, positioning rod and clamp, so that the titrator can be adapted to different specifications of burettes to meet different testing needs. The detachable burette can also improve the cleanliness of the equipment and avoid cross-contamination between different reagents. Attached Figure Description

[0017] The accompanying drawings are provided to further illustrate the present invention and form part of the specification. They are used together with the embodiments of the present invention to explain the present invention, but do not constitute a limitation thereof. In the drawings:

[0018] Figure 1 This is a schematic diagram of the overall structure of this utility model;

[0019] Figure 2 This is a top view of the present invention;

[0020] Figure 3 This is a utility model Figure 2 Enlarged view of point A in the middle;

[0021] Figure 4 This is a schematic diagram of the internal structure of the support column of this utility model;

[0022] Figure 5 This is a utility model Figure 4 Enlarged view of point B in the middle;

[0023] Figure 6 This is a schematic diagram of the connection between the toothed column and the support rod of this utility model;

[0024] Figure 7 This is a schematic diagram of the connection between the toothed column and the gear in this utility model;

[0025] In the diagram: 1. Titrator; 2. Display screen; 3. Placement slot; 4. Stirring table; 5. Positioning slot; 6. Support column; 61. Connecting slot; 7. Gear column; 8. Motor; 9. Rotating rod; 10. Gear; 11. Support rod; 12. Lead screw; 13. Knob; 14. Positioning rod; 15. Clamping plate; 16. Burette. Detailed Implementation

[0026] The following detailed, non-limiting description of the present invention, in conjunction with preferred embodiments and accompanying drawings, is provided. Obviously, the described embodiments are merely some, not all, of the embodiments of the present invention. All other embodiments obtained by those skilled in the art based on the embodiments of the present invention without inventive effort are within the scope of protection of the present invention.

[0027] Please see Figure 1-5 This utility model provides a technical solution: a vanadium electrolyte concentration detection device, including a titrator 1 for accurately measuring the concentration of vanadium electrolyte. A display screen 2 is installed on one side of the titrator 1 for setting various parameters in the detection. A placement groove 3 is opened on the upper surface of the titrator 1 for placing the titrant required for the detection. A stirring table 4 is installed on the side of the titrator 1 away from the placement groove 3, and the solution is uniformly mixed by magnetic stirring. A positioning groove 5 is opened on the upper surface of the stirring table 4 for placing the vanadium electrolyte.

[0028] refer to Figures 1-3A support column 6 is installed on the side of the titrator 1 near the stirring table 4. The support column 6 has a hollow structure, and a groove is opened on the outer wall of the side of the support column 6 near the stirring table 4. A support rod 11 is installed in the groove. The outer end of the support rod 11 has a hollow frame structure. A lead screw 12 is rotatably connected to the inner wall of one side of the hollow frame of the support rod 11. The lead screw 12 has a structure with opposite threads at both ends. The other end of the lead screw 12 passes through the inner wall of the other side of the hollow frame of the support rod 11, and a knob 13 is fixedly connected to this end. Turning the knob 13 can perform titration. As the lead screw 12 rotates, a positioning rod 14 is fixedly connected to one side of the lead screw 12. Two opposing clamping plates 15 are movably connected to the body of the positioning rod 14. The lead screw 12 passes through the clamping plates 15 and is movably connected to the clamping plates 15 by threads. A burette 16 is arranged between the two clamping plates 15. There is a large space between the lead screw 12 and the positioning rod 14, which is sufficient for the burette 16 to be inserted. After the lead screw 12 rotates, the two clamping plates 15 will move in opposite directions, thereby adjusting the distance between the two clamping plates 15.

[0029] refer to Figures 4-5 The inner wall of the support column 6 is provided with symmetrical connecting grooves 61. A toothed column 7 is slidably connected inside the connecting groove 61. The toothed column 7 is a square column structure with several toothed grooves evenly opened on one side. A motor 8 is installed on the side of the toothed column 7 with toothed grooves. The motor 8 is connected to the display screen 2 for signal control.

[0030] refer to Figure 6 The end of the support rod 11 is fixedly connected to the toothed column 7 on the side opposite to the tooth groove. The motor 8 is fixedly connected to the inner wall of the support column 6. A rotating rod 9 is fixedly connected to the output end of the motor 8. The other end of the rotating rod 9 is rotatably connected to the inner wall of the support column 6. A gear 10 is fixedly connected to the rod body of the rotating rod 9. (Reference) Figure 7 The gear 10 meshes with the tooth groove on the gear column 7; after the motor 8 runs, the rotating rod 9 drives the gear 10 to rotate, and the gear column 7 meshes with the gear 10 to drive the gear column 7 to move up and down in the connecting groove 61, thereby enabling the support rod 11 to drive the burette 16 to move up and down.

[0031] In this embodiment, a burette 16 with a suitable capacity is selected according to the requirements of the test. The titration cup containing the vanadium electrolyte sample is placed in the positioning groove 5. The titrant required for the test is placed in the placement groove 3 and connected to the selected burette 16 through a tube. The burette 16 is inserted into the hollow part of the support rod 11. The distance between the clamping plates 15 is adjusted by rotating the knob 13 until the clamping plates 15 fix the burette 16.

[0032] The height of the burette 16 is adjusted by rotating the drive motor 8, so that the height of the burette 16 can be controlled according to the amount of sample liquid, preventing the burette 16 from being too high and causing the titrant to drip rapidly into the test solution and splashing the solution, thus greatly improving the safety of the test.

[0033] After setting the parameters of the detection process via display screen 2, the detection begins. While the titrant is added to the sample, the stirring table 4 performs magnetic stirring. That is, a small magnetic ball placed at the bottom of the titration cup is driven to rotate by a rotating magnetic field set inside the titrator 1, thereby achieving effective stirring of the solution. The titrator 1 then detects the concentration of the vanadium electrolyte.

[0034] In the description of this utility model, it should be understood that the terms "upper", "lower", "front", "rear", "left", "right", etc., indicate the orientation or positional relationship based on the orientation or positional relationship shown in the accompanying drawings, and are only for the convenience of describing this utility model, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of this utility model.

[0035] Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of this utility model, and are not intended to limit it. Although this utility model has been described in detail with reference to the foregoing embodiments, those skilled in the art should understand that modifications can still be made to the technical solutions described in the foregoing embodiments, or equivalent substitutions can be made to some of the technical features. Such modifications or substitutions do not cause the essence of the corresponding technical solutions to deviate from the spirit and scope of the technical solutions of the embodiments of this utility model.

Claims

1. A vanadium electrolyte concentration detection device, comprising a titrator (1), characterized in that: A support column (6) is riveted to one side of the titrator (1). A set of opposing connecting grooves (61) are provided on the inner wall of the support column (6). A toothed column (7) is slidably connected inside the connecting groove (61). The toothed column (7) is a square column structure with several toothed grooves evenly provided on one side. A motor (8) is installed on the side of the toothed column (7) with toothed grooves. The motor (8) is fixedly connected to the inner wall of the support column (6). A rotating rod (9) is fixedly connected to the output end of the motor (8). The other end of the rotating rod (9) is rotatably connected to the inner wall of the support column (6). A gear (10) is fixedly connected to the rod body of the rotating rod (9). The gear (10) meshes with the tooth groove on the gear column (7).

2. The vanadium electrolyte concentration detection device according to claim 1, characterized in that: The support column (6) has a hollow structure. A groove is provided on one side of the outer wall of the support column (6). A support rod (11) is provided in the groove. The outer end of the support rod (11) has a hollow frame structure.

3. The vanadium electrolyte concentration detection device according to claim 2, characterized in that: The end of the support rod (11) is fixedly connected to the tooth column (7) on the side opposite to the tooth groove side.

4. The vanadium electrolyte concentration detection device according to claim 2, characterized in that: A lead screw (12) is rotatably connected to one side of the hollow frame of the support rod (11). The lead screw (12) has a structure with opposite thread directions at both ends. The other end of the lead screw (12) passes through the other side of the hollow frame of the support rod (11) and is fixedly connected to a knob (13). A positioning rod (14) is fixedly connected to one side of the lead screw (12). Two opposing clamps (15) are movably connected to the rod body of the positioning rod (14). The lead screw (12) and the clamps (15) are movably connected by threads.

5. The vanadium electrolyte concentration detection device according to claim 4, characterized in that: A burette (16) is provided between the two clamps (15).

6. The vanadium electrolyte concentration detection device according to claim 1, characterized in that: A display screen (2) is installed on one side of the titrator (1), and a placement groove (3) is provided on the upper surface of the titrator (1).

7. The vanadium electrolyte concentration detection device according to claim 6, characterized in that: A stirring table (4) is installed on the side of the titrator (1) away from the placement groove (3), and a positioning groove (5) is provided on the upper surface of the stirring table (4).

8. The vanadium electrolyte concentration detection device according to claim 6, characterized in that: The motor (8) is connected to the display screen (2) via signal.

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