dimethylamine salt reactor
By introducing an anti-clogging mechanism into the dimethylamine salt reactor, and using springs and a vibration motor to drive the filter box to vibrate, the problem of blockage in the discharge pipe caused by crystal accumulation was solved, thus achieving smooth discharge of materials in the reactor and increased production.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- CHANGZHOU FEIYU CHEM
- Filing Date
- 2025-06-26
- Publication Date
- 2026-06-30
AI Technical Summary
Dimethylamine salts are prone to crystallization and accumulation in the reactor, leading to blockage of the discharge pipe during the discharge process, which affects the reaction cycle and yield.
A dimethylamine salt reactor with an anti-clogging mechanism was designed, comprising a spring, a filter box, a vibration motor, a filter plate, and an outlet. The filter box is driven to vibrate by the vibration motor to prevent crystals from accumulating in the discharge pipe.
It effectively prevents blockages during the discharge process, ensures smooth discharge of materials from the reactor, and increases the output per unit time.
Smart Images
Figure CN224422852U_ABST
Abstract
Description
Technical Field
[0001] This application relates to the field of reactor technology, specifically to dimethylamine salt reactors. Background Technology
[0002] Dimethylamine salts are a class of salt compounds formed by the reaction of dimethylamine ((CH3)2NH) with acids. The most representative of these is dimethylamine hydrochloride (chemical formula C2H8ClN, CAS number 506-59-2).
[0003] A dimethylamine salt reactor is an industrial device specifically designed to handle chemical reactions related to dimethylamine salts. Its core function is to convert or recover dimethylamine salts by controlling reaction conditions.
[0004] For example, patent CN207614820U discloses a dimethylamine salt reactor for preparing N,N-dimethylaminoacrylate. This patent filters the items by connecting a filter screen inside the reaction chamber, ensuring the items are clean.
[0005] However, dimethylamine salts are prone to react with acidic substances under certain conditions to form insoluble salts, or crystallize due to temperature and concentration changes during distillation and reaction. These crystals tend to accumulate in the reactor, causing blockage in the discharge pipe during the discharge process. Poor discharge leads to material accumulation in the reactor, prolonging the reaction cycle and reducing the yield per unit time.
[0006] Therefore, it is necessary to provide a dimethylamine salt reactor to solve the above problems.
[0007] It should be noted that the information disclosed in this background section is only for understanding the background technology of this application concept, and therefore may include information that does not constitute prior art. Summary of the Invention
[0008] Based on the aforementioned problems in the existing technology, the problem to be solved by this application is to provide a dimethylamine salt reactor, which solves the problem that crystals easily accumulate in the reactor, causing blockage in the discharge pipe during the discharge process.
[0009] The technical solution adopted by this application to solve its technical problem is: a dimethylamine salt reactor, comprising:
[0010] Fixture;
[0011] A reactor, mounted on the upper end of the frame, having a discharge pipe;
[0012] An anti-blocking mechanism is installed on the discharge pipe, and the anti-blocking mechanism includes:
[0013] A spring, which is mounted on the mounting bracket;
[0014] A filter box, which is mounted on the other end of the spring;
[0015] A flexible hose is installed on the discharge pipe, and the other end of the hose is connected to the filter box.
[0016] A vibration motor is installed on both sides of the filter box;
[0017] A filter plate, which is inclinedly disposed inside the filter box;
[0018] An outlet is installed at the lower end of the filter box;
[0019] The slag discharge port is located on one side of the filter box.
[0020] Furthermore, the slag discharge port is located at the lower end of the filter plate.
[0021] Furthermore, the reactor includes a fixed sleeve fixedly disposed on the upper end of the fixed frame, a sealing plate fixedly disposed on the upper end of the fixed sleeve, and a reaction vessel fixedly disposed inside the fixed sleeve at the lower end of the sealing plate.
[0022] Furthermore, there is a heat-insulating cavity between the fixing sleeve and the reaction vessel. A water inlet is fixedly provided at the upper end of one side of the fixing sleeve, and a drain outlet is fixedly provided at the lower end of the other side of the fixing sleeve. The drain outlet and the water inlet are connected to the heat-insulating cavity.
[0023] Furthermore, the sealing plate is provided with a feed inlet, which is connected to the inside of the reaction vessel. The sealing plate is also provided with an air inlet, which is also connected to the inside of the reaction vessel. A discharge pipe is fixedly provided at the lower end of the reaction vessel.
[0024] Furthermore, a motor is fixedly installed at the upper end of the sealing plate, and the output belt of the motor extends through the sealing plate into the interior of the reaction vessel and is fixedly connected to a stirring shaft. A stirring paddle is fixedly installed on the outside of the stirring shaft.
[0025] The beneficial effect of this application is that the dimethylamine salt reactor provided by this application, by setting an anti-clogging mechanism, achieves the effect of preventing clogging.
[0026] In addition to the purposes, features, and advantages described above, this application has other purposes, features, and advantages. A further detailed description of this application will be provided below with reference to the figures. Attached Figure Description
[0027] The accompanying drawings, which form part of this application, are used to provide a further understanding of this application. The illustrative embodiments of this application and their descriptions are used to explain this application and do not constitute an undue limitation of this application.
[0028] In the attached diagram:
[0029] Figure 1 This is a schematic diagram of the dimethylamine salt reactor in this application;
[0030] Figure 2 This is a schematic cross-sectional view of the dimethylamine salt reactor in this application;
[0031] Figure 3 for Figure 1 A schematic diagram of the anti-blocking mechanism in the middle;
[0032] Figure 4 for Figure 1 A schematic diagram of an explosion at a central fire prevention and control mechanism;
[0033] The following are the labeling elements in the figure:
[0034] 1. Fixing frame; 2. Reactor; 20. Fixing sleeve; 21. Sealing plate; 22. Reaction vessel; 23. Feed inlet; 24. Motor; 25. Stirring shaft; 26. Stirring paddle; 27. Water inlet; 28. Drain outlet; 29. Air inlet; 30. Discharge pipe; 4. Anti-clogging mechanism; 40. Hose; 41. Filter box; 42. Filter plate; 43. Outlet; 44. Spring; 45. Vibration motor; 46. Slag discharge port. Detailed Implementation
[0035] It should be noted that, unless otherwise specified, the embodiments and features described in this application can be combined with each other. This application will now be described in detail with reference to the accompanying drawings and embodiments.
[0036] To enable those skilled in the art to better understand the present application, the technical solutions in the embodiments of the present application will be clearly and completely described below with reference to the accompanying drawings. Obviously, the described embodiments are only some embodiments of the present application, and not all embodiments. Based on the embodiments in the present application, all other embodiments obtained by those of ordinary skill in the art without creative effort should fall within the scope of protection of the present application.
[0037] like Figures 1-2 As shown, this application provides a dimethylamine salt reactor, which is installed on the ground or a steel frame platform and is mainly used to synthesize compounds such as N,N-dimethylaminoacrylate. Specifically, the dimethylamine salt reactor includes a fixed frame 1 and a reactor 2 fixedly installed on the upper end of the fixed frame 1. The reactor 2 is the main place for chemical reactions.
[0038] The reactor 2 includes a fixed sleeve 20 fixedly installed on the upper end of the fixed frame 1, and a sealing plate 21 fixedly installed on the upper end of the fixed sleeve 20. At the same time, a reaction vessel 22 is fixedly installed inside the fixed sleeve 20. The reaction vessel 22 is used to store raw materials such as dimethylamine salt to be processed.
[0039] It should be noted that there is an insulation cavity (not shown in the figure) between the fixed sleeve 20 and the reaction vessel 22. At the same time, a water inlet 27 is fixedly installed on the upper end of one side of the fixed sleeve 20, and a drain outlet 28 is fixedly installed on the lower end of the other side of the fixed sleeve 20. The drain outlet 28 and the water inlet 27 are connected to the insulation cavity so that cooling water can be injected through the water inlet 27 during the reaction process to control the reaction temperature, and then the cooling water is discharged through the drain outlet 28.
[0040] Meanwhile, a feed inlet 23 is provided on the sealing plate 21. The feed inlet 23 is connected to the inside of the reaction vessel 22 so that raw materials such as dimethylamine salt can be introduced into the inside of the reaction vessel 22 through the feed inlet 23. An air inlet 29 is also provided on the sealing plate 21. The air inlet 29 is also connected to the inside of the reaction vessel 22 so that inert gas can be introduced into the inside of the reaction vessel 22 for use.
[0041] Furthermore, a discharge pipe 30 is fixedly installed at the lower end of the reaction vessel 22. The discharge pipe 30 extends through the fixed sleeve 20 to the outside to facilitate the discharge of reaction products.
[0042] To ensure a full reaction, a motor 24 is fixedly installed on the upper end of the sealing plate 21. The output of the motor 24 is fixedly connected to a stirring shaft 25. The stirring shaft 25 passes through the sealing plate 21 and extends into the interior of the reaction vessel 22. At the same time, a stirring paddle 26 is fixedly installed on the outside of the stirring shaft 25 so that during the reaction process, the stirring paddle 26 can be driven to rotate inside the reaction vessel 22 by starting the motor 24, thereby mixing the materials, accelerating the reaction, and preventing local overheating.
[0043] Before the mixing reaction begins, raw materials such as dimethylamine salt are first added through the feed inlet 23. Then, the motor 24 is started to drive the stirring paddle 26 to mix the materials. During the stirring process, cooling water is injected through the water inlet 27 to maintain the reaction temperature. In the mixing process, inert gas is introduced through the air inlet 29 to complete the subsequent reaction and mixing operations. Finally, the reactants are discharged through the discharge pipe 30.
[0044] To prevent blockages during the drainage process, such as Figures 1-4 As shown, an anti-blocking mechanism 4 is provided at the discharge pipe 30. This anti-blocking mechanism 4 prevents blockage by separately discharging the crystals and liquid.
[0045] The anti-clogging mechanism 4 includes multiple sets of springs 44 fixedly arranged around the fixed frame 1, and a filter box 41 is fixedly arranged at the other end of the spring 44. At the same time, a vibration motor 45 is fixedly arranged on both sides of the filter box 41, so that the vibration motor 45 can be activated to drive the filter box 41 to vibrate on the fixed frame 1.
[0046] Meanwhile, a flexible tube 40 is fixedly installed on the discharge pipe 30, and the other end of the flexible tube 40 is connected to the filter box 41, so that the reactants can be introduced into the filter box 41 through the flexible tube 40.
[0047] Furthermore, a filter plate 42 is inclinedly arranged inside the filter box 41. The filter plate 42 is used to intercept large crystal particles. When the reactants are introduced into the filter box 41, they will be intercepted by the filter plate 42 as they flow through it. Large crystal particles are retained on the filter plate 42, while the pure product continues to flow out through the filter plate 42. An outlet 43 is fixedly opened at the lower end of the filter box 41, so that the pure product can be exported through the outlet 43 for subsequent processing.
[0048] Meanwhile, a slag discharge port 46 is provided at the lower end of the filter plate 42 in the filter box 41. The slag discharge port 46 is used to discharge large crystal particles intercepted on the filter plate 42. When the reaction products are continuously discharged, impurities will gradually accumulate on the filter plate 42. When a certain amount is accumulated, the vibration motor 45 can be started. The vibration motor 45 transmits vibration to the filter plate 42 through the spring 44, which loosens the impurities on the filter plate 42 and gradually slides through the inclined filter plate 42 to the slag discharge port 46. Finally, the crystals are discharged from the slag discharge port 46.
[0049] During the discharge process, the reactants are first introduced into the filter box 41 through the hose 40, and the crystals are intercepted by the inclined filter plate 42. At this time, the pure product is discharged from the outlet 43 through the filter plate 42. Then, the vibration motor 45 is started to vibrate the filter plate 42 through the spring 44, causing the crystals on the surface to be discharged to the slag outlet 46, thereby achieving the effect of preventing discharge blockage.
[0050] The above description is merely a preferred embodiment of this application and is not intended to limit this application. Various modifications and variations can be made to this application by those skilled in the art. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of this application should be included within the protection scope of this application.
Claims
1. A dimethylamine salt reactor characterized by: include: Fixture (1); A reactor (2) is mounted on the upper end of the frame (1) and has a discharge pipe (30); An anti-blocking mechanism (4) is installed on the discharge pipe (30), and the anti-blocking mechanism (4) includes: A spring (44) is mounted on the bracket (1); A filter box (41) is mounted on the other end of the spring (44); A hose (40) is installed on the discharge pipe (30), and the other end of the hose (40) is connected to the filter box (41); A vibration motor (45) is installed on both sides of the filter box (41); A filter plate (42) is inclinedly disposed inside the filter box (41); Outlet (43) is installed at the lower end of the filter box (41); Slag discharge port (46) is located on one side of the filter box (41).
2. The dimethylamine salt reactor of claim 1, wherein: The slag discharge port (46) is located at the lower end of the filter plate (42).
3. The dimethylamine salt reactor of claim 1, wherein: The reactor (2) includes a fixed sleeve (20) fixedly installed on the upper end of the fixed frame (1), a sealing plate (21) fixedly installed on the upper end of the fixed sleeve (20), and a reaction vessel (22) fixedly installed inside the fixed sleeve (20) at the lower end of the sealing plate (21).
4. The dimethylamine salt reactor of claim 3, wherein: There is a heat-insulating cavity between the fixed sleeve (20) and the reaction vessel (22). A water inlet (27) is fixedly provided on the upper end of one side of the fixed sleeve (20), and a drain outlet (28) is fixedly provided on the lower end of the other side of the fixed sleeve (20). The drain outlet (28) and the water inlet (27) are connected to the heat-insulating cavity.
5. The dimethylamine salt reactor of claim 3, wherein: The sealing plate (21) is provided with a feed inlet (23), which is connected to the inside of the reaction vessel (22). The sealing plate (21) is provided with an air inlet (29), which is also connected to the inside of the reaction vessel (22). A discharge pipe (30) is fixedly provided at the lower end of the reaction vessel (22).
6. The dimethylamine salt reactor according to claim 3, characterized in that: A motor (24) is fixedly installed on the upper end of the sealing plate (21). The output belt of the motor (24) extends through the sealing plate (21) into the interior of the reaction vessel (22) and is fixedly connected to a stirring shaft (25). A stirring paddle (26) is fixedly installed on the outside of the stirring shaft (25).