Pressure and temperature adjustable synthesis device for producing silicone resin
By introducing components such as a pressure pump, electronic pressure gauge, pressure relief pipe, jacket, internal heating element, and temperature sensor into the silicone resin synthesis equipment, the problem of inaccurate pressure and temperature regulation was solved, enabling real-time monitoring and precise control of parameters inside the reactor, thereby improving the uniformity and quality of silicone resin synthesis.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- SUQIAN TONGCHUAN CHEM TECH CO LTD
- Filing Date
- 2025-06-27
- Publication Date
- 2026-07-10
AI Technical Summary
Existing silicone resin synthesis equipment lacks efficient and precise pressure and temperature control mechanisms, resulting in uneven reactions and unstable product quality.
The system employs components such as a pressure pump, electronic pressure gauge, pressure relief pipe, jacket, internal heating element, temperature controller, and temperature sensor to achieve real-time monitoring and precise control of pressure and temperature inside the vessel. The combined design of the stirring components optimizes the material mixing effect.
Precise control of pressure and temperature inside the reactor was achieved, which improved the uniformity of the reaction and the quality of the product, and increased the synthesis efficiency and yield of silicone resin.
Smart Images
Figure CN224475009U_ABST
Abstract
Description
Technical Field
[0001] This application relates to the field of silicone resin synthesis technology, and more specifically to a pressure and temperature adjustable synthesis apparatus for the production of organosilicon resin. Background Technology
[0002] Silicone resins are a class of polymeric compounds with polysiloxane as the main chain structure and alternating organic groups and silicon-oxygen bonds (Si–O–Si) in their molecules. They are typical organic-inorganic hybrid materials. Due to their highly cross-linked molecular structure, silicone resins combine the flexibility of organic resins with the stability of inorganic materials. They possess excellent properties such as high temperature resistance, cold resistance, weather resistance, strong electrical insulation, hydrophobic surface, and anti-sticking and mold-release properties. Therefore, they are widely used in many fields such as electronics, aerospace, automotive industry, architectural coatings, and mold manufacturing.
[0003] In the production of silicone resins, the siloxane chain structure is typically constructed through reactions such as hydrolytic condensation or cyclic ring-opening polymerization, and further cross-linking forms a thermosetting network structure. This process places extremely high demands on the stability of the reaction environment, especially the pressure and temperature control within the reaction chamber. Reaction pressure and temperature are key factors affecting the reaction rate, degree of condensation, and the performance of the final product.
[0004] However, existing silicone resin synthesis equipment typically lacks efficient and precise pressure and temperature control mechanisms, making it difficult to monitor and regulate changes in key parameters during the reaction process in real time. On the one hand, improper pressure control may lead to gas escape from the reaction chamber or uneven distribution of reactants, thus affecting the uniformity of the reaction and the molecular structure of the product. On the other hand, imprecise temperature control can cause the reaction rate to be too slow or the reaction to overheat, affecting the yield and quality of the silicone resin. Utility Model Content
[0005] In view of the shortcomings of the existing technology, the purpose of this application is to provide a pressure and temperature adjustable synthesis apparatus for the production of organosilicon resin, so as to solve the problems mentioned in the background art.
[0006] According to one aspect of this application, a pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin includes a vessel body, a lid, a stirring assembly, a feed pipe, a pressure pump, an electronic pressure gauge, a pressure relief pipe, a jacket, an inner disc-type heating element, a temperature controller, and a temperature sensor. The vessel body is cylindrical, with a closed bottom and an open top. The top opening of the vessel body is fixedly and sealed to the lid. A stirring assembly is fixedly installed on the lid, extending into the interior of the vessel body. A feed pipe is fixedly provided on the lid and communicates with the interior of the vessel body. A pressure pump is fixedly installed on the lid, with its outlet pipe communicating with the interior of the vessel body. An electronic pressure gauge is fixedly installed on the lid, and the probe of the electronic pressure gauge... The pressure relief pipe is fixedly installed on the cover of the vessel body, extending into the interior of the vessel body. The pressure relief pipe is connected to the interior of the vessel body and a pressure relief solenoid valve is fixedly installed on it. The electronic pressure gauge is electrically connected to the pressurizing pump and the pressure relief solenoid valve respectively. A jacket is fixedly installed on the outer wall of the vessel body along its circumference. A hollow cavity is formed between the inner side wall of the jacket and the outer wall of the vessel body. An inner disc heating tube is arranged in the hollow cavity and is in contact with the outer wall of the vessel body. A temperature controller is fixedly installed on the outer wall of the jacket. Several temperature sensors are fixedly installed on the side wall of the jacket along its circumference. The probes of the temperature sensors extend into the interior of the vessel body. The temperature controller is electrically connected to the temperature sensors and the inner disc heating tube respectively.
[0007] Preferably, the temperature sensors are distributed in two layers along the axial direction of the vessel body, with four temperature sensors in each layer. The four temperature sensors in each layer are equidistant from each other along the circumference of the vessel body, and the distance between the temperature sensors in the upper and lower layers is half the internal height of the vessel body.
[0008] Preferably, the stirring assembly includes a drive motor, a stirring shaft, a frame-type stirring blade, an axial-flow blade, and a spiral stirring paddle. The drive motor is fixedly installed at the center of the top of the cover. The output shaft of the drive motor passes through the top of the cover and is fixedly connected to the upper end of the stirring shaft. The stirring shaft extends axially along the vessel body and its lower end is located above the bottom of the vessel body. The frame-type stirring blade, the axial-flow blade, and the spiral stirring paddle are fixedly installed on the stirring shaft along its axial direction. The outer shape of the frame-type stirring blade is adapted to the inner sidewall of the vessel body and the two slide in contact. The frame-type stirring blade is recessed inward at the height corresponding to the temperature sensor. The axial-flow blade is horizontally arranged, and the spiral stirring paddle is arranged along the axial direction of the stirring shaft.
[0009] Preferably, the axis of the stirring shaft coincides with the axis of the vessel body, and the frame-type stirring blade, axial flow blade and spiral stirring paddle are fixedly mounted on the stirring shaft from top to bottom. The upper end of the frame-type stirring blade is fixedly connected to the upper part of the stirring shaft and its lower end is not connected. The lower end of the spiral stirring paddle is located above the bottom of the frame-type stirring blade.
[0010] Preferably, a discharge pipe is fixedly provided at the bottom of the vessel body, the discharge pipe is set off from the center of the bottom of the vessel body, and a discharge control valve is provided on the discharge pipe.
[0011] Preferably, an observation window is fixedly and sealed at the top of the feed pipe.
[0012] Preferably, a support leg is fixedly provided at the bottom of the vessel body.
[0013] The advantages of this application compared to existing technologies are:
[0014] 1. By setting up a pressure pump, electronic pressure gauge and pressure relief pipe, the pressure inside the synthesis reactor can be monitored and precisely controlled in real time.
[0015] 2. The temperature control system, consisting of a jacket, an inner disc heating tube, a temperature controller, and a temperature sensor, can efficiently and accurately regulate the temperature inside the vessel.
[0016] 3. The combined design of frame-type stirring blades, axial flow blades, and spiral stirring paddles in the stirring assembly greatly optimizes the stirring effect of the synthesized materials. Attached Figure Description
[0017] Figure 1 This is a perspective view of a pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin according to an embodiment of this application.
[0018] Figure 2 This is a cross-sectional perspective view of a pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin according to an embodiment of this application.
[0019] Figure 3 This is a main cross-sectional view of a pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin according to an embodiment of this application.
[0020] Reference numerals: 1. Vessel body; 2. Cover body; 3. Stirring assembly; 31. Drive motor; 32. Stirring shaft; 33. Frame-type stirring blade; 331. Clearance groove; 34. Axial flow blade; 35. Spiral stirring paddle; 4. Feed pipe; 5. Pressure pump; 6. Electronic pressure gauge; 7. Pressure relief pipe; 8. Jacket; 9. Inner disc heating element; 10. Temperature controller; 11. Temperature sensor; 12. Pressure relief solenoid valve; 13. Discharge pipe; 14. Discharge control valve; 15. Observation window; 16. Support leg. Detailed Implementation
[0021] To make the content of this application easier to understand, the technical solutions in the embodiments of this application will be clearly and completely described below with reference to the accompanying drawings. It should be noted that the terms "front," "rear," "left," "right," "upper," and "lower" used in the following description refer to the accompanying drawings. Figure 3 In the context of direction, the terms "inside" and "outside" refer to directions toward or away from the geometric center of a specific component, respectively.
[0022] like Figures 1-3 As shown, a pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin includes a vessel body 1, a cover body 2, a stirring assembly 3, a feed pipe 4, a pressure pump 5, an electronic pressure gauge 6, a pressure relief pipe 7, a jacket 8, an inner disc heating element 9, a temperature controller 10, and a temperature sensor 11. The vessel body 1 has a cylindrical structure, with a support leg 16 fixedly installed at the bottom. The bottom of the vessel body 1 is closed, and its top is open. The top opening of the vessel body 1 is fixedly and sealed to the cover body 2. The feed pipe 4 is fixedly installed on the cover body 2 and communicates with the interior of the vessel body 1. An observation window 15 is fixedly and sealed at the top of the feed pipe 4. The pressure pump 5 is fixedly installed on the cover body 2, and the outlet pipe of the pressure pump 5 communicates with the interior of the vessel body 1. An electronic pressure gauge 6 is fixedly installed on the cover body 2. The probe extends into the interior of the reactor body 1. A pressure relief pipe 7 is fixedly installed on the cover 2, and the pressure relief pipe 7 is connected to the interior of the reactor body 1 and a pressure relief solenoid valve 12 is fixedly installed on it. An electronic pressure gauge 6 is electrically connected to the pressurizing pump 5 and the pressure relief solenoid valve 12 respectively. In the above design, by setting up the pressurizing pump 5, the electronic pressure gauge 6 and the pressure relief pipe 7, the pressure inside the synthesis reactor can be monitored and precisely controlled in real time. The electronic pressure gauge 6 monitors the pressure inside the reactor in real time and feeds the data back to the pressurizing pump 5 and the pressure relief solenoid valve 12. When the pressure is insufficient, the pressurizing pump 5 automatically starts to replenish gas into the reactor to ensure that the pressure inside the reactor is stable. When the pressure is too high, the pressure relief solenoid valve 12 opens quickly and releases excess gas through the pressure relief pipe 7 to prevent gas from escaping from the synthesis reactor or uneven distribution of the synthesized product, thus effectively improving product quality.
[0023] A jacket 8 is fixedly installed circumferentially on the outer wall of the vessel body 1. A hollow cavity is formed between the inner wall of the jacket 8 and the outer wall of the vessel body 1. An inner disc heating tube 9 is installed in the hollow cavity and is in contact with the outer wall of the vessel body 1. A temperature controller 10 is fixedly installed on the outer wall of the jacket 8. Several temperature sensors 11 are fixedly installed circumferentially on the side wall of the jacket 8. The temperature sensors 11 are distributed in two layers along the axial direction of the vessel body 1, with four temperature sensors 11 in each layer. The four temperature sensors 11 in each layer are equidistant from each other circumferentially on the vessel body 1. The distance between the two layers of temperature sensors 11 is half the internal height of the vessel body 1. The probe of each temperature sensor 11 extends into the interior of the vessel body 1. The temperature controller 10 is electrically connected to the temperature sensor 11 and the inner disc heating tube 9. In the above design, the temperature control system composed of the jacket 8, the inner disc heating tube 9, the temperature controller 10, and the temperature sensor 11 can efficiently and accurately regulate the synthesis temperature. The multi-layer temperature sensors 11 distributed along the circumference and axis of the reactor body 1 can monitor the temperature changes at different locations inside the reactor in real time and transmit the data to the temperature controller 10. The temperature controller 10 intelligently adjusts the power of the inner disc heating tube 9 according to the difference between the set temperature and the actual monitored temperature to ensure that the temperature inside the reactor is always maintained within the set range, avoiding slow synthesis rate or overheating inside the reactor due to imprecise temperature control, thereby improving the synthesis efficiency and quality of silicone resin.
[0024] A stirring assembly 3 is fixedly installed on the cover 2. The stirring assembly 3 includes a drive motor 31, a stirring shaft 32, frame-type stirring blades 33, axial flow blades 34, and a spiral stirring paddle 35. The drive motor 31 is fixedly installed at the center of the top of the cover 2. The output shaft of the drive motor 31 passes through the top of the cover 2 and is fixedly connected to the upper end of the stirring shaft 32. The stirring shaft 32 extends axially along the vessel body 1, and its lower end is located above the bottom of the vessel body 1. The axis of the stirring shaft 32 coincides with the axis of the vessel body 1. A frame-type stirring blade 33, an axial flow blade 34, and a spiral stirring paddle 35 are fixedly mounted sequentially from top to bottom along the axial direction of the shaft 32. The upper end of the frame-type stirring blade 33 is fixedly connected to the upper part of the stirring shaft 32, while its lower end is not connected. The outer shape of the frame-type stirring blade 33 is adapted to the inner wall of the vessel body 1, and the two slide in contact. A relief groove 331 is recessed inward on the frame-type stirring blade 33 at the height corresponding to the installation of the temperature sensor 11, so that the frame-type stirring blade 33 can rotate to avoid the temperature sensor. To avoid interference between the two, the axial flow blades 34 and the spiral impeller 35 are arranged horizontally along the axial direction of the stirring shaft 32, with the lower end of the spiral impeller 35 positioned above the bottom of the frame-type stirring blades 33. In the above design, the combined design of the frame-type stirring blades 33, axial flow blades 34, and spiral impeller 35 in the stirring assembly 3 greatly optimizes the stirring effect of the synthesized materials. The outer side of the frame-type stirring blades 33 slides in contact with the inner wall of the vessel body 1, which can effectively scrape off the material adhering to the vessel wall and prevent the material from sticking to the wall. The horizontal arrangement of the axial flow blades 34 enables the material to be fully mixed in the horizontal direction. The spiral impeller 35 promotes the axial flow of the material. The three stirring components work together to achieve full mixing of the material in all directions and at multiple angles in the vessel, improving the uniformity and efficiency of the synthesis. At the same time, the avoidance groove 331 design on the frame-type stirring blades 33 cleverly avoids interference with the temperature sensor 11 probe, ensuring the normal operation of the stirring assembly 3 and the temperature monitoring system.
[0025] A discharge pipe 13 is fixedly provided at the bottom of the vessel body 1. The discharge pipe 13 is set off from the center of the bottom of the vessel body 1. This design allows the opening of the discharge pipe 13 to avoid the rotation axis of the frame-type stirring blade 33, so as to facilitate smooth discharge. A discharge control valve 14 is provided on the discharge pipe 13. In this design, the discharge pipe 13 is set off from the center of the bottom of the vessel body 1, which effectively avoids the rotation axis of the frame-type stirring blade 33, making the discharge process smoother, avoiding the obstruction of the stirring blade and the resulting poor discharge or residue, improving production efficiency, reducing material waste, and facilitating the collection and processing of subsequent products.
[0026] The above embodiments are only used to illustrate the technical solutions of the embodiments of this application, and are not intended to limit them. Although the embodiments of this application have been described in detail with reference to the foregoing embodiments, those skilled in the art should understand that modifications can still be made to the technical solutions described in the foregoing embodiments, or equivalent substitutions can be made to some of the technical features, without departing from the spirit and scope defined by the claims of this application.
Claims
1. A pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin, comprising a vessel body (1), a cover body (2), a stirring assembly (3), a feed pipe (4), a pressure pump (5), an electronic pressure gauge (6), a pressure relief pipe (7), a jacket (8), an inner disc heating element (9), a temperature controller (10), and a temperature sensor (11), characterized in that, The vessel body (1) is cylindrical, with a closed bottom and an open top. The top opening of the vessel body (1) is fixedly and sealed to the cover (2). A stirring assembly (3) is fixedly installed on the cover (2), extending into the interior of the vessel body (1). A feed pipe (4) is fixedly installed on the cover (2) and connected to the interior of the vessel body (1). A pressure pump (5) is fixedly installed on the cover (2), with its outlet pipe connected to the interior of the vessel body (1). An electronic pressure gauge (6) is fixedly installed on the cover (2), with its probe extending into the interior of the vessel body (1). A pressure relief pipe (7) is fixedly installed on the cover (2) and connected to the interior of the vessel body (1). A pressure relief solenoid valve (12) is fixedly installed on it. The electronic pressure gauge (6) is electrically connected to the pressure pump (5) and the pressure relief solenoid valve (12) respectively. A jacket (8) is fixedly provided on the outer side wall of the vessel body (1) along its circumference. A hollow cavity is formed between the inner side wall of the jacket (8) and the outer side wall of the vessel body (1). An inner disc heating tube (9) is provided in the hollow cavity and the inner disc heating tube (9) is in contact with the outer side wall of the vessel body (1). A temperature controller (10) is fixedly installed on the outer side wall of the jacket (8). Several temperature sensors (11) are fixedly installed on the side wall of the jacket (8) along its circumference. The probe of the temperature sensor (11) extends into the interior of the vessel body (1). The temperature controller (10) is electrically connected to the temperature sensor (11) and the inner disc heating tube (9) respectively.
2. The pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin according to claim 1, characterized in that, Several temperature sensors (11) are distributed in two layers along the axial direction of the vessel body (1). There are four temperature sensors (11) in each layer, and the four temperature sensors (11) in each layer are equidistant from each other along the circumference of the vessel body (1). The distance between the temperature sensors (11) in the upper and lower layers is half the internal height of the vessel body (1).
3. The pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin according to claim 1, characterized in that, The stirring assembly (3) includes a drive motor (31), a stirring shaft (32), a frame-type stirring blade (33), an axial flow blade (34), and a spiral stirring paddle (35). The drive motor (31) is fixedly installed at the center of the top of the cover (2). The output shaft of the drive motor (31) passes through the top of the cover (2) and is fixedly connected to the upper end of the stirring shaft (32). The stirring shaft (32) extends axially along the vessel body (1) and its lower end is located above the bottom of the vessel body (1). (32) A frame-type stirring blade (33), an axial flow blade (34) and a spiral stirring paddle (35) are fixedly provided along its axial direction. The outer shape of the frame-type stirring blade (33) is adapted to the inner side wall of the vessel body (1) and the two slide in contact. A relief groove (331) is recessed inward at the height corresponding to the temperature sensor (11). The axial flow blade (34) is horizontally arranged. The spiral stirring paddle (35) is arranged along the axial direction of the stirring shaft (32).
4. The pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin according to claim 3, characterized in that, The axis of the stirring shaft (32) coincides with the axis of the vessel body (1). The frame-type stirring blade (33), the axial flow blade (34), and the spiral stirring paddle (35) are fixedly mounted on the stirring shaft (32) from top to bottom. The upper end of the frame-type stirring blade (33) is fixedly connected to the upper part of the stirring shaft (32), and its lower end is not connected. The lower end of the spiral stirring paddle (35) is located above the bottom of the frame-type stirring blade (33).
5. The pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin according to claim 1, characterized in that, The bottom of the vessel body (1) is fixedly provided with a discharge pipe (13), which is offset from the center of the bottom of the vessel body (1). A discharge control valve (14) is provided on the discharge pipe (13).
6. The pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin according to claim 1, characterized in that, The top of the feed pipe (4) is fixedly sealed with an observation window (15).
7. The pressure- and temperature-adjustable synthesis apparatus for producing organosilicon resin according to claim 1, characterized in that, The bottom of the vessel body (1) is fixedly provided with a support leg (16).