A reaction device for a damascone cyclization process

Abstract

The utility model discloses a kind of amberket cyclization process reaction devices, it is related to chemical equipment technical field, including platform, platform top surface is equipped with processing barrel, platform bottom is fixedly connected with apron, apron is communicated, filter assembly is provided in apron, processing barrel bottom is communicated with filter assembly, apron side is provided with protective box, protective box is fixedly connected with platform, drive assembly is installed in protective box, drive assembly is transmission connection with filter assembly, apron below is provided with collection box.The utility model in the processing barrel is used to carry out amberket cyclization reaction related processing operation, apron provides mounting space for filter assembly, drive assembly provides power for filter assembly, to provide basic device structure for amberket cyclization process reaction and subsequent processing;And the utility model is by the vibration of filter assembly to material is separated, simultaneously drive assembly provides horizontal power, the combination of both greatly improves screening efficiency, and reduces the occurrence of jamming.

Description

Technical Field

[0001] This utility model relates to the field of chemical equipment technology, and in particular to a reaction device for ambroxanone cyclization process. Background Technology

[0002] In the production of ambroxanone, the process involves the synthesis of methyl-3-penten-2-one, a diene addition process, and a cyclization process. The synthesis process of 3-methyl-3-penten-2-one is as follows: under conditions of 35-40℃, butanone and catalyst KGC are added to a strong acid solution, the temperature is raised to 50-70℃, acetaldehyde is added, the mixture is stirred for 2-4 hours, cooled to room temperature, and the pH is adjusted to neutral. Ambroxanone has a unique, mellow, and soft woody and amber aroma. As a flavoring agent and fixative, it is widely used in perfumes, cosmetics, soaps, detergents, and other daily chemical products. In addition to its use in daily chemical fragrances, ambroxanone can also be used in tobacco flavoring. As an important component and additive in tobacco flavorings, it has a good effect on improving the aroma quality of tobacco.

[0003] Existing reaction devices use vibration to screen materials, but single vibration is inefficient and insufficient for screening large residues, and is prone to clogging.

[0004] Therefore, this invention provides a reaction apparatus for ambroxanone cyclization process to solve the problems existing in the prior art. Utility Model Content

[0005] To achieve the above objectives, this utility model provides the following solution: This utility model provides a reaction apparatus for ambroxanone cyclization, including a platform, a processing barrel installed on the top surface of the platform, a surrounding plate fixedly connected to the bottom surface of the platform, the surrounding plate being interconnected vertically, a filter assembly disposed within the surrounding plate, the bottom of the processing barrel being connected to the filter assembly, a protective box disposed on one side of the surrounding plate, the protective box being fixedly connected to the platform, a drive assembly installed within the protective box, the drive assembly being drively connected to the filter assembly, and a collection box disposed below the surrounding plate.

[0006] Optionally, the filter assembly includes a sieve frame located directly below the processing barrel. Mounting plates are respectively provided on both sides of the sieve frame, and extension plates are respectively fixedly connected to both sides of the bottom of the sieve frame. The extension plates are slidably connected to the mounting plates, and a power component is drivenly connected to the bottom of the extension plates. The power component is fixedly connected to the mounting plates.

[0007] Optionally, the power component includes a first motor fixedly connected to the mounting plate, the output end of the first motor being fixedly connected to a connecting shaft, the other end of the connecting shaft being rotatably connected to another mounting plate, and eccentric blocks being symmetrically fixedly connected to the connecting shaft, the eccentric blocks being in contact with the extension plate.

[0008] Optionally, one end of a spring is symmetrically fixedly connected to the top of the screen frame, and the other end of the spring is fixedly connected to the top of the mounting plate.

[0009] Optionally, the drive assembly includes a second motor fixedly connected to the inner wall of the protective box. A disk is fixedly connected to the output end of the second motor. An eccentric column is fixedly connected to the disk. One end of the eccentric column is hinged to a hinge rod. The other end of the hinge rod is hinged to the mounting plate. The protective box is provided with a large opening that is adapted to the swing angle of the hinge rod.

[0010] Optionally, limit rods are slidably connected to the four corners of the mounting plate, and the end of the limit rod away from the mounting plate is fixedly connected to the inner wall of the enclosure.

[0011] Optionally, a cleaning device is provided on one side of the screen frame, one end of which extends into the screen frame and scrapes off the internal residue, and a slag collection box for collecting the residue is fixedly connected to the other side of the screen frame.

[0012] Optionally, support legs are fixedly connected to the four corners of the platform's bottom surface.

[0013] This utility model discloses the following technical effects: It includes main components such as a platform, processing barrel, surrounding plate, filter assembly, protective box, drive assembly, and collection box. The processing barrel is used for processing operations related to the ambergris cyclization reaction. The surrounding plate provides installation space for the filter assembly, which performs filtration functions such as solid-liquid separation. The drive assembly provides power to the filter assembly. The collection box is used to collect the filtered product. All components work together to provide a basic device structure for the ambergris cyclization process and subsequent treatment. Furthermore, this utility model uses the vibration of the filter assembly to separate the material, while the drive assembly provides horizontal power. The combination of these two methods greatly improves the screening efficiency and reduces clogging. Attached Figure Description

[0014] The accompanying drawings, which form part of this application, are used to provide a further understanding of this application. The illustrative embodiments and descriptions of this application are used to explain this application and do not constitute an undue limitation of this application. In the drawings:

[0015] Figure 1 This is a schematic diagram of the structure of this utility model;

[0016] Figure 2 This is a schematic diagram of the internal structure of the enclosure panel of this utility model;

[0017] Figure 3 This is a top view of the structure of the protective box of this utility model;

[0018] Figure 4This is a top view of the structure of the sieve frame of this utility model;

[0019] In the diagram: 1. Platform; 2. Processing barrel; 3. Protective box; 4. Support leg; 5. Enclosure; 6. Collection box; 7. Screen frame; 8. Spring; 9. Mounting plate; 10. Limiting rod; 11. First motor; 12. Connecting shaft; 13. Eccentric block; 14. Hinge rod; 15. Second motor; 16. Disc; 17. Eccentric column; 18. Large opening; 19. Slag collection box; 20. Cleaning device. Detailed Implementation

[0020] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0021] To make the above-mentioned objectives, features and advantages of this utility model more apparent and understandable, the utility model will be further described in detail below with reference to the accompanying drawings and specific embodiments.

[0022] Reference Figures 1-4 As shown, this embodiment provides a reaction apparatus for ambergris cyclization process, including a platform 1, a processing barrel 2 installed on the top surface of the platform 1, a surrounding plate 5 fixedly connected to the bottom surface of the platform 1, the surrounding plate 5 being vertically connected, a filter assembly being installed inside the surrounding plate 5, the bottom of the processing barrel 2 being connected to the filter assembly, a protective box 3 being installed on one side of the surrounding plate 5, the protective box 3 being fixedly connected to the platform 1, a drive assembly being installed inside the protective box 3, the drive assembly being connected to the filter assembly via transmission, and a collection box 6 being installed below the surrounding plate 5.

[0023] This invention comprises a platform 1, a processing barrel 2, a surrounding plate 5, a filter assembly, a protective box 3, a drive assembly, and a collection box 6. The processing barrel 2 is used for processing operations related to the ambergris cyclization reaction. The surrounding plate 5 provides installation space for the filter assembly, which performs solid-liquid separation and other filtration functions. The drive assembly provides power to the filter assembly. The collection box 6 is used to collect the filtered product. All components work together to provide a basic device structure for the ambergris cyclization process and subsequent processing. Furthermore, this invention uses the vibration of the filter assembly to separate the material, while the drive assembly provides horizontal power. The combination of these two methods greatly improves the screening efficiency and reduces the occurrence of clogging.

[0024] Further refining the design, the filter assembly includes a screen frame 7 located directly below the processing barrel 2. Mounting plates 9 are positioned on both sides of the screen frame 7, and extension plates are fixedly connected to both sides of the bottom of the screen frame 7. The extension plates are slidably connected to the mounting plates 9, and a power component is driven to the bottom of the extension plates, which is fixedly connected to the mounting plates 9. The screen frame 7, located directly below the processing barrel 2, facilitates the filtration of materials flowing down from the barrel 2. The mounting plates 9 provide mounting support for the screen frame 7 and other components. The extension plates, slidably connected to the mounting plates 9, provide guidance and connection for the movement of the screen frame 7. The power component, fixedly connected to the mounting plates 9, drives the extension plates, thereby moving the screen frame 7. This structural design allows the screen frame 7 to achieve specific movements under power, enhancing the filtration effect and improving filtration efficiency and preventing screen clogging through vibration.

[0025] Further refining the design, the power component includes a first motor 11 fixedly connected to the mounting plate 9. A connecting shaft 12 is fixedly connected to the output end of the first motor 11, and the other end of the connecting shaft 12 is rotatably connected to another mounting plate 9. Eccentric blocks 13 are symmetrically fixedly connected to the connecting shaft 12, and the eccentric blocks 13 contact the extension plate. The power component uses the first motor 11 as the power source, connecting the two mounting plates 9 via the connecting shaft 12 to ensure structural stability. The eccentric blocks 13 are symmetrically fixedly connected to the connecting shaft 12, and they contact the extension plate. When the first motor 11 drives the connecting shaft 12 to rotate, the special shape of the eccentric blocks 13 causes the extension plate to vibrate up and down, thereby causing the screen frame 7 to vibrate. This vibration method effectively improves the filtration speed and quality, allowing materials to pass through the screen frame 7 more quickly while reducing material residue on the screen frame 7.

[0026] Further refining the design, one end of a spring 8 is symmetrically fixedly connected to the top of the screen frame 7, and the other end of the spring 8 is fixedly connected to the top of the mounting plate 9. The spring 8 plays a role in buffering and assisting vibration during the vibration of the screen frame 7. When the screen frame 7 moves downwards, the spring 8 is stretched, providing upward elastic force; when the screen frame 7 moves upwards, the spring 8 is compressed, further enhancing the upward force, making the vibration of the screen frame 7 more stable and effective, and also helping to extend the service life of the screen frame 7 and related components.

[0027] Further refining the design, the drive assembly includes a second motor 15 fixedly connected to the inner wall of the protective box 3. A disc 16 is fixedly connected to the output end of the second motor 15, and an eccentric column 17 is fixedly connected to the disc 16. One end of a hinge rod 14 is hinged to the eccentric column 17, and the other end of the hinge rod 14 is hinged to the mounting plate 9. The protective box 3 has a large opening 18, which accommodates the swing angle of the hinge rod 14. The drive assembly drives the disc 16 to rotate via the second motor 15, causing the eccentric column 17 on the disc 16 to rotate accordingly. The eccentric column 17 is hinged to one end of the hinge rod 14, and the other end of the hinge rod 14 is hinged to the mounting plate 9. This structure converts the rotational motion of the disc 16 into the reciprocating swing motion of the hinge rod 14, thereby driving the mounting plate 9 and the entire filter assembly to reciprocate. This provides another form of power to the filter assembly, allowing for the selection of appropriate drive methods and motion forms according to different process requirements, enhancing the adaptability and flexibility of the device. The protective box 3 is provided with a large opening 18 that is adapted to the swing angle of the hinge rod 14, so that the hinge rod 14 can swing freely without affecting the normal operation of the drive component.

[0028] Further refining the design, limit rods 10 are slidably connected to the four corners of the mounting plate 9, with the end of the limit rod 10 furthest from the mounting plate 9 fixedly connected to the inner wall of the enclosure 5. The limit rods 10 restrict and guide the movement of the mounting plate 9, preventing it from shifting or moving excessively under the action of the drive assembly. This ensures that the mounting plate 9 can only reciprocate linearly along the direction of the limit rods 10, thereby enabling the filter assembly to work stably and accurately, improving the reliability and stability of the device.

[0029] Further refining the design, a cleaning device 20 is installed on one side of the screen frame 7. One end of the cleaning device 20 extends into the screen frame 7 to scrape away the internal residue, while a slag collection box 19 is fixedly connected to the other side of the screen frame 7 to collect the residue. The cleaning device 20 (existing technology, not described in detail) extends into the screen frame 7 to scrape away the internal residue, while the slag collection box 19 is fixedly connected to the other side to collect the residue. This design allows for timely cleaning of the residue inside the screen frame 7 during or after filtration, preventing residue from clogging the screen holes and affecting the filtration effect, ensuring the continuous and effective operation of the screen frame 7. It also facilitates centralized treatment of the residue, improving production efficiency and environmental hygiene.

[0030] Further refining the design, support legs 4 are fixedly connected to the four corners of the bottom surface of platform 1. The support legs 4 provide stable support for the entire device, enabling the device to be placed stably on the work site, reducing the adverse effects on the processing and filtration effect caused by device shaking or instability, and ensuring the smooth progress of the ambergris cyclization process.

[0031] In the description of this utility model, it should be understood that the terms "longitudinal", "lateral", "up", "down", "front", "back", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", etc., indicate the orientation or positional relationship based on the orientation or positional relationship shown in the accompanying drawings. They are only for the convenience of describing this utility model and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation. Therefore, they should not be construed as limitations on this utility model.

[0032] The embodiments described above are merely preferred embodiments of the present utility model and are not intended to limit the scope of the present utility model. Various modifications and improvements made to the technical solutions of the present utility model by those skilled in the art without departing from the spirit of the present utility model should fall within the protection scope defined by the claims of the present utility model.

Claims

1. A reaction apparatus for ambroxanone cyclization process, characterized in that: The system includes a platform (1), a processing barrel (2) installed on the top surface of the platform (1), a surrounding plate (5) fixedly connected to the bottom surface of the platform (1), the surrounding plate (5) being vertically connected, a filter assembly being installed inside the surrounding plate (5), the bottom of the processing barrel (2) being connected to the filter assembly, a protective box (3) being installed on one side of the surrounding plate (5), the protective box (3) being fixedly connected to the platform (1), a drive assembly being installed inside the protective box (3), the drive assembly being connected to the filter assembly in a transmission manner, and a collection box (6) being installed below the surrounding plate (5). The filter assembly includes a sieve frame (7) located directly below the processing barrel (2). Mounting plates (9) are respectively provided on both sides of the sieve frame (7). Extension plates are fixedly connected to both sides of the bottom of the sieve frame (7). The extension plates are slidably connected to the mounting plates (9). A power component is driven to the bottom of the extension plate. The power component is fixedly connected to the mounting plates (9).

2. The ambergris ketone cyclization process reaction apparatus according to claim 1, characterized in that: The power component includes a first motor (11) fixedly connected to the mounting plate (9). The output end of the first motor (11) is fixedly connected to a connecting shaft (12). The other end of the connecting shaft (12) is rotatably connected to another mounting plate (9). An eccentric block (13) is symmetrically fixedly connected to the connecting shaft (12). The eccentric block (13) is in contact with the extension plate.

3. The ambergris ketone cyclization process reaction apparatus according to claim 1, characterized in that: The top of the sieve frame (7) is symmetrically fixedly connected to one end of a spring (8), and the other end of the spring (8) is fixedly connected to the top of the mounting plate (9).

4. The ambergris ketone cyclization process reaction apparatus according to claim 1, characterized in that: The drive assembly includes a second motor (15) fixedly connected to the inner wall of the protective box (3). The output end of the second motor (15) is fixedly connected to a disc (16). An eccentric column (17) is fixedly connected to the disc (16). One end of the eccentric column (17) is hinged to a hinge rod (14). The other end of the hinge rod (14) is hinged to the mounting plate (9). The protective box (3) is provided with a large opening (18). The large opening (18) is adapted to the swing angle of the hinge rod (14).

5. The ambergris ketone cyclization process reaction apparatus according to claim 4, characterized in that: Limiting rods (10) are slidably connected to the four corners of the mounting plate (9), and the end of the limiting rod (10) away from the mounting plate (9) is fixedly connected to the inner wall of the enclosure (5).

6. The ambergris ketone cyclization process reaction apparatus according to claim 1, characterized in that: A cleaning device (20) is provided on one side of the screen frame (7). One end of the cleaning device (20) extends into the screen frame (7) and scrapes off the internal residue. A slag collection box (19) for collecting residue is fixedly connected to the other side of the screen frame (7).

7. The ambergris ketone cyclization process reaction apparatus according to claim 1, characterized in that: The platform (1) has four fixed legs (4) at the four corners of its bottom surface.

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