Moisturizing composition containing honey extract as well as preparation method and application of moisturizing composition

Abstract

The invention relates to a skin care product, in particular to a moisturizing composition containing a honey extract as well as a preparation method and application of the moisturizing composition. The invention relates to a moisturizing composition containing a honey extract. The moisturizing composition is prepared from 33.5 to 35 parts of propylene glycol dicaprylate / dicaprate, 1 to 3 parts of selammonium chloride hectorite, 0.5 to 2 parts of propylene glycol carbonate, 15 to 18 parts of ethylhexyl palmitate, 9 to 12 parts of hydrogenated coconut oil glycerides, 3.5 to 5 parts of beewax, 3.5 to 5 parts of paraffin, 3 to 5 parts of butyrospermum parkii butter and 2 to 3 parts of meadowfoam seed oil. The composition is prepared from the following raw materials in parts by weight: 20-30 parts of propylene glycol, 0.5-3 parts of butanediol, 17.5-22 parts of honey extract, 8-10 parts of PEG-7 glyceryl cocoate and 2-3 parts of caprylic / capric glyceride polyglycerol-10 esters. 0.1 to 0.5 part of sea buckthorn fruit oil and 0.1 to 0.3 part of essence; the problems of high honey viscosity and foreign body sensation are solved through extraction treatment, and then the moisturizing and anti-aging effects on skin are improved through compatibility of various thickening agents, skin conditioners, emollients and the like.

Description

Technical Field

[0001] The invention relates to skin care products, in particular to a moisturizing composition containing honey extract and a preparation method and application thereof. Background Art

[0002] Research has found that the nourishing ingredients contained in honey can be used for skin conditioning. For example, a Chinese patent discloses a firming and moisturizing mask prepared with West Lake lotus root powder, grape seed essential oil, and honey, application number 201611227171.3, which records: West Lake lotus root powder 0.6-1.4 parts, milk 0.08-0.12 parts, yogurt 0.05-0.15 parts, honey 0.08-0.12 parts, sea duck egg white 0.09-0.11 parts, grape seed essential oil 0.015-0.025 parts; Beneficial effects: The present invention mainly uses West Lake lotus root powder, milk, yogurt, honey, sea duck egg white, and grape seed essential oil, which are seven raw material formulas, without conflicting toxic and side effects, and can effectively dredge, moisturize the skin, replenish moisture, thereby improving skin quality, and has no dependence and side effects.

[0003] The disadvantages of the prior art are that if high-concentration honey is used, its high viscosity will cause a foreign body sensation; if low-concentration honey is used, the concentration level of its active substances cannot achieve an ideal conditioning effect. Summary of the invention

[0004] In view of the deficiencies in the prior art, one of the objects of the present invention is to provide a moisturizing composition containing honey extract, a second object of the present invention is to provide a method for preparing the moisturizing composition containing honey extract, and a third object of the present invention is to provide an application of the moisturizing composition containing honey extract.

[0005] One of the purposes of the present invention is achieved through the following technical solutions:

[0006] A moisturizing composition containing honey extract, comprising the following raw materials in parts by weight:

[0007] Component A: 33.5-35 parts of propylene glycol dicaprylate / dicaprate, 1-3 parts of stearalkonium hectorite, 0.5-2 parts of propylene carbonate, 15-18 parts of ethylhexyl palmitate, 9-12 parts of hydrogenated coconut glycerides, 3.5-5 parts of beeswax, 3.5-5 parts of paraffin, 3-5 parts of shea butter (BUTYROSPERMUMPARKII) and 2-3 parts of Limnanthes alba seed oil;

[0008] Component B: 0.5-3 parts of butylene glycol, 17.5-22 parts of honey extract, 8-10 parts of PEG-7 glyceryl cocoate and 2-3 parts of caprylic / capric glycerides polyglyceryl-10 esters;

[0009] Component C: 0.1-0.5 parts of sea buckthorn (HIPPOPHAE RHAMNOIDES) fruit oil and 0.1-0.3 parts of essence (daily use).

[0010] Specifically, the raw material of the honey extract is at least one of acacia honey and sunflower honey.

[0011] Specifically, the extraction method of the honey extract is:

[0012] Step 1, mixing the raw material and anhydrous ethanol in equal weight and homogenizing to obtain honey wine;

[0013] Step 2, place the mead in a constant temperature environment of 30-37°C and let it stand;

[0014] Step 3, after the honey wine has completed stratification (that is, the bottom precipitate no longer continues to increase), the bottom precipitate is extracted, and the precipitate is evaporated under low vacuum conditions to obtain the honey extract.

[0015] Specifically, the homogenization method is stirring at a speed of 1000-2000 r / min for 5-10 min, followed by defoaming treatment.

[0016] Specifically, the anhydrous ethanol is ethanol with a purity of 95% or more.

[0017] Specifically, the low vacuum condition is a pressure of 80-90 kPa and a temperature of 10-20° C. Drying at a lower temperature can avoid inactivation of biologically active substances.

[0018] Specifically, the evaporation method is to reduce the ethanol concentration of the precipitate to 65% (v / v) or below.

[0019] The second object of the present invention is achieved by the following technical solutions:

[0020] A method for preparing a moisturizing composition containing honey extract comprises the following steps:

[0021] S1, weigh the raw materials;

[0022] S2, putting component A into an emulsifying pot, stirring, heating, dissolving and homogenizing;

[0023] S3, after cooling, add component B into the emulsifying pot, disperse evenly, stir to dissolve and keep warm;

[0024] S4, cooling down during stirring, adding component C into an emulsifying pot, and stirring evenly to obtain a moisturizing composition containing honey extract.

[0025] Specifically, in step S2, the mixture is heated to 85-90° C. and homogenized for 3-5 minutes until no particles are formed.

[0026] Specifically, in step S3, the temperature is lowered to 80-85° C., and the temperature is kept for 20 minutes, and stirring is maintained during the temperature keeping period.

[0027] Specifically, in step S4, the temperature is lowered to below 40°C.

[0028] The second object of the present invention is achieved by the following technical solutions:

[0029] A moisturizing composition containing honey extract is used in cosmetics, skin care products and health care products for repelling honey-eating midges (Culicoides melleus). The invention unexpectedly finds that the composition has the effect of repelling specific flies and insects.

[0030] The beneficial effects of the present invention are as follows: the present invention solves the problems of high viscosity and foreign body sensation of honey through extraction treatment, and secondly, enhances the moisturizing and anti-aging effects on the skin through the combination of a variety of thickeners, skin conditioners, emollients, etc. DETAILED DESCRIPTION

[0031] The following is further described in conjunction with specific implementation methods:

[0032] All raw materials in this application are purchased through normal channels unless otherwise specified.

[0033] Example 1

[0034] Extraction of honey extract:

[0035] Robinia honey (purchased from Zhejiang Jiangshan Hengliang Bee Products Co., Ltd.) and anhydrous ethanol (purity of 95%) were mixed in equal weights and homogenized. The homogenization method was stirring at a speed of 1000 r / min for 5 minutes, and then defoaming treatment was performed to obtain honey wine.

[0036] Place the mead in a constant temperature environment at 30°C and let it stand;

[0037] After the honey wine is layered, the bottom precipitate is extracted and evaporated under low vacuum conditions to obtain a honey extract. The low vacuum conditions are an air pressure of 80 kPa and a temperature of 10° C. The evaporation method is to reduce the ethanol concentration of the precipitate to 64% (v / v).

[0038] Preparation of moisturizing composition containing honey extract:

[0039] Weigh the following raw materials in parts by weight:

[0040] Component A: 33.5 parts of propylene glycol dicaprylate / dicaprate, 1 part of stearalkonium hectorite, 0.5 parts of propylene carbonate, 15 parts of ethylhexyl palmitate, 9 parts of hydrogenated coconut glycerides, 3.5 parts of beeswax, 3.5 parts of paraffin, 3 parts of avocado tree butter and 2 parts of white meadowfoam seed oil;

[0041] Component B: 0.5 parts of butylene glycol, 17.5 parts of honey extract, 8 parts of PEG-7 glyceryl cocoate and 2 parts of caprylic / capric glycerides polyglyceryl-10 esters;

[0042] Component C: 0.1 part of sea buckthorn fruit oil and 0.1 part of essence (daily use).

[0043] Put component A into an emulsifying pot, stir and heat to 85°C, dissolve and homogenize for 3 minutes.

[0044] Cool down to 80℃, put component B into the emulsifying pot, disperse evenly, stir to dissolve and keep warm; keep warm for 20 minutes, keep stirring during the keeping warm period.

[0045] The temperature was lowered to 39° C. during stirring, and component C was added to an emulsifying pot and stirred evenly to obtain a moisturizing composition containing a honey extract.

[0046] Example 2

[0047] Extraction of honey extract:

[0048] The raw material acacia honey and anhydrous ethanol (purity of 95%) are mixed in equal weights and homogenized. The homogenization method is stirring at a speed of 2000r / min for 10min, and then defoaming treatment is performed to obtain honey wine.

[0049] Place the mead in a constant temperature environment of 37°C and let it stand;

[0050] After the honey wine is layered, the bottom precipitate is extracted and evaporated under low vacuum conditions to obtain a honey extract. The low vacuum conditions are an air pressure of 90 kPa and a temperature of 20° C. The evaporation method is to reduce the ethanol concentration of the precipitate to 64% (v / v).

[0051] Preparation of moisturizing composition containing honey extract:

[0052] Weigh the following raw materials in parts by weight:

[0053] Component A: 35 parts of propylene glycol dicaprylate / dicaprate, 3 parts of stearalkonium hectorite, 2 parts of propylene carbonate, 18 parts of ethylhexyl palmitate, 12 parts of hydrogenated coconut glycerides, 5 parts of beeswax, 5 parts of paraffin, 5 parts of avocado butter and 3 parts of white meadowfoam seed oil;

[0054] Component B: 3 parts of butylene glycol, 22 parts of honey extract, 10 parts of PEG-7 glyceryl cocoate and 3 parts of caprylic / capric glycerides polyglyceryl-10 esters;

[0055] Component C: 0.5 parts of sea buckthorn fruit oil and 0.3 parts of essence (daily use).

[0056] Put component A into an emulsifying pot, stir and heat to 90°C to dissolve and homogenize. The homogenization time is 5 minutes.

[0057] Cool down to 85℃, put component B into the emulsifying pot, disperse evenly, stir to dissolve and keep warm; keep warm for 20 minutes, keep stirring during the keeping warm period.

[0058] The temperature was lowered to 38° C. during stirring, and component C was added to an emulsifying pot and stirred evenly to obtain a moisturizing composition containing a honey extract.

[0059] Example 3

[0060] Extraction of honey extract:

[0061] Acacia honey and anhydrous ethanol (purity of 95%) are mixed in equal weights and homogenized. The homogenization method is stirring at a speed of 1500 r / min for 7 minutes, and then defoaming treatment is performed to obtain honey wine.

[0062] Place the mead in a constant temperature environment of 35℃ and let it stand;

[0063] After the honey wine is layered, the bottom precipitate is extracted and evaporated under low vacuum conditions to obtain a honey extract. The low vacuum conditions are an air pressure of 85 kPa and a temperature of 15° C. The evaporation method is to reduce the ethanol concentration of the precipitate to 64% (v / v).

[0064] Preparation of moisturizing composition containing honey extract:

[0065] Weigh the following raw materials in parts by weight:

[0066] Component A: 34 parts of propylene glycol dicaprylate / dicaprate, 2 parts of stearalkonium hectorite, 1 part of propylene carbonate, 17 parts of ethylhexyl palmitate, 11 parts of hydrogenated coconut glycerides, 4 parts of beeswax, 4 parts of paraffin, 4 parts of shea butter and 2.5 parts of white meadowfoam seed oil;

[0067] Component B: 1.5 parts of butylene glycol, 19 parts of honey extract, 9 parts of PEG-7 glyceryl cocoate and 2.5 parts of caprylic / capric glycerides polyglyceryl-10 esters;

[0068] Component C: 0.3 parts of sea buckthorn fruit oil and 0.2 parts of essence (daily use).

[0069] Put component A into an emulsifying pot, stir and heat to 88°C, dissolve and homogenize, and the homogenization time is 4 minutes.

[0070] Cool down to 83°C, put component B into the emulsifying pot, disperse evenly, stir to dissolve and keep warm; keep warm for 20 minutes, and keep stirring during the keeping warm period.

[0071] The temperature was lowered to 37° C. during stirring, and component C was added to an emulsifying pot and stirred evenly to obtain a moisturizing composition containing a honey extract.

[0072] Example 4

[0073] Acacia honey was replaced with sunflower honey (purchased from Hangzhou Changqing Bee Industry Co., Ltd.), and the remaining steps were the same as in Example 3.

[0074] Comparative Example 1

[0075] Weigh the following raw materials in parts by weight:

[0076] Component A: 34 parts of propylene glycol dicaprylate / dicaprate, 2 parts of stearalkonium hectorite, 1 part of propylene carbonate, 17 parts of ethylhexyl palmitate, 11 parts of hydrogenated coconut glycerides, 4 parts of beeswax, 4 parts of paraffin, 4 parts of shea butter and 2.5 parts of white meadowfoam seed oil;

[0077] Component B: 1.5 parts of butylene glycol, 19 parts of honey, 9 parts of PEG-7 glyceryl cocoate and 2.5 parts of caprylic / capric glycerides polyglyceryl-10 esters;

[0078] Component C: 0.3 parts of sea buckthorn fruit oil and 0.2 parts of essence (daily use).

[0079] Put component A into an emulsifying pot, stir and heat to 88°C, dissolve and homogenize, and the homogenization time is 4 minutes.

[0080] Cool down to 83°C, put component B into the emulsifying pot, disperse evenly, stir to dissolve and keep warm; keep warm for 20 minutes, and keep stirring during the keeping warm period.

[0081] The temperature was lowered to 37° C. during stirring, and component C was added to an emulsifying pot and stirred evenly to obtain a moisturizing composition containing honey.

[0082] Comparative Example 2

[0083] A skin-tightening and moisturizing facial mask prepared with West Lake lotus root starch, grape seed essential oil and honey, application number 201611227171.3, and the technical solution recorded in its embodiment 1.

[0084] Moisturizing experiment

[0085] The purpose of the experiment is to verify that the product of the present invention has moisturizing properties.

[0086] Experimental method: 2g of Examples 1-4 and Comparative Example 1 were evenly applied on the skin of volunteers' arms, and the moisture content was tested using a skin moisture tester 3 hours after application, and repeated 9 times. The volunteers were all college students, female, aged between 19 and 21 years old, and there were 9 people.

[0087] The experimental results are shown in Table 1.

[0088] Table 1 Water content statistics

[0089] sample Example 1 Example 2 Example 3 Example 4 Comparative Example 1 Average moisture content (%) 35.1 35.1 35.5 35.2 35.6

[0090] As can be seen from Table 1, the moisturizing property of the product obtained by the present invention is not substantially different from that of the product using honey, which means that the present invention has qualified moisturizing performance.

[0091] Anti-aging experiment

[0092] The purpose of the experiment is to verify that the product of the present invention has anti-aging effect.

[0093] Experimental method: HaCaT cells were inoculated in a 96-well plate and cultured to a density of 80%. A blank group, a model group, and an experimental group were set up, and 6 replicate wells were set up in each group to take the average. The blank group was not irradiated with UVB, and 10 μL of culture medium was added for 2 hours, and then cultured at 37°C for 24 hours before being used in the experiment. The HaCaT cells in the model group were treated with 10 μL of culture medium for 2 hours, and then irradiated with 60 mJ / cm2 of UVB, and cultured at 37°C for 24 hours before being used in the experiment. The HaCaT cells in the experimental group were treated with 10 μL of culture medium (skin care product content 0.5 mg / mL) for 2 hours, and then irradiated with 60 mJ / cm2 of UVB, and cultured at 37°C for 24 hours before being used in the experiment. Centrifuge for 10 minutes at 4°C and 12000 r / min, and collect the supernatant. The protein in the supernatant was quantified using a BCA protein quantification kit to determine the final concentration of 10 μg / mL. The expression level of secretory protein MMP-1 was determined according to the instructions of the enzyme-linked immunosorbent assay (ELISA) kit, and the inhibition rate of MMP-1 (matrix metalloproteinase) was calculated.

[0094] The experimental results are shown in Table 2.

[0095] Table 2 Statistical table of the inhibition rate of each sample on MMP-1

[0096] sample Example 1 Example 2 Example 3 Example 4 Comparative Example 1 Comparative Example 2 Inhibition rate of MMP-1 (%) 5.67 5.71 5.69 5.65 4.46 2.88

[0097] As shown in Table 2, the inhibition rate of MMP in Comparative Example 1 using ordinary honey dropped significantly. It can be inferred that the honey extract used in the present invention has a better anti-aging effect on the skin after being combined with other raw materials.

[0098] Anti-worm experiment

[0099] The purpose of the experiment is to verify that the present invention does not attract specific pests.

[0100] Experimental method: Cut filter paper with a diameter of 9 cm into two equal halves. In the experimental group, take 1 g of the products prepared in Examples 1-4 and Comparative Examples 1-2 respectively and place them on one half of the filter paper (treated side), and the other half of the filter paper as a control (control side). Then reconnect the two halves of the filter paper, fix them with adhesive paper and place them in a culture dish with the same diameter. Apply solid glue to the bottom of the dish to prevent the test insects from drilling under the filter paper. Put a glass ring with an inner diameter of 8 cm and a height of 5 cm and coated with polytetrafluoroethylene on the inner wall into the culture dish to prevent the test insects from climbing up. Inoculate 30 honey-eating midges (Culicoides melleus) in each dish, do not add feed to the dish, and add a wire mesh cover to prevent the test insects from escaping. Repeat 3 times. Put the filter paper into an insect culture box, check the number of insects on the treated side and the control side after 3 o'clock, and calculate the repellency rate. Among them, repellency rate (%) = (number of insects on the control side - number of insects on the treated side) / number of insects on the control side × 100%.

[0101] The experimental results are shown in Table 3.

[0102] Table 3 Repellency Statistics

[0103]

[0104] As is known, honey-eating Culicoides like to eat honey, so Comparative Example 2 will attract honey-eating Culicoides, and although Comparative Example 1 contains honey, the other raw materials of the present invention synergistically produce a certain repelling effect, so although the repelling effect of Comparative Example 1 is poor, it does not produce an attraction effect on honey-eating Culicoides. The present invention produces an obvious repelling effect on honey-eating Culicoides through the synergy of various raw materials.

[0105] The above embodiments and descriptions are only for illustrating the principles and best embodiments of the present invention. Without departing from the spirit and scope of the present invention, the present invention may be subject to various changes and improvements, all of which fall within the scope of the present invention to be protected.

Claims

1. A moisturizing composition containing honey extract, characterized in that: The invention comprises the following raw materials in parts by weight: Component A: 33.5-35 parts of propylene glycol dicaprylate / dicaprate, 1-3 parts of stearalkonium hectorite, 0.5-2 parts of propylene carbonate, 15-18 parts of ethylhexyl palmitate, 9-12 parts of hydrogenated coconut glycerides, 3.5-5 parts of beeswax, 3.5-5 parts of paraffin, 3-5 parts of avocado butter and 2-3 parts of white meadowfoam seed oil; Component B: 0.5-3 parts of butylene glycol, 17.5-22 parts of honey extract, 8-10 parts of PEG-7 glyceryl cocoate and 2-3 parts of caprylic / capric glycerides polyglyceryl-10 esters; Component C: 0.1-0.5 parts of sea buckthorn fruit oil and 0.1-0.3 parts of essence.

2. The moisturizing composition containing honey extract according to claim 1, characterized in that: The raw material of the honey extract is at least one of acacia honey and sunflower honey.

3. The moisturizing composition containing honey extract according to claim 1, characterized in that: The extraction method of the honey extract is: Step 1, mixing the raw material and anhydrous ethanol in equal weight and homogenizing to obtain honey wine; Step 2, place the mead in a constant temperature environment of 30-37°C and let it stand; Step 3, after the honey wine is layered, the bottom precipitate is extracted, and the precipitate is evaporated under low vacuum conditions to obtain a honey extract.

4. The moisturizing composition containing honey extract according to claim 3, characterized in that: The homogenization method is to stir at a speed of 1000-2000 r / min for 5-10 minutes, and then perform defoaming treatment; The anhydrous ethanol is ethanol with a purity of 95% or more.

5. The moisturizing composition containing honey extract according to claim 3, characterized in that: The low vacuum conditions are air pressure 80-90 kPa and temperature 10-20°C.

6. The moisturizing composition containing honey extract according to claim 3, characterized in that: The evaporation method is to reduce the ethanol concentration of the precipitate to 65% (v / v) or below.

7. A method for preparing a moisturizing composition containing honey extract according to claim 1, characterized in that: The following steps are involved: S1, weigh the raw materials; S2, putting component A into an emulsifying pot, stirring, heating, dissolving and homogenizing; S3, after cooling, add component B into the emulsifying pot, disperse evenly, stir to dissolve and keep warm; S4, cooling down during stirring, adding component C into an emulsifying pot, and stirring evenly to obtain a moisturizing composition containing honey extract.

8. The method for preparing a moisturizing composition containing a honey extract according to claim 7, characterized in that: In step S2, the mixture is heated to 85-90° C. and homogenized for 3-5 minutes until no particles are left.

9. The method for preparing a moisturizing composition containing honey extract according to claim 7, characterized in that: In the step S3, the temperature is lowered to 80-85°C, and the heat preservation time is 20 minutes, and stirring is maintained during the heat preservation period; in the step S4, the temperature is lowered to below 40°C.

10. A use of the moisturizing composition containing honey extract according to claim 1, characterized in that: Use in cosmetics, skin care products and health care products that have the function of repelling honey-feeding midges.

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