A high-efficiency hydrogen fluoride purification device
By designing a high-efficiency hydrogen fluoride purification device with structures such as sliding blocks and fixed blocks, the problems of cumbersome sealing operation and limited filtration accuracy of existing devices have been solved, achieving rapid sealing and efficient filtration and cooling effects.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- HENAN HUANGHE NEW MATERIAL TECHNOLOGY CO LTD
- Filing Date
- 2025-07-03
- Publication Date
- 2026-07-03
AI Technical Summary
Existing hydrogen fluoride purification devices are cumbersome in sealed operation, making efficient operation difficult. The fixed structure of the filter module limits the filtration accuracy and lacks coordination with the cooling structure, making it difficult to achieve impurity isolation and temperature-controlled purification.
A high-efficiency hydrogen fluoride purification device was designed, comprising a disc, a can, a cover, a fixed ring, a sliding block, a connecting rod, a plug, and a fixed block. The device achieves rapid sealing through the cooperation of the sliding block and the fixed block, and achieves efficient filtration and cooling by combining a water pump, water pipes, a cooling ring, and a filter screen.
It enables rapid sealed operation in the hydrogen fluoride purification process, improves filtration accuracy and cooling efficiency, and enhances the synergistic effect of impurity isolation and temperature-controlled purification.
Smart Images
Figure CN224442394U_ABST
Abstract
Description
Technical Field
[0001] This utility model relates to the field of fluorine chemical purification technology, and in particular to a high-efficiency hydrogen fluoride purification device. Background Technology
[0002] Currently, hydrogen fluoride, as an important inorganic fluoride, has wide applications in various fields such as electronics, medicine, metallurgy, and chemicals. Especially in the preparation of high-purity electronic-grade hydrogen fluoride, the requirements for purity and impurity control are extremely high. Hydrogen fluoride reacts readily with moisture and oxidizing impurities, exhibiting high corrosiveness and volatility. Therefore, the purification process requires a high degree of technical coordination between temperature control, filtration, and condensation structures.
[0003] Regarding the aforementioned issues, traditional hydrogen fluoride purification devices mostly employ a method of heating and distilling the gas in a tank, then guiding the gas through a condensation system to recover the liquid product. Condensation largely relies on an external cooling water source or cooling pipelines. In most devices, the gas-liquid mixture directly enters a collector for settling. Common equipment includes simple piping connections and fixing mechanisms for connection to processing systems or transfer modules.
[0004] However, these existing devices have several problems in practical use. First, some devices are cumbersome in terms of connection and sealing operations, which is not conducive to efficient operation by workers, especially when frequently loading and unloading particulate materials, as the device is inconvenient to open and close and cannot be locked securely. Second, most filter modules are fixed structures, which limits the filtration accuracy and lacks coordination with the cooling structure, making it difficult to simultaneously achieve impurity isolation and temperature-controlled purification.
[0005] To address the above problems, a high-efficiency hydrogen fluoride purification device is proposed. Utility Model Content
[0006] To overcome the above shortcomings, this utility model provides a high-efficiency hydrogen fluoride purification device, which aims to improve the problem of cumbersome structure during sealed operation of a previous high-efficiency hydrogen fluoride purification device.
[0007] To achieve the above objectives, the present invention adopts the following technical solution: a high-efficiency hydrogen fluoride purification device, comprising a disc, a tank fixedly connected to the top of the disc, a fixed ring fixedly connected to the top of the tank, a cover plate rotatably connected to the top of the fixed ring, a fixing mechanism provided at the top of the fixed ring, a pipe installed on the side wall of the tank, a collection box provided at the end of the pipe away from the tank, a cooling mechanism provided inside the collection box, the cooling mechanism comprising a water pump, a water pipe fixedly connected to the output end of the water pump, a cooling ring fixedly connected to the end of the water pipe away from the water pump, a water pipe fixedly connected to one end of the cooling ring, a water collection tank fixedly connected to the outer side of the water pipe, and a water tank connected to the input end of the water pump via a pipe 8.
[0008] As a further description of the above technical solution:
[0009] The fixing structure includes a sliding block 1, an insert post 1 is provided inside the sliding block 1, a connecting rod is rotatably connected to the outside of the insert post 1, one end of the connecting rod is rotatably connected to the insert post 2, a sliding block 2 is provided outside the insert post 2, and fixing blocks are symmetrically connected to both sides of the sliding block 1, and a fixing cylinder is provided inside the fixing block.
[0010] As a further description of the above technical solution:
[0011] A heater is provided at the center of the bottom of the disc, and multiple support columns are arranged around the bottom of the disc.
[0012] As a further description of the above technical solution:
[0013] An exhaust pipe is fixedly connected to the top of the tank.
[0014] As a further description of the above technical solution:
[0015] A sliding block is provided on the outer side of the cover plate, and a cylinder is fixedly connected to the top of the cover plate. A pull ring is fixedly connected to the top of the cylinder.
[0016] As a further description of the above technical solution:
[0017] The pipe is equipped with a filter screen.
[0018] As a further description of the above technical solution:
[0019] A fixing ring is provided on the outside of the pipe, and two fixing blocks are symmetrically arranged on the top of the fixing ring. Bolts are threadedly connected between the interiors of the two fixing blocks.
[0020] As a further description of the above technical solution:
[0021] The top of the fixing ring is provided with multiple bolts.
[0022] This utility model has the following beneficial effects:
[0023] 1. In this utility model, through the design of sliding block, connecting rod, insert post, fixing block and fixing cylinder, when placing granular objects, the worker pulls the pull ring to open the cover plate. At the same time, the sliding block at one end of the cover plate drives the connecting rod to move to the designated position. When the fixed cylinder inside the fixing block is inserted into the opening groove inside the fixing ring for fixing, the cover plate is quickly fixed.
[0024] 2. In this utility model, with the coordinated structure of water tank, water pipe, water pump, cooling ring, and collection box, after the hydrogen fluoride crystals are purified, the hydrogen fluoride crystals enter the fixed block set inside the collection box through the pipe. At the same time, the water pump draws water from the water tank and delivers it to the cooling ring set inside the collection box through the water pipe. The cooling ring cools the hydrogen fluoride crystals on the top fixed block and filters impurities through the filter screen. Attached Figure Description
[0025] Figure 1 This is a three-dimensional schematic diagram of a high-efficiency hydrogen fluoride purification device proposed in this utility model.
[0026] Figure 2 This is a schematic diagram of the sliding block of a high-efficiency hydrogen fluoride purification device proposed in this utility model.
[0027] Figure 3 This is a schematic diagram of the cooling ring structure of a high-efficiency hydrogen fluoride purification device proposed in this utility model;
[0028] Figure 4 This is a schematic diagram of the fixed block structure of a high-efficiency hydrogen fluoride purification device proposed in this utility model.
[0029] Legend:
[0030] 1. Disc; 2. Heater; 3. Support column; 4. Tank; 5. Cover plate; 6. Fixing ring; 7. Exhaust pipe; 8. Pipe; 9. Fixing ring; 10. Collection box; 11. Water pipe one; 12. Water pump; 13. Water tank; 14. Cylinder; 15. Pull ring; 16. Sliding block one; 17. Insert post one; 18. Connecting rod; 19. Insert post two; 20. Sliding block two; 21. Fixing block; 22. Fixing cylinder; 23. Filter screen; 24. Cooling ring; 25. Fixing block; 26. Water pipe two; 27. Collection water tank. Detailed Implementation
[0031] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.
[0032] Reference Figures 1-3An embodiment of this utility model provides a high-efficiency hydrogen fluoride purification device, comprising a disc 1, a tank 4 fixedly connected to the top of the disc 1, a fixing ring 6 fixedly connected to the top of the tank 4, a cover plate 5 rotatably connected to the top of the fixing ring 6, a fixing mechanism provided on the top of the fixing ring 6, a pipe 8 installed on the side wall of the tank 4, a collection box 10 provided at the end of the pipe 8 away from the tank 4, a cooling mechanism provided inside the collection box 10, the cooling mechanism including a water pump 12, a water pipe 11 fixedly connected to the output end of the water pump 12, a cooling ring 24 fixedly connected to the end of the water pipe 11 away from the water pump 12, a water pipe 26 fixedly connected to one end of the cooling ring 24, a water collection tank 27 fixedly connected to the outside of the water pipe 26, and a water tank 13 connected to the input end of the water pump 12 on the side wall of the cooling ring 24 through the pipe 8.
[0033] Specifically, the device includes a disc 1, a tank 4 fixedly connected to the top of the disc 1, a fixing ring 6 fixedly connected to the top of the tank 4, which secures the device during operation. A cover plate 5 is rotatably connected to the top of the fixing ring 6, and a fixing mechanism is provided on the top of the fixing ring 6 to quickly fix the cover plate 5. A pipe 8 is installed on the side wall of the tank 4, and a collection box 10 is provided at the end of the pipe 8 away from the tank 4. After purification, the liquid crystals enter the collection box 10 through the pipe 8. A cooling mechanism is provided inside the collection box 10 to cool the crystals. The mechanism includes a water pump 12, with a water pipe 11 fixedly connected to the output end of the water pump 12. During cooling, the water pump 12 draws water from the water tank 13. A cooling ring 24 is fixedly connected to the end of the water pipe 11 away from the water pump 12. A water pipe 26 is fixedly connected to one end of the cooling ring 24. After cooling, the water flows through the water pipe 26 into the collection tank 27. The outside of the water pipe 26 is fixedly connected to the side wall of the cooling ring 24. The input end of the water pump 12 is connected to the water tank 13 through a pipe 8. During cooling, water is transported to the cooling ring 24 through the pipe 8 for cooling.
[0034] Reference Figures 1-3 The fixed structure includes a sliding block 16, with a post 17 inside the sliding block 16. A connecting rod 18 is rotatably connected to the outside of the post 17. One end of the connecting rod 18 is rotatably connected to a post 19. A sliding block 20 is provided outside the post 19. Fixed blocks 21 are symmetrically connected to both sides of the sliding block 16. A fixed cylinder 22 is provided inside the fixed block 21.
[0035] Specifically, the fixing structure includes a sliding block 16, with a post 17 inside the sliding block 16. During operation, the connecting rod 18 rotates inside the post 17 inside the sliding block 16. The connecting rod 18 is rotatably connected to the outside of the post 17. One end of the connecting rod 18 is rotatably connected to a post 19. During the rotation, one end of the connecting rod 18 rotates in the post 19. A sliding block 20 is provided on the outside of the post 19. Fixing blocks 21 are symmetrically connected on both sides of the sliding block 16. Fixing cylinders 22 are provided inside the fixing blocks 21. When the cover plate 5 reaches the designated position, it is inserted through the fixing cylinders 22 inside the fixing blocks 21 on the outside of the sliding block 16.
[0036] Reference Figures 1-3 A heater 2 is provided at the center of the bottom of the disc 1, and multiple support columns 3 are arranged around the bottom of the disc 1.
[0037] Specifically, a heater 2 is provided at the center of the bottom of the disc 1, and multiple support columns 3 are arranged around the bottom of the disc 1. The support columns 3 at the bottom provide fixed support when the machine is working.
[0038] Reference Figures 1-3 The top of the can 4 is fixedly connected to an exhaust pipe 7.
[0039] Specifically, an exhaust pipe 7 is fixedly connected to the top of the tank 4, and exhaust is carried out through the exhaust pipe 7 at the top of the tank 4 during the purification process.
[0040] Reference Figures 1-3 A sliding block 16 is provided on the outer side of the cover plate 5, and a cylinder 14 is fixedly connected to the top of the cover plate 5. A pull ring 15 is fixedly connected to the top of the cylinder 14.
[0041] Specifically, a sliding block 16 is provided on the outer side of the cover plate 5, and a cylinder 14 is fixedly connected to the top of the cover plate 5. A pull ring 15 is fixedly connected to the top of the cylinder 14. The pull ring 15 drives the cover plate 5 to open for material discharge.
[0042] Reference Figures 1-3 The inside of pipe 8 is equipped with a filter screen 23.
[0043] Specifically, a filter screen 23 is installed inside the pipe 8. After the liquid crystals are purified, impurities are filtered out through the filter screen 23 installed inside the pipe 8.
[0044] Reference Figures 1-4 A fixing ring 9 is provided on the outside of the pipe 8. Two fixing blocks 25 are symmetrically arranged on the top of the fixing ring 9. Bolts are threadedly connected between the interior of the two fixing blocks 25.
[0045] Specifically, a fixing ring 9 is provided on the outside of the pipe 8. Two fixing blocks 25 are symmetrically arranged on the top of the fixing ring 9. The two fixing blocks 25 are used for assembly and disassembly. Bolts are threaded between the two fixing blocks 25. When the fixing ring 9 is assembled, the fixing blocks 25 at the top are fixed by the internal bolts.
[0046] Reference Figures 1-3 The top of the fixing ring 6 is provided with multiple bolts.
[0047] Specifically, the top of the fixing ring 6 is provided with multiple bolts, and the fixing ring 6 is fixed by the bolts on the top during fixing.
[0048] Working principle: When the machine is started and hydrogen fluoride crystals are added into the tank 4, the worker pulls the pull ring 15 to open the bottom cover 5. At the same time, the sliding block 16 at one end of the cover 5 moves the connecting rod 18 on the outside of the insert 17. When it reaches the designated position, the fixing cylinder 22 inside the fixing block 21 on both sides of the sliding block 16 is inserted into the opening groove set inside the fixing ring 6 for fixation. When the hydrogen fluoride crystals enter the tank 4, the heater 2 at the bottom heats and purifies them. During the purification process, the exhaust is vented through the exhaust pipe 7 at the top of the tank 4. After the liquid crystals are purified, they are filtered for impurities through the filter screen 23 set inside the pipe 8. After the impurities are filtered, they enter the fixing block 25 inside the collection tank 10. The water pump 12 draws water from the water tank 13 and delivers it to the cooling ring 24 at the bottom of the collection tank 10 through the water pipe 11. The cooling ring 24 cools and lowers the temperature of the filtered hydrogen fluoride crystals on the fixing block 25. The cooled water flows back to the collection water tank 27 through the water pipe 26.
[0049] Finally, it should be noted that the above description is only a preferred embodiment of the present utility model and is not intended to limit the present utility model. Although the present utility model has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments or make equivalent substitutions for some of the technical features. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present utility model should be included within the protection scope of the present utility model.
Claims
1. A device for the high-efficiency purification of hydrogen fluoride comprising a disc (1), characterized in that: A can (4) is fixedly connected to the top of the disc (1). A fixed ring (6) is fixedly connected to the top of the can (4). A cover plate (5) is rotatably connected to the top of the fixed ring (6). A fixing mechanism is provided on the top of the fixed ring (6). A pipe (8) is installed on the side wall of the can (4). A collection box (10) is provided at the end of the pipe (8) away from the can (4). A cooling mechanism is provided inside the collection box (10). The cooling mechanism includes a water pump (12). A water pipe (11) is fixedly connected to the output end of the water pump (12). A cooling ring (24) is fixedly connected to the end of the water pipe (11) away from the water pump (12). A water pipe (26) is fixedly connected to the end of the cooling ring (24). A water collection tank (27) is fixedly connected to the outside of the water pipe (26). A water tank (13) is connected to the input end of the water pump (12) through the pipe (8).
2. The hydrogen fluoride high-efficiency purification device according to claim 1, characterized in that: The fixing mechanism includes a sliding block (16), inside which is a plug (17), and a connecting rod (18) is rotatably connected to the outside of the plug (17). One end of the connecting rod (18) is rotatably connected to a plug (19), and a sliding block (20) is provided on the outside of the plug (19). Fixing blocks (21) are symmetrically connected on both sides of the sliding block (16), and a fixing cylinder (22) is provided inside the fixing block (21).
3. The hydrogen fluoride high-efficiency purification device according to claim 1, characterized in that: A heater (2) is provided at the bottom center of the disc (1), and multiple support columns (3) are arranged around the bottom of the disc (1).
4. The hydrogen fluoride high-efficiency purification device according to claim 1, characterized in that: An exhaust pipe (7) is fixedly connected to the top of the can (4).
5. The hydrogen fluoride high-efficiency purification device according to claim 1, characterized in that: A sliding block (16) is provided on the outer side of the cover plate (5), and a cylinder (14) is fixedly connected to the top of the cover plate (5). A pull ring (15) is fixedly connected to the top of the cylinder (14).
6. The hydrogen fluoride high-efficiency purification device according to claim 1, characterized in that: The inside of the pipe (8) is equipped with a filter screen (23).
7. The hydrogen fluoride high-efficiency purification device according to claim 1, characterized in that: A fixing ring (9) is provided on the outside of the pipe (8), and two fixing blocks (25) are symmetrically arranged on the top of the fixing ring (9). Bolts are threadedly connected between the interiors of the two fixing blocks (25).
8. The hydrogen fluoride high-efficiency purification device according to claim 1, characterized in that: The top of the fixed ring (6) is provided with multiple bolts.