Full-automatic ammonolysis instrument

Abstract

The utility model belongs to the technical field of ammonolysis devices, and particularly relates to a full-automatic ammonolysis instrument which comprises a waste liquid collecting bottle, a reaction box and a control box, an ammonolysis reaction pot assembly is arranged in the reaction box and comprises a pot body and an ammonolysis pot body cover, a heating diaphragm and a heating disc are used for heating at the same time, the heating time is shortened, and the control box is arranged on the control box. The flange belongs to a fixed connecting surface at the top end of the pot body, is rigid and can provide supporting and sealing references, the ammonolysis pot body cover is a movable sealing element, is also rigid and can cover an opening of the pot body, and the sealing ring is made of an elastic material, can be extruded bidirectionally by the flange and the ammonolysis pot body cover, and can deform to fill a gap and block leakage; and when the air pressure upwards jacks up the ammonolysis pot body cover, the sealing ring is extruded between the ammonolysis pot body cover and the flange to realize sealing, the higher the air pressure is, the tighter the sealing ring is attached, the sealing effect is better, and compared with bolt sealing, the sealing performance of the sealing ring is better.

Description

Technical Field

[0001] This utility model relates to the technical field of ammonia hydrolysis devices, specifically a fully automatic ammonia hydrolyzer. Background Technology

[0002] Ammonolysis is an important step in DNA synthesis and a significant factor affecting primer quality, yield, and purity. Ammonolysis refers to the process by which organic compounds containing various functional groups are converted into amine compounds under the action of an amination agent.

[0003] Existing ammonia hydrolysis apparatuses are bulky, complex to operate, and have long reaction times. Most are fixed by bolts, posing significant safety hazards and failing to meet the requirements for large-scale ammonia hydrolysis production in industrial and laboratory settings.

[0004] Therefore, a fully automated ammonia hydrolysis apparatus is proposed to solve the above problems. Utility Model Content

[0005] The purpose of this invention is to provide a fully automatic ammonia hydrolysis apparatus to solve the problems mentioned in the background art, such as the existing ammonia hydrolysis apparatus being bulky, complex to operate, large in size, having a long ammonia hydrolysis reaction time, and posing significant sealing safety hazards, which cannot meet the requirements for large-scale ammonia hydrolysis production in industrial and laboratory settings.

[0006] To achieve the above objectives, this utility model provides the following technical solution: a fully automatic ammonia hydrolysis apparatus, comprising a waste liquid collection bottle, a reaction chamber, and a control box. An ammonia hydrolysis reaction vessel assembly is installed inside the reaction chamber. The ammonia hydrolysis reaction vessel assembly includes a vessel body and an ammonia hydrolysis vessel cover. The vessel body is located inside the reaction chamber, and the ammonia hydrolysis vessel cover is located above the reaction chamber. A heating diaphragm is provided on the outer wall surface of the vessel body. A heating plate is connected to the bottom of the vessel body, and a flange is connected to the upper surface of the vessel body. A sealing ring is provided between the ammonia hydrolysis vessel cover and the flange. The interior of the vessel body is a chamber, and a pressure gauge is installed on the upper part of the vessel body.

[0007] Preferably, the control box has a display screen in the middle of the front wall, a power switch, a cooling fan, and a buzzer warning light on the side. The control box has an internal power supply connected to the power switch and a control board connected to the internal power supply.

[0008] Preferably, the pot body is provided with a second air inlet and a first exhaust / liquid outlet, with the first exhaust / liquid outlet located below the second air inlet.

[0009] Preferably, the side wall surface of the reaction chamber is provided with a first air inlet, and the first air inlet is located at one end of the reaction chamber and connected to a one-way valve.

[0010] Preferably, a first solenoid valve is provided in the lower center of the interior of the reaction chamber, a pressure transmitter is provided on the side of the first solenoid valve near the control box, and an unloading valve is provided on the rear side of the pressure transmitter.

[0011] Preferably, a second solenoid valve is provided at the lower center of the inside of the control box, and a switch ball valve, a second vent / liquid port and a third vent / liquid port are respectively provided on the side wall of the control box.

[0012] Compared with the prior art, the beneficial effects of this utility model are: the heating diaphragm and the heating plate heat simultaneously, shortening the heating time and thus greatly improving the ammonia hydrolysis efficiency; the flange is a fixed connection surface at the top of the pot body, which is rigid and can provide support and sealing reference; the ammonia hydrolysis pot body cover is a movable sealing element, which is also rigid and can cover the pot body opening; the sealing ring is an elastic material that can be squeezed bidirectionally by the flange and the ammonia hydrolysis pot body cover, which can deform to fill the gap and block leakage; when the air pressure pushes the ammonia hydrolysis pot body cover upward, the sealing ring is squeezed between the ammonia hydrolysis pot body cover and the flange to achieve a seal; and the higher the air pressure, the tighter the sealing ring adheres, resulting in a better sealing effect. Compared with the use of bolt sealing, the sealing ring has better sealing performance. Attached Figure Description

[0013] Figure 1 This is a three-dimensional structural diagram of the present invention;

[0014] Figure 2 This is a schematic diagram of the internal structure of this utility model;

[0015] Figure 3 This is a schematic diagram of the gas path structure of this utility model;

[0016] Figure 4 This is an enlarged schematic diagram of the flange structure of this utility model;

[0017] Figure 5 This is a schematic cross-sectional view of the lid of the ammonia hydrolysis pot of this utility model.

[0018] In the diagram: 1. Waste liquid collection bottle; 2. Reaction chamber; 3. Control box; 4. Display screen; 5. Power switch; 6. Cooling fan; 7. Buzzer warning light; 8. Ammonium hydrolysis reactor assembly; 9. Pressure gauge; 10. Ammonium hydrolysis reactor cover; 11. Chamber; 12. First air inlet; 13. Check valve; 14. First solenoid valve; 15. Pressure transmitter; 16. Unloading valve; 17. Second solenoid valve; 18. Second air inlet; 19. First exhaust / liquid port; 20. Switch ball valve; 21. Second exhaust / liquid port; 22. Third exhaust / liquid port; 23. Heating diaphragm; 24. Heating plate; 25. Sealing ring; 26. Flange. Detailed Implementation

[0019] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0020] In the description of this utility model, it should be noted that the terms "upper," "lower," "inner," "outer," "top / bottom," etc., indicating the orientation or positional relationship are based on the orientation or positional relationship shown in the accompanying drawings, and are only for the convenience of describing this utility model and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of this utility model. Furthermore, the terms "first" and "second" are used for descriptive purposes only and should not be construed as indicating or implying relative importance.

[0021] In the description of this utility model, it should be noted that, unless otherwise explicitly specified and limited, the terms "installed," "equipped with," "sleeved / connected," "connected," etc., should be interpreted broadly. For example, "connection" can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium; it can be a connection within two components. Those skilled in the art can understand the specific meaning of the above terms in this utility model based on the specific circumstances. Example

[0022] Please see Figure 1-5This utility model provides a technical solution: a fully automatic ammonia hydrolysis apparatus, including a waste liquid collection bottle 1, a reaction chamber 2, and a control box 3. The inlet of the waste liquid collection bottle 1 is connected to a pipeline (not shown in the figure), which can be quickly connected to a drain port. The reaction chamber 2 is equipped with an ammonia hydrolysis reaction vessel assembly 8, which includes a vessel body and an ammonia hydrolysis vessel cover 10. The vessel body is located inside the reaction chamber 2, and the ammonia hydrolysis vessel cover 10 is located above the reaction chamber 2. A heating diaphragm 23 is provided on the outer wall surface of the vessel body, and a heating plate 24 is connected to the bottom of the vessel body. The upper surface of the pot body is connected to a flange 26. A sealing ring 25 is provided between the ammonia hydrolysis pot body cover 10 and the flange 26. The interior of the pot body is a chamber 11, and a sample rack is installed inside the chamber 11. A pressure gauge 9 is installed on the upper part of the pot body, through which the pressure inside the pot body can be directly observed. A pressure rod assembly is also installed on the ammonia hydrolysis pot body cover 10, including a knob and a metal pressure rod. The knob is a manual operation end, and the force is transmitted through a screw pair when rotated. The two ends of the metal pressure rod are fixed on the flange support, and the middle presses down on the ammonia hydrolysis pot body cover 10 to achieve "three-point" uniform force. When in use, rotating the top knob clockwise causes the metal pressure rod to move downward through the screw drive, uniformly squeezing the ammonia hydrolysis pot body cover 10 and compressing the sealing ring 25 to ensure the overall sealing of the equipment. After opening the cover, rotating the knob counterclockwise causes the pressure rod to retract upward with the screw drive, releasing the downward pressure on the ammonia hydrolysis pot body cover 10.

[0023] The control box 3 has a display screen 4 in the middle of its front wall, a power switch 5, a cooling fan 6, and a buzzer warning light 7 on its side. Inside the control box 3, there is a built-in power supply connected to the power switch 5 and a control board connected to the built-in power supply. The pot body has a second air inlet 18 and a first exhaust / liquid outlet 19, and a thermometer is installed to measure the temperature of the pot body. The first exhaust / liquid outlet 19 is below the second air inlet 18. The reaction chamber 2 has a first air inlet 12 on its side wall surface, located within the reaction chamber. One end of the reaction chamber 2 is connected to a one-way valve 13. A first solenoid valve 14 is provided in the lower middle part of the interior of the reaction chamber 2. A pressure transmitter 15 is provided on the side of the first solenoid valve 14 near the control box 3. An unloading valve 16 is provided on the rear side of the pressure transmitter 15. A second solenoid valve 17 is provided in the lower middle part of the interior of the control box 3. A switch ball valve 20, a second exhaust / liquid port 21 and a third exhaust / liquid port 22 are respectively provided on the side wall of the control box 3. The second solenoid valve 17, the first exhaust / liquid port 19 and the switch ball valve 20 are connected by a three-way connector.

[0024] Working Principle: The first scenario of this device involves adding ammonia: When the solenoid valve 14 is not open and there is no pressure in the pot chamber, open the ammonia hydrolysis pot cover 10, add an appropriate amount of ammonia to the chamber 11, then place the sample to be hydrolyzed onto the sample rack, close the ammonia hydrolysis pot cover 10, and start powering the heating diaphragm 23 and heating plate 24 through the control box 3. When the temperature in the chamber 11 reaches the required temperature for ammonia hydrolysis (generally 90℃), the sample begins the deammoniation reaction. After the sample has completed deammoniation, close the control box 3, depressurize and cool down, remove the sample, close the ammonia hydrolysis pot cover 10, open the first solenoid valve 14 and the second solenoid valve 17 to enter the waste ammonia discharge mode, and discharge the waste ammonia water after the deammoniation reaction into the waste liquid collection bottle 1. A manual waste ammonia discharge mode is also added, which can be achieved by rotating the switch ball 20 to discharge the waste ammonia water. Waste liquid collection bottle 1; Next, the ammonia addition situation: When the first solenoid valve 14 is not open and there is no gas pressure in the pot cavity, open the ammonia hydrolysis pot body cover 10, add an appropriate amount of water to the chamber 11 (mainly to prevent the chamber 11 from dry burning during heating, which would affect the service life of the pot body), then put the sample to be ammonia hydrolyzed on the sample rack, close the ammonia hydrolysis pot body cover 10, and the control box 3 starts to supply power to the heating diaphragm 23 and heating plate 24 for heating. When the temperature in the chamber 11 reaches the temperature required for ammonia hydrolysis (generally 90℃), ammonia is added, and the sample begins to undergo ammonia removal reaction. After the sample has completed ammonia removal, the control box 3 is closed, the pressure is released and the temperature is lowered, the sample is taken out, the ammonia hydrolysis pot body cover 10 is closed, the first solenoid valve 14 and the second solenoid valve 17 are opened to enter the waste liquid discharge mode, and the wastewater after the ammonia removal reaction is discharged into the waste liquid collection bottle 1.

[0025] The foregoing has shown and described the basic principles, main features, and advantages of this utility model. It is obvious to those skilled in the art that this utility model is not limited to the details of the exemplary embodiments described above, and that it can be implemented in other specific forms without departing from the spirit or basic characteristics of this utility model. Therefore, the embodiments should be considered exemplary and non-limiting in all respects. The scope of this utility model is defined by the appended claims rather than the foregoing description. Therefore, it is intended that all variations falling within the meaning and scope of equivalents of the claims be included within this utility model, and no reference numerals in the claims should be considered as limiting the scope of the claims.

[0026] Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made to these embodiments without departing from the principles and spirit of the present invention, the scope of which is defined by the appended claims and their equivalents.

Claims

1. A fully automatic ammonia hydrolyzer, characterized in that: The system includes a waste liquid collection bottle (1), a reaction chamber (2), and a control box (3). The reaction chamber (2) is equipped with an ammonium hydrolysis reaction vessel assembly (8). The ammonium hydrolysis reaction vessel assembly (8) includes a vessel body and an ammonium hydrolysis vessel cover (10). The vessel body is located inside the reaction chamber (2), and the ammonium hydrolysis vessel cover (10) is located above the reaction chamber (2). A heating diaphragm (23) is provided on the outer wall surface of the vessel body. A heating plate (24) is connected to the bottom of the vessel body. A flange (26) is connected to the upper surface of the vessel body. A sealing ring (25) is provided between the ammonium hydrolysis vessel cover (10) and the flange (26). The interior of the vessel body is a chamber (11), and a pressure gauge (9) is installed on the upper part of the vessel body.

2. The fully automatic ammonia hydrolyzer according to claim 1, characterized in that: The control box (3) has a display screen (4) in the middle of the front wall, a power switch (5), a cooling fan (6), and a buzzer warning light (7) on the side. The control box (3) has an internal power supply connected to the power switch (5) and a control board connected to the internal power supply.

3. The fully automatic ammonia hydrolyzer according to claim 1, characterized in that: The pot body is provided with a second air inlet (18) and a first exhaust / liquid outlet (19), with the first exhaust / liquid outlet (19) located below the second air inlet (18).

4. The fully automatic ammonia hydrolyzer according to claim 1, characterized in that: The side wall surface of the reaction chamber (2) is provided with a first air inlet (12), and a one-way valve (13) is connected to one end of the reaction chamber (2).

5. The fully automatic ammonia hydrolyzer according to claim 1, characterized in that: The reaction chamber (2) is provided with a first solenoid valve (14) in the lower middle part. The first solenoid valve (14) is provided with a pressure transmitter (15) on the side near the control box (3). The pressure transmitter (15) is provided with an unloading valve (16) on the rear side.

6. The fully automatic ammonia hydrolyzer according to claim 1, characterized in that: The control box (3) is provided with a second solenoid valve (17) at the lower center of the interior. The control box (3) is provided with a ball valve (20), a second exhaust / liquid port (21) and a third exhaust / liquid port (22) on the side wall.

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