Low-e coated glass with low reflectivity developed for energy efficiency

Abstract

The invention relates to a coated (20) glass (10) having high visible transmittance and low internal and external reflectivity, configured for use in architectural applications and vehicles.

Description

[0001] LOW-E COATED GLASS WITH LOW REFLECTIVITY DEVELOPED FOR ENERGY EFFICIENCY

[0002] TECHNICAL FIELD

[0003] The invention relates to a low-e coating with infrared reflective layers for use as daylight transmitting and thermal insulating glass.

[0004] PRIOR ART

[0005] One of the factors that differentiate the optical properties of glasses is the coating applications made on the glass surface. One of the coating applications is the magnetic field-assisted sputtering method in a vacuum environment. This method is a frequently used method particularly in the production of architectural and automotive coatings with low-e properties. The transmittance and reflectivity values of the glasses coated with said method in the visible, near-infrared and infrared regions can be obtained at the targeted levels.

[0006] Apart from transmittance and reflectivity values, selectivity is also an important parameter in coated glass. Selectivity is defined in ISO 9050 (2003) as the ratio of the visible region transmittance value to the solar factor. Selectivity values of coatings can also be kept at the targeted levels by the number of Ag layers they comprise, the type of nucleating layer used, and the parametric optimizations of the layers.

[0007] The coating mentioned in the patent with publication number US11565968B2 comprises at least one silver-based functional metallic layer and at least one zinc- based metallic layer located above and / or below the silver-based functional metallic layer. Positioned above and / or below this silver-based functional metallic layer mentioned, there is at least one nickel oxide-based layer separating the zinc-based layer from the functional layer.

[0008] In conclusion, this invention relates to a new coated glass structure achieved in the relevant technical field. BRIEF DESCRIPTION OF THE INVENTION

[0009] The present invention relates to a coated glass for eliminating the above-mentioned disadvantages and bringing new advantages to the relevant technical field.

[0010] The main object of the invention is to provide a coated glass with high transmittance properties.

[0011] Another object of the invention is to provide a coated glass with reduced internal and external reflectivity value.

[0012] Another object of the invention is to provide a coated glass with reduced angular color value variation.

[0013] In order to fulfill all of the aforementioned objects and those that will arise from the detailed description below, the present invention is a coated glass comprising at least one functional layer and having high visible transmittance and low internal and external reflectivity, configured for use in architectural applications and vehicles. Accordingly, the invention is characterized in that, in order to achieve the targeted transmittance and reflectivity, it comprises a first dielectric layer in the form of an oxide with high refractive index and in the thickness range of 12 nm to 35 nm, positioned in contact with the glass; a second dielectric layer containing zinc in the form of an oxide with medium refractive index, positioned on said first dielectric layer; a fourth dielectric layer containing zinc in the form of an oxide with medium refractive index; and a fifth dielectric layer in the form of an oxide or nitride or oxynitride, positioned in contact with said fourth dielectric layer.

[0014] Another preferred embodiment of the invention is that the first dielectric layer comprises at least one or a plurality of the following materials: TiOx, TiNx, TiOxNy, TiSiZrOxNy, NbNx, NbOx, NbOxNy, NbZrOx.

[0015] Another preferred embodiment of the invention is that the fifth dielectric layer comprises Si. Another preferred embodiment of the invention is that the coating comprises at least one first functional layer.

[0016] Another preferred embodiment of the invention is that the coating comprises a second functional layer positioned above the first functional layer when arranged outward from the glass.

[0017] Another preferred embodiment of the invention is that it comprises at least a third dielectric layer between the first functional layer and the second functional layer.

[0018] Another preferred embodiment of the invention is that said third dielectric layer preferably has high refractive index.

[0019] Another preferred embodiment of the invention is that it comprises a barrier layer below said third dielectric layer.

[0020] BRIEF DESCRIPTION OF THE DRAWING

[0021] Fig. 1 shows an overall representative view of the coated glass.

[0022] Fig. 2 shows an alternative representative view of the coated glass.

[0023] Fig. 3 shows another alternative representative view of the coated glass.

[0024] REFERENCE NUMERALS GIVEN IN THE DRAWING

[0025] 10 Coated glass

[0026] 20 Coating

[0027] 21 First Dielectric Layer

[0028] 22 Second Dielectric Layer

[0029] 23 First Functional Layer

[0030] 24 First Barrier Layer

[0031] 25 Third Dielectric Layer

[0032] 26 Second Functional Layer

[0033] 27 Second Barrier Layer 28 Fourth Dielectric Layer

[0034] 29 Fifth Dielectric layer

[0035] DETAILED DESCRIPTION OF THE INVENTION

[0036] In this detailed description, the coated (20) glass (10) subject to the invention is explained by way of example only for a better understanding of the subject, which will not create any limiting effect.

[0037] The production of the multilayer coated (20) glass (10) for architecture and automotive is carried out by the sputtering method. This invention generally relates to multilayer coated (20) glasses (10) used as daylight transmitting and thermal insulating glass (10), and the content and application of said multilayer coating (20). The multilayer coated (20) glass (10) subject to the invention can also be used in double glazing units and laminated structures in the architectural and automotive sectors.

[0038] The term “optical performance” mentioned in the invention refers, for the multilayer coated (20) glass (10) used on the second surface in a double glazing unit, to the visible region light transmittance (hereinafter referred to as %TVis), the total solar energy transmittance, the visible region internal and external reflectivity values, and the CIE L*, a*, b* color values in the case of single glazing. The term high transmittance refers to 68% and above in a double glazing unit. The term low reflectivity refers to 12% and below in a double glazing unit.

[0039] The refractive indices of all layers in the multilayer coated (20) glass (10) subject to the invention were determined using computational methods based on the optical constants obtained from single layer measurements. Said refractive indices are the refractive index data at 550 nm.

[0040] As a result of experimental studies conducted to develop a multilayer coating (20) arrangement that is preferred both in terms of ease of production and optical properties, the following data were determined.

[0041] In order to obtain a multilayer coated (20) glass (10), a multilayer coating (20) consisting of multiple layers of metal, metal oxide, and metal nitride / oxynitride layers located on the surface of glass (10) was developed using the sputtering method. Said layers are deposited on top of each other in a vacuum environment. At least one and / or more of the tempering, partial tempering, annealing, lamination and bending processes can be used together as heat treatment.

[0042] The term high refractive index as used in this invention covers the range from 2.2 to 2.7 The term medium refractive index covers the range from 1.8 to 2.2. The term low refractive index covers values below 1.8.

[0043] The coating (20) subject to the invention comprises at least 1 functional layer. Thanks to said coating (20), the reflectivity values of the coated (20) glass (10) can be reduced.

[0044] In the multilayer coating (20) subject to the invention, a first dielectric layer (21) is positioned on the glass (10). The first dielectric layer (21) is positioned in contact with the glass (10) and comprises at least one layer in the dielectric structure. The first dielectric layer (21) comprises at least one or a plurality of the following materials in combination: SixNy, SiOxNy, ZnAINx, ZnAIOx, ZnAIOxNy, ZnSnNx, ZnSnOx, ZnSnOxNy, TaOx, TaOxNy, TiOx, TiNx, TiOxNy, TiSiZrOxNy, ZrNx, ZrOx, ZrOxNy, SiZrN, SiZrOx, SiZrOxNy, WZrOx, NbNx, NbOx, NbOxNy, NbZrOx. In the preferred embodiment, the first dielectric layer (21) comprises TiOx. In an alternative embodiment, the first dielectric layer (21) comprises NbOx.

[0045] The thickness of the first dielectric layer (21) is between 12 nm and 35 nm. In the preferred embodiment, the thickness of the first dielectric layer (21) is between 15 nm and 31 nm. Most preferably, the thickness of the first dielectric layer (21) is between 18 nm and 28 nm.

[0046] The refractive index of the materials used in the first dielectric layer (21) is between 1.8 and 2.7. In the preferred embodiment, the refractive index of the materials used in the first dielectric layer (21) is between 2.2 and 2.7. Thus, using a higher index material in the first dielectric layer (21) compared to glass (10) helps to reduce the external reflectivity values of coated (20) glass (10).

[0047] A second dielectric layer (22) is positioned on the first dielectric layer (21). Said second dielectric layer (22) comprises at least one or a plurality of the following materials: ZnAINx, ZnAIOx, ZnAIOxNy, ZnSnNx, ZnSnOx, ZnSnOxNy. In the preferred embodiment, the second dielectric layer (22) comprises ZnAIOx.

[0048] The thickness of the second dielectric layer (22) is between 1.5 nm and 15 nm. In the preferred embodiment, the thickness of the first dielectric layer (22) is between 2 nm and 12 nm. Most preferably, the thickness of the first dielectric layer (22) is between 2 nm and 8 nm.

[0049] The second dielectric layer (22) acts as a nucleating layer for a subsequent first functional layer (23). Therefore, the thickness of the second dielectric layer (22) and the coating parameters are important particularly for the electrical properties of the multilayer coating (20). The refractive index of the materials used in the second dielectric layer (22) is between 1.8 and 2.2.

[0050] A first functional layer (23) is positioned on the second dielectric layer (22). Ag layer is used as the first functional layer (23). The thickness of the first functional layer is between 5 nm and 19 nm. In the preferred embodiment, the thickness of the first functional layer (23) is between 5 nm and 16 nm. Most preferably, the thickness of the first functional layer (23) is between 7 nm and 13 nm.

[0051] A first barrier layer (24) is positioned on the first functional layer (23). At least one of NiCr, NiCrOx, TiOx, ZnSnOx, ZnAIOx, ZnOxis used as the first barrier layer (24). In the preferred embodiment, the first barrier layer (24) comprises one of ZnAIOx, NiCr or NiCrOx. In one embodiment of the invention, NiCr is used as the first barrier layer (24). In another alternative embodiment of the invention, NiCrOx is used as the first barrier layer (24). In an embodiment of the invention, ZnAIOx is used as the first barrier layer (24). The first barrier layer (24) serves to prevent deterioration of the functional layer (23) and to maintain its infrared reflective property. Infrared defines the wavelength range of the electromagnetic spectrum between 780 nm and 50 pm.

[0052] If NiCrOx is used as the first barrier layer (24), its thickness is between 0.5 nm and 6 nm. In the preferred embodiment, if NiCrOx is used as the first barrier layer (24), its thickness is between 0.5 nm and 5 nm. Most preferably, if NiCrOx is used as the first barrier layer (24), its thickness is between 1 nm and 3 nm. If NiCr is used as the first barrier layer (24), its thickness is between 0.5 nm and 5 nm. In the preferred embodiment, if NiCr is used as the first barrier layer (24), its thickness is between 0.5 nm and 4 nm. Most preferably, if NiCr is used as the first barrier layer (24), its thickness is between 0.5 nm and 2 nm.

[0053] If ZnAIOx is used as the first barrier layer (24), its thickness is between 2 nm and 8 nm. In the preferred embodiment, if ZnAIOx is used as the first barrier layer (24), its thickness is between 2 nm and 7 nm. Most preferably, if ZnAIOx is used as the first barrier layer (24), its thickness is between 2 nm and 6 nm.

[0054] A third dielectric layer (25) is positioned above the first barrier layer (24). The third dielectric layer (25) comprises at least one or a plurality of the following materials in combination: TiOx, TiNx, TiOxNy, TiSiZrOxNy, NbNx, NbOx, NbOxNy, NbTiOx, NbZrOx.

[0055] The thickness of the third dielectric layer (25) is between 40 nm and 100 nm. In the preferred embodiment, the thickness of the third dielectric layer (25) is between 45 nm and 90 nm. Most preferably, the thickness of the third dielectric layer (25) is between 50 nm and 75 nm. The use of a third dielectric layer (25) with an optical thickness above 100 nm, positioned between the two functional layers, contributes to the reduction of both the internal and external reflectivity values of the coating (20).

[0056] Accordingly, in a preferred embodiment of the invention, a high refractive index material is used as the third dielectric layer (25). In an embodiment of the invention, the third dielectric layer (25) comprises NbOx. In another alternative embodiment, the third dielectric layer (25) comprises NbTiOx.

[0057] A second first functional layer (26) is positioned on the third dielectric layer (25). Ag layer is used as the second functional layer (26). The thickness of the second functional layer (26) is between 6 nm and 20 nm. In the preferred embodiment, the thickness of the second functional layer (26) is between 6 nm and 17 nm. Most preferably, the thickness of the second functional layer (26) is between 8 nm and 14 nm. A second barrier layer (27) is located on the second functional layer (26). At least one of NiCr, NiCrOx, TiOx, ZnSnOx, ZnAIOx, ZnOxis used as the second barrier layer (27). In a preferred embodiment of the invention, ZnAIOx is used as the second barrier layer (27). In another embodiment of the invention, NiCr is used as the second barrier layer (27). In another alternative embodiment of the invention, NiCrOx is used as the second barrier layer (27).

[0058] The thickness of the second barrier layer (27) is between 0.5 nm and 10 nm. In the preferred embodiment, the thickness of the second barrier layer (27) is between 1 nm and 8 nm. Most preferably, the thickness of the second barrier layer (27) is between 2 nm and 7 nm.

[0059] If NiCrOx is used as the second barrier layer (27), its thickness is between 0.5 nm and 6 nm. In the preferred embodiment, if NiCrOx is used as the second barrier layer (27), its thickness is between 0.5 nm and 5 nm. Most preferably, if NiCrOx is used as the second barrier layer (27), its thickness is between 1 nm and 3 nm.

[0060] If NiCr is used as the second barrier layer (27), its thickness is between 0.5 nm and 5 nm. In the preferred embodiment, if NiCr is used as the second barrier layer (27), its thickness is between 0.5 nm and 4 nm. Most preferably, if NiCr is used as the second barrier layer (27), its thickness is between 0.5 nm and 2 nm.

[0061] If ZnAIOx is used as the second barrier layer (27), its thickness is between 0.5 nm and 10 nm. In the preferred embodiment, if ZnAIOx is used as the second barrier layer (27), its thickness is between 1 nm and 8 nm. Most preferably, if ZnAIOx is used as the second barrier layer (27), its thickness is between 2 nm and 7 nm.

[0062] A fourth dielectric layer (28) is positioned above the second barrier layer (27). The fourth dielectric layer (28) comprises at least one or a plurality of the following materials in combination: SixNy, SiOx, SiOxNy, ZnAINx, ZnAIOx, ZnAIOxNy, ZnSnNx, ZnSnOx, ZnSnOxNy, TaOx, TaOxNy, TiOx, TiNx, TiOxNy, TiSiZrOxNy, ZrNx, ZrOx, ZrOxNy, SiZrN, SiZrOx, SiZrOxNy, WZrOx, NbNx, NbOx, NbOxNy, NbZrOx.

[0063] In the preferred embodiment, the fourth dielectric layer (28) comprises ZnSnOx. The thickness of the fourth dielectric layer (28) is between 18 nm and 50 nm. In the preferred embodiment, the thickness of the fourth dielectric layer (28) is between 23 nm and 45 nm. Most preferably, the thickness of the fourth dielectric layer (28) is between 27 nm and 40 nm.

[0064] A fifth dielectric layer (29) is located above the fourth dielectric layer (28). It comprises at least one or a plurality of the following materials in combination as the fifth dielectric layer (29): SixNy, SiOx, SiOxNy, ZnAINx, ZnAIOx, ZnAIOxNy, ZnSnNx, ZnSnOx, ZnSnOxNy, TaOx, TaOxNy, TiOx, TiNx, TiOxNy, TiSiZrOxNy, ZrNx, ZrOx, ZrOxNy, SiZrN, SiZrOx, SiZrOxNy, WZrOx, NbNx, NbOx, NbOxNy, NbZrOx. In the preferred embodiment, the fifth dielectric layer (29) comprises SixNy.

[0065] The thickness of the fifth dielectric layer (29) is between 1 nm and 13 nm. In the preferred embodiment, the thickness of the fifth dielectric layer (29) is between 1 nm and 10 nm. Most preferably, the thickness of the fifth dielectric layer (29) is between 2 nm and 7 nm.

[0066] In the coating (20) subject to the invention, it is crucial to use a first dielectric layer (21) with high refractive index between the glass (10) and the first functional layer (23) and preferably in contact with the glass (10), and a second dielectric layer (22) with low thickness and medium refractive index positioned between said first dielectric layer (21) and the first functional layer (23). In an embodiment of the invention, the second dielectric layer (22) is in contact with the first dielectric layer (21) and the first functional layer (23). This contributes to the reduction of the reflectivity values of the coated (20) glass (10).

[0067] The combination of the fourth dielectric layer (28) and the fifth dielectric layer (29), which are used as the last two layers in the coating (20), similarly contributes to the reduction of the reflectivity values of the coated (20) glass (10). In addition, in this combination, particularly the nitride structure of the fifth dielectric layer (29) increases the resistance of the coating (20) against external mechanical factors. In addition to all above, the fact that the dielectric layers used in the coating (20) are in oxide form contributes to and increases the chemical resistance of the structure.

[0068] In the coating (20) subject to the invention, the optical thickness of the third dielectric layer (25) is above 100 nm, which is crucial for achieving the targeted optical performance. In this context, the ratio of the other dielectric layers to the third dielectric layer (25) is also important. In order to achieve low reflectivity and high transmittance values, the ratio of the optical thickness of the third dielectric layer (25) to the sum of the optical thicknesses of the fourth dielectric layer (28) and the fifth dielectric layer (29) in the coating (20) should be between 1.6 and 2.0. At the same time, the ratio of the optical thickness of the third dielectric layer (25) to the optical thickness of the first dielectric layer (21) should be between 2.3 and 2.7 to achieve similarly low reflectivity and high transmittance values. It is also important that the ratio of the optical thickness of the first dielectric layer (21) to the sum of the optical thicknesses of the fourth dielectric layer (28) and the fifth dielectric layer (29) is below 1.

[0069] When these ratios are achieved, the coating (20) is ensured to have the following properties:

[0070] • Internal and external reflectivity values below 12%,

[0071] • Visible transmittance value above 68%,

[0072] • Angular color variation between 0-75 degrees within ±1 level, and

[0073] • Reflectivity a* value between 0 and -3, and reflectivity b* value between 0 and +3, both on the glass (10) side and on the coating (20) side.

[0074] In this way, glass (10) with neutral tones, high transmittance and low reflectivity coatings (20) can be obtained for aesthetic purposes. The obtained coated (20) glass (10) can have a g value between 25-65%.

[0075] An embodiment of the invention is as follows;

[0076] Glass / first dielectric layer (21) / second dielectric layer (22) / first functional layer (23) / second barrier layer (27) / fourth dielectric layer (28) / fifth dielectric layer (29).

[0077] An example embodiment of the invention is as follows;

[0078] - A glass (10)

[0079] - A first dielectric layer (21) in the form of an oxide with high refractive index

[0080] - A second dielectric layer (22) in the form of an oxide with medium refractive index

[0081] - A first functional layer (23) - A fourth dielectric layer (28) containing zinc in the form of an oxide with medium refractive index

[0082] - A fifth dielectric layer (29) containing Si in the form of oxide or nitride or oxynitride

[0083] Preferably, the first dielectric layer (21) is in contact with the glass (10). Thus, the external reflectivity values of the coated (20) glass (10) are reduced. The fourth dielectric layer (28) is also in contact with the fifth dielectric layer (29). Thus, the optical performance values of the coated (20) glass (10) can be obtained at the targeted levels.

[0084] Accordingly, an embodiment of the invention is as follows;

[0085] - A glass (10)

[0086] - A first dielectric layer (21) comprising at least one or a plurality of the following materials: TiOx, TiNx, TiOxNy, TiSiZrOxNy, NbNx, NbOx, NbOxNy, NbZrOx,

[0087] - A second dielectric layer (22) comprising at least one or a plurality of the following materials: ZnAINx, ZnAIOx, ZnAIOxNy, ZnSnNx, ZnSnOx, ZnSnOxNy,

[0088] - A first functional layer (23) comprising Ag,

[0089] - A second barrier layer (27) comprising at least one of NiCr, NiCrOx, TiOx, ZnSnOx, ZnAIOx, ZnOx,

[0090] - A fourth dielectric layer (28) comprising at least one or a plurality of the following materials: ZnAINx, ZnAIOx, ZnAIOxNy, ZnSnNx, ZnSnOx, ZnSnOxNy,

[0091] - A fifth dielectric layer (29) comprising at least one or a plurality of the following materials: SixNy, SiOxNy, ZnAINx, ZnAIOxNy, ZnSnNx, ZnSnOxNy, TaOxNy, TiNx, TiOxNy, TiSiZrOxNy, ZrNx, ZrOxNy, SiZrN, SiZrOxNy, NbNx, NbOxNy.

[0092] Another embodiment of the invention is as follows;

[0093] Glass / first dielectric layer (21) I second dielectric layer (22) / first functional layer (23) / first barrier layer (24) I third dielectric layer (25) I second functional layer (26) I second barrier layer (27) / fourth dielectric layer (28) / fifth dielectric layer (29).

[0094] Accordingly, an embodiment of the invention is as follows; - A glass (10)

[0095] - A first dielectric layer (21) comprising at least one or a plurality of the following materials: TiOx, TiNx, TiOxNy, TiSiZrOxNy, NbNx, NbOx, NbOxNy, NbZrOx,

[0096] - A second dielectric layer (22) comprising at least one or a plurality of the following materials: ZnAINx, ZnAIOx, ZnAIOxNy, ZnSnNx, ZnSnOx, ZnSnOxNy,

[0097] - A first functional layer (23) comprising Ag,

[0098] - A first barrier layer (24) comprising at least one of NiCr, NiCrOx, TiOx, ZnSnOx, ZnAIOx, ZnOx,

[0099] - A third dielectric layer (25) comprising at least one or a plurality of the following materials: TiOx, TiNx, TiOxNy, TiSiZrOxNy, NbNx, NbOx, NbOxNy, NbTiOx, NbZrOx,

[0100] - A second functional layer (26) comprising Ag,

[0101] - A second barrier layer (27) comprising at least one of NiCr, NiCrOx, TiOx, ZnSnOx, ZnAIOx, ZnOx,

[0102] - A fourth dielectric layer (28) comprising at least one or a plurality of the following materials: SixNy, SiOxNy, SiOx, ZnAINx, ZnAIOx, ZnAIOxNy, ZnSnNx, ZnSnOx, ZnSnOxNy, TaOx, TaOxNy, TiOx, TiNx, TiOxNy, TiSiZrOxNy, ZrNx, ZrOx, ZrOxNy, SiZrN, SiZrOx, SiZrOxNy, WZrOx, NbNx, NbOx, NbOxNy, NbZrOx,

[0103] - A fifth dielectric layer (29) comprising at least one or a plurality of the following materials: SixNy, SiOx, SiOxNy, ZnAINx, ZnAIOx, ZnAIOxNy, ZnSnNx, ZnSnOx, ZnSnOxNy, TaOx, TaOxNy, TiOx, TiNx, TiOxNy, TiSiZrOxNy, ZrNx, ZrOx, ZrOxNy, SiZrN, SiZrOx, SiZrOxNy, WZrOx, NbNx, NbOx, NbOxNy, NbZrOx.

[0104] The scope of protection of the invention is specified in the appended claims and cannot be limited to what is described for illustrative purposes in this detailed description. It is clear that a person skilled in the art can produce similar embodiments in the light of what is explained above, without deviating from the main theme of the invention.

Claims

CLAIMS1. A coated (20) glass (10) comprising at least one functional layer having a high visible transmittance and low internal and external reflectivity, configured for use in architectural applications and vehicles, characterized in that, in order to achieve the targeted transmittance and reflectivity, it comprises a first dielectric layer (21) in the form of an oxide with high refractive index and in the thickness range of 12 nm to 35 nm, positioned in contact with the glass (10); a second dielectric layer (22) containing zinc in the form of an oxide with medium refractive index, positioned on said first dielectric layer (21).

2. A coated (20) glass (10) according to claim 1, characterized in that the first dielectric layer (21) comprises at least one or a plurality of the following materials: TiOx, TiNx, TiOxNy, TiSiZrOxNy, NbNx, NbOx, NbOxNy, NbZrOx.

3. A coated (20) glass (10) according to claim 1, characterized in that the fifth dielectric layer (29) comprises Si.

4. A coated (20) glass (10) according to claim 1, characterized in that the coating comprises at least one first functional layer (23).

5. A coated (20) glass (10) according to claims 1 and 4, characterized in that the coating (20) comprises a second functional layer (26) positioned on the first functional layer (23) when arranged outwardly from the glass (10).

6. A coated (20) glass (10) according to claim 5, characterized in that it comprises at least a third dielectric layer (25) between the first functional layer (23) and the second functional layer (26).

7. A coated (20) glass (10) according to claim 6, characterized in that said third dielectric layer (25) preferably has a high refractive index.

8. A coated (20) glass (10) according to claim 5, characterized in that it comprises a barrier layer (24) below said third dielectric layer (25).

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